Summary of the invention
For above-mentioned prior art, the invention provides a kind of black fungus super-micro instant electuary with blood fat reducing function, its adsorptivity is strong, water imbibition strong, good water solubility, rapidly dissolvable, good mouthfeel, has hypoglycemic, reducing blood lipid, radioresistance, raising immunity, antithrombotic, anticancer, fat-reducing, mends the effects such as iron; Present invention also offers its preparation method.
The present invention is achieved by the following technical solutions:
There is a black fungus super-micro instant electuary for blood fat reducing function, be made up of the component of following weight portion: black fungus Ultramicro-powder 4.5 ~ 5.5 parts, degreasing black bean powder 2.5 ~ 3.5 parts, 2.5 ~ 3.5 parts, rock sugar.Preferably, the component of following weight portion can also be comprised: jasmine pollen 0.02 ~ 0.03 part, lilium pollen 0.02 ~ 0.03 part, 0.04 ~ 0.06 part of (adding of jasmine pollen, lilium pollen, tangerine peel powder of tangerine peel powder, have and regulate mouthfeel and deliquescent effect, there is collaborative effect for reducing blood fat simultaneously).Preferred further, be made up of the component of following weight portion: black fungus Ultramicro-powder 5 parts, degreasing black bean powder 3 parts, 3 parts, rock sugar.Preferred further again, be made up of the component of following weight portion: black fungus Ultramicro-powder 5 parts, degreasing black bean powder 3 parts, 3 parts, rock sugar, jasmine pollen 0.025 part, lilium pollen 0.025 part, tangerine peel powder 0.05 part.
Wherein, described black fungus Ultramicro-powder prepares by the following method: get black fungus, and removal surface impurity and hard root divide, after cleaning-drying, tentatively pulverize with whirlwind type crushing machine, cross 100 mesh sieves, obtain meal, again meal jet mill is carried out air-flow ultramicro grinding, in vacuum drying chamber, be dried to constant weight, obtain black fungus Ultramicro-powder, its particle diameter is 10 ~ 50 μm, average grain diameter 25 μm, sealing is preserved, and prevents the moisture absorption.
Described degreasing black bean powder prepares by the following method: (degreasing black soya bean is the accessory substance after black soya bean raw material extracts oil by grease factory to extracting degreasing black soya bean, directly obtain from grease factory, for conventional products existing in prior art), fry, pulverize with whirlwind type crushing machine, cross 100 mesh sieves, obtain degreasing black bean powder, sealing is preserved.
Described jasmine pollen prepares by the following method: Jasmine raw material → cleaning impurity elimination → cleaning → drying → coarse crushing → ultramicro grinding (mode of described coarse crushing, ultramicro grinding is with the preparation method of above-mentioned black fungus Ultramicro-powder).
Described lilium pollen prepares by the following method: lily raw material → cleaning impurity elimination → cleaning → drying → coarse crushing → ultramicro grinding.
Described tangerine peel powder prepares by the following method: dried orange peel raw material → cleaning impurity elimination → cleaning → drying → coarse crushing → ultramicro grinding.
The described preparation method with the black fungus super-micro instant electuary of blood fat reducing function is: by each component (black fungus Ultramicro-powder, rock sugar, or and: degreasing black bean powder, jasmine pollen, lilium pollen, tangerine peel powder) mixing mixing, aseptic packaging after sterilizing, to obtain final product.Technological process is as follows:
Black fungus raw material → cleaning impurity elimination → cleaning → drying → coarse crushing → ultramicro grinding;
Degreasing black soya bean → coarse crushing;
Above-mentioned bi-material mixes → sterilizing → packaging with rock sugar.
Time edible, warm water Instant Drinks, stir, one time 1 bag (1 bag 10 grams).
The black fungus super-micro instant electuary with blood fat reducing function of the present invention, not only solve the problem that black fungus Ultramicro-powder absorptivity is low, also solve the problem that ultrafine powder is instant, and, add black bean powder and rock sugar to balance black fungus powder nutrition, make it to become better product of serving for human health.The black fungus super-micro instant electuary with blood fat reducing function of the present invention, blood fat reducing function is significantly better than black fungus raw material, meal, dissolubility is good, mouthfeel is good, there is the physiological functions such as lipopenicillinase, antithrombotic, radioresistance, anti-oxidant, antitumor, hypoglycemic, fat-reducing, beauty treatment, clearing lung-heat, the crowd being applicable to each age level eats, and has good economic benefit.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is further illustrated.
Instrument, reagent, material etc. involved in following embodiment, unless otherwise noted, be existing conventional instrument, reagent, material etc. in prior art, obtain by regular commercial sources.Experimental technique involved in following embodiment, detection method etc., unless otherwise noted, are existing normal experiment method in prior art, detection method etc.
Test the contrast of blood fat reducing function of 1 black fungus Ultramicro-powder, black fungus meal
Test method: adopt arbitrary sampling method that 40 mouse are divided into 4 groups, i.e. Basal control group (A group), high fat control group (B group), meal dosage group (C group) and Ultramicro-powder dosage group (D group), often organizes 10.Give A group basal feed, B, C, D group all gives high lipid food (basal feed: lard: cholesterol is 80: 19: 1), every morning feeding once, freely take food drinking-water, 12h periodicity of illumination, temperature is 22 ± 1 DEG C, and humidity is 65%.After 10 days, Basal control group and each random selecting of high lipid food group 3 mouse, pluck eyeball and get eyeground blood, detects serum total cholesterol (TC) level, determine the foundation of hyperlipemia model.
Described basal feed is standard mouse grain, and the formula of described high lipid food is: basal feed: lard: cholesterol=80: 19: 1, mass ratio.
After setting up hyperlipemia model, A group gives basal feed every day; B group gives high lipid food; C group gives the black fungus meal of mouse 100mg/kg.d dosage every day except giving high lipid food; While D group gives high lipid food, every day gives the black fungus Ultramicro-powder of mouse 100mg/kg.d dosage.Within one week, measure a Mouse Weight.A, B, C, D4 group is freely drunk water.Feed after 35 days, get eyeground blood after fasting 24h and put into test tube, after stripping serum, detect T-CHOL (TC), triglycerides (TG), HDL (HDL-C) level.Judge whether black fungus powder has effect of reducing blood lipid by These parameters.Each index is all used
represent.T inspection is adopted to compare whether have conspicuousness with hyperlipemia model control group.
Described black fungus meal prepares by the following method: get black fungus, and removal surface impurity and hard root divide, and tentatively pulverize after cleaning-drying with whirlwind type crushing machine, crosses 100 mesh sieves, obtains meal.
Described black fungus Ultramicro-powder prepares by the following method: get black fungus, and removal surface impurity and hard root divide, after cleaning-drying, tentatively pulverize with whirlwind type crushing machine, cross 100 mesh sieves, obtain meal, then meal jet mill is carried out air-flow ultramicro grinding, constant weight is dried in vacuum drying chamber, obtain black fungus Ultramicro-powder, its particle diameter is 10 ~ 50 μm, average grain diameter 25 μm, sealing is preserved, and prevents the moisture absorption.
Result of the test:
After (1) 4 group of mouse high lipid food feeds 10d, get Basal control group and each 3 mouse of high lipid food group at random, pluck eyeball and get blood, measure mice serum total cholesterol level, results contrast is as shown in table 1.
Table 1 is set up mouse TC before and after hyperlipemia model and is compared
Note: compare with hyperlipemia model group, " * " reaches the level of signifiance (P < 0.05), and " * * " reaches the pole level of signifiance (P < 0.01)
Mouse is in nursing after 10 days as can be seen from Table 1, and serum total cholesterol content obviously raises, and compared with Basal control group, high lipid food group serum TC content all reaches significant difference (P < 0.05).Illustrate that high fat diet can cause mice serum TC to raise, hyperlipemia model is successfully prepared.
(2) black fungus powder to mouse to serum total cholesterol (TC) TC content in table 2.
Table 2 serum total cholesterol (TC) content
Note: compare with hyperlipemia model group, " * " reaches the level of signifiance (P < 0.05), and " * * " reaches the pole level of signifiance (P < 0.01)
Table 2 result shows: compared with high fat control group, black fungus meal has the effect reducing TC, but do not reach remarkable result, Ultramicro-powder reduces hyperlipidemic mice TC and reaches significant difference (P < 0.05), reduce 7.56% and 12.04% respectively, Ultramicro-powder group TC level drops to Basal control group phase same level substantially.
(3) on the impact of Triglycerides in Serum (TG):
Give mouse polysaccharide after 35 days, in serum, TG content is in table 3.
Table 3 serum triglyceride (TG) content
Note: compare with hyperlipemia model group, " * " reaches the level of signifiance (P < 0.05), and " * * " reaches the pole level of signifiance (P < 0.01)
Result of study shows: relative to high fat control group, black fungus meal reaches significant difference (P < 0.05) in reduction mice serum TG content, and Ultramicro-powder reaches pole significant difference (P < 0.01), reduce 12.00% and 22% respectively.Illustrate that black fungus powder has the effect reducing mice serum TG, and Ultramicro-powder reduces the effect of serum TG, and comparatively meal is more remarkable.
(4) on the impact of serum middle-high density lipoprotein (HDL-C):
Give mouse black fungus powder after 35 days, in serum, HDL-C content is in table 4.
Table 4 serum high-density LP (HDL-C) content
Note: compare with hyperlipemia model group, " * " reaches the level of signifiance (P < 0.05), and " * * " reaches the pole level of signifiance (P < 0.01)
Result shows: black fungus meal and Ultramicro-powder all reach pole significant difference improving in serum high-density LP content, but Ultramicro-powder group improves the effect of HDL-C in serum, and comparatively meal group is more obvious.Meal group and Ultramicro-powder group improve 58.73% and 73.02% respectively.
Find after above-mentioned animal experiment study, the lipid-lowering effect of black fungus Ultramicro-powder obviously improves.Hypolipemic function test proves that black fungus Ultramicro-powder group reduces blood fat better effects if than meal group, and black fungus Ultramicro-powder group has and reduces T-CHOL (P < 0.05) significantly, reduces triglycerides (P < 0.01) and pole extremely significantly and significantly improve HDL (P < 0.01) and act on.
Experiment 2 has the research of the black fungus super-micro instant granule best proportioning of blood fat reducing function
1. material and equipment
Material: black fungus, degreasing black soya bean.
Equipment: pulverizer, jet mill, electric heating constant-temperature blowing drying box, glutinous analyzer, electronic analytical balance, centrifuge, constant temperature blender with magnetic force.
2. experimental technique
The preparation of 2.1 black fungus Ultramicro-powders, degreasing black bean powder
Black fungus Ultramicro-powder: get black fungus, removal surface impurity and hard root divide, and tentatively pulverize with whirlwind type crushing machine, cross 100 mesh sieves, obtain meal, again meal jet mill is carried out air-flow ultramicro grinding, in vacuum drying chamber, be dried to constant weight, obtain black fungus Ultramicro-powder, its, average grain diameter 150 μm, sealing is preserved, and prevents the moisture absorption.
Black bean powder: extracting degreasing black soya bean, fries, and pulverizes with whirlwind type crushing machine, crosses 100 mesh sieves, obtains black bean powder, and sealing is preserved.
Instant: get black fungus Ultramicro-powder, black bean powder and rock sugar (rock sugar is pulverized with whirlwind type crushing machine in advance, crosses 100 mesh sieves), mixing mixing, to obtain final product.
The mensuration of 2.2 viscositys
Computing formula: A=k × a
In formula, A is viscosity, mPas; K is the coefficient under different rotor, different rotating speeds; A is the reading of viscosity analyzer.
2.3 sensory evaluation
Adopt descriptive analysis test method, select 10 colleagues to evaluate.By random sequence, rice paste is supplied to assessment officer, giving a mark to each index and making corresponding sense organ describes.Standards of grading are in table 5.
The mensuration of the instant index of 2.4 electuary
(1) mensuration of wetability: the deionized water 200ml adding 25 DEG C in 250ml beaker, takes 0.5g sample and is evenly laid on the water surface, measures and is added to time (s) required for the complete sedimentation of sample from sample.
(2) dispersed mensuration: take 5g sample and be put in 100ml beaker, add the deionization 50ml of 25 DEG C, stir in constant temperature blender with magnetic force with the rotating speed of 800r/min, record and all disperse the required time (s) to powder agglomates from stirring.
(3) mensuration of solubility: accurate weighing sample 5.00g sample, is placed in 50ml small beaker, adds deionized water 30ml, with magnetic stirrer 30min under room temperature condition, instant is fully dissolved.Solution is transferred in 50ml volumetric flask completely, uses deionized water constant volume, fully shake up.Get 15ml, put into centrifuge tube, the centrifugal 10min of 3000r/min, gets supernatant, proceeds in weighing disk, heats 20min in a water bath, then puts into 105 DEG C of drying boxes and dries to constant mass.Computing formula is as follows:
In formula, X is sample solubility, g/100g; M is sample quality, g; M
1for weighing disk quality, g; M
2for quality after weighing disk and insoluble matter drying, g; B is sample moisture.
Table 5 sensory evaluation scores standard
3. results and analysis
The most adaptive ratio of 3.1 black fungus Ultramicro-powders and degreasing black bean powder
Selected black fungus Ultramicro-powder and degreasing black bean powder proportioning are respectively 0: 5,5: 5,5: 4,5: 3,5: 2,5: 1,5: 0, rock sugar mass fraction is 40%, sample thief 5g, in 100ml beaker, adds 50ml water (90 DEG C) and reconstitutes, and is cooled to room temperature after fully stirring.
As seen from Figure 1, along with the minimizing of degreasing black bean powder addition, the viscosity of electuary is obvious ascendant trend.This is that hydrone enters starch crystallite binding structure due to hydrogen bond rupture between starch molecule after gelatinization, and molecule randomness increases, and the viscosity of starch-aqueous systems is relatively high.The existence of degreasing black bean powder have impact on hydrone and enters, and the viscosity of starch-aqueous systems is damaged, the content of starch of black fungus powder than the height of black soya bean, easy gelatinization, therefore the viscosity of the high nourishing medicinal granule of black fungus powder proportioning is higher than the low viscosity of black fungus powder proportioning.From table 6, the subjective appreciation of degreasing black bean powder on nourishing medicinal granule has impact, along with the increase of degreasing black bean powder addition, the ratio that the good sample of instant sensory evaluation scores concentrates on black fungus powder and black bean powder be 5: 2,5: 3,5: 4 scope in (it is preferred that 5: 3).Reason is black fungus powder is taupe, and degreasing black bean powder is faint yellow, and then color and luster is more shallow in its content increase, but its content increase makes the viscosity of nourishing medicinal granule decline to some extent, and taste bad, fragrance is thin out.
The sensory evaluation scores of electuary under table 6 different ratios of raw materials
3.2 reconstitute the impact of water temperature on electuary
Choose black fungus Ultramicro-powder and degreasing black bean powder proportioning 5: 3, rock sugar mass fraction is 40%, and sample thief 5g, in 100ml beaker, adds 50ml60 respectively, 70,80,90,100 DEG C of water reconstitute, and is cooled to room temperature after fully stirring.
As seen from Figure 2, along with the increase reconstituting water temperature, the viscosity of nourishing medicinal granule improves.Water temperature is 60 DEG C time, and viscosity is 271.6mPas, and when 80 DEG C, viscosity is 1939.5mPas, changes greatly.After 80 DEG C, viscosity is all at 1900 ~ 2500mPas, and change is little.This be due to temperature lower time do not reach the gelatinization point of nourishing medicinal granule, the viscosity of nourishing medicinal granule is lower, and when temperature is greater than 80 DEG C, instant gelatinization is comparatively abundant, and viscosity is higher.Therefore select about 80 DEG C water temperatures more suitable.
Table 7 difference reconstitutes the sensory evaluation scores of electuary under water temperature
As can be seen from Table 7, after temperature reaches 80 DEG C, electuary obtains sufficient gelatinization, and it is consistent that this and starch are greater than 70 DEG C of theories just starting gelatinization in temperature, and temperature is higher, and starch is gelatinization more early.Under 85 ~ 90 DEG C of conditions, occur the phenomenon that viscosity jumps when 5 ~ 6s, and about 20 rear viscositys just start to rise under 70 ~ 80 DEG C of conditions.This is because starch crystal avalanche under higher temperature is accelerated.The instant of abundant gelatinization produces special fragrance and flavour, and now the viscosity of nourishing medicinal granule is also higher, and the indexs such as mouthfeel all reach good level.
3.3 rock sugar additions are on the impact of electuary
Choose black fungus Ultramicro-powder and degreasing black bean powder proportioning 5: 3, rock sugar mass fraction is 30,35,40,45,50%, and sample thief 5g, in 100ml beaker, adds 50ml90 DEG C of water respectively and reconstitutes, and is cooled to room temperature after fully stirring.
As seen from Figure 3, along with the increase of rock sugar addition, the viscosity of nourishing medicinal granule declines to some extent.Reason is that rock sugar has the effect of similar water molecule as Small molecular, certain diluting effect is had to starch molecular chain, delay the mobility of starch molecular chain, or permeate with sugar in starch gelatinization process and enter starch granules inside, interact with multiple hydroxyls of starch molecule, hinder the imbibition of starch, thus viscosity when making gelatinization declines [8].Control group is not 3200mPas with the viscosity of rock sugar, and when rock sugar mass fraction is 50%, viscosity is 1367mPas.As can be seen here, with charge ratio with reconstitute water temperature and compare, rock sugar addition has some to affect on nourishing medicinal granule viscosity.
The sensory evaluation scores of electuary under the different rock sugar addition of table 8
As a kind of sweetener, the addition increasing rock sugar within the specific limits will inevitably make the taste of nourishing medicinal granule become agreeable to the taste.As seen from Table 8, rock sugar add be mainly manifested in nourishing medicinal granule flavour and mouthfeel on, also little on color and luster impact, select rock sugar mass fraction to be 35%, 40%, 45% more suitable.
3.4 the orthogonal experiment of mixing formula
According to single factor experiment result, carry out the orthogonal test of 3 factor 3 levels, with subjective appreciation and viscosity measurement for evaluation index, determine the optimum formula of instant.Orthogonal test water-glass is as shown in table 9, and result of the test is as shown in table 10.As shown in Table 10, the order that each factor affects conspicuousness to instant is B > A > C.Reconstituting water temperature is the key factor affecting the abundant gelatinization of instant, and can improve the local flavor of product; The color and luster of the addition major effect instant of degreasing black bean powder; Add rock sugar mainly in order to increase the sugariness of instant, little to viscosity.The flavour of viscosity major effect nourishing medicinal granule, and then organoleptic quality is affected.Viscosity is not more high better, and when viscosity is 2178mPas, sensory evaluation scores is up to 90 points.By the synthesis result of subjective appreciation and viscosity measurement, determine that the best of breed of instant is A
2b
3c
3, namely the proportioning of black fungus powder and black bean powder is 5: 3, and reconstituting water temperature is 90 DEG C, and the addition mass fraction of rock sugar is 40%.This combination product is carried out subjective appreciation again, and total score is 90.5 points.
Table 9 orthogonal array
Table 10 orthogonal experiments
The mensuration of the instant index of 3.5 electuary
Instant (best of breed, namely the proportioning of black fungus powder and degreasing black bean powder is 5: 3, and reconstituting water temperature is 90 DEG C, and the addition mass fraction of rock sugar is 40%) and commercially available black sesame powder are done comparative analysis, and instant capacity index determining result is as shown in table 11.
Table 11 black fungus super-micro instant instant and commercially available black sesame powder instant capacity Indexes Comparison
The solubility of instant is 94.31g/ (100g), and black sesame powder is 95.78 (g/100g), and the two is very close; The wetability of instant is 120.0s, and black sesame powder is 95.5s, and the two is more or less the same; The dispersiveness of instant is 240.0s, and black sesame powder is 112.5s, and the two has the difference of jitter time, may be the granularity of finished product instant little not caused by.Account for 40% by each index solubility, wettability account for 30%, dispersiveness account for 30% weight analysis, comprehensively think, instant capacity overall target and the commercially available black sesame powder of finished product instant do not have significant difference, therefore can be used as a kind of convenient instant electuary and eat.
Embodiment 1 preparation has the black fungus super-micro instant electuary of blood fat reducing function
Formula is: black fungus Ultramicro-powder 5 parts, degreasing black bean powder 3 parts, 3 parts, rock sugar.
Preparation method is: by black fungus Ultramicro-powder, rock sugar, degreasing black bean powder mixing mixing, aseptic packaging after sterilizing, to obtain final product.Time edible, warm water Instant Drinks, stir, one time 1 bag (1 bag 10 grams).
Described black fungus Ultramicro-powder prepares by the following method: get black fungus, and removal surface impurity and hard root divide, after cleaning-drying, tentatively pulverize with whirlwind type crushing machine, cross 100 mesh sieves, obtain meal, then meal jet mill is carried out air-flow ultramicro grinding, constant weight is dried in vacuum drying chamber, obtain black fungus Ultramicro-powder, its particle diameter is 10 ~ 50 μm, average grain diameter 25 μm, sealing is preserved, and prevents the moisture absorption.
Described degreasing black bean powder prepares by the following method: extracting degreasing black soya bean, fries, and pulverizes with whirlwind type crushing machine, crosses 100 mesh sieves, obtains degreasing black bean powder, and sealing is preserved.
Described rock sugar is first pulverized with whirlwind type crushing machine, crosses 100 mesh sieves, for subsequent use.Lower same.
Embodiment 2 preparation has the black fungus super-micro instant electuary of blood fat reducing function
Formula is: black fungus Ultramicro-powder 5 parts, degreasing black bean powder 3 parts, 3 parts, rock sugar, jasmine pollen 0.025 part, lilium pollen 0.025 part, tangerine peel powder 0.05 part.
Preparation method is: by black fungus Ultramicro-powder, rock sugar, degreasing black bean powder, jasmine pollen, lilium pollen and tangerine peel powder mixing mixing, aseptic packaging after sterilizing, to obtain final product.Time edible, warm water Instant Drinks, stir, one time 1 bag (1 bag 10 grams).
Described jasmine pollen prepares by the following method: Jasmine raw material → cleaning impurity elimination → cleaning → drying → coarse crushing → ultramicro grinding.
Described lilium pollen prepares by the following method: lily raw material → cleaning impurity elimination → cleaning → drying → coarse crushing → ultramicro grinding.
Described tangerine peel powder prepares by the following method: dried orange peel raw material → cleaning impurity elimination → cleaning → drying → coarse crushing → ultramicro grinding.
The other the same as in Example 1.