CN104687253B - A method for reducing electronic tobacco filter and a sense of sweet gas comprising the electronic cigarette filter tips - Google Patents

A method for reducing electronic tobacco filter and a sense of sweet gas comprising the electronic cigarette filter tips Download PDF

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CN104687253B
CN104687253B CN201510003053.3A CN201510003053A CN104687253B CN 104687253 B CN104687253 B CN 104687253B CN 201510003053 A CN201510003053 A CN 201510003053A CN 104687253 B CN104687253 B CN 104687253B
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filter
polymer compound
electronic
sense
polyhydroxy
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CN104687253A (en
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韩敬美
段沅杏
李寿波
杨柳
张霞
杨继
赵伟
陈永宽
缪明明
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云南中烟工业有限责任公司
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Abstract

本发明公开了一种降低电子烟烟气甜腻感的滤嘴,其中所述滤嘴的滤嘴基质中包含一种或多种多羟基高分子化合物,所述多羟基高分子化合物经过水分平衡,处于吸附水蒸气饱和状态。 The present invention discloses a method for reducing electronic tobacco sense sweet gas filter, wherein the filter of the filter matrix comprises one or more polyhydroxy polymer compound, a polyhydroxy polymer compound has a moisture balance , the adsorption of water vapor saturation. 本发明的滤嘴具有降低电子烟烟气甜腻感的作用,同时还可以降低电子烟烟气的干燥感,制备工艺简单,成本低廉。 The filter of the present invention have a reduced sense of electronic tobacco sweet gas effect, while reducing a sense of electronic tobacco drying gas, simple preparation process and low cost.

Description

一种降低电子烟烟气甜腻感的滤嘴以及包含该滤嘴的电子烟 A method for reducing electronic tobacco filter and a sense of sweet gas comprising the electronic cigarette filter tips

技术领域 FIELD

[0001] 本发明涉及一种电子烟滤嘴,具体涉及一种降低电子烟烟气甜腻感的滤嘴及包含该滤嘴的电子烟。 [0001] The present invention relates to an electronic cigarette filter, in particular to a sweet reducing gas flu electronic tobacco filter comprising the filter and the electronic cigarette.

背景技术 Background technique

[0002] 世界卫生组织将电子烟(又名电子尼古丁传送系统)官方定义为一种能够向肺传输尼古丁的消费品。 [0002] The World Health Organization electronic cigarette (known as electronic nicotine delivery systems) is defined as the official transmission capable of nicotine to the lungs consumer. 目前对电子烟产品没有统一的标准,各个厂家生产电子烟所使用的原料不同,因此电子烟烟液的主要化学成分也有所不同。 At present no uniform standard electronic cigarette products, all manufacturers of electronic material used in various cigarette, so the main chemical components electronic tobacco was also different. 很多研究人员利用GC_MS、HPLC等仪器对烟液的成分进行了分析,其中丙二醇、甘油、水和烟碱约占电子烟烟液质量的95%,而电子烟烟气的主要成分也是丙二醇、甘油、水和烟碱。 Many researchers use GC_MS, HPLC and other equipment components of liquid smoke were analyzed, wherein propylene glycol, glycerol, water and nicotine tobacco smoke was about 95% by mass of the electron, and the main components of electronic tobacco gas is propylene glycol, glycerol , water and nicotine. 在电子烟烟液中的丙二醇和甘油一方面作为电子烟烟液的溶剂,一方面作为电子烟烟气形成的介质,它们虽然增加了电子烟烟气的保润效果,但同时也给电子烟烟气带来了甜腻感,使吸烟者喉部感到不适。 Propylene glycol and glycerin solution in electronic tobacco electronic tobacco aspect as a solvent solution, on the one hand as a medium for electronic tobacco gas formation, although they increase the effect of electron-Run tobacco smoke gas, but also to electronic cigarette It brought a sense of sweet smoke, smokers throat discomfort. 而且,研究发现,即便将这些多元醇的用量减少至维持溶解和发烟所需要的最低量,仍有甜腻感存在。 Furthermore, studies have found that the minimum amount will be reduced even if the amount of these polyhydric alcohols to dissolve and maintain the desired fuming still sweet sense of presence.

[0003] 目前,为了去除电子烟烟气的甜腻感采用的一般方法为寻找替换溶剂法。 [0003] Currently, the general method for electronic tobacco sense sweet gas employed to find alternative solvent removal process. 但是暂时没有找到合适、安全的溶剂进行替换。 But we do not find a suitable and safe solvent replacement.

[0004] 提高电子烟吸食的安全性和舒适感是当前电子烟研究的一个重要方向。 [0004] improve the safety and comfort of electronic cigarette smoking is an important direction of current research electronic cigarette.

发明内容 SUMMARY

[0005] 本发明的目的在于提供一种能有效降低电子烟烟气甜腻感的滤嘴及包含该滤嘴的电子烟。 [0005] The object of the present invention is to provide an electronic tobacco can effectively reduce the sense of sweet gas and a filter comprising the filter of the electronic cigarette.

[0006] 本发明的目的通过以下技术方案予以实现。 [0006] The object of the present invention is realized by the following technical solutions.

[0007] 本发明第一方面涉及一种降低电子烟烟气甜腻感的滤嘴,其中所述滤嘴的滤嘴基质中包含一种或多种多羟基高分子化合物,所述多羟基高分子化合物经过水分平衡,处于吸附水蒸气饱和状态。 [0007] The first aspect of the present invention relates to a method for reducing electronic tobacco sense sweet gas filter, wherein the filter of the filter matrix comprises one or more polyhydroxy polymer compound, the multi-high hydroxyl molecular compound has a moisture equilibrium, the adsorption of water vapor saturation.

[0008] 通过处理使所述多羟基高分子化合物处于吸附水蒸气饱和状态,目的在于降低电子烟烟气的甜腻感。 [0008] By processing the polymer compound is a polyhydroxy saturated water vapor adsorption, aims to reduce the sense of electronic tobacco sweet gas. 推测其原理为:当被加热至40°C左右的电子烟烟雾通过该滤嘴时,滤嘴中的所述多羟基高分子化合物中的水分子逐渐脱附,暴露出来的吸附位进而能够吸附多元醇,从而降低甜腻感。 The principle is inferred: when the left and right was heated to 40 ° C electronic cigarette smoke through the filter, the filter in the plurality of water molecules desorbed gradually hydroxyl polymer compound, and further exposed adsorption sites capable of adsorbing polyhydric alcohol, to reduce the sweet sensation.

[0009] 实验发现,本发明的滤嘴在降低甜腻感的同时还降低了电子烟烟气的干燥感,从而无需通过在电子烟烟液中加水来降低干燥感,解决了电子烟烟液中不能含水过多,否则会造成电子烟烟液对脂溶性香精香料溶解度差和易变质的问题。 [0009] It was found that the filter of the present invention while reducing the sweet sensation also reduces the sense of electronic tobacco drying gas, thereby eliminating the need to reduce the feeling of dryness in the electronic tobacco by adding liquid water, the solution was electronic tobacco It can not be too much water, otherwise it will cause problems for electronic tobacco liquid fat-soluble flavors and fragrances poor solubility and ease of deterioration.

[0010] 所述滤嘴的制备方法为将经过水分平衡的多羟基高分子化合物以粉末状加入到滤嘴基质中,在复合嘴棒成型机上制成复合滤嘴。 [0010] The method of preparing the filter through the water balance of the polyhydroxy polymer compound in powder form is added to the filter matrix, a composite filter in a composite filter rod machine.

[0011] 在优选的实施方案中,所述滤嘴基质为醋酸纤维丝束、丙酸纤维丝束或聚丙烯丝束。 [0011] In a preferred embodiment, the matrix is ​​a cellulose acetate filter tow, fiber tow or polypropylene tow acid.

[0012] 在优选的实施方案中,所述多羟基高分子化合物为壳聚糖、聚乙烯醇、环糊精或多羟基螯合树脂。 [0012] In a preferred embodiment, the polyhydroxy polymer compound is chitosan, polyvinyl alcohol, cyclodextrin or polyhydroxy chelating resin.

[0013] 在优选的实施方案中,所述多羟基高分子化合物的添加量为滤嘴基质质量的1%-20% 〇 [0013] In a preferred embodiment, the multi-mass filter matrix added in an amount of 1% of the hydroxyl groups of the polymer compound billion -20%

[0014] 在优选的实施方案中,所述多羟基高分子化合物的水分平衡条件为:温度为15-30 °C,湿度为60-100%,平衡时间为12-48h。 [0014] In a preferred embodiment, the polyhydroxy polymer compound is water balance conditions: a temperature of 15-30 ° C, humidity of 60-100%, equilibration time was 12-48h. 所述多羟基高分子化合物经过上述平衡后达到吸附水蒸气饱和状态。 After the above-described polyhydroxy polymer compound adsorption reached equilibrium saturated water vapor.

[0015] 在优选的实施方案中,所述滤嘴的结构为一元功能型滤嘴或二元复合滤嘴或三元复合滤嘴。 [0015] In a preferred embodiment, the filter structure filters functional monohydric or dihydric or trihydric composite filter composite filters. 所述滤嘴也可以是更多元复合滤嘴。 The filter element may also be a more complex filter. 复合滤嘴的元数是根据整个滤嘴是由几段不同滤嘴复合而成来确定的。 Number of symbols is based on the entire composite filter the filter is a composite filter formed by the different paragraphs determined. 复合滤嘴一般由二段滤嘴组成,或在二段滤嘴间留一空隙,填加所需的吸附剂。 Usually the composite filter composed of two-stage filter, or leaving a gap between the two-stage filter, added to fill the required adsorbent. 复合滤嘴的制备通常是通过嘴棒成型机将二种或三种不同的滤嘴复合在一起。 Preparation of composite filters generally filter rod forming machine by two or three different filter composition together. 通常二元复合滤嘴一段滤材为醋酸纤维,另一段为成型纸或生产过程中掺入添加剂(例如活性炭)的醋酸纤维功能型滤嘴;三元滤嘴则是将三段不同的滤嘴由嘴棒成型机复合而成。 Typically binary complex filter section of cellulose acetate filter, incorporation of another section of cellulose acetate filter functional additive (e.g. activated carbon) is formed of paper or the production process; three yuan filter sucked three segments different filter compounded by the filter rod forming machine.

[0016] 在优选的实施方案中,所述滤嘴的嘴端部具有封膜或封盖。 [0016] In a preferred embodiment, the mouth end of the filter having a sealing film or cover. 封膜或封盖的作用为防止在存储过程中预吸附的水脱附。 The closure or sealing film role to prevent the process of pre-stored in the desorption of water adsorbed. 封膜或封盖可以在抽吸时取下。 Sealing film or the closure can be removed at the time of suction.

[0017] 本发明第二方面涉及一种电子烟,其具有如本发明第一方面所述的降低电子烟烟气甜腻感的滤嘴。 [0017] The second aspect of the present invention relates to an electronic cigarette, having as a first aspect of the present invention to reduce electronic tobacco sweet feeling gas filter.

[0018] 本发明的有益效果为: [0018] Advantageous effects of the present invention are:

[0019] 1、本发明的电子烟滤嘴中的多羟基高分子化合物能有效吸附电子烟烟气中的甘油、丙二醇等多羟基溶剂,有效降低电子烟烟气的甜腻感,从而改善电子烟烟气的吸食品质,而又对电子烟吸食品质无不利影响; [0019] 1, the electronic cigarette filter polyhydroxy polymer compound of the present invention can effectively adsorb electronic tobacco gas glycerol, propylene glycol, polyhydroxy solvents, reduce the sense of sweet electronic tobacco gas, thereby improving the electron smoking quality tobacco smoke gas, but the electronic cigarette smoking without adversely affecting the quality of;

[0020] 2、本发明的电子烟滤嘴在降低电子烟烟气甜腻感的同时还可以降低其干燥感,这是由于本发明的电子烟滤嘴中的多羟基高分子化合物经过水分平衡,处于吸附水蒸气饱和状态,当其受热时其中的水分挥发出来,从而降低电子烟烟气的干燥感;本发明的电子烟滤嘴无需通过在电子烟烟液中加水来降低干燥感,解决了电子烟烟液中不能含水过多否则会造成电子烟烟液对脂溶性香精香料溶解度差和易变质的问题; [0020] 2, the electronic cigarette filter according to the present invention, while reducing electronic tobacco sweet gas may also reduce the feeling of dryness, which is due to electronic cigarette filter according to the present invention the polyhydroxy polymer compound has a moisture balance , the adsorption of water vapor saturation, wherein when it is heated to evaporate water, thereby reducing the sense of electronic tobacco drying gas; electronic cigarette filter according to the present invention with water in the liquid electronic tobacco without the need to reduce the feeling of dryness, solved electronic tobacco smoke was not too much water otherwise it will cause problems for poor solubility of fat-soluble flavors and spices and ease of modification of electronic tobacco liquid;

[0021] 3、制备工艺简单、成本低廉。 [0021] 3. The preparation process is simple and low cost.

具体实施方式 Detailed ways

[0022] 下面结合实施例对本发明作进一步的说明,但不应理解为对本发明的限制。 [0022] The following embodiments in conjunction with embodiments of the present invention will be further described, but should not be construed as limiting the present invention.

[0023] 实施例 [0023] Example

[0024] 对比实施例 [0024] Comparative Example

[0025] 仅包含滤嘴基质醋酸纤维的普通电子烟滤嘴0。 [0025] Common electronic cigarette filter containing only cellulose acetate filter matrix 0.

[0026] 实施例1-13 [0026] Example 1-13

[0027] 将多羟基高分子化合物壳聚糖、聚乙烯醇、环糊精和多羟基螯合树脂中的一种或多种经过水分平衡,得到处于吸附水蒸气达饱和状态的改性添加剂。 [0027] The polyhydroxy polymer compound chitosan, polyvinyl alcohol, cyclodextrin polyhydroxy chelating resin and one or more through the water balance, modifying additive resulting in saturation of adsorption of water vapor. 然后将这些经过处理的多羟基高分子化合物按相对于实施例1-13中各滤嘴基质一定的质量比加入到各滤嘴基质中,制成电子烟滤嘴1-13,根据实际需要也可以将以上滤嘴与醋酸纤维滤嘴通过嘴棒成型机复合成二元复合滤嘴或三元复合滤嘴。 These are then processed through the polyhydroxy polymer compound according to Examples 1-13 with respect to each of the embodiments of the filter constant mass ratio matrix was added to each filter matrix, the electronic cigarette made of a filter 1-13, according to actual needs also acetate fiber filter with filter above may be combined into binary complex or ternary complex filter through the mouth of the filter rod machine.

[0028] 对比实施例及实施例1-13滤嘴基质中的添加材料、添加量及滤嘴基质如表1所示: [0028] Comparative Examples 1-13 and add filter matrix material in this embodiment, the filter matrix and the addition amount shown in Table 1:

[0029] 表1:对比实施例及实施例1-13中的滤嘴情况 [0029] Table 1: Examples 1-13 of the filter case and Comparative Example embodiments

Figure CN104687253BD00051

[0031] 实施例1-13中所用的多羟基高分子化合物类型以及所述多羟基高分子化合物的在水分平衡过程中的平衡温度、平衡时间以及平衡湿度如表2所示: [0031] Example 1-13 polyhydroxy polymer compound equilibrium temperature and the type of the polyhydroxy polymer compound in the water balance of the process, and the equilibrium moisture equilibration time shown in Table 2:

[0032] 表2:实施例1-13中多羟基高分子化合物的水分平衡条件 [0032] Table 2: Examples Moisture equilibrium polyhydroxy polymer compound of embodiment 1-13

Figure CN104687253BD00061

[0034] 以对比实施例及实施例1-13中的滤嘴0-13为滤嘴制成电子烟,电子烟其余部分完全相同。 [0034] In Comparative Examples 1-13 and the filter of Example 0-13 as electronic cigarette made of a filter, the same as the rest of the electronic cigarette. 对制成的不同电子烟进行人工抽吸并以人工评吸的方式进行评判,在抽吸过程中评价甜腻感及干燥感,结果如表3所示,其中得分越高,说明甜腻感或干燥感越低,口感越好: Different electronic cigarette made manually aspirated and the manner of doing Smoking judge, sweet sensation and dry feeling evaluated during aspiration, the results shown in Table 3, wherein the higher the score, the sense explained sweet or lower the dryness, the better the taste:

[0035] 表3:包含对比实施例及实施例1-13的滤嘴的电子烟吸食口感评价 [0035] Table 3: Comparative Example comprises Examples 1-13 and filter electronic cigarette smoking embodiment sensory evaluation

Figure CN104687253BD00071

[0037]通过表3对电子烟烟气甜腻感和干燥感的评价结果可以看出,本发明的滤嘴相对于现有技术中的滤嘴可以显著降低电子烟烟气的甜腻感并降低其干燥感。 [0037] As can be seen by the results of the evaluation electronic tobacco sweet gas and dry feel in Table 3, the filter of the present invention relative to the prior art sense of the filter can significantly reduce the sweet gas and electronic tobacco reduce dryness.

Claims (6)

1. 一种降低电子烟烟气甜腻感的滤嘴,其特征在于,所述滤嘴的滤嘴基质中包含一种或多种多羟基高分子化合物,所述多羟基高分子化合物经过水分平衡,处于吸附水蒸气饱和状态;所述多羟基高分子化合物为壳聚糖、聚乙烯醇、环糊精或多羟基螯合树脂;所述多羟基高分子化合物的水分平衡条件为:温度为15-30°c,湿度为60-100%,平衡时间为12-48h〇 1. A method for reducing electronic tobacco sense sweet gas filter, wherein the filter of the filter matrix comprises one or more polyhydroxy polymer compound, the polymer compound has a moisture polyhydroxy equilibrium, the adsorption of water vapor saturation; the polyhydroxy polymer compound is chitosan, polyvinyl alcohol, cyclodextrin or polyhydroxy chelating resin; equilibrium moisture condition of the polyhydroxy polymer compound is: temperature 15-30 ° c, humidity of 60-100%, equilibration time 12-48h〇
2. 根据权利要求1所述的滤嘴,其特征在于,所述滤嘴基质为醋酸纤维丝束、丙酸纤维丝束或聚丙烯丝束。 2. The filter according to claim 1, wherein the matrix is ​​a cellulose acetate filter tow, fiber tow or polypropylene tow acid.
3. 根据权利要求1所述的滤嘴,其特征在于,所述多羟基高分子化合物的添加量为滤嘴基质质量的1%_20%。 3. The filter according to claim 1, wherein the addition amount of 1% _20% by mass of the matrix of the filter polyhydroxy polymer compound.
4. 根据权利要求1所述的滤嘴,其特征在于,所述滤嘴的结构为一元功能型滤嘴、二元复合滤嘴或三元复合滤嘴。 4. The filter according to claim 1, characterized in that said filter structure is a filter-type neuronal function, filter binary complex or ternary composite filters.
5. 根据权利要求1所述的滤嘴,其特征在于,所述滤嘴的嘴端部具有封膜或封盖。 5. The filter according to claim 1, wherein the mouth end of the filter having a sealing film or cover.
6. —种电子烟,其特征在于,具有权利要求1所述的降低电子烟烟气甜腻感的滤嘴。 6. - electronic cigarette, characterized in that, having reduced electronic tobacco claim sweet gas filter of claim 1 sense.
CN201510003053.3A 2015-01-05 2015-01-05 A method for reducing electronic tobacco filter and a sense of sweet gas comprising the electronic cigarette filter tips CN104687253B (en)

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