CN104490657A - Menthol microcapsule and application of menthol microcapsule in toothpaste - Google Patents

Menthol microcapsule and application of menthol microcapsule in toothpaste Download PDF

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CN104490657A
CN104490657A CN 201410711659 CN201410711659A CN104490657A CN 104490657 A CN104490657 A CN 104490657A CN 201410711659 CN201410711659 CN 201410711659 CN 201410711659 A CN201410711659 A CN 201410711659A CN 104490657 A CN104490657 A CN 104490657A
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menthol
microcapsule
toothpaste
microcapsules
application
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CN 201410711659
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Chinese (zh)
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袁彦洁
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重庆小丸科贸有限公司
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Abstract

The invention discloses a menthol microcapsule and application of the menthol microcapsule in toothpaste. According to the menthol microcapsule disclosed by the invention, a capsule wall comprises oxidized starch; a capsule core comprises menthol and an active material; a mass ratio of the capsule core to the capsule wall is (1 to 2)-(1 to 4); the menthol microcapsule is prepared by virtue of a spray drying method; the embedding rate of the microcapsule is 93 percent; and the embedding effect is excellent. The menthol microcapsule disclosed by the invention is added into the toothpaste, a refreshing and lasting flavor is brought to the toothpaste, the toothpaste has a certain biological effect by virtue of the embedded active ingredient in the microcapsule, and the application range of the toothpaste is widened.

Description

一种薄荷脑微胶囊及其在牙膏中的应用 Menthol one kind of the microcapsules and its application in a toothpaste

技术领域 FIELD

[0001] 本发明属于微胶囊领域,具体涉及一种薄荷脑微胶囊及其在牙膏中的应用。 [0001] The present invention belongs to the field of microcapsules, in particular to a microcapsule menthol Its Application in toothpaste.

[0002] [0002]

背景技术 Background technique

[0003] 牙膏作为日常生活用品,每天被人们用来清洁牙齿,是最主要的洁齿、爽口产品。 [0003] toothpaste as daily necessities, every day people are used to clean teeth, tooth cleaning is the most important, tasty products. 随着人们生活水平的提高,传统具有清洁功能的牙膏已经不能满足消费者的需求,而目前市面上的牙膏产品多数采用传统加工工艺制得,比较单一,逐渐地不具有市场前景。 As people's living standards improve, the traditional toothpaste has a cleaning function can not meet consumer demand, while the majority of products currently on the market toothpaste made using the traditional process, relatively simple, gradually has no market prospects. 开发更具有市场前景的牙膏产品刻不容缓。 Toothpaste product development, market prospects more urgent.

[0004] 传统的香精因比较容易挥发且容易氧化变质,而限制了使用范围。 [0004] Comparison of traditional flavor due to oxidative deterioration and easily volatile, and limit the use range. 微胶囊技术作为一种新技术,可以将热敏或光敏性物质通过包埋的方式保护起来,从而减少香精香料与外界不良环境因素接触,进而可以防止其氧化变质,减少了其挥发损失的可能性,让香味达到缓慢释放的效果。 Microencapsulation technology as a new technology, the thermosensitive or photosensitive material may be protected by embedding manner, to reduce contact with the outside flavors and fragrances adverse environmental factors, and thus it is possible to prevent oxidative deterioration which reduces the volatilization losses may sex, let scent achieve slow release of results. 然而目前添加入牙膏中的微胶囊产品,仅对香精成分如薄荷进行包埋,即仅给现有牙膏带来了清新的香气,其市场拓宽前景仍有限,不能满足人们对养生健康日益增加的需求。 However, there is added to toothpaste microcapsule products, flavors and ingredients such as peppermint only be embedded, that just brings fresh scent to existing toothpaste, broaden its market prospects are still limited, can not meet the people's growing health healthy demand.

[0005] 植物精华是日前倍受大众关注的热点,植物精华即对植物中的生物活性物质进行提取,使这些生物活性物质富集,让人们能直接利用到最核心的生物活性而达到一定的养生效果,如抗衰老,抗炎症,杀菌等。 [0005] plant extracts is much focus public attention recently, namely plant extracts of plant bioactive substances were extracted, so that these biologically active substances enriched, so that people can directly use the core of the biological activity of certain health effects, such as anti-aging, anti-inflammatory, sterilization and so on. 由此可见,将这一概念引入牙膏产品中,将带来一定的市场效益。 Thus, the introduction of the concept of toothpaste products, the market will bring some benefits. 然而这些植物活性成分也是热敏或光敏性物质,容易受外界环境影响而破坏,因此如何对这些植物活性成分进行保护也是要考虑的问题之一。 However, these plants are also heat-sensitive active ingredients or photosensitive material, vulnerable to external influences and damage, so how protection is also one of the issues to be considered active ingredients of these plants.

[0006] [0006]

发明内容 SUMMARY

[0007] 针对现有技术存在的上述不足,本发明是针对现有牙膏产品较为单一,且香精、植物精华等易被外界环境影响所破坏,而提供一种包裹薄荷脑和活性成分的微胶囊及其在牙膏中的应用。 [0007] For the above-described disadvantages of the prior art, the present invention is directed to a more conventional single dentifrice product, and flavors, plant extracts and other easily damaged by the external environment, to provide microcapsules An enclosing menthol and the active ingredient and its application in toothpaste.

[0008] 为了解决上述技术问题,本发明采用如下技术方案:一种薄荷脑微胶囊,囊壁包括氧化淀粉,囊芯包括薄荷脑和活性物质;所述囊芯和囊壁的质量比为1:2~1:4 ;所述薄荷脑微胶囊通过喷雾干燥法制得。 [0008] To solve the above problems, the present invention adopts the following technical solutions: A menthol microcapsule wall include oxidized starch, the capsule core comprising the active substance and menthol; mass ratio of the core and the wall of the bladder 1 : 2 to 1: 4; the menthol microcapsules obtained by spray drying.

[0009] 一种薄荷脑微胶囊在牙膏中的应用,采用上述薄荷脑微胶囊。 Application in toothpaste [0009] A microcapsule menthol, menthol above-described microcapsules.

[0010] 相比现有技术,本发明具有如下有益效果: [0010] Compared with the prior art, the present invention has the following advantages:

1、本发明薄荷脑微胶囊,颗粒为规整的球形,囊壁具有均匀的厚度,且具有均匀的强度,能保留微胶囊完美的球形不被破坏,不会造成囊芯泄露的问题。 1, menthol microcapsules of the invention, particles of regular spherical shape, having a uniform wall thickness and uniform strength can be retained perfectly spherical microcapsule is not destroyed, it will not cause the capsule core leakage problems.

[0011] 2、本发明薄荷脑微胶囊为固体坚硬的颗粒,但是当被添加入牙膏中,在牙膏中浸润一段时间后,可以溶胀变软,使消费者在刷牙时,可以通过外力,破坏微胶囊的结构,进而可以让其中的成分瞬间释放,达到效果。 [0011] 2, menthol microcapsules of the invention is a hard solid particles, but when added into toothpaste, the toothpaste in some time after wetting, the swelling can be softened, so that consumers during brushing, by an external force, damage structure of the microcapsules, and further wherein the composition allows instant release, achieve the desired effect.

[0012] 3、本发明薄荷脑微胶囊包埋效果好,包埋率达93%,可以对包埋在其中的香精和活性成分起到良好的保护作用。 [0012] 3, the present invention is menthol embedding effect good microencapsulation, embedded in 93%, to be embedded in the flavors and active ingredients which play a good protective effect.

[0013] 4、本发明薄荷脑微胶囊中添加了金缕梅、蔓越莓或葡萄籽提取物,可以通过这些活性物质的生物活性,达到一定的预防治疗效果,赋予了牙膏一定的生物功效,拓宽了牙膏的应用面。 [0013] 4, the present invention microcapsule menthol added hamamelis, cranberry, or grape seed extract, by biological activity of these active substances, a certain therapeutic effect of preventing, given the biological efficacy of certain toothpaste broaden the application of surface toothpaste.

[0014] [0014]

具体实施方式 detailed description

[0015] 下面结合实施例对本发明作进一步详细说明。 [0015] The following embodiments in conjunction with embodiments of the present invention is described in further detail.

[0016] 本发明中如无特别说明,所用原料均为市售。 [0016] In the present invention, unless otherwise indicated, the raw materials are commercially available.

[0017] 实施例1 [0017] Example 1

以马铃薯氧化淀粉为囊壁主要原料,薄荷脑和金缕梅提取物为囊芯主要原料,其中金缕梅提取物可以通过超临界萃取方式得到,本实施例按照上述方法实现: Oxidized potato starch as the main raw material wall, witch hazel extract and menthol as core main raw material, wherein witch hazel extract can be obtained by supercritical extraction embodiment, the present embodiment implements the above method:

(1)称取40g薄荷脑和1g金缕梅提取物,溶于10mL乙醇中,搅拌均匀; (1) Weigh 1g 40g menthol and witch hazel extract, dissolved in 10mL of ethanol, stir;

(2)称取10g马铃薯氧化淀粉,溶于200mL纯水中,加热至90°C,搅拌反应30min,得到糊化淀粉溶液; (2) Weigh 10g oxidized potato starch, dissolved in 200mL of purified water and heated to 90 ° C, the reaction was stirred for 30min, to obtain a solution of gelatinized starch;

(3)向步骤(2)糊化淀粉溶液中添加步骤(I)配好的溶液,用超高速分散机混合均匀,运用喷雾干燥机,对混合溶液进行喷雾干燥,得本实施例1薄荷脑微胶囊,该微胶囊直径为1000 μ mD (3) step (2) of gelatinized starch was added in step (I) with a good solution, ultra high-speed disperser with mixing, using a spray dryer, the mixed solution was spray-dried to give Example 1 of the present embodiment Menthol microcapsules, the microcapsules having a diameter of 1000 μ mD

[0018] (4)将薄荷脑微胶囊以0.2%质量百分数的添加量加入到牙膏中,搅拌均匀,得添加薄荷脑微胶囊的牙膏。 [0018] (4) The microcapsules menthol added in an amount of 0.2% added to the mass percentage of toothpaste, stir, add toothpaste to obtain microcapsule menthol.

[0019] 通过实验测得,该微胶囊包埋率达93.11%,对包埋的物质具有极佳的保护作用。 [0019] measured experimentally, the microencapsulation rate of 93.11%, has excellent protective effect on substance embedded. 本实施例薄荷脑微胶囊通过薄荷脑和金缕梅提取物的协同作用,给牙膏带来清新的风味,且使牙膏具有杀菌的效果,抑制了口腔的真菌感染;金缕梅中含有的特殊柔敏因子,能舒缓牙龈,可以有效避免牙周炎的发生,给消费者带来多重的消费体验。 Special contained witch hazel; Example menthol microcapsules synergistically menthol and witch hazel extract, to bring a fresh flavor to toothpaste, toothpaste and having a bactericidal effect, inhibit fungal infections of the oral cavity of the present embodiment soft, sensitive factor, can soothe the gums, can effectively prevent the occurrence of periodontitis, giving consumers multiple shopping experience.

[0020] 实施例2 [0020] Example 2

以大米氧化淀粉为囊壁主要原料,薄荷脑和蔓越莓提取物为囊芯主要原料,其中蔓越莓提取物可以通过超声波辅助提取的方式得到,本实施例按照上述方法实现: Oxidized rice starch as the main raw material wall, cranberry extract and menthol as core main raw material, wherein the cranberry extract may be obtained by ultrasound-assisted extraction manner, the present embodiment implements the above method:

(1)称取120g薄荷脑和20g金缕梅提取物,溶于200mL无水乙醇中,搅拌均匀; (1) Weigh 120g 20g menthol and witch hazel extract, was dissolved in 200mL anhydrous ethanol, mix well;

(2)称取420g大米氧化淀粉,溶于500mL纯水中,加热至10(TC,搅拌反应40min,得到糊化淀粉溶液; (2) Weigh 420g of rice starch oxidized, dissolved in 500mL of purified water and heated to 10 (TC, the reaction was stirred for 40min, to obtain a solution of gelatinized starch;

(3)向步骤(2)糊化淀粉溶液中添加步骤(I)配好的溶液,用超高速分散机混合均匀,运用喷雾干燥机,对混合溶液进行喷雾干燥,得本实施例2薄荷脑微胶囊,该微胶囊直径为1400 μ mD (3) step (2) of gelatinized starch was added in step (I) with a good solution, ultra high-speed disperser with mixing, using a spray dryer, the mixed solution was spray-dried to give Example 2 of the present embodiment Menthol microcapsules, the microcapsules having a diameter of 1400 μ mD

[0021] (4)将薄荷脑微胶囊以0.3%质量百分数的添加量加入到牙膏中,搅拌均匀,得添加了薄荷脑微胶囊的牙膏。 [0021] (4) The microcapsules menthol added in an amount of 0.3% added to the mass percentage of toothpaste, stir, add toothpaste to obtain microcapsule menthol.

[0022] 通过实验测得,该微胶囊包埋率达93.62%,对包埋的物质具有极佳的保护作用。 [0022] measured experimentally, the microencapsulation rate of 93.62%, has excellent protective effect on substance embedded. 本实施例薄荷脑微胶囊通过薄荷脑和蔓越莓提取物的协同作用,给牙膏带来清新的风味,且使牙膏具有杀菌的效果,抑制了口腔的致病菌的生长与繁殖,阻止了致病菌与口腔细胞的粘附,有效地预防了感染类疾病的发生,给消费者带来多重的消费体验。 Menthol present embodiment synergistically microcapsule menthol and cranberry extracts bring fresh flavor to toothpaste, toothpaste and having a bactericidal effect, inhibits the growth and reproduction of pathogenic bacteria in the oral cavity, preventing adhesion of oral bacteria and cells, effectively prevent the occurrence of infective diseases, giving consumers multiple shopping experience.

[0023] 实施例3 [0023] Example 3

以芭蕉芋氧化淀粉为囊壁主要原料,薄荷脑和葡萄籽提取物为囊芯主要原料,其中葡萄籽提取物可以通过微波辅助萃取的方式得到,本实施例按照上述方法实现: Canna starch is oxidized to the main wall material, menthol, and grape seed extract as core main raw material, wherein the grape seed extract can be obtained by microwave assisted extraction manner, the present embodiment implements the above method:

(1)称取80g薄荷脑和1g葡萄籽提取物,溶于150mL乙醇中,搅拌均匀; (1) Weigh 1g 80g menthol and grape seed extract, was dissolved in 150mL of ethanol, stir;

(2)称取360g芭蕉芋氧化淀粉,溶于600mL纯水中,加热至95°C,搅拌反应35min,得到糊化淀粉溶液; (2) Weigh 360g canna starch oxidized, dissolved in 600mL of purified water and heated to 95 ° C, the reaction was stirred for 35min, to obtain a solution of gelatinized starch;

(3)向步骤(2)糊化淀粉溶液中添加步骤(I)配好的溶液,用超高速分散机混合均匀,运用喷雾干燥机,对混合溶液进行喷雾干燥,得本实施例3薄荷脑微胶囊,该微胶囊直径为1800 μ mD (3) step (2) of gelatinized starch was added in step (I) with a good solution, ultra high-speed disperser with mixing, using a spray dryer, the mixed solution was spray-dried to give Example 3 of the present embodiment Menthol microcapsules, the microcapsules having a diameter of 1800 μ mD

[0024] (4)将薄荷脑微胶囊以0.5%质量百分数的添加量加入到牙膏中,搅拌均匀,得添加了薄荷脑微胶囊的牙膏。 [0024] (4) The microcapsules menthol added in an amount of 0.5% added to the mass percentage of toothpaste, stir, add toothpaste to obtain microcapsule menthol.

[0025] 通过实验测得,该微胶囊包埋率达93.75%,对包埋的物质具有极佳的保护作用。 [0025] measured experimentally, the microencapsulation rate of 93.75%, has excellent protective effect on substance embedded. 本实施例薄荷脑微胶囊通过薄荷脑和葡萄籽提取物的协同作用,给牙膏带来清新的风味,且使牙膏具有黏膜保护作用,可以有效地保护口腔黏膜,预防了口腔炎、口腔溃疡的发生,给消费者带来多重的消费体验。 Menthol present embodiment synergistic microcapsules by menthol extract and grape seed, to bring a fresh flavor to toothpaste, toothpaste and mucosal protective effect, can effectively protect the oral mucosa, the preventing stomatitis, oral ulcers occur, giving consumers multiple shopping experience.

[0026] 最后说明的是,以上实施例仅用以说明本发明的技术方案而非限制,尽管申请人参照较佳实施例对本发明进行了详细说明,本领域的普通技术人员应当理解,对本发明的技术方案进行修改或者等同替换,而不脱离本发明技术方案的宗旨和范围的,均应涵盖在本发明的权利要求范围当中。 [0026] Finally is noted that, the above embodiments are intended to illustrate and not limit the present invention, although the applicant of the present invention has been described in detail with reference to preferred embodiments, those of ordinary skill in the art will be appreciated that the present invention technical solutions modifications or equivalent replacements without departing from the spirit and scope of the technical solutions of the present invention, which should fall in the scope of claims of the present invention as claimed.

Claims (7)

  1. 1.一种薄荷脑微胶囊,其特征在于:囊壁包括氧化淀粉,囊芯包括薄荷脑和活性物质;所述囊芯和囊壁的质量比为1:2~1:4 ;所述薄荷脑微胶囊通过喷雾干燥法制得。 A microcapsule menthol, characterized in that: the wall comprises oxidized starch, the capsule core comprising the active substance and menthol; mass ratio of the core and a capsule wall is 1: 2 to 1: 4; the mint brain microcapsules obtained by spray drying.
  2. 2.根据权利要求1所述薄荷脑微胶囊,其特征在于,所述微胶囊的直径为1000~1800μ m0 1-menthol according to claim microcapsules, wherein said microcapsules having a diameter of 1000 ~ 1800μ m0
  3. 3.根据权利要求1所述薄荷脑微胶囊,其特征在于,所述氧化淀粉选自马铃薯氧化淀粉、大米氧化淀粉或芭蕉芋氧化淀粉。 3. The method of claim 1 menthol microcapsules, wherein said oxide is selected from potato starch, oxidized starch, oxidized starch, rice starch or oxidized Canna.
  4. 4.根据权利要求1所述薄荷脑微胶囊,其特征在于,所述活性物质选自金缕梅、蔓越莓或葡萄籽提取物。 1-menthol according to the microcapsules claimed in claim, characterized in that the active substance is selected from witch hazel, cranberry, or grape seed extract.
  5. 5.根据权利要求4所述薄荷脑微胶囊,其特征在于,所述薄荷脑与活性物质的质量比为4:1〜8:1。 4 according to the claim microcapsule menthol, wherein the menthol and the mass ratio of the active material 4: 1~8: 1.
  6. 6.薄荷脑微胶囊在牙膏中的应用,其特征在于,采用权利要求1~5任一薄荷脑微胶囊。 6. Application in toothpaste menthol microcapsules, wherein any one of 1 to 5 using a microcapsule menthol claims.
  7. 7.薄荷脑微胶囊在牙膏中的应用,其特征在于,采用权利要求1~5任一薄荷脑微胶囊,所述薄荷脑微胶囊按0.2-0.5%质量百分数的添加量,加入到牙膏中。 7. Application of the microcapsule menthol in toothpaste, characterized in that, using any one of claims 1 to 5, a microcapsule menthol, a menthol microcapsules by adding an amount of 0.2-0.5% by mass percent, was added to a toothpaste .
CN 201410711659 2014-12-01 2014-12-01 Menthol microcapsule and application of menthol microcapsule in toothpaste CN104490657A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105411875A (en) * 2015-12-14 2016-03-23 安徽丰乐香料有限责任公司 Preparation method of high-content menthol talcum powder

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105411875A (en) * 2015-12-14 2016-03-23 安徽丰乐香料有限责任公司 Preparation method of high-content menthol talcum powder

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