CN104478558A - Aquatic weed growth promoter with antibacterial effect - Google Patents
Aquatic weed growth promoter with antibacterial effect Download PDFInfo
- Publication number
- CN104478558A CN104478558A CN201410654909.9A CN201410654909A CN104478558A CN 104478558 A CN104478558 A CN 104478558A CN 201410654909 A CN201410654909 A CN 201410654909A CN 104478558 A CN104478558 A CN 104478558A
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- aquatic
- growth promoter
- microbial effect
- nano silicon
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Classifications
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
- C05D9/00—Other inorganic fertilisers
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
Abstract
The invention discloses an aquatic weed growth promoter with an antibacterial effect. The aquatic weed growth promoter comprises the following components in parts by weight: 2-5 parts of nano silicon oxide, 3-10 parts of humic acid, 8-15 parts of Chinese angelica, 10-20 parts of folium isatidis, 5-10 parts of roots of large-flowered skullcap, 5-10 parts of fructus aurantii, 3-5 parts of fructus forsythia, 2-10 parts of licorice and 1-3 parts of a dispersant. The invention also provides a preparation method of the aquatic weed growth promoter. The aquatic weed growth promoter with the antibacterial effect, provided by the invention, not only can promote healthy growth of aquatic weeds, but also can disinfect and purify fisheries water, and is nontoxic and favorable for environmental protection.
Description
Technical field:
The present invention relates to aquaculture field, be specifically related to a kind of growth promoter for aquatic with anti-microbial effect.
Background technology:
In the freshwater shrimps and crabs class pond aquaculture of China, the growth of pasture and water is stablized maintenance pond ecosystem, and raising cultured output and benefit have great importance.Pasture and water are habitat and the sanctuary of many hydrocoles, meanwhile, are also many animals, as the food of snail, teal etc.Under light illumination, oxygen pours in water by pasture and water constantly, thus provides sufficient oxygen to aquatic animal.Therefore, in aquaculture, it is extremely important for how making pasture and water grow fast.
At present, plant-growth regulator the most frequently used on market is Plant hormones regulators,gibberellins, ethrel, naphthylacetic acid etc. mainly, and it not only can make breeding water be polluted, and also can remain toxic substance in the animal body of edible pasture and water.
Summary of the invention:
For solving the problem, the invention provides a kind of growth promoter for aquatic with anti-microbial effect.The growth promoter for aquatic with anti-microbial effect provided by the invention, not only can promote pasture and water healthy growth, all right sterilization and disinfection, and fisheries water of purifying waste water is nontoxic, is conducive to environment protection.
For achieving the above object, the present invention adopts following technical scheme:
There is a growth promoter for aquatic for anti-microbial effect, with parts by weight, comprise following component:
Nano silicon oxide 2-5 part, humic acids 3-10 part, Radix Angelicae Sinensis 8-15 part,
Leaf of Indigowoad 10-20 part, root of large-flowered skullcap 5-10 part, Fructus Aurantii 5-10 part,
Capsule of weeping forsythia 3-5 part, Radix Glycyrrhizae 2-10 part, dispersion agent 1-3 part.
Preferred as technique scheme, a kind of growth promoter for aquatic with anti-microbial effect, with parts by weight, comprises following component:
Nano silicon oxide 3 parts, humic acids 5 parts, Radix Angelicae Sinensis 10 parts,
Leaf of Indigowoad 12 parts, the root of large-flowered skullcap 5 parts, Fructus Aurantii 7 parts,
The capsule of weeping forsythia 3 parts, 5 parts, Radix Glycyrrhizae, dispersion agent 1 part.
For solving the problem, present invention also offers the preparation method of described nano silicon oxide, comprising the following steps:
(1) get tetraethoxy in an Erlenmeyer flask, add ethanol, glacial acetic acid respectively, be uniformly mixed;
(2) continue dropwise to add triethylamine in Erlenmeyer flask, stir 20-40min, obtain mixed solution;
(3) mixed solution step (2) obtained, at 120-180 DEG C, refluxes, and continues to stir during backflow, after 5-15h, stops stirring and backflow;
(4) mixed solution in Erlenmeyer flask is cooled to room temperature, filters and obtain white precipitate, precipitate 5-10 time with deionized water wash, be transferred in glassware by the precipitation after washing, 80 DEG C of vacuum-dryings, obtain nano silicon oxide.
Preferred as technique scheme, in step (1), the volume ratio of tetraethoxy, ethanol, glacial acetic acid is 1:20:20.
Preferred as technique scheme, step (3) described reflux temperature is 180 DEG C, and return time is 12h.
Preferred as technique scheme, preparing gained nano silicon oxide is spheroidal particle, and particle diameter is 5-10nm.
Present invention also offers the preparation method that this has the pasture and water promotor of anti-microbial effect, comprise the following steps:
(1) Radix Angelicae Sinensis, Leaf of Indigowoad, the root of large-flowered skullcap, Fructus Aurantii, the capsule of weeping forsythia, Radix Glycyrrhizae are dried, be milled into powder, be transferred in homogenizer, and add the ethanol of 98%, under the state of 8000-12000 rev/min, stir 5-10h, filter, obtain extracting solution;
(2) extracting solution is transferred in beaker adds humic acids, be uniformly mixed, obtain mixed solution;
(3) add nano silicon oxide, dispersion agent, ultrasonic 2-3h in the mixing solutions obtained to step (2), obtain the growth promoter for aquatic with anti-microbial effect.
Preferred as technique scheme, in step (1), the mass ratio of powder and ethanol is 1:10.
Preferred as technique scheme, step (3) described dispersion agent is sodium lauryl sulphate.
Beneficial effect of the present invention is:
(1) the nano silicon oxide good dispersity prepared, degree of crystallinity is high, and its element silicon contained is equivalent to growth hormone, when growing for pasture and water, can promote the quick healthy growth of pasture and water; And under light illumination, nano silicon oxide transition of electron can occur, thus form hydroxyl radical free radical isoreactivity group, it can destroy bacteria cell wall, thus is killed by bacterium, reaches the effect of purifying waste water.
(2) growth promoter for aquatic with anti-microbial effect provided by the invention, nontoxic, is conducive to environment protection.
Embodiment:
For a better understanding of the present invention, below by several case study on implementation the present invention further explained and illustrate, but this can't form any restriction to the present invention.
Embodiment 1
There is a growth promoter for aquatic for anti-microbial effect, with parts by weight, comprise following component:
Nano silicon oxide 2 parts, humic acids 3 parts, Radix Angelicae Sinensis 8 parts,
Leaf of Indigowoad 10 parts, the root of large-flowered skullcap 5 parts, Fructus Aurantii 5 parts,
The capsule of weeping forsythia 3 parts, 2 parts, Radix Glycyrrhizae, dispersion agent 1 part.
Its preparation method, comprises the following steps:
(1) 8 parts of Radix Angelicae Sinensis, 10 portions of Leaf of Indigowoad, 5 portions of roots of large-flowered skullcap, 5 portions of Fructus Aurantiis, 3 portions of capsules of weeping forsythia, 2 portions of Radix Glycyrrhizaes are dried, be milled into powder, be transferred in homogenizer, and add the ethanol of 98%, under the state of 8000 revs/min, stir 5h, filter, obtain extracting solution;
(2) extracting solution is transferred in beaker adds 3 parts of humic acidss, be uniformly mixed, obtain mixed solution;
(3) add 2 parts of nano silicon oxides, 1 part of dispersion agent in the mixing solutions obtained to step (2), ultrasonic 2h, obtains the growth promoter for aquatic with anti-microbial effect.
Embodiment 2
There is a growth promoter for aquatic for anti-microbial effect, with parts by weight, comprise following component:
Nano silicon oxide 5 parts, humic acids 10 parts, Radix Angelicae Sinensis 15 parts,
Leaf of Indigowoad 20 parts, the root of large-flowered skullcap 10 parts, Fructus Aurantii 10 parts,
The capsule of weeping forsythia 5 parts, 10 parts, Radix Glycyrrhizae, dispersion agent 3 parts.
Its preparation method, comprises the following steps:
(1) 15 parts of Radix Angelicae Sinensis, 20 portions of Leaf of Indigowoad, 10 portions of roots of large-flowered skullcap, 10 portions of Fructus Aurantiis, 5 portions of capsules of weeping forsythia, 10 portions of Radix Glycyrrhizaes are dried, be milled into powder, be transferred in homogenizer, and add the ethanol of 98%, under the state of 12000 revs/min, stir 10h, filter, obtain extracting solution;
(2) extracting solution is transferred in beaker adds 10 parts of humic acidss, be uniformly mixed, obtain mixed solution;
(3) add 5 parts of nano silicon oxides, 3 parts of dispersion agents in the mixing solutions obtained to step (2), ultrasonic 3h, obtains the growth promoter for aquatic with anti-microbial effect.
Embodiment 3
There is a growth promoter for aquatic for anti-microbial effect, with parts by weight, comprise following component:
Nano silicon oxide 3 parts, humic acids 5 parts, Radix Angelicae Sinensis 9 parts,
Leaf of Indigowoad 12 parts, the root of large-flowered skullcap 6 parts, Fructus Aurantii 6 parts,
The capsule of weeping forsythia 4 parts, 3 parts, Radix Glycyrrhizae, dispersion agent 2 parts.
Its preparation method, comprises the following steps:
(1) 9 parts of Radix Angelicae Sinensis, 12 portions of Leaf of Indigowoad, 6 portions of roots of large-flowered skullcap, 6 portions of Fructus Aurantiis, 4 portions of capsules of weeping forsythia, 3 portions of Radix Glycyrrhizaes are dried, be milled into powder, be transferred in homogenizer, and add the ethanol of 98%, under the state of 9000 revs/min, stir 6h, filter, obtain extracting solution;
(2) extracting solution is transferred in beaker adds 5 parts of humic acidss, be uniformly mixed, obtain mixed solution;
(3) add 3 parts of nano silicon oxides, 2 parts of dispersion agents in the mixing solutions obtained to step (2), ultrasonic 20min, obtains the growth promoter for aquatic with anti-microbial effect.
Embodiment 4
There is a growth promoter for aquatic for anti-microbial effect, with parts by weight, comprise following component:
Nano silicon oxide 3 parts, humic acids 5 parts, Radix Angelicae Sinensis 10 parts,
Leaf of Indigowoad 12 parts, the root of large-flowered skullcap 5 parts, Fructus Aurantii 7 parts,
The capsule of weeping forsythia 3 parts, 5 parts, Radix Glycyrrhizae, dispersion agent 1 part.
Its preparation method, comprises the following steps:
(1) 10 parts of Radix Angelicae Sinensis, 12 portions of Leaf of Indigowoad, 5 portions of roots of large-flowered skullcap, 7 portions of Fructus Aurantiis, 3 portions of capsules of weeping forsythia, 5 portions of Radix Glycyrrhizaes are dried, be milled into powder, be transferred in homogenizer, and add the ethanol of 98%, under the state of 10000 revs/min, stir 7h, filter, obtain extracting solution;
(2) extracting solution is transferred in beaker adds 5 parts of humic acidss, be uniformly mixed, obtain mixed solution;
(3) add 3 parts of nano silicon oxides, 1 part of dispersion agent in the mixing solutions obtained to step (2), ultrasonic 40min, obtains the growth promoter for aquatic with anti-microbial effect.
Embodiment 5
There is a growth promoter for aquatic for anti-microbial effect, with parts by weight, comprise following component:
Nano silicon oxide 3 parts, humic acids 6 parts, Radix Angelicae Sinensis 12 parts,
Leaf of Indigowoad 16 parts, the root of large-flowered skullcap 8 parts, Fructus Aurantii 8 parts,
The capsule of weeping forsythia 4 parts, 6 parts, Radix Glycyrrhizae, dispersion agent 2 parts.
Its preparation method, comprises the following steps:
(1) 12 parts of Radix Angelicae Sinensis, 16 portions of Leaf of Indigowoad, 8 portions of roots of large-flowered skullcap, 8 portions of Fructus Aurantiis, 4 portions of capsules of weeping forsythia, 6 portions of Radix Glycyrrhizaes are dried, be milled into powder, be transferred in homogenizer, and add the ethanol of 98%, under the state of 11000 revs/min, stir 8h, filter, obtain extracting solution;
(2) extracting solution is transferred in beaker adds 6 parts of humic acidss, be uniformly mixed, obtain mixed solution;
(3) add 3 parts of nano silicon oxides, 2 parts of dispersion agents in the mixing solutions obtained to step (2), ultrasonic 100min, obtains the growth promoter for aquatic with anti-microbial effect.
Embodiment 6
There is a growth promoter for aquatic for anti-microbial effect, with parts by weight, comprise following component:
Nano silicon oxide 3 parts, humic acids 9 parts, Radix Angelicae Sinensis 14 parts,
Leaf of Indigowoad 18 parts, the root of large-flowered skullcap 9 parts, Fructus Aurantii 9 parts,
The capsule of weeping forsythia 4 parts, 9 parts, Radix Glycyrrhizae, dispersion agent 2 parts.
Its preparation method, comprises the following steps:
(1) 14 parts of Radix Angelicae Sinensis, 18 portions of Leaf of Indigowoad, 9 portions of roots of large-flowered skullcap, 9 portions of Fructus Aurantiis, 4 portions of capsules of weeping forsythia, 9 portions of Radix Glycyrrhizaes are dried, be milled into powder, be transferred in homogenizer, and add the ethanol of 98%, under the state of 11000 revs/min, stir 9h, filter, obtain extracting solution;
(2) extracting solution is transferred in beaker adds 9 parts of humic acidss, be uniformly mixed, obtain mixed solution;
(3) add 3 parts of nano silicon oxides, 2 parts of dispersion agents in the mixing solutions obtained to step (2), ultrasonic 140min, obtains the growth promoter for aquatic with anti-microbial effect.
The growth promoter for aquatic with anti-microbial effect above-mentioned case obtained is applied to the cultivation of pasture and water respectively, and mark is sample 1, sample 2, sample 3, sample 4, sample 5, sample 6, every day observes, and records the time that pasture and water in each sample fill whole water body case, records as follows:
Form 1
From form 1, when the growth promoter for aquatic that embodiment 4 obtains being applied to pasture and water growth, pasture and water fill the shortest time of whole water body case, and the pasture and water speed of growth is the fastest, and effect is best.
The present invention can summarize with other the specific form without prejudice to spirit of the present invention or principal character.Therefore, no matter from which point, above-mentioned case study on implementation of the present invention all can only be thought explanation of the present invention and can not limit the present invention, therefore any change in the implication suitable with claims of the present invention and scope, all think to be included in the scope of claims of the present invention.
Claims (9)
1. there is a growth promoter for aquatic for anti-microbial effect, it is characterized in that, with parts by weight, comprise following component:
Nano silicon oxide 2-5 part, humic acids 3-10 part, Radix Angelicae Sinensis 8-15 part,
Leaf of Indigowoad 10-20 part, root of large-flowered skullcap 5-10 part, Fructus Aurantii 5-10 part,
Capsule of weeping forsythia 3-5 part, Radix Glycyrrhizae 2-10 part, dispersion agent 1-3 part.
2. a kind of growth promoter for aquatic with anti-microbial effect as claimed in claim 1, is characterized in that, with parts by weight, comprise following component:
Nano silicon oxide 3 parts, humic acids 5 parts, Radix Angelicae Sinensis 10 parts,
Leaf of Indigowoad 12 parts, the root of large-flowered skullcap 5 parts, Fructus Aurantii 7 parts,
The capsule of weeping forsythia 3 parts, 5 parts, Radix Glycyrrhizae, dispersion agent 1 part.
3. a kind of growth promoter for aquatic with anti-microbial effect as claimed in claim 1, it is characterized in that, the preparation method of described nano silicon oxide, comprises the following steps:
(1) get tetraethoxy in an Erlenmeyer flask, add ethanol, glacial acetic acid respectively, be uniformly mixed;
(2) continue dropwise to add triethylamine in Erlenmeyer flask, stir 20-40min, obtain mixed solution;
(3) mixed solution step (2) obtained, at 120-180 DEG C, refluxes, and continues to stir during backflow, after 5-15h, stops stirring and backflow;
(4) mixed solution in Erlenmeyer flask is cooled to room temperature, filters and obtain white precipitate, precipitate 5-10 time with deionized water wash, be transferred in glassware by the precipitation after washing, 80 DEG C of vacuum-dryings, obtain nano silicon oxide.
4. a kind of growth promoter for aquatic with anti-microbial effect as claimed in claim 3, is characterized in that: in step (1), the volume ratio of tetraethoxy, ethanol, glacial acetic acid is 1:20:20.
5. a kind of growth promoter for aquatic with anti-microbial effect as claimed in claim 3, it is characterized in that: step (3) described reflux temperature is 180 DEG C, return time is 12h.
6. a kind of growth promoter for aquatic with anti-microbial effect as claimed in claim 3, is characterized in that: preparing gained nano silicon oxide is spheroidal particle, and particle diameter is 5-10nm.
7. a kind of preparation method with the growth promoter for aquatic of anti-microbial effect as claimed in claim 1, is characterized in that comprising the following steps:
(1) Radix Angelicae Sinensis, Leaf of Indigowoad, the root of large-flowered skullcap, Fructus Aurantii, the capsule of weeping forsythia, Radix Glycyrrhizae are dried, be milled into powder, be transferred in homogenizer, and add the ethanol of 98%, under the state of 8000-12000 rev/min, stir 5-10h, filter, obtain extracting solution;
(2) extracting solution is transferred in beaker adds humic acids, be uniformly mixed, obtain mixed solution;
(3) add nano silicon oxide, dispersion agent, ultrasonic 2-3h in the mixing solutions obtained to step (2), obtain the growth promoter for aquatic with anti-microbial effect.
8. a kind of preparation method with the growth promoter for aquatic of anti-microbial effect as claimed in claim 7, is characterized in that: in step (1), the mass ratio of powder and ethanol is 1:10.
9. a kind of preparation method with the growth promoter for aquatic of anti-microbial effect as claimed in claim 7, is characterized in that: step (3) described dispersion agent is sodium lauryl sulphate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410654909.9A CN104478558A (en) | 2014-11-17 | 2014-11-17 | Aquatic weed growth promoter with antibacterial effect |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410654909.9A CN104478558A (en) | 2014-11-17 | 2014-11-17 | Aquatic weed growth promoter with antibacterial effect |
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| CN104478558A true CN104478558A (en) | 2015-04-01 |
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| CN201410654909.9A Pending CN104478558A (en) | 2014-11-17 | 2014-11-17 | Aquatic weed growth promoter with antibacterial effect |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105948855A (en) * | 2016-04-29 | 2016-09-21 | 固镇玉鹏生态农业文化园有限公司 | Nutrition material for improving growth of waterweeds in fish pond |
| CN106187541A (en) * | 2016-07-27 | 2016-12-07 | 包永兵 | A kind of alimentation composition preventing mango anthracnose |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1980750A (en) * | 2004-06-07 | 2007-06-13 | S·K·托塔斯里 | A composition for growth of diatom algae |
| CN101306965A (en) * | 2008-05-21 | 2008-11-19 | 中国水产科学研究院淡水渔业研究中心 | Growth promoter for aquatic in aquaculture pond |
| CN104030801A (en) * | 2014-05-20 | 2014-09-10 | 安徽三星化工有限责任公司 | Bioactive slow-release compound fertilizer for promoting growth |
-
2014
- 2014-11-17 CN CN201410654909.9A patent/CN104478558A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1980750A (en) * | 2004-06-07 | 2007-06-13 | S·K·托塔斯里 | A composition for growth of diatom algae |
| CN101306965A (en) * | 2008-05-21 | 2008-11-19 | 中国水产科学研究院淡水渔业研究中心 | Growth promoter for aquatic in aquaculture pond |
| CN104030801A (en) * | 2014-05-20 | 2014-09-10 | 安徽三星化工有限责任公司 | Bioactive slow-release compound fertilizer for promoting growth |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105948855A (en) * | 2016-04-29 | 2016-09-21 | 固镇玉鹏生态农业文化园有限公司 | Nutrition material for improving growth of waterweeds in fish pond |
| CN106187541A (en) * | 2016-07-27 | 2016-12-07 | 包永兵 | A kind of alimentation composition preventing mango anthracnose |
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Application publication date: 20150401 |