CN104474908B - A kind of hollow fiber ultrafiltration membrane hole blocking method - Google Patents

A kind of hollow fiber ultrafiltration membrane hole blocking method Download PDF

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Publication number
CN104474908B
CN104474908B CN201410650176.1A CN201410650176A CN104474908B CN 104474908 B CN104474908 B CN 104474908B CN 201410650176 A CN201410650176 A CN 201410650176A CN 104474908 B CN104474908 B CN 104474908B
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hollow fiber
ultrafiltration membrane
fiber ultrafiltration
film
emulsion paint
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CN104474908A (en
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陈泉学
郝艳杰
丁愿辉
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Abstract

The present invention relates to a kind of hollow fiber ultrafiltration membrane hole blocking method, it is characterised in that carry out according to the following steps: 1) smoothed out with the fingers by Board Lot hollow fiber ultrafiltration membrane silk along being bundled into pencil, load film shell; Pencil hollow fiber ultrafiltration membrane film silk one or both ends are cut flat; 2) emulsion paint, putty powder and water being proportionally configured to stifled hole glue, each substances in percentage by weight meter, wherein emulsion paint to be 65%-75%, putty powder be 1%-2.2%, water are 22.8%-34%; 3) the stifled hole glue configured is evenly coated in cuts on flat film tow end face in the complete shutoff in film silk hole. Above-mentioned stifled hole operation just enters follow-up epoxy sealing casting operation after completing. The man-hour of film pipe plug opening operation can be reduced to the 10% of former technique process man-hour by aforesaid method compared with traditional film pipe plug opening method, and substantially increases production efficiency under the prerequisite ensured the quality of products.

Description

A kind of hollow fiber ultrafiltration membrane hole blocking method
Technical field
The invention belongs to polysulfone hollow fiber ultrafiltration membrane system manufacturing technology field, particularly relate to a kind of hollow fiber ultrafiltration membrane hole blocking method.
Background technology
Polysulfone hollow fiber ultrafiltration membrane system is made up of hollow fiber ultrafiltration membrane silk, epoxy resin embedding adhesive, pipe core, hollow fiber ultrafiltration membrane plastic shell. manufacturing of polysulfone hollow fiber ultrafiltration membrane system is that on dress silk platform, hollow fiber ultrafiltration membrane is organized into pencil, two ends put mesh bag after tying, then hollow fiber ultrafiltration membrane tow is loaded in polysulfone hollow fiber ultrafiltration membrane system plastic shell, make hollow fiber ultrafiltration membrane tow in being axially placed in polysulfone hollow fiber ultrafiltration membrane system plastic shell, again hollow fiber ultrafiltration membrane tow two ends plugging material brush is blocked up, and inject epoxy resin embedding adhesive and the space between each hollow fiber ultrafiltration membrane silk is carried out shutoff, need to cut away cast layer after solidification completely, expose the interior hole of hollow fiber ultrafiltration membrane silk. what select for hollow fiber ultrafiltration membrane tow two ends plugging material at present is that terra alba and water are allocated according to a certain percentage, then block up with hairbrush brush, wait 10min-15min, after gypsum becomes dry completely, film silk end face is dialled loose, and the gypsum powder being clipped between film silk must be cleaned out, then carry out next procedure, dial the loose and cleaning about 3min-5min of gypsum.
Summary of the invention
It is an object of the invention to solve existing technical deficiency, it is to increase production efficiency and quality product, it is provided that a kind of hollow fiber ultrafiltration membrane hole blocking method, the film silk hole of shutoff of the present invention, not only not needing to wait that latex becomes dry, nor need cleaning, namely brush can carry out next procedure after having blocked up at once.
The present invention realizes the technical scheme that above-mentioned purpose adopts:
A kind of hollow fiber ultrafiltration membrane hole blocking method, it is characterised in that carry out according to the following steps: Board Lot hollow fiber ultrafiltration membrane silk is smoothed out with the fingers along being bundled into pencil by (1), loads film shell; Pencil hollow fiber ultrafiltration membrane film silk one or both ends are cut flat; (2) emulsion paint, putty powder and water being proportionally configured to stifled hole glue, each substances in percentage by weight meter, wherein emulsion paint to be 65%-75%, putty powder be 1%-2.2%, water are 22.8%-34%;(3) the stifled hole glue configured is evenly coated in cuts on flat film tow end face in the complete shutoff in film silk hole.
In step (2), the concocting method of stifled hole glue is: by water and putty powder according to the rules ratio pour in agitator, stirred even with the rotating speed of 400r/min; Then pour into respectively in agitator for two parts that the emulsion paint of regulation ratio are divided into equivalent, first part of emulsion paint is poured in agitator, stirs after 10-30 minute, then pours the 2nd part of emulsion paint into, churning time is identical with the churning time of first part, stirs obtained stifled hole glue after terminating.
After hollow fiber ultrafiltration membrane of the present invention stifled hole operation completes, just enter follow-up epoxy sealing casting operation. The man-hour of film pipe plug opening operation can be reduced to the 10% of former technique process man-hour by the inventive method compared with traditional film pipe plug opening method, and stifled hole glue brush is complete carries out subsequent processing immediately, and substantially increases production efficiency under the prerequisite ensured the quality of products.
Embodiment
Below in conjunction with example, invention is described further, but should not limit the scope of the invention with this.
Embodiment 1
Preparation stifled hole glue: each substances in percentage by weight meter, wherein emulsion paint 65%, putty powder 1%, water 34%; Water and putty powder are poured in agitator, is stirred even with the rotating speed of 400r/min; Then pouring into respectively in agitator for two parts that 65% emulsion paint are divided into equivalent, first part of emulsion paint is poured in agitator, stirs after 10 minutes, then pours the 2nd part of emulsion paint into, stirs 10 minutes, stirs obtained stifled hole glue after terminating;
Get the inside and outside polyethersulfone PES film silk through 0.9mm/1.6mm of some amount, switch to applicable length, be organized into pencil, load in the film shell that diameter is 90mm, film silk two end-grain cutting being put down, then free-hand being spread upon by pre-configured stifled hole glue is cut on flat film silk end face, emulsion thickness 2mm; After having filled fixture, injection ring oxygen sealing glue solidifying obtains membrane module; Cured layer detects after cutting, and sealing layer quality is good.
Embodiment 2
Preparation stifled hole glue: each substances in percentage by weight meter, wherein emulsion paint 75%, putty powder 2.2%, water 22.8%; Water and putty powder are poured in agitator, is stirred even with the rotating speed of 400r/min; Then pouring into respectively in agitator for two parts that 75% emulsion paint are divided into equivalent, first part of emulsion paint is poured in agitator, stirs after 30 minutes, then pours the 2nd part of emulsion paint into, stirs 30 minutes, stirs obtained stifled hole glue after terminating;
Get the inside and outside polyvinylchloride film silk through 1.5mm/2.5mm of some amount, switch to applicable length, be organized into pencil, load in the film shell that diameter is 90mm, film silk two end-grain cutting is put down, then with scraper pre-configured stifled hole glue is spread upon and cut on flat film silk end face, emulsion thickness 1mm; After having filled fixture, injection ring oxygen sealing glue solidifying obtains membrane module; Cured layer detects after cutting, and sealing layer quality is good.
Embodiment 3
Preparation stifled hole glue: each substances in percentage by weight meter, wherein emulsion paint 70%, putty powder 1.5%, water 28.5%; Water and putty powder are poured in agitator, is stirred even with the rotating speed of 400r/min; Then pouring into respectively in agitator for two parts that 70% emulsion paint are divided into equivalent, first part of emulsion paint is poured in agitator, stirs after 20 minutes, then pours the 2nd part of emulsion paint into, stirs 20 minutes, stirs obtained stifled hole glue after terminating;
Get the inside and outside polyvinylidene difluoride (PVDF) pvdf membrane silk through 0.7mm/1.3mm of some amount, switch to applicable length, it is organized into pencil, load in the film shell that diameter is 90mm, film silk two end-grain cutting is put down, then being spread upon by pre-configured stifled hole glue with scraper cuts on flat film silk end face, emulsion thickness 1.5mm;After having filled fixture, injection ring oxygen sealing glue solidifying obtains membrane module; Cured layer detects after cutting, and sealing layer quality is good.

Claims (2)

1. a hollow fiber ultrafiltration membrane hole blocking method, carries out according to the following steps: Board Lot hollow fiber ultrafiltration membrane silk is smoothed out with the fingers along being bundled into pencil by (1), loads film shell; Pencil hollow fiber ultrafiltration membrane film silk one or both ends are cut flat; It is characterized in that: emulsion paint, putty powder and water are proportionally configured to stifled hole glue by (2), each substances in percentage by weight meter, wherein emulsion paint to be 65%-75%, putty powder be 1%-2.2%, water are 22.8%-34%; (3) the stifled hole glue configured is evenly coated in cuts on flat film tow end face in the complete shutoff in film silk hole.
2. hollow fiber ultrafiltration membrane hole blocking method as claimed in claim 1 a kind of, it is characterised in that: in step (2), the concocting method of stifled hole glue is: by water and putty powder according to the rules ratio pour in agitator, stirred even with the rotating speed of 400r/min; Then pour into respectively in agitator for two parts that the emulsion paint of regulation ratio are divided into equivalent, first part of emulsion paint is poured in agitator, stirs after 10-30 minute, then pours the 2nd part of emulsion paint into, churning time is identical with the churning time of first part, stirs obtained stifled hole glue after terminating.
CN201410650176.1A 2014-11-14 2014-11-14 A kind of hollow fiber ultrafiltration membrane hole blocking method Active CN104474908B (en)

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CN104474908B true CN104474908B (en) 2016-06-08

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110960988B (en) * 2018-09-28 2022-05-24 鸿翌科技有限公司 Hollow fiber membrane packaging method
CN112774451B (en) * 2020-12-18 2022-05-13 武汉艾科滤膜技术有限公司 Hollow fiber membrane pre-plugging hole treatment method
CN112755820B (en) * 2021-01-11 2023-04-28 湖北中泉环保技术有限公司 Hollow fiber ultrafiltration membrane treatment fluid and application thereof

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JPS6349205A (en) * 1986-08-18 1988-03-02 Nok Corp Production of hollow yarn module
EP1249268B1 (en) * 2000-05-05 2005-04-06 Zenon Environmental Inc. Potting method to reduce fibre twinning
CN103657421B (en) * 2012-09-18 2015-10-21 新奥科技发展有限公司 The preparation method of hollow fiber separation membrane component
CN103785295B (en) * 2014-02-27 2016-01-27 天邦膜技术国家工程研究中心有限责任公司 A kind of hollow fiber film assembly apparatus for pouring and method thereof

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