CN104431188A - Method for processing mint composite herbal tea - Google Patents
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- CN104431188A CN104431188A CN201410783571.7A CN201410783571A CN104431188A CN 104431188 A CN104431188 A CN 104431188A CN 201410783571 A CN201410783571 A CN 201410783571A CN 104431188 A CN104431188 A CN 104431188A
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Abstract
The invention discloses a method for processing mint composite herbal tea. The method comprises the following steps of firstly, adding water into mint, folium mori, chrysanthemum, platycodon grandiflorum and liquorice respectively, and extracting so as to obtain water extracts; mixing the obtained water extracts of mint, folium mori, chrysanthemum, platycodon grandiflorum and liquorice according to the volume ratios of (16.7-37.0) to (17.4-55.6) to (9.1-38.1) to (3.7-26.1) to (3.7-19.0), and filtering; filling; and sterilizing. According to the invention, mint is used as the main raw material and is matched with folium mori, chrysanthemum, platycodon grandiflorum and liquorice, so that the mint composite herbal tea is pure in mouthfeel, is unique in flavor, and has the effects of clearing away heat, detoxifying, resisting oxidation and the like; the clearance rates to DPPH free radical and ABTS free radical respectively can reach 82.49+/-6.55% and 83.87+/-3.94% and are much higher than those of the market brand herbal tea, and the clearance rates of the market brand herbal tea are respectively only 25.16+/-1.99% and 19.67+/-2.53%.
Description
Technical field
The invention belongs to technical field of health care food, particularly relate to a kind of processing method of peppermint compound cold tea.
Background technology
Peppermint is broad-spectrum spice crop, because it contains the multiple ter penoids such as menthol, menthones, has special fragrance and mouthfeel.And its non-volatile chemical becomes to be mainly flavones and phenolic compound.As traditional Chinese herbal medicines, its existing treatment anemopyretic cold, wind-warm syndrome, from the beginning of the important medical value of the cards such as, headache, hot eyes, have scavenging free radicals anti-oxidant simultaneously, antibacterially wait health-care effect.Applicable exploitation becomes various health beverages.
Summary of the invention
For solving the problems of the technologies described above, the invention provides a kind of is primary raw material with peppermint, is equipped with mulberry leaf, chrysanthemum, Radix Glycyrrhizae, balloonflower root, develops pure in mouth feel, unique flavor have the health-care cold tea of the effect such as clearing heat and detoxicating, anti-oxidant.
For achieving the above object, the present invention is achieved by the following technical solutions.
A processing method for peppermint compound cold tea, described method comprises the steps:
(1) by peppermint, mulberry leaf, chrysanthemum, balloonflower root, Radix Glycyrrhizae extracting in water separately:
Peppermint Water extract: mixed by weight 1:10 ~ 1:60 with water by peppermint, Extracting temperature 30 ~ 100 DEG C, extraction time 5 ~ 65min, obtains Peppermint Water extract, for subsequent use after cold filtration;
Mulberry leaf Aqueous extracts: mixed by weight 1:10 ~ 1:15 with water by mulberry leaf, Extracting temperature 90 ~ 100 DEG C, extracts 2 ~ 3 times and extracts 1 ~ 1.5h at every turn, merge Aqueous extracts, for subsequent use after cold filtration;
Chrysanthemum water extract: mixed by weight 1:80 ~ 1:100 with water by chrysanthemum, Extracting temperature 90 ~ 100 DEG C, extraction time 20 ~ 25min, obtains chrysanthemum water extract, for subsequent use after cold filtration; :
Balloonflower root Aqueous extracts: mixed by weight 1:30 ~ 1:50 with water by balloonflower root, Extracting temperature 90 ~ 100 DEG C, extraction time 25 ~ 30min, obtains balloonflower root Aqueous extracts, for subsequent use after cold filtration;
Licorice water extract: Radix Glycyrrhizae is mixed by weight 1:10 ~ 1:13 with water, Extracting temperature 90 ~ 100 DEG C, extraction time 1.5 ~ 2h, filter, Radix Glycyrrhizae after filtration mixes by weight 1:10 ~ 1:12 with water by second time, Extracting temperature 90 ~ 100 DEG C, extraction time 1.5 ~ 2h, merge Aqueous extracts, for subsequent use after cold filtration;
(2) allocate: Peppermint Water extract obtained for step (1), mulberry leaf Aqueous extracts, chrysanthemum water extract, balloonflower root Aqueous extracts, licorice water extract 16.7 ~ 37.0:17.4 by volume ~ 55.6:9.1 ~ 38.1:3.7 ~ 26.1:3.7 ~ 19.0 are mixed, filters;
(3) filling;
(4) sterilization, namely obtains described peppermint compound cold tea.
Show allocated peppermint compound cold tea antioxidation in vitro experiment invention, it can reach 82.49 ± 6.55% and 83.87 ± 3.94% far away higher than commercially available brand cold tea respectively to the clearance rate of DPPH free radical and ABTS free radical.
Further, in described step (1), the preparation method of Peppermint Water extract is: mixed by weight 1:40 with water by peppermint, Extracting temperature 100 DEG C, extraction time 45min, obtains Peppermint Water extract, for subsequent use after cold filtration;
Mulberry leaf Aqueous extracts: mixed by weight 1:12 with water by mulberry leaf, Extracting temperature 100 DEG C, extracts and extract 1h 2 times at every turn, merges Aqueous extracts, for subsequent use after cold filtration;
The preparation method of chrysanthemum water extract is: mixed by weight 1:100 with water by chrysanthemum, Extracting temperature 100 DEG C, extraction time 25min, obtains chrysanthemum water extract, for subsequent use after cold filtration;
The preparation method of balloonflower root Aqueous extracts is: mixed by weight 1:50 with water by balloonflower root, Extracting temperature 100 DEG C, extraction time 25min, obtains balloonflower root Aqueous extracts, for subsequent use after cold filtration;
The preparation method of licorice water extract is: mixed by weight 1:13 with water by Radix Glycyrrhizae, Extracting temperature 100 DEG C, extraction time 2h, filter, the Radix Glycyrrhizae after filtration mixes by weight 1:12 with water by second time, Extracting temperature 100 DEG C, extraction time 2h, merges Aqueous extracts, for subsequent use after cold filtration.Carry out water extraction with this optimization method and get rear Peppermint Water solution total polyphenols yield for 12.79 ± 0.68mg/g, polyphenol compound be in peppermint medicinal material except volatile oil component main oxidation-resistant active ingredient; The extract of other raw materials also reaches optimum at sense organ and non-oxidizability.
Further, in described step (2), the proportioning of allotment is: Peppermint Water extract step (1) obtained, mulberry leaf Aqueous extracts, chrysanthemum water extract, balloonflower root Aqueous extracts, licorice water extract by volume 25:25:20:15:10 mix.In all raw material extract, peppermint, mulberry leaf aqueous extract general flavone and Determination of Polyphenols are higher than other medicinal materials, and analysis result shows, peppermint extract consumption is remarkable to antipyretic beverage sensory evaluation influence.
In described step (1), each extract is cooled to 4 DEG C after extracting; 1m aperture membrane filtration is adopted in described step (1), (2).In the health drink of Chinese medicine extract allotment, because each chemical composition is as more in materials such as polyphenol, alkaloid, tannin, protein, composition is shown in and easily interacts and form macromolecular complex thing and produce precipitation, the each raw materials of traditional Chinese medicinal materials aqueous extract of the present invention all can produce precipitation after 4 DEG C of sub-cooled, to each aqueous extract respectively through be less than 1m aperture membrane filtration and allotment complete after secondary filter effectively can remove precipitation and obtain the bright brownish red antipyretic beverage of clarification.
By add different white granulated sugar amount (2,4,6,8,10g/100ml peppermint compound cold tea) peppermint compound cold tea is allocated, result shows that the white granulated sugar cold tea taste adding 6g/ (100ml peppermint compound cold tea) is best, and sugariness is suitable.
Beneficial effect: compared with prior art, the invention has the advantages that:
Cold tea of the present invention is primary raw material with peppermint, is equipped with mulberry leaf, chrysanthemum, Radix Glycyrrhizae, balloonflower root, pure in mouth feel, and unique flavor also has clearing heat and detoxicating, anti-oxidant effect of Denging; It can reach 82.49 ± 6.55% and 83.87 ± 3.94% far away higher than commercially available brand cold tea respectively to the clearance rate of DPPH free radical and ABTS free radical, and this cold tea clearance rate is only 25.16 ± 1.99% and 19.67 ± 2.53 respectively.
Accompanying drawing explanation
Fig. 1 solid-liquid ratio is on the impact of extracting Determination of Polyphenols;
Fig. 2 extraction time is on the impact of Determination of Polyphenols;
Fig. 3 Extracting temperature is on the impact of extracting Determination of Polyphenols.
Detailed description of the invention
Below in conjunction with example, the present invention is described in further detail.
Peppermint optimization for extracting condition scheme: carry out single factor experiment respectively with rate of charge, Extracting temperature, extraction time, according to single factor experiment result, utilizes orthogonal experiments to determine peppermint medicinal material water extraction process scheme.
1. single factor experiment
1.1 solid-liquid ratios are on the impact of total polyphenols yield
Peppermint and water charge ratio establish 1:10,1:20,1:30,1:40,1:50,1:60, Extracting temperature 100 DEG C, extraction time 45min, filter centrifugation after water extraction.Carry out polyphenol content mensuration, often process repetition 3 times.Result is as Fig. 1.
1.2 extraction time
Extraction time establishes 5,15,25,35,45,55,65min, according to solid-liquid ratio 1:60, Extracting temperature 100 DEG C, filter centrifugation while hot after water extraction.Carry out polyphenol content mensuration, often process repetition 3 times.Result as shown in Figure 2.
1.3 Extracting temperature
Temperature Treatment establishes 30,40,50,60,70,80,90,100 DEG C, according to solid-liquid ratio 1:60, and extraction time 45min.Filter centrifugation while hot after water extraction.Carry out polyphenol content mensuration, often process repetition 3 times.Result as shown in Figure 3.
2. orthogonal test
On single factor experiment basis, to extract Determination of Polyphenols for index, choose solid-liquid ratio, extraction time, Extracting temperature be examination factor, each factor design 3 levels, each factor level is in table 1, and result of the test is in table 2.
Table 1 orthogonal test factor level table
Table 2 peppermint total polyphenols extracts orthogonal experiments
Table 3 orthogonal design analysis of variance table
Shown by quadrature analysis result in table 2, the each factor of Peppermint Water extraction polyphenol affects size sequence and is: solid-liquid ratio > extraction time > Extracting temperature, show that the optimum extraction condition that Peppermint Water extracts on polyphenol technology theory is A according to the intuitive analysis of each factor K value
3b
2c
3i.e. solid-liquid ratio 1:40, extraction time 45min, Extracting temperature 100 DEG C.The results of analysis of variance shows, factor A solid-liquid ratio and factor B extraction time are extracted in the level of α=0.05 peppermint total polyphenols remarkable impact, and factor C extraction time is not remarkable on peppermint total polyphenols extraction impact.
Measuring peppermint total polyphenols yield through analysis after carrying out 3 repeating test to optimum organization is 12.79 ± 0.68mg/g, illustrates that this extraction process is stablized feasible.
Other raw material optimization for extracting condition schemes:
Mulberry leaf Aqueous extracts: mixed by weight 1:10 ~ 1:15 with water by mulberry leaf, Extracting temperature 90 ~ 100 DEG C, extracts 2 ~ 3 times and extracts 1 ~ 1.5h at every turn, merge Aqueous extracts, for subsequent use after cold filtration;
Chrysanthemum water extract: mixed by weight 1:80 ~ 1:100 with water by chrysanthemum, Extracting temperature 90 ~ 100 DEG C, extraction time 20 ~ 25min, obtains chrysanthemum water extract, for subsequent use after cold filtration; :
Balloonflower root Aqueous extracts: mixed by weight 1:30 ~ 1:50 with water by balloonflower root, Extracting temperature 90 ~ 100 DEG C, extraction time 25 ~ 30min, obtains balloonflower root Aqueous extracts, for subsequent use after cold filtration;
Licorice water extract: Radix Glycyrrhizae is mixed by weight 1:10 ~ 1:13 with water, Extracting temperature 90 ~ 100 DEG C, extraction time 1.5 ~ 2h, filter, Radix Glycyrrhizae after filtration mixes by weight 1:10 ~ 1:12 with water by second time, Extracting temperature 90 ~ 100 DEG C, extraction time 1.5 ~ 2h, merge Aqueous extracts, for subsequent use after cold filtration.
By comparing, under following condition, gained Aqueous extracts reaches optimum in sense organ and non-oxidizability etc.
Mulberry leaf Aqueous extracts: mixed by weight 1:12 with water by mulberry leaf, Extracting temperature 100 DEG C, extracts and extract 1h 2 times at every turn, merges Aqueous extracts, for subsequent use after cold filtration;
Chrysanthemum water extract: mixed by weight 1:100 with water by chrysanthemum, Extracting temperature 100 DEG C, extraction time 25min, obtains chrysanthemum water extract, for subsequent use after cold filtration;
Balloonflower root Aqueous extracts: mixed by weight 1:50 with water by balloonflower root, Extracting temperature 100 DEG C, extraction time 25min, obtains balloonflower root Aqueous extracts, for subsequent use after cold filtration;
Licorice water extract: Radix Glycyrrhizae is mixed by weight 1:13 with water, Extracting temperature 100 DEG C, extraction time 2h, filter, the Radix Glycyrrhizae after filtration mixes by weight 1:12 with water by second time, Extracting temperature 100 DEG C, extraction time 2h, merges Aqueous extracts, for subsequent use after cold filtration.
The processing method of peppermint compound cold tea
1. the preparation of each raw material extract:
Peppermint: extraction process is determined by above-mentioned test.By solid-liquid ratio 1:40, Extracting temperature 100 DEG C, extraction time 45min, obtains Peppermint Water extract, for subsequent use after cold filtration.
Mulberry leaf: solid-liquid ratio 1:12, Extracting temperature 100 DEG C, extracts and extracts 1h 2 times at every turn, merges Aqueous extracts, for subsequent use after cold filtration.
Chrysanthemum: solid-liquid ratio 1:100, Extracting temperature 100 DEG C, extraction time 25min, for subsequent use after Aqueous extracts cold filtration.
Balloonflower root: solid-liquid ratio 1:50, Extracting temperature 100 DEG C, extraction time 25min, for subsequent use after Aqueous extracts cold filtration.
Radix Glycyrrhizae: solid-liquid ratio 1:13, Extracting temperature 100 DEG C, extraction time 2h, second time solid-liquid ratio 1:12 Extracting temperature 100 DEG C, extraction time 2h, for subsequent use after merging Aqueous extracts cold filtration.
2. antipyretic beverage formulation optimization
2.1 peppermint composite cold tea beverage formula orthogonal tests
Mixed by a certain percentage by the Aqueous extracts of five kinds of raw materials, optimal proportion is tested with sensory evaluation scores for determining by 5 factor 4 horizontal quadratures, and design orthogonal arrage is in table 4.
Table 4 peppermint composite cold tea beverage technique quadrature factor water-glass
For ensureing reliability and the objectivity of sensory evaluation, by 10 composition of personnel Review Teams from different geographical, all ages and classes, different sexes, all valuation officers have certain professional knowledge, good hyperesthesia and basic subjective appreciation knowledge and skill, and before evaluation, valuation officer is done and evaluates training, carry out integrated sensory's evaluation by Review Team according to clarity, color and luster, local flavor, mouthfeel etc., sensory evaluation standard is in table 5.
Table 5 product sensory evaluation criterion
As can be seen from table 6 orthogonal experiments and intuitive analysis, the factorial arrangement order affecting sensory evaluation is B > A > C > D > E, and best of breed is A
1b
1c
1d
1e
1, namely the volume ratio of peppermint, mulberry leaf, chrysanthemum, balloonflower root, Radix Glycyrrhizae five kinds of extracts is 25:25:20:15:10.The results of analysis of variance (table 7) shows, peppermint extract consumption is remarkable to the effect of antipyretic beverage technogenic influence, and the impact of other several extract consumptions does not reach the level of signifiance.
Table 6 peppermint composite cold tea beverage technique orthogonal experiments
K
1, K
2, K
3, represent horizontal average; R represents extreme difference
The variance analysis of table 7 peppermint composite cold tea beverage technique orthogonal test
Below test all adopt peppermint, mulberry leaf, chrysanthemum, balloonflower root, Radix Glycyrrhizae five kinds of extracts volume ratio be the peppermint compound cold tea of 25:25:20:15:10.
2.2 white granulated sugar consumptions are on the impact of peppermint compound cold tea mouthfeel
By add different white granulated sugar amount (2,4,6,8,10g/100ml peppermint compound cold tea) peppermint compound cold tea is allocated, result shows that the white granulated sugar cold tea taste adding 6g/ (100ml peppermint compound cold tea) is best, and sugariness is suitable.
2.3 peppermint compound cold tea non-oxidizability comparative tests
The clearance rate of peppermint compound cold tea to DPPH free radical and ABTS free radical the results are shown in Table 8.In several Chinese medicine extract contained by cold tea, the oxidation resistance of peppermint, mulberry leaf is the strongest, and peppermint compound cold tea to the scavenging action of DPPH and ABTS free radical all more than 80%, there is very strong antioxidation.Record the clearance rate of commercially available cold tea king Lao Ji to DPPH and be only 25.16 ± 1.99%, ABTS free radical is known that rate is 19.67 ± 2.53.In addition, in the present invention, measured peppermint compound cold tea and contained each extracts of Chinese herbal medicine thereof are to DPPH and ABTS free radical scavenging activity all higher than positive control 500mol/L Trolox solution, and positive control DPPH and ABTS free radical scavenging activity are respectively 6.88 ± 0.46% and 11.23 ± 0.89%.
Table 8 peppermint compound cold tea and contained Chinese medicine extract antioxidant activity in vitro
2.4 peppermint compound cold tea flavones and polyphenol contents
The present invention determines general flavone and the Determination of Polyphenols of peppermint compound cold tea and contained each extracts of Chinese herbal medicine thereof respectively, the results are shown in Table 9.In all raw material extract, peppermint, mulberry leaf aqueous extract general flavone and Determination of Polyphenols are higher than other medicinal materials.The peppermint compound cold tea general flavone content prepared is 0.39 ± 0.01mg/ml, and Determination of Polyphenols is 0.99 ± 0.11mg/ml.
Table 9 peppermint compound cold tea and contained Chinese medicine extract flavones and polyphenol content
In the health drink of Chinese medicine extract allotment, because each chemical composition is as more in materials such as polyphenol, alkaloid, tannin, protein, composition is shown in and easily interacts and form macromolecular complex thing and produce precipitation, the each raw materials of traditional Chinese medicinal materials aqueous extract of the present invention all can produce precipitation after 4 DEG C of sub-cooled, to each aqueous extract respectively through be less than 1m aperture membrane filtration and allotment complete after secondary filter effectively can remove precipitation and obtain the bright brownish red antipyretic beverage of clarification.
Eventually pass high-temperature short-time sterilization, selective temperature is between 100-110 DEG C, and the time, 15-20min was advisable.
The present invention is illustrated according to above-described embodiment, should be appreciated that above-described embodiment does not limit the present invention in any form, and all employings are equal to replacement or the technical scheme that obtains of equivalent transformation mode, all drop within protection scope of the present invention.
Claims (8)
1. a processing method for peppermint compound cold tea, is characterized in that, described method comprises the steps:
(1) by peppermint, mulberry leaf, chrysanthemum, balloonflower root, Radix Glycyrrhizae extracting in water separately:
Peppermint Water extract: mixed by weight 1:10 ~ 1:60 with water by peppermint, Extracting temperature 30 ~ 100 DEG C, extraction time 5 ~ 65 min, obtains Peppermint Water extract, for subsequent use after cold filtration;
Mulberry leaf Aqueous extracts: mixed by weight 1:10 ~ 1:15 with water by mulberry leaf, Extracting temperature 90 ~ 100 DEG C, extracts 2 ~ 3 times and extracts 1 ~ 1.5h at every turn, merge Aqueous extracts, for subsequent use after cold filtration;
Chrysanthemum water extract: mixed by weight 1:80 ~ 1:100 with water by chrysanthemum, Extracting temperature 90 ~ 100 DEG C, extraction time 20 ~ 25min, obtains chrysanthemum water extract, for subsequent use after cold filtration; :
Balloonflower root Aqueous extracts: mixed by weight 1:30 ~ 1:50 with water by balloonflower root, Extracting temperature 90 ~ 100 DEG C, extraction time 25 ~ 30min, obtains balloonflower root Aqueous extracts, for subsequent use after cold filtration;
Licorice water extract: Radix Glycyrrhizae is mixed by weight 1:10 ~ 1:13 with water, Extracting temperature 90 ~ 100 DEG C, extraction time 1.5 ~ 2h, filter, Radix Glycyrrhizae after filtration mixes by weight 1:10 ~ 1:12 with water by second time, Extracting temperature 90 ~ 100 DEG C, extraction time 1.5 ~ 2h, merge Aqueous extracts, for subsequent use after cold filtration;
(2) allocate: Peppermint Water extract obtained for step (1), mulberry leaf Aqueous extracts, chrysanthemum water extract, balloonflower root Aqueous extracts, licorice water extract 16.7 ~ 37.0:17.4 by volume ~ 55.6:9.1 ~ 38.1:3.7 ~ 26.1:3.7 ~ 19.0 can be mixed, filter;
(3) filling;
(4) sterilization, obtains described peppermint compound cold tea.
2. the processing method of a kind of peppermint compound cold tea according to claim 1, it is characterized in that, in described step (1), the preparation method of Peppermint Water extract is: mixed by weight 1:40 with water by peppermint, Extracting temperature 100 DEG C, extraction time 45 min, obtain Peppermint Water extract, for subsequent use after cold filtration;
Mulberry leaf Aqueous extracts: mixed by weight 1:12 with water by mulberry leaf, Extracting temperature 100 DEG C, extracts and extract 1h 2 times at every turn, merges Aqueous extracts, for subsequent use after cold filtration;
The preparation method of chrysanthemum water extract is: mixed by weight 1:100 with water by chrysanthemum, Extracting temperature 100 DEG C, extraction time 25min, obtains chrysanthemum water extract, for subsequent use after cold filtration;
The preparation method of balloonflower root Aqueous extracts is: mixed by weight 1:50 with water by balloonflower root, Extracting temperature 100 DEG C, extraction time 25min, obtains balloonflower root Aqueous extracts, for subsequent use after cold filtration;
The preparation method of licorice water extract is: mixed by weight 1:13 with water by Radix Glycyrrhizae, Extracting temperature 100 DEG C, extraction time 2h, filter, the Radix Glycyrrhizae after filtration mixes by weight 1:12 with water by second time, Extracting temperature 100 DEG C, extraction time 2h, merges Aqueous extracts, for subsequent use after cold filtration.
3. the processing method of a kind of peppermint compound cold tea according to claim 1, is characterized in that, in described step (1), each extract is cooled to 4 DEG C after extracting.
4. the processing method of a kind of peppermint compound cold tea according to claim 1, is characterized in that, adopts 1 μm of aperture membrane filtration in described step (1), (2).
5. the processing method of a kind of peppermint compound cold tea according to claim 1, it is characterized in that, in described step (2), the proportioning of allotment is: Peppermint Water extract step (1) obtained, mulberry leaf Aqueous extracts, chrysanthemum water extract, balloonflower root Aqueous extracts, licorice water extract by volume 25:25:20:15:10 mix.
6. the processing method of a kind of peppermint compound cold tea according to claim 1, is characterized in that, adds white granulated sugar, add white granulated sugar 2 ~ 10g in every 100mL peppermint compound cold tea in described step (2) during allotment.
7. the processing method of a kind of peppermint compound cold tea according to claim 6, is characterized in that, adds described white granulated sugar 6g in every 100mL peppermint compound cold tea.
8. the processing method of a kind of peppermint compound cold tea according to claim 1, is characterized in that, in described step (4), sterilizing adopts high-temperature short-time sterilization, temperature 100-110 DEG C, time 15-20min.
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| CN107752004A (en) * | 2017-10-23 | 2018-03-06 | 广东工业大学 | A kind of composition and its application, health products |
| CN111903815A (en) * | 2020-08-03 | 2020-11-10 | 深圳市有用功投资发展有限公司 | Herbal tea composition and preparation method thereof |
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