CN104403537A - Impact-resistant and abrasion-resistant anti-interference coating and preparation method thereof - Google Patents
Impact-resistant and abrasion-resistant anti-interference coating and preparation method thereof Download PDFInfo
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- CN104403537A CN104403537A CN201410671614.2A CN201410671614A CN104403537A CN 104403537 A CN104403537 A CN 104403537A CN 201410671614 A CN201410671614 A CN 201410671614A CN 104403537 A CN104403537 A CN 104403537A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
- C09D7/62—Additives non-macromolecular inorganic modified by treatment with other compounds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses an impact-resistant and abrasion-resistant anti-interference coating. The impact-resistant and abrasion-resistant anti-interference coating is characterized by being prepared from the following raw materials in parts by weight: 15-20 parts of polyvinyl acetate, 22-28 parts of polyurethane resin, 15-17 parts of calcium rosin ester, 13-16 parts of xylene, 1-2 parts of a polyamide anti-settling agent, 4-6 parts of chlorinated rubber, 4-6 parts of titanium dioxide, 1-2 parts of tripolycyanamide, 2-3 parts of palm wax, 2-3 parts of ammonium borate, 2-3 parts of a cross-linking agent TAIC, 4-6 parts of precipitated barium sulphate, 1-2 parts of an anti-aging agent ODA, 3-5 parts of high abrasion furnace black, 4-6 parts of ethyl alcohol, 6-9 parts of n-butyl acetate and 4-7 parts of an auxiliary. The coating disclosed by the invention has tenacity, impact resistance and water resistance; when the surface of a base material is coated with the coating, the adhesive force is strong, the coating is smooth, unlikely to become yellow and high in resistance to light and weather, and meanwhile the mechanical property is good; through the addition of the auxiliary, the coating is good in dispersibility, and also has an anti-electromagnetic interference effect; the coating disclosed by the invention is high in drying speed and high in production efficiency.
Description
Technical field
The present invention relates to a kind of paint and preparation method thereof, particularly a kind of shock-resistant wear-resisting anti-interference coating and preparation method thereof.
Background technology
the economic fast development of society, city size and city scope constantly expand, in order to meet the ever-increasing needs of electricity need load, according to the rule of " power engineering " substation site selection, substation should try one's best near load center, the electric energy loss of transformer substation system can be reduced like this, voltage loss and non-ferrous metal waste, therefore progressively the higher 110KV of some voltage ranges is built in city and above substation has become a kind of development trend, but the harm problem of the factors such as electromagnetic radiation to Residents and environment of high voltage substation but can not be ignored.Electromagnetic radiation refers to that energy is transmitted into the phenomenon in space by emissive source with electromagnetic wave.Have the place of alternating-current just to have hertzian wave, have hertzian wave to produce electromagnetic radiation, it can to human body and environmental danger.
Summary of the invention
The object of this invention is to provide a kind of shock-resistant wear-resisting anti-interference coating and preparation method thereof.
In order to realize object of the present invention, the present invention is by following scheme implementation:
A kind of shock-resistant wear-resisting anti-interference coating, is made up of the raw material of following weight part: polyvinyl acetate 15-20, urethane resin 22-28, rosin calcium fat 15-17, dimethylbenzene 13-16, polymeric amide anti-settling agent 1-2, chlorinated rubber 4-6, titanium dioxide 4-6, trimeric cyanamide 1-2, palm wax 2-3, ammonium borate 2-3, linking agent TAIC2-3, process white 4-6, anti-aging agent ODA 1-2, high wear-resistant carbon black 3-5, ethanol 4-6, N-BUTYL ACETATE 6-9, auxiliary agent 4-7;
Described auxiliary agent is made up of the raw material of following weight part: aluminate coupling agent DL-4111-2, polyisobutene 4-6, trihydroxy ethylamine oleate soap 1-2, two Lauryl Alcohol ester 1-3, cyclohexanone peroxide 1-2, zinc acetylacetonate 2-3, Oil of Eucalyptus 3-5, antioxidant MB 1-2, methacrylic acid 5-8, β-dimethyl-aminoethylmethacrylate 12-15, BIT 2-3, molybdenum oxide 3-5, bismuth oxide 2-4, silver-coated copper powder 4-6, carbon black 3-5, Conductive mica 5-7, ethanol 2-4, sodium laurylsulfonate 1-2; Preparation method is that molybdenum oxide, bismuth oxide, silver-coated copper powder, carbon black, Conductive mica are added to ball milling 2-3 hour in ball mill by (1), be added to 600-800 ° of C in calcining furnace again and calcine 20-30 minute, taking out to pulverize is added in the mixing solutions of aluminate coupling agent DL-411 and ethanol, ultrasonic disperse 10-20 minute, dries rear and sodium laurylsulfonate mixing for standby use; (2) be added in reactor by methacrylic acid, β-dimethyl-aminoethylmethacrylate, zinc acetylacetonate, Oil of Eucalyptus, raised temperature, to 70-80 ° of C, adds cyclohexanone peroxide, stirring reaction 1-2 hour; (3) product of step (1) is added in step (2), continues reaction 20-30 minute, then add polyamide wax and other surplus materialss, be fully uniformly mixed.
The shock-resistant wear-resisting anti-interference coating of one of the present invention, be made up of following concrete steps:
(1) titanium dioxide, ammonium borate, process white, high wear-resistant carbon black are added in the mixing solutions of ethanol, N-BUTYL ACETATE and dimethylbenzene, ultrasonic disperse 20-30 minute, adds polymeric amide anti-settling agent, anti-aging agent ODA, auxiliary agent continuation stirring reaction 30-40 minute when being heated to 50-80 ° of C;
(2) product of step (1) is continued raised temperature to 80-90 ° of C, add polyvinyl acetate, urethane resin, rosin calcium fat, chlorinated rubber, linking agent TAIC, 1200-1400 rev/min lower high-speed mixing stirring reaction 1-2 hour;
(3) surplus materials is added in the product of step (2), is added to grinding machine for grinding after mixing and is uniformly dispersed, filter and obtain the material that fineness is 20-40 μm, pack.
Advantage of the present invention is: the coating of coating of the present invention has toughness, shock-resistant, water tolerance, and be coated in substrate surface sticking power large, coating is smooth, inhibited from yellowing, fast light, weathering resistance is excellent, good mechanical property simultaneously; The auxiliary agent added, makes coating good dispersity, also has the effect of electromagnetism interference, and coating rate of drying of the present invention is fast, and production efficiency is high.
specific embodiments
Below by specific examples, the present invention is described in detail.
A kind of shock-resistant wear-resisting anti-interference coating, is made up of the raw material of following weight part (kilogram): polyvinyl acetate 17, urethane resin 27, rosin calcium fat 16, dimethylbenzene 15, polymeric amide anti-settling agent 1, chlorinated rubber 5, titanium dioxide 4, trimeric cyanamide 1, palm wax 2, ammonium borate 2, linking agent TAIC2, process white 5, anti-aging agent ODA 1, high wear-resistant carbon black 4, ethanol 4, N-BUTYL ACETATE 7, auxiliary agent 5;
Described auxiliary agent is made up of the raw material of following weight part (kilogram): aluminate coupling agent DL-411 2, polyisobutene 5, trihydroxy ethylamine oleate soap 1, two Lauryl Alcohol ester 2, cyclohexanone peroxide 1, zinc acetylacetonate 2, Oil of Eucalyptus 4, antioxidant MB 1, methacrylic acid 7, β-dimethyl-aminoethylmethacrylate 13, BIT 2, molybdenum oxide 4, bismuth oxide 3, silver-coated copper powder 5, carbon black 4, Conductive mica 7, ethanol 3, sodium laurylsulfonate 1; Preparation method is that molybdenum oxide, bismuth oxide, silver-coated copper powder, carbon black, Conductive mica are added to ball milling 2-3 hour in ball mill by (1), be added to 600-800 ° of C in calcining furnace again and calcine 20-30 minute, taking out to pulverize is added in the mixing solutions of aluminate coupling agent DL-411 and ethanol, ultrasonic disperse 10-20 minute, dries rear and sodium laurylsulfonate mixing for standby use; (2) be added in reactor by methacrylic acid, β-dimethyl-aminoethylmethacrylate, zinc acetylacetonate, Oil of Eucalyptus, raised temperature, to 70-80 ° of C, adds cyclohexanone peroxide, stirring reaction 1-2 hour; (3) product of step (1) is added in step (2), continues reaction 20-30 minute, then add polyamide wax and other surplus materialss, be fully uniformly mixed.
The shock-resistant wear-resisting anti-interference coating of one of the present invention, be made up of following concrete steps:
(1) titanium dioxide, ammonium borate, process white, high wear-resistant carbon black are added in the mixing solutions of ethanol, N-BUTYL ACETATE and dimethylbenzene, ultrasonic disperse 20-30 minute, adds polymeric amide anti-settling agent, anti-aging agent ODA, auxiliary agent continuation stirring reaction 30-40 minute when being heated to 50-80 ° of C;
(2) product of step (1) is continued raised temperature to 80-90 ° of C, add polyvinyl acetate, urethane resin, rosin calcium fat, chlorinated rubber, linking agent TAIC, 1200-1400 rev/min lower high-speed mixing stirring reaction 1-2 hour;
(3) surplus materials is added in the product of step (2), is added to grinding machine for grinding after mixing and is uniformly dispersed, filter and obtain the material that fineness is 20-40 μm, pack.
Paint paint film of the present invention is smooth, without lump, and hardness: 3H, sticking power: 1 grade, thermotolerance experiment (300 ° of C, 120h): paint film is complete, do not come off, alkali resistance experiment (72h): non-foaming, wrinkle resistant, do not come off, acid resistance experiment (72h): non-foaming, wrinkle resistant, does not come off, artificial ageing resistance is tested: 1200h is non-foaming, do not peel off, flawless, and electromagnetic shielding rate is tested: 48dB.
Claims (2)
1. a shock-resistant wear-resisting anti-interference coating, it is characterized in that, be made up of the raw material of following weight part: polyvinyl acetate 15-20, urethane resin 22-28, rosin calcium fat 15-17, dimethylbenzene 13-16, polymeric amide anti-settling agent 1-2, chlorinated rubber 4-6, titanium dioxide 4-6, trimeric cyanamide 1-2, palm wax 2-3, ammonium borate 2-3, linking agent TAIC2-3, process white 4-6, anti-aging agent ODA 1-2, high wear-resistant carbon black 3-5, ethanol 4-6, N-BUTYL ACETATE 6-9, auxiliary agent 4-7;
Described auxiliary agent is made up of the raw material of following weight part: aluminate coupling agent DL-4111-2, polyisobutene 4-6, trihydroxy ethylamine oleate soap 1-2, two Lauryl Alcohol ester 1-3, cyclohexanone peroxide 1-2, zinc acetylacetonate 2-3, Oil of Eucalyptus 3-5, antioxidant MB 1-2, methacrylic acid 5-8, β-dimethyl-aminoethylmethacrylate 12-15, BIT 2-3, molybdenum oxide 3-5, bismuth oxide 2-4, silver-coated copper powder 4-6, carbon black 3-5, Conductive mica 5-7, ethanol 2-4, sodium laurylsulfonate 1-2; Preparation method is that molybdenum oxide, bismuth oxide, silver-coated copper powder, carbon black, Conductive mica are added to ball milling 2-3 hour in ball mill by (1), be added to 600-800 ° of C in calcining furnace again and calcine 20-30 minute, taking out to pulverize is added in the mixing solutions of aluminate coupling agent DL-411 and ethanol, ultrasonic disperse 10-20 minute, dries rear and sodium laurylsulfonate mixing for standby use; (2) be added in reactor by methacrylic acid, β-dimethyl-aminoethylmethacrylate, zinc acetylacetonate, Oil of Eucalyptus, raised temperature, to 70-80 ° of C, adds cyclohexanone peroxide, stirring reaction 1-2 hour; (3) product of step (1) is added in step (2), continues reaction 20-30 minute, then add polyamide wax and other surplus materialss, be fully uniformly mixed.
2. a kind of shock-resistant wear-resisting anti-interference coating according to claim 1, is characterized in that, be made up of following concrete steps:
(1) titanium dioxide, ammonium borate, process white, high wear-resistant carbon black are added in the mixing solutions of ethanol, N-BUTYL ACETATE and dimethylbenzene, ultrasonic disperse 20-30 minute, adds polymeric amide anti-settling agent, anti-aging agent ODA, auxiliary agent continuation stirring reaction 30-40 minute when being heated to 50-80 ° of C;
(2) product of step (1) is continued raised temperature to 80-90 ° of C, add polyvinyl acetate, urethane resin, rosin calcium fat, chlorinated rubber, linking agent TAIC, 1200-1400 rev/min lower high-speed mixing stirring reaction 1-2 hour;
(3) surplus materials is added in the product of step (2), is added to grinding machine for grinding after mixing and is uniformly dispersed, filter and obtain the material that fineness is 20-40 μm, pack.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410671614.2A CN104403537A (en) | 2014-11-21 | 2014-11-21 | Impact-resistant and abrasion-resistant anti-interference coating and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410671614.2A CN104403537A (en) | 2014-11-21 | 2014-11-21 | Impact-resistant and abrasion-resistant anti-interference coating and preparation method thereof |
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| CN104403537A true CN104403537A (en) | 2015-03-11 |
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| CN201410671614.2A Pending CN104403537A (en) | 2014-11-21 | 2014-11-21 | Impact-resistant and abrasion-resistant anti-interference coating and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107506656A (en) * | 2017-08-21 | 2017-12-22 | 深圳市四季宏胜科技有限公司 | A kind of WIFI movable storage devices |
| CN110670369A (en) * | 2019-10-16 | 2020-01-10 | 南通绿芭蕉纺织品有限公司 | High-toughness anti-abrasion cloth |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1200390A (en) * | 1997-05-26 | 1998-12-02 | 四川联合大学 | Electromagnetic wave shielding coating, and method for preparing same |
| US20040028859A1 (en) * | 1998-09-11 | 2004-02-12 | Legrande Wayne B. | Electrically conductive and electromagnetic radiation absorptive coating compositions and the like |
| CN1935916A (en) * | 2006-09-29 | 2007-03-28 | 华侨大学 | Graphite base electromagnetic shielding composite coating and its preparing method |
| CN101275052A (en) * | 2008-05-14 | 2008-10-01 | 海洋化工研究院 | Corrosion-resistant electromagnetic screen coating and preparation thereof |
| CN102250518A (en) * | 2011-06-17 | 2011-11-23 | 天津中油渤星工程科技有限公司 | Double-rubber anti-corrosion coating and preparation method thereof |
| CN103756509A (en) * | 2014-01-09 | 2014-04-30 | 成都理工大学 | Functional coating for preventing electromagnetic wave radiation pollution and preparation method thereof |
-
2014
- 2014-11-21 CN CN201410671614.2A patent/CN104403537A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1200390A (en) * | 1997-05-26 | 1998-12-02 | 四川联合大学 | Electromagnetic wave shielding coating, and method for preparing same |
| US20040028859A1 (en) * | 1998-09-11 | 2004-02-12 | Legrande Wayne B. | Electrically conductive and electromagnetic radiation absorptive coating compositions and the like |
| CN1935916A (en) * | 2006-09-29 | 2007-03-28 | 华侨大学 | Graphite base electromagnetic shielding composite coating and its preparing method |
| CN101275052A (en) * | 2008-05-14 | 2008-10-01 | 海洋化工研究院 | Corrosion-resistant electromagnetic screen coating and preparation thereof |
| CN102250518A (en) * | 2011-06-17 | 2011-11-23 | 天津中油渤星工程科技有限公司 | Double-rubber anti-corrosion coating and preparation method thereof |
| CN103756509A (en) * | 2014-01-09 | 2014-04-30 | 成都理工大学 | Functional coating for preventing electromagnetic wave radiation pollution and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107506656A (en) * | 2017-08-21 | 2017-12-22 | 深圳市四季宏胜科技有限公司 | A kind of WIFI movable storage devices |
| CN110670369A (en) * | 2019-10-16 | 2020-01-10 | 南通绿芭蕉纺织品有限公司 | High-toughness anti-abrasion cloth |
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Application publication date: 20150311 |