CN104397057A - Ripening pesticide for plants, and preparation method thereof - Google Patents

Ripening pesticide for plants, and preparation method thereof Download PDF

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Publication number
CN104397057A
CN104397057A CN201410615704.XA CN201410615704A CN104397057A CN 104397057 A CN104397057 A CN 104397057A CN 201410615704 A CN201410615704 A CN 201410615704A CN 104397057 A CN104397057 A CN 104397057A
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China
Prior art keywords
parts
ripening
pesticide
accelerating
plant
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Pending
Application number
CN201410615704.XA
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Chinese (zh)
Inventor
姬胜国
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QINGDAO RUIZHI AGRICULTURAL TECHNOLOGY SERVICE Co Ltd
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QINGDAO RUIZHI AGRICULTURAL TECHNOLOGY SERVICE Co Ltd
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Priority to CN201410615704.XA priority Critical patent/CN104397057A/en
Publication of CN104397057A publication Critical patent/CN104397057A/en
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Abstract

The invention discloses a ripening pesticide for plants, and a preparation method thereof. The ripening pesticide is characterized in that the ripening pesticide comprises, by weight, 30-70 parts of animal fat, 10-30 parts of loess, 10-30 parts of Crocus sativus, 30-40 parts of calcium oxide, 50-80 parts of triethanolamine, 25-40 parts of organosiloxane, 20-40 parts of potassium sulfate, 18-30 parts of magnesium sulfate, 25-40 parts of sodium tripolyphosphate and 50-90 parts of an absorption composite solvent. The ripening pesticide is prepared through different methods according to different components, the temperature and the operating time are strictly controlled, effective components of medicines are extracted to prepare a pesticide, the pesticide is blended with the absorption composite solvent to obtain the ripening pesticide for ripening plants and crops, and the growth time of ripened plants is shortened by 10-20%; and the ripening pesticide also has certain pest killing, control and prevention efficacies, and can substitute chemical pesticides to kill and eliminate pest harms, and the pest killing rate of the ripening pesticide is 90-94%.

Description

Ripening-accelerating pesticide of one Plants and preparation method thereof
Technical field
The present invention relates to the ripening-accelerating pesticide of a Plants, the invention still further relates to the preparation method of the ripening-accelerating pesticide of a Plants, belong to agricultural chemicals product production field.
Background technology
Agricultural chemicals can be used for kill insects, fungi and other damages to crops growth biology.The agricultural chemicals used the earliest has dichlorodiphenyl trichloroethane, hexachlorcyclohexane etc., and they can eliminate destructive insects in a large number.But their good stability, can long-term existence in the environment, and constantly accumulates in animals and plants and human body, is eliminated for this reason.Use organophosphorous pesticide instead afterwards, as dichlorvos etc., substitute initial agricultural chemicals.But their toxicity is too large, very large to the harm of people and animals.In recent years, the agricultural chemicals of a collection of high-efficiency low-toxicity occurs, is found now and has narrow spectrum agricultural chemicals, be i.e. steroids agricultural chemicals.
The definition of agricultural chemicals broad sense refer to for prevent, eliminate or control to endanger agricultural, the disease of forestry, worm, grass and other pests and on purpose regulating plant, insect growth chemosynthesis or derive from biology, a kind of material of other natural materials or the mixture of several material and preparation thereof.Refer in agricultural production, for ensureing, promoting the growth of plant and crops, a class medicine of the desinsection used, sterilization, kill harmful animal (or weeds) is referred to as.Refer in particular to agriculturally for anti-worm and the medicament such as coordinate plant growth, weeding of curing the disease.
Physical property agricultural chemicals belongs to a branch in biopesticide category.It refers to the stable active ingredient utilized contained by plant, after using, makes it exempt from or alleviates the plant resource preparation that the pests such as disease, worm, weeds cause harm by certain method to recipient plant.Various botanical pesticide is not single a kind of compound usually, but all or part of organic substance of plant organism, complicated component is changeable, but is generally included in all kinds of materials such as alkaloid, glucosides, toxic protein, volatile essential oils, tannin, resin, organic acid, ester, ketone, terpene.In broad terms, the plant of being rich in these high physiological activators is all likely processed to pesticidal preparations, and its quantity and material classification are enriched.
For a long time, to some plants of the Nature growth, as the plants such as paddy rice, the seedlings of cereal crops, various vegetable and fruit, fruit, flowers and trees, flower seedling, trees, sapling and crops have carried out the research progress in more than ten years, the insect pest principle of plant and crops is conducted in-depth research, but the extent of injury of these chemical pesticides is still very large, therefore, be badly in need of finding a kind of plant pesticide and preparation method thereof, alleviate current agricultural chemicals pressure.
Summary of the invention
The object of the invention is to for deficiency of the prior art, ripening-accelerating pesticide of one Plants and preparation method thereof is provided, strict temperature control and operating time, extract the effective ingredient of medicine, make agricultural chemicals, and with absorb double solvents and dissolve for the accelerating the ripening of plant and crops, also there is effect that certain desinsection controls worm and insect protected in passing, replace chemical pesticide desinsection to remove the evil, killing rate is 90 ~ 94%.
For solving the problems of the technologies described above, the technical solution used in the present invention is: the ripening-accelerating pesticide of a Plants, its innovative point is: comprise following composition and weight portion thereof: animal tallow 30 ~ 70 parts, loess 10 ~ 30 parts, safflower 10 ~ 30 parts, 30 ~ 40 parts, calcium oxide, triethanolamine 50 ~ 80 parts, organosiloxane 25 ~ 40 parts, potassium sulfate 20 ~ 40 parts, 18 ~ 30 parts, magnesium sulfate, sodium phosphate trimer 25 ~ 40 parts and absorption double solvents 50 ~ 90 parts.
Further, described absorption double solvents comprises plant attaching agent, easily lyosoption and emulsifier, and described plant attaching agent, the easily concentration ratio of lyosoption and emulsifier three are 1 ~ 2:1.2 ~ 2.5:1.5 ~ 2.
Further, described absorption double solvents comprises plant attaching agent, easily lyosoption and emulsifier, and described plant attaching agent, the easily concentration ratio of lyosoption and emulsifier three are 1.5:1.8:1.8.
Further, comprise following composition and weight portion thereof: animal tallow 40 ~ 50 parts, loess 20 ~ 26 parts, safflower 18 ~ 24 parts, 35 ~ 38 parts, calcium oxide, triethanolamine 65 ~ 70 parts, organosiloxane 28 ~ 36 parts, potassium sulfate 24 ~ 32 parts, 22 ~ 28 parts, magnesium sulfate, sodium phosphate trimer 30 ~ 34 parts and absorption double solvents 68 ~ 76 parts.
Further, comprise following composition and weight portion thereof: animal tallow 46 parts, loess 24 parts, safflower 22 parts, 37 parts, calcium oxide, triethanolamine 66 parts, organosiloxane 30 parts, potassium sulfate 28 parts, 25 parts, magnesium sulfate, sodium phosphate trimer 32 parts and absorption double solvents 72 parts.
Another object of the present invention is to provide a kind of preparation method of the ripening-accelerating pesticide according to claim 1 plant, and its innovative point is: specifically comprise the following steps:
(1) animal tallow of proportional quantity, loess and safflower are broken into fine powder according to proportional quantity, put into water, be heated to 50 ~ 60 DEG C, solution also, after keeping 1 ~ 2h, filters by continuous stirring, then filtrate heating is concentrated into 20 ~ 30%, cooling, packing, for subsequent use;
(2) calcium oxide of proportional quantity, triethanolamine, organosiloxane, potassium sulfate, magnesium sulfate and sodium phosphate trimer are worn into fine powder, mix, put into water, with hot-water soak 2 ~ 3h that temperature is 50 ~ 60 DEG C, sealing refining, after being filtered by solution, removing impurity and filter residue, carry out distillation recrystallization;
(3) product in step (1) and step (2) is joined in the absorption double solvents of proportional quantity successively, heat to 90 ~ 95 DEG C of sealing refining 1 ~ 2h, then filter, filtrate is heated concentration and evaporation 10 ~ 30%, cool.
Further, the filtrate heating in described step (1) is concentrated into 23%.
Further, in described step (2), temperature controls is 56 DEG C.
Further, in described step (3), filtrate is heated concentration and evaporation to 18%.
Beneficial effect of the present invention is as follows:
(1) ripening-accelerating pesticide of the present invention adopts diverse ways according to different compositions, strict temperature control and operating time, extract the effective ingredient of medicine, make agricultural chemicals, and with absorb double solvents and dissolve for the accelerating the ripening of plant and crops, accelerate the ripening that to shorten the plant growth time be 10 ~ 20%; And also there is effect that certain desinsection controls worm and insect protected, replace chemical pesticide desinsection to remove the evil, killing rate is 90 ~ 94%.
(2) ripening-accelerating pesticide of the present invention adds plant attaching agent, easily lyosoption and the emulsifier of effective dose, improves the control efficiency of pesticide emulsion in water, reduces working concentration, and reduce cost.
Embodiment
Below in conjunction with specific embodiment, technical scheme of the present invention is elaborated.
Embodiment 1
The ripening-accelerating pesticide of one Plants, its innovative point is: comprise following composition and weight portion thereof: animal tallow 30 ~ 70 parts, loess 10 ~ 30 parts, safflower 10 ~ 30 parts, 30 ~ 40 parts, calcium oxide, triethanolamine 50 ~ 80 parts, organosiloxane 25 ~ 40 parts, potassium sulfate 20 ~ 40 parts, 18 ~ 30 parts, magnesium sulfate, sodium phosphate trimer 25 ~ 40 parts and absorption double solvents 50 ~ 90 parts.
Wherein, absorb double solvents and comprise plant attaching agent, easily lyosoption and emulsifier, described plant attaching agent, the easily concentration ratio of lyosoption and emulsifier three are 1 ~ 2:1.2 ~ 2.5:1.5 ~ 2.
The preparation method of the ripening-accelerating pesticide of one Plants, its innovative point is: specifically comprise the following steps:
(1) animal tallow of proportional quantity, loess and safflower are broken into fine powder according to proportional quantity, put into water, be heated to 50 ~ 60 DEG C, solution also, after keeping 1 ~ 2h, filters by continuous stirring, then filtrate heating is concentrated into 20 ~ 30%, cooling, packing, for subsequent use;
(2) calcium oxide of proportional quantity, triethanolamine, organosiloxane, potassium sulfate, magnesium sulfate and sodium phosphate trimer are worn into fine powder, mix, put into water, with hot-water soak 2 ~ 3h that temperature is 50 ~ 60 DEG C, sealing refining, after being filtered by solution, removing impurity and filter residue, carry out distillation recrystallization;
(3) product in step (1) and step (2) is joined in the absorption double solvents of proportional quantity successively, heat to 90 ~ 95 DEG C of sealing refining 1 ~ 2h, then filter, filtrate is heated concentration and evaporation 10 ~ 30%, cool.
Ripening-accelerating pesticide of the present invention adopts diverse ways according to different compositions, strict temperature control and operating time, extract the effective ingredient of medicine, make agricultural chemicals, and with absorb double solvents and dissolve accelerating the ripening for plant and crops, accelerating the ripening, to shorten the plant growth time be 10%; And also there is effect that certain desinsection controls worm and insect protected, replace chemical pesticide desinsection to remove the evil, killing rate is 90%.
Embodiment 2
The ripening-accelerating pesticide of one Plants, comprise following composition and weight portion thereof: animal tallow 40 ~ 50 parts, loess 20 ~ 26 parts, safflower 18 ~ 24 parts, 35 ~ 38 parts, calcium oxide, triethanolamine 65 ~ 70 parts, organosiloxane 28 ~ 36 parts, potassium sulfate 24 ~ 32 parts, 22 ~ 28 parts, magnesium sulfate, sodium phosphate trimer 30 ~ 34 parts and absorption double solvents 68 ~ 76 parts.
On the basis of embodiment 1, use the identical preparation method of embodiment 1, obtain the product of the present embodiment.
Ripening-accelerating pesticide of the present invention adopts diverse ways according to different compositions, strict temperature control and operating time, extract the effective ingredient of medicine, make agricultural chemicals, and with absorb double solvents and dissolve accelerating the ripening for plant and crops, accelerating the ripening, to shorten the plant growth time be 15%; And also there is effect that certain desinsection controls worm and insect protected, replace chemical pesticide desinsection to remove the evil, killing rate is 92%.
Embodiment 3
The ripening-accelerating pesticide of one Plants, comprise following composition and weight portion thereof: animal tallow 46 parts, loess 24 parts, safflower 22 parts, 37 parts, calcium oxide, triethanolamine 66 parts, organosiloxane 30 parts, potassium sulfate 28 parts, 25 parts, magnesium sulfate, sodium phosphate trimer 32 parts and absorption double solvents 72 parts.
On the basis of embodiment 1, use the identical preparation method of embodiment 1, change related experiment parameter, be specially: the filtrate heating in step (1) is concentrated into 23%; In step (2), temperature controls is 56 DEG C; Filtrate is heated concentration and evaporation to 18% in (3) by step, obtains the product of the present embodiment.
Ripening-accelerating pesticide of the present invention adopts diverse ways according to different compositions, strict temperature control and operating time, extract the effective ingredient of medicine, make agricultural chemicals, and with absorb double solvents and dissolve accelerating the ripening for plant and crops, accelerating the ripening, to shorten the plant growth time be 20%; And also there is effect that certain desinsection controls worm and insect protected, replace chemical pesticide desinsection to remove the evil, killing rate is 94%.

Claims (9)

1. the ripening-accelerating pesticide of a Plants, it is characterized in that: comprise following composition and weight portion thereof: animal tallow 30 ~ 70 parts, loess 10 ~ 30 parts, safflower 10 ~ 30 parts, 30 ~ 40 parts, calcium oxide, triethanolamine 50 ~ 80 parts, organosiloxane 25 ~ 40 parts, potassium sulfate 20 ~ 40 parts, 18 ~ 30 parts, magnesium sulfate, sodium phosphate trimer 25 ~ 40 parts and absorption double solvents 50 ~ 90 parts.
2. the ripening-accelerating pesticide of plant according to claim 1, it is characterized in that: described absorption double solvents comprises plant attaching agent, easily lyosoption and emulsifier, described plant attaching agent, the easily concentration ratio of lyosoption and emulsifier three are 1 ~ 2:1.2 ~ 2.5:1.5 ~ 2.
3. the ripening-accelerating pesticide of plant according to claim 2, it is characterized in that: described absorption double solvents comprises plant attaching agent, easily lyosoption and emulsifier, described plant attaching agent, the easily concentration ratio of lyosoption and emulsifier three are 1.5:1.8:1.8.
4. the ripening-accelerating pesticide of plant according to claim 1, it is characterized in that: comprise following composition and weight portion thereof: animal tallow 40 ~ 50 parts, loess 20 ~ 26 parts, safflower 18 ~ 24 parts, 35 ~ 38 parts, calcium oxide, triethanolamine 65 ~ 70 parts, organosiloxane 28 ~ 36 parts, potassium sulfate 24 ~ 32 parts, 22 ~ 28 parts, magnesium sulfate, sodium phosphate trimer 30 ~ 34 parts and absorption double solvents 68 ~ 76 parts.
5. the ripening-accelerating pesticide of the plant according to claim 1 or 3, it is characterized in that: comprise following composition and weight portion thereof: animal tallow 46 parts, loess 24 parts, safflower 22 parts, 37 parts, calcium oxide, triethanolamine 66 parts, organosiloxane 30 parts, potassium sulfate 28 parts, 25 parts, magnesium sulfate, sodium phosphate trimer 32 parts and absorption double solvents 72 parts.
6. a preparation method for the ripening-accelerating pesticide of plant according to claim 1, is characterized in that: specifically comprise the following steps:
(1) animal tallow of proportional quantity, loess and safflower are broken into fine powder according to proportional quantity, put into water, be heated to 50 ~ 60 DEG C, solution also, after keeping 1 ~ 2h, filters by continuous stirring, then filtrate heating is concentrated into 20 ~ 30%, cooling, packing, for subsequent use;
(2) calcium oxide of proportional quantity, triethanolamine, organosiloxane, potassium sulfate, magnesium sulfate and sodium phosphate trimer are worn into fine powder, mix, put into water, with hot-water soak 2 ~ 3h that temperature is 50 ~ 60 DEG C, sealing refining, after being filtered by solution, removing impurity and filter residue, carry out distillation recrystallization;
(3) product in step (1) and step (2) is joined in the absorption double solvents of proportional quantity successively, heat to 90 ~ 95 DEG C of sealing refining 1 ~ 2h, then filter, filtrate is heated concentration and evaporation 10 ~ 30%, cool.
7. the preparation method of the ripening-accelerating pesticide of plant according to claim 4, is characterized in that: the filtrate heating in described step (1) is concentrated into 23%.
8. the preparation method of the ripening-accelerating pesticide of plant according to claim 4, is characterized in that: in described step (2), temperature controls is 56 DEG C.
9. the preparation method of the ripening-accelerating pesticide of plant according to claim 4, is characterized in that: filtrate is heated concentration and evaporation to 18% in (3) by described step.
CN201410615704.XA 2014-11-05 2014-11-05 Ripening pesticide for plants, and preparation method thereof Pending CN104397057A (en)

Priority Applications (1)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107047644A (en) * 2016-12-14 2017-08-18 安徽东健化工科技有限公司 A kind of forest is taken precautions against calamities pesticidal preparations with desinsection
CN107372629A (en) * 2017-09-05 2017-11-24 南通派斯第农药化工股份有限公司 A kind of improved environment protection agricultural chemicals
CN107372642A (en) * 2017-09-05 2017-11-24 南通派斯第农药化工股份有限公司 A kind of improved environment protection agricultural chemicals
CN107467078A (en) * 2017-09-05 2017-12-15 南通派斯第农药化工股份有限公司 A kind of modified formulation of pesticide
CN107494607A (en) * 2017-09-05 2017-12-22 南通派斯第农药化工股份有限公司 A kind of modified green nuisance free pesticide
CN107494631A (en) * 2017-09-06 2017-12-22 南通派斯第农药化工股份有限公司 A kind of Novel environment-friendlypesticide pesticide

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101427692A (en) * 2007-11-06 2009-05-13 邓运春 Plant pesticide and preparation method thereof
CN101755855A (en) * 2008-11-27 2010-06-30 刘兴廉 Ripening-accelerating pesticide
CN103535348A (en) * 2013-09-23 2014-01-29 杨博葳 Pesticide
CN103891777A (en) * 2012-12-27 2014-07-02 南通优尼科化工有限公司 Pesticide
CN104068072A (en) * 2014-06-19 2014-10-01 陈啟文 Novel pesticide

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101427692A (en) * 2007-11-06 2009-05-13 邓运春 Plant pesticide and preparation method thereof
CN101755855A (en) * 2008-11-27 2010-06-30 刘兴廉 Ripening-accelerating pesticide
CN103891777A (en) * 2012-12-27 2014-07-02 南通优尼科化工有限公司 Pesticide
CN103535348A (en) * 2013-09-23 2014-01-29 杨博葳 Pesticide
CN104068072A (en) * 2014-06-19 2014-10-01 陈啟文 Novel pesticide

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107047644A (en) * 2016-12-14 2017-08-18 安徽东健化工科技有限公司 A kind of forest is taken precautions against calamities pesticidal preparations with desinsection
CN107372629A (en) * 2017-09-05 2017-11-24 南通派斯第农药化工股份有限公司 A kind of improved environment protection agricultural chemicals
CN107372642A (en) * 2017-09-05 2017-11-24 南通派斯第农药化工股份有限公司 A kind of improved environment protection agricultural chemicals
CN107467078A (en) * 2017-09-05 2017-12-15 南通派斯第农药化工股份有限公司 A kind of modified formulation of pesticide
CN107494607A (en) * 2017-09-05 2017-12-22 南通派斯第农药化工股份有限公司 A kind of modified green nuisance free pesticide
CN107494631A (en) * 2017-09-06 2017-12-22 南通派斯第农药化工股份有限公司 A kind of Novel environment-friendlypesticide pesticide

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