CN104327631A - Improved-hardness heat-radiation aqueous coating for glass doors, and its preparation method - Google Patents

Improved-hardness heat-radiation aqueous coating for glass doors, and its preparation method Download PDF

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Publication number
CN104327631A
CN104327631A CN201410538913.9A CN201410538913A CN104327631A CN 104327631 A CN104327631 A CN 104327631A CN 201410538913 A CN201410538913 A CN 201410538913A CN 104327631 A CN104327631 A CN 104327631A
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parts
coating
acid
water
resin
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Inventor
章功国
王泾文
段宗银
李纯金
陈超
王淑妍
张少伍
王晓芬
谢勇
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Maanshan Hengyi Machinery Manufacturing Co Ltd
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Maanshan Hengyi Machinery Manufacturing Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D133/00Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F220/00Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
    • C08F220/02Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
    • C08F220/10Esters
    • C08F220/12Esters of monohydric alcohols or phenols
    • C08F220/16Esters of monohydric alcohols or phenols of phenols or of alcohols containing two or more carbon atoms
    • C08F220/18Esters of monohydric alcohols or phenols of phenols or of alcohols containing two or more carbon atoms with acrylic or methacrylic acids
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/08Anti-corrosive paints
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/16Antifouling paints; Underwater paints
    • C09D5/1656Antifouling paints; Underwater paints characterised by the film-forming substance
    • C09D5/1662Synthetic film-forming substance
    • C09D5/1675Polyorganosiloxane-containing compositions
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/16Antifouling paints; Underwater paints
    • C09D5/1687Use of special additives
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F220/00Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
    • C08F220/02Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
    • C08F220/10Esters
    • C08F220/12Esters of monohydric alcohols or phenols
    • C08F220/16Esters of monohydric alcohols or phenols of phenols or of alcohols containing two or more carbon atoms
    • C08F220/18Esters of monohydric alcohols or phenols of phenols or of alcohols containing two or more carbon atoms with acrylic or methacrylic acids
    • C08F220/1804C4-(meth)acrylate, e.g. butyl (meth)acrylate, isobutyl (meth)acrylate or tert-butyl (meth)acrylate
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00Specific properties of additives
    • C08K2201/011Nanostructured additives
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00Specific properties of additives
    • C08K2201/014Additives containing two or more different additives of the same subgroup in C08K

Abstract

The invention discloses an improved-hardness heat-radiation aqueous coating for glass doors. The coating is prepared by using the following raw materials, by weight, 30-34 parts of aqueous hydroxy acrylic resin, 7-9 parts of an aqueous film forming assistant, 2-4 parts of hexamethyldisiloxane, 18-22 parts of aqueous gadoleic acid resin, 1-2 parts of nanometer sericite powder, 1-2 parts of a pigment, 4-7 parts of inorganic nanometer ceramic resin, 1-2 parts of magnesium dialkyl sulfosuccinate, 0.3-0.4 parts of octadecanamide, 0.2-0.4 parts of polyether modified polysiloxane, 0.3-0.4 parts of azodiisobutyronitrile, 0.4-0.7 parts of sodium phytate, 0.5-1.0 part of a silane coupling agent KH792, 1-2 parts of triethanolamine borate, 0.6-1.2 parts of magnesium tungstate, 2-3 parts of nanometer charcoal powder, 1-2 parts of flake graphene, 0.3-0.6 parts of urea, 2-3 parts of diethylenetriamine and 13-16 parts of deionized water. The coating has the advantages of ageing resistance, strong adhesion, corrosion resistance, pollution resistance, fouling resistance, mutual coordination of the added nanopowders, good filling property, increase of the smoothness and the flatness of a coating film of the coating, and good heat radiation property.

Description

A kind of raising hardness heat radiating type glass door use coating and preparation method thereof
Technical field
The present invention relates to a kind of coating and preparation method thereof, particularly a kind of raising hardness heat radiating type glass door use coating and preparation method thereof.
Background technology
Indoor and outdoor, between space and space boundary has been linked up in the appearance of glass, allows Home Fashion & Design Shanghai there occurs revolutionary leap.And the Technology of present coating imparts the more artistry of glass and functional.Although existing glass paint can meet the demand of people to a certain extent, but the glass paint that market is sold mostly is oil paint, its filmogen is mainly from petroleum chemicals, and its solvent also adopts organic solvent more, usually containing toxic substances such as formaldehyde, free TDI and dimethylbenzene, these materials constantly come out in glass paint production process and use procedure, not only cause environmental pollution, and damage HUMAN HEALTH; Compared with traditional solvent based coating, water-borne coatings has that price is low, use safety, saving resource and the energy, reduce the advantage such as environmental pollution and public hazards, because becoming the Main way of current development coatings industry, so glass paint is developed by solvent-borne type hydrotropisms, it is the inexorable trend adapting to environment protection requirement development, and along with the continuous expansion of Application Areas, more and more higher requirement is proposed to glass paint functional performance, the requirement having surmounted traditional decoration far away and beautified.
Acrylic resin paint has good gloss retention, tint retention, quick-drying and erosion resistance, along with the enhancing of people's environmental consciousness and the constantly sound of law, acrylic resin paint also hydrotropisms's paint development gradually, water-borne acrylic resin because of transparent color and luster, protect that light tint retention is good, glossiness is good, good heat resistance, corrosion-resistant and stain resistance good, the advantage such as cheap is widely used.The present invention, by the waterborne film-forming auxiliary agent added, is applied to family decoration glass door, has film forming properties excellent, ageing-resistant, strong adhesion, corrosion-resistant, stain resistance and good etc. the feature of didirtresistance.
Summary of the invention
The object of this invention is to provide a kind of raising hardness heat radiating type glass door use coating and preparation method thereof.
In order to realize object of the present invention, the present invention is by following scheme implementation:
A kind of raising hardness heat radiating type glass door use coating, be made up of the raw material of following weight part: water based acrylic resin 30-34, waterborne film-forming auxiliary agent 7-9, hexamethyldisiloxane 2-4, water-based olefin(e) acid resin 18-22, nanometer sericite in powder 1-2, pigment 1-2, inorganic nano ceramic resin 4-7, dialkyl acid sulfonic acid magnesium 1-2, stearic amide 0.3-0.4, Siloxane-Oxyalkylene Copolymers 0.2-0.4, Diisopropyl azodicarboxylate 0.3-0.4, sodium phytate 0.4-0.7, silane coupling agent KH7920.5-1.0, triethanolamine borate 1-2, magnesium wolframate 0.6-1.2, nano wood powdered carbon 2-3, crystalline flake graphite alkene 1-2, urea 0.3-0.6, diethylenetriamine 2-3, deionized water 13-16,
Described waterborne film-forming auxiliary agent is made up of the raw material of following weight part: the different monooctyl ester 1-2 of 3-thiohydracrylic acid, methyl methacrylate 13-16, butyl acrylate 22-25, Propylene glycol monoacrylate 12-15, methacrylic acid 8-11, benzoyl peroxide 1-3, Diisopropyl azodicarboxylate 0.5-1.0, butylacetate 18-22, AAEM 4-6, dimethylethanolamine 3-4, polyborosiloxane 2-3, nm-class rutile-type TiO 2 3-5, silane coupling agent KH5601-2, dehydrated alcohol 10-15, distilled water 100-150, nm-class rutile-type TiO 2, polyborosiloxane and dehydrated alcohol are added in round-bottomed flask fully to stir and ultrasonic vibration 10-20min by preparation method, and slowly add silane coupling agent KH560 be heated to backflow, isothermal reaction 1-2 hour, filters and uses distilled water wash three dry for standby.By methyl methacrylate, butyl acrylate, Propylene glycol monoacrylate, the benzoyl peroxide mixing formation monomer mixed solution of methacrylic acid and 10-30% is for subsequent use, butylacetate is heated to 120-140 ° of C, add the monomer mixture solution of 10-20%, above-mentioned material for subsequent use, the different monooctyl ester of 3-thiohydracrylic acid and Diisopropyl azodicarboxylate, insulation reaction 45 minutes, slowly drip remaining mixed monomer solution and benzoyl peroxide again, guarantee to drip in 1.5 hours to terminate, constant temperature keeps adding dimethylethanolamine and distilled water after 2-3 hour, the azeotrope of heating desolvation and distilled water, add AAEM mixing and stirring again and can obtain waterborne film-forming auxiliary agent.
One of the present invention improves hardness heat radiating type glass door use coating, is made up of following concrete steps:
(1) deionized water, sodium phytate, Siloxane-Oxyalkylene Copolymers, dialkyl acid sulfonic acid magnesium, urea mixing are added in Scattered Kettle, to stir 3-5 minute under the condition of 600-800 rev/min;
(2) rotating speed is adjusted to 900-1000 rev/min, in Scattered Kettle, adds hexamethyldisiloxane, stearic amide, Diisopropyl azodicarboxylate, triethanolamine borate stirring 6-8 minute;
(3) rotating speed is adjusted to 1400-1600 rev/min, adds water based acrylic resin, waterborne film-forming auxiliary agent, water-based olefin(e) acid resin, inorganic nano ceramic resin, diethylenetriamine stirring 15-25 minute;
(4) rotating speed is adjusted to 1000-1200 rev/min, adds silane coupling agent KH792, pigment, nano wood powdered carbon, magnesium wolframate, crystalline flake graphite alkene, nanometer sericite in powder stirring 20-30 minute successively;
(5) be added in sand mill and carry out grinding distribution by the material after dispersion, after filtering, fineness is less than 20 μm and packs.
Advantage of the present invention is: it is excellent that the present invention has film forming properties by the waterborne film-forming auxiliary agent added, ageing-resistant, strong adhesion, corrosion-resistant, stain resistance and good etc. the effect of didirtresistance, inorganic nano ceramic resin can increase the hardness of film, wear resistance, weathering resistance, stain resistance and the performance such as high temperature resistant, and the multiple nano-powder that coating of the present invention adds is coordinated mutually, and fillibility is good, add the smooth of coating and planarization, good heat dissipation effect.
specific embodiments
Below by specific examples, the present invention is described in detail.
A kind of raising hardness heat radiating type glass door use coating, be made up of the raw material of following weight part (kilogram): water based acrylic resin 32, waterborne film-forming auxiliary agent 8, hexamethyldisiloxane 2, water-based olefin(e) acid resin 20, nanometer sericite in powder 2, pigment 2, inorganic nano ceramic resin 4, dialkyl acid sulfonic acid magnesium 2, stearic amide 0.3, Siloxane-Oxyalkylene Copolymers 0.2, Diisopropyl azodicarboxylate 0.3, sodium phytate 0.6, silane coupling agent KH7920.8, triethanolamine borate 2, magnesium wolframate 0.8, nano wood powdered carbon 3, crystalline flake graphite alkene 1, urea 0.5, diethylenetriamine 3, deionized water 15,
Described waterborne film-forming auxiliary agent is made up of the raw material of following weight part (kilogram): the different monooctyl ester 1 of 3-thiohydracrylic acid, methyl methacrylate 14, butyl acrylate 24, Propylene glycol monoacrylate 13, methacrylic acid 10, benzoyl peroxide 2, Diisopropyl azodicarboxylate 0.7, butylacetate 20, AAEM 5, dimethylethanolamine 3, polyborosiloxane 3, nm-class rutile-type TiO 24, silane coupling agent KH5601.5, dehydrated alcohol 15, distilled water 110; Nm-class rutile-type TiO 2, polyborosiloxane and dehydrated alcohol are added in round-bottomed flask fully to stir and ultrasonic vibration 10-20min by preparation method, and slowly add silane coupling agent KH560 be heated to backflow, isothermal reaction 1-2 hour, filters and uses distilled water wash three dry for standby.By methyl methacrylate, butyl acrylate, Propylene glycol monoacrylate, the benzoyl peroxide mixing formation monomer mixed solution of methacrylic acid and 10-30% is for subsequent use, butylacetate is heated to 120-140 ° of C, add the monomer mixture solution of 10-20%, above-mentioned material for subsequent use, the different monooctyl ester of 3-thiohydracrylic acid and Diisopropyl azodicarboxylate, insulation reaction 45 minutes, slowly drip remaining mixed monomer solution and benzoyl peroxide again, guarantee to drip in 1.5 hours to terminate, constant temperature keeps adding dimethylethanolamine and distilled water after 2-3 hour, the azeotrope of heating desolvation and distilled water, add AAEM mixing and stirring again and can obtain waterborne film-forming auxiliary agent.
One of the present invention improves hardness heat radiating type glass door use coating, is made up of following concrete steps:
(1) deionized water, sodium phytate, Siloxane-Oxyalkylene Copolymers, dialkyl acid sulfonic acid magnesium, urea mixing are added in Scattered Kettle, to stir 3-5 minute under the condition of 600-800 rev/min;
(2) rotating speed is adjusted to 900-1000 rev/min, in Scattered Kettle, adds hexamethyldisiloxane, stearic amide, Diisopropyl azodicarboxylate, triethanolamine borate stirring 6-8 minute;
(3) rotating speed is adjusted to 1400-1600 rev/min, adds water based acrylic resin, waterborne film-forming auxiliary agent, water-based olefin(e) acid resin, inorganic nano ceramic resin, diethylenetriamine stirring 15-25 minute;
(4) rotating speed is adjusted to 1000-1200 rev/min, adds silane coupling agent KH792, pigment, nano wood powdered carbon, magnesium wolframate, crystalline flake graphite alkene, nanometer sericite in powder stirring 20-30 minute successively;
(5) be added in sand mill and carry out grinding distribution by the material after dispersion, after filtering, fineness is less than 20 μm and packs.
After paint solidification of the present invention, hardness of paint film is 5H, and sticking power experiment is 0 grade, wear resistance experiment (0.5g/r)/mg:5.0, shock resistance is tested: 50cm, water tolerance experiment (600h): without exception, resistance to boiling water experiment (100 ° of C >=24h): not loss of gloss, non-foaming, allows slightly to change, can restore, alcohol resistance experiment (soaked in absolute ethyl alcohol 24h): without exception, salt fog resistance experiment (12h): unchanged, artificial ageing resistance is tested: 1000h is non-foaming, do not peel off, flawless.

Claims (2)

1. one kind is improved hardness heat radiating type glass door use coating, it is characterized in that, be made up of the raw material of following weight part: water based acrylic resin 30-34, waterborne film-forming auxiliary agent 7-9, hexamethyldisiloxane 2-4, water-based olefin(e) acid resin 18-22, nanometer sericite in powder 1-2, pigment 1-2, inorganic nano ceramic resin 4-7, dialkyl acid sulfonic acid magnesium 1-2, stearic amide 0.3-0.4, Siloxane-Oxyalkylene Copolymers 0.2-0.4, Diisopropyl azodicarboxylate 0.3-0.4, sodium phytate 0.4-0.7, silane coupling agent KH7920.5-1.0, triethanolamine borate 1-2, magnesium wolframate 0.6-1.2, nano wood powdered carbon 2-3, crystalline flake graphite alkene 1-2, urea 0.3-0.6, diethylenetriamine 2-3, deionized water 13-16,
Described waterborne film-forming auxiliary agent is made up of the raw material of following weight part: the different monooctyl ester 1-2 of 3-thiohydracrylic acid, methyl methacrylate 13-16, butyl acrylate 22-25, Propylene glycol monoacrylate 12-15, methacrylic acid 8-11, benzoyl peroxide 1-3, Diisopropyl azodicarboxylate 0.5-1.0, butylacetate 18-22, AAEM 4-6, dimethylethanolamine 3-4, polyborosiloxane 2-3, nm-class rutile-type TiO 2 3-5, silane coupling agent KH5601-2, dehydrated alcohol 10-15, distilled water 100-150, nm-class rutile-type TiO 2, polyborosiloxane and dehydrated alcohol are added in round-bottomed flask fully to stir and ultrasonic vibration 10-20min by preparation method, and slowly add silane coupling agent KH560 be heated to backflow, isothermal reaction 1-2 hour, filters and uses distilled water wash three dry for standby,
By methyl methacrylate, butyl acrylate, Propylene glycol monoacrylate, the benzoyl peroxide mixing formation monomer mixed solution of methacrylic acid and 10-30% is for subsequent use, butylacetate is heated to 120-140 ° of C, add the monomer mixture solution of 10-20%, above-mentioned material for subsequent use, the different monooctyl ester of 3-thiohydracrylic acid and Diisopropyl azodicarboxylate, insulation reaction 45 minutes, slowly drip remaining mixed monomer solution and benzoyl peroxide again, guarantee to drip in 1.5 hours to terminate, constant temperature keeps adding dimethylethanolamine and distilled water after 2-3 hour, the azeotrope of heating desolvation and distilled water, add AAEM mixing and stirring again and can obtain waterborne film-forming auxiliary agent.
2. one improves hardness heat radiating type glass door use coating according to claim 1, it is characterized in that, is made up of following concrete steps:
(1) deionized water, sodium phytate, Siloxane-Oxyalkylene Copolymers, dialkyl acid sulfonic acid magnesium, urea mixing are added in Scattered Kettle, to stir 3-5 minute under the condition of 600-800 rev/min;
(2) rotating speed is adjusted to 900-1000 rev/min, in Scattered Kettle, adds hexamethyldisiloxane, stearic amide, Diisopropyl azodicarboxylate, triethanolamine borate stirring 6-8 minute;
(3) rotating speed is adjusted to 1400-1600 rev/min, adds water based acrylic resin, waterborne film-forming auxiliary agent, water-based olefin(e) acid resin, inorganic nano ceramic resin, diethylenetriamine stirring 15-25 minute;
(4) rotating speed is adjusted to 1000-1200 rev/min, adds silane coupling agent KH792, pigment, nano wood powdered carbon, magnesium wolframate, crystalline flake graphite alkene, nanometer sericite in powder stirring 20-30 minute successively;
(5) be added in sand mill and carry out grinding distribution by the material after dispersion, after filtering, fineness is less than 20 μm and packs.
CN201410538913.9A 2014-10-14 2014-10-14 Improved-hardness heat-radiation aqueous coating for glass doors, and its preparation method Pending CN104327631A (en)

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CN111777910A (en) * 2020-07-28 2020-10-16 天津中航百慕新材料技术有限公司 Water-based graphite allyl acid-polysiloxane coating and preparation method thereof

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CN105820624A (en) * 2016-05-13 2016-08-03 珠海市远康企业有限公司 Nanometer ceramic and graphene compound paint for outdoor lamp and preparation method thereof
CN109233642A (en) * 2018-08-29 2019-01-18 邯郸市邯山区靓鱼宝水产饲料制造有限公司 A kind of water paint and preparation method thereof with anti-static effect
CN111777910A (en) * 2020-07-28 2020-10-16 天津中航百慕新材料技术有限公司 Water-based graphite allyl acid-polysiloxane coating and preparation method thereof

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Application publication date: 20150204