CN104131292A - Conveniently-cleaned anti-corrosion composite polishing fluid and preparation method thereof - Google Patents
Conveniently-cleaned anti-corrosion composite polishing fluid and preparation method thereof Download PDFInfo
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- CN104131292A CN104131292A CN201410308876.2A CN201410308876A CN104131292A CN 104131292 A CN104131292 A CN 104131292A CN 201410308876 A CN201410308876 A CN 201410308876A CN 104131292 A CN104131292 A CN 104131292A
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- parts
- auxiliary agent
- sodium
- polishing fluid
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- 238000005498 polishing Methods 0.000 title claims abstract description 20
- 239000002131 composite material Substances 0.000 title claims abstract description 11
- 238000002360 preparation method Methods 0.000 title claims abstract description 8
- 238000005260 corrosion Methods 0.000 title abstract description 4
- 239000012530 fluid Substances 0.000 title abstract 5
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 20
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- 230000003670 easy-to-clean Effects 0.000 claims abstract description 10
- 235000019329 dioctyl sodium sulphosuccinate Nutrition 0.000 claims abstract description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229910000420 cerium oxide Inorganic materials 0.000 claims abstract description 7
- 239000008367 deionised water Substances 0.000 claims abstract description 7
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 7
- BMMGVYCKOGBVEV-UHFFFAOYSA-N oxo(oxoceriooxy)cerium Chemical compound [Ce]=O.O=[Ce]=O BMMGVYCKOGBVEV-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 239000004408 titanium dioxide Substances 0.000 claims abstract description 7
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims abstract description 5
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims abstract description 4
- -1 phosphate ester Chemical class 0.000 claims abstract description 4
- 235000010413 sodium alginate Nutrition 0.000 claims abstract description 4
- 239000000661 sodium alginate Substances 0.000 claims abstract description 4
- 229940005550 sodium alginate Drugs 0.000 claims abstract description 4
- RYYKJJJTJZKILX-UHFFFAOYSA-M sodium octadecanoate Chemical compound [Na+].CCCCCCCCCCCCCCCCCC([O-])=O RYYKJJJTJZKILX-UHFFFAOYSA-M 0.000 claims abstract description 3
- 239000000463 material Substances 0.000 claims description 13
- 238000003756 stirring Methods 0.000 claims description 12
- 239000007788 liquid Substances 0.000 claims description 9
- 238000002156 mixing Methods 0.000 claims description 9
- CDOUZKKFHVEKRI-UHFFFAOYSA-N 3-bromo-n-[(prop-2-enoylamino)methyl]propanamide Chemical compound BrCCC(=O)NCNC(=O)C=C CDOUZKKFHVEKRI-UHFFFAOYSA-N 0.000 claims description 7
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 6
- 229920002785 Croscarmellose sodium Polymers 0.000 claims description 6
- BAPJBEWLBFYGME-UHFFFAOYSA-N Methyl acrylate Chemical compound COC(=O)C=C BAPJBEWLBFYGME-UHFFFAOYSA-N 0.000 claims description 6
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 claims description 6
- 229960001681 croscarmellose sodium Drugs 0.000 claims description 6
- 235000010947 crosslinked sodium carboxy methyl cellulose Nutrition 0.000 claims description 6
- 239000003995 emulsifying agent Substances 0.000 claims description 6
- 239000012467 final product Substances 0.000 claims description 6
- 238000009413 insulation Methods 0.000 claims description 6
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims description 6
- 239000003795 chemical substances by application Substances 0.000 claims description 4
- 150000003014 phosphoric acid esters Chemical class 0.000 claims description 3
- 235000019353 potassium silicate Nutrition 0.000 claims description 3
- LLHKCFNBLRBOGN-UHFFFAOYSA-N propylene glycol methyl ether acetate Chemical compound COCC(C)OC(C)=O LLHKCFNBLRBOGN-UHFFFAOYSA-N 0.000 claims description 3
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 3
- 229910001220 stainless steel Inorganic materials 0.000 abstract description 8
- 239000010935 stainless steel Substances 0.000 abstract description 8
- 229910052751 metal Inorganic materials 0.000 abstract description 6
- 239000002184 metal Substances 0.000 abstract description 6
- 238000005516 engineering process Methods 0.000 abstract description 2
- 230000007774 longterm Effects 0.000 abstract description 2
- 231100000252 nontoxic Toxicity 0.000 abstract description 2
- 230000003000 nontoxic effect Effects 0.000 abstract description 2
- 238000001179 sorption measurement Methods 0.000 abstract description 2
- 239000013556 antirust agent Substances 0.000 abstract 2
- 229960000878 docusate sodium Drugs 0.000 abstract 2
- APSBXTVYXVQYAB-UHFFFAOYSA-M sodium docusate Chemical compound [Na+].CCCCC(CC)COC(=O)CC(S([O-])(=O)=O)C(=O)OCC(CC)CCCC APSBXTVYXVQYAB-UHFFFAOYSA-M 0.000 abstract 2
- 229910019142 PO4 Inorganic materials 0.000 abstract 1
- 239000010410 layer Substances 0.000 abstract 1
- 239000010452 phosphate Substances 0.000 abstract 1
- 239000002344 surface layer Substances 0.000 abstract 1
- 239000004094 surface-active agent Substances 0.000 abstract 1
- 239000000047 product Substances 0.000 description 6
- 239000000126 substance Substances 0.000 description 4
- 238000004140 cleaning Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 230000007797 corrosion Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 241000533950 Leucojum Species 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 238000003486 chemical etching Methods 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 238000009533 lab test Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- PVGBHEUCHKGFQP-UHFFFAOYSA-N sodium;n-[5-amino-2-(4-aminophenyl)sulfonylphenyl]sulfonylacetamide Chemical compound [Na+].CC(=O)NS(=O)(=O)C1=CC(N)=CC=C1S(=O)(=O)C1=CC=C(N)C=C1 PVGBHEUCHKGFQP-UHFFFAOYSA-N 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000011179 visual inspection Methods 0.000 description 1
Abstract
A disclosed conveniently-cleaned anti-corrosion composite polishing fluid is characterized by being prepared from the following raw materials in parts by weight: 11-14 parts of cerium oxide, 5-7 parts of titanium dioxide, 3-4 parts of antirust agent T747, 5-7 parts of ethanol, 2-4 parts of phosphate ester, 5-7 parts of isopropanol, 4-7 parts of docusate sodium, 3-5 parts of sodium stearate, 2-4 parts of sodium alginate, 5-7 parts of an auxiliary agent, and 300 parts of deionized water. By adding docusate sodium and other surfactants, the polishing fluid is capable of forming a long-term conveniently-cleaned physical adsorption surface layer on a processed metal surface and helps to improve the surface state. By adding the auxiliary agent, the polishing fluid has good wear resistance, dispersity, lubricity and film-forming property. By adding the antirust agent, an antirust layer can be formed on a metal surface. The mixed polishing fluid is safe, non-toxic, simple in preparation technology, high in polishing speed, easy to clean, and applicable to polishing of stainless steel products.
Description
Technical field
The present invention relates to technical field of surface, particularly etch-proof composite polishing liquid of a kind of easy to clean and preparation method thereof.
Background technology
Stainless steel refers to the steel of the chemical etching dielectric corrosions such as the weak corrosive medium such as resistance to air, steam, water and acid, alkali, salt.The product of stainless material is very many at present, and part shape complexity is various, and operation is more in the course of processing.Stainless steel in use inevitably can produce scuffing, damage etc., thereby stainless steel product can not normally be used.Because the complexity such as shape size of stainless steel part are various, therefore traditional mechanical polishing mode can not meet the requirement of product, and the method for electropolishing also cannot meet for the product with certain size, and the homogeneity of electropolishing is relatively poor simultaneously.
The shape that is not subject to part, the restriction of size are processed in chemical rightenning, do not need special instrument, and disposablely can process more part, chemical rightenning is to utilize the surface of the chemical solution of definite composition to microcosmic injustice, the metal at outstanding position is dissolved fast, thereby smooth microcosmic is plane surface not, reach bright effect.Hardware shapes rear surface can adhere to one deck greasy dirt or other chemicals conventionally; utensil uses after for some time the corrosion by environment for use; on surface, can produce rusty stain; for attractive in appearance and increase the service life; conventional special-purpose metal cleaner or rumbling compound cleared up surperficial dirt, but existing rumbling compound product exist return fast, the applicable metal species of rust narrow, clean halfway problem.
Summary of the invention
The object of this invention is to provide etch-proof composite polishing liquid of a kind of easy to clean and preparation method thereof.
In order to realize object of the present invention, the present invention passes through following scheme implementation:
The etch-proof composite polishing liquid of easy to clean, is made by the raw material of following weight part: cerium oxide 11-14, titanium dioxide 5-7, rust-preventive agent T747 3-4, ethanol 5-7, phosphoric acid ester 2-4, Virahol 5-7, Dioctyl Sodium Sulfosuccinate 4-7, sodium stearate 3-5, sodium alginate 2-4, auxiliary agent 5-7, deionized water 300;
Described auxiliary agent is made by the raw material of following weight part: aluminium sesquioxide 4-6, nano titanium oxide 5-7, water glass 1-2,1-Methoxy-2-propyl acetate 3-4, Lauryl Alcohol ester 2-3, methyl acrylate 2-4, croscarmellose sodium 2-3, emulsifier BP 4-5, water 50-54; First preparation method adds aluminium sesquioxide, nano titanium oxide, croscarmellose sodium, emulsifier BP in the water of half amount, grind 1-2 hour, then slowly add all the other remaining components, slowly be heated to 70 ℃-80 ℃, stirring reaction 30-50 minute under 300-500 rev/min of condition, is cooled to room temperature and get final product.
The etch-proof composite polishing liquid of a kind of easy to clean of the present invention, by following concrete steps, made:
(1) cerium oxide, titanium dioxide, Dioctyl Sodium Sulfosuccinate are mixed, add appropriate deionized water, be heated to 30 ℃-35 ℃, grind 25-35 minute, obtain mixing A material;
(2) all the other remaining components except auxiliary agent are joined in reactor, be uniformly mixed, be slowly heated to 35 ℃-45 ℃, insulation 1-1.5 hour, obtains mixing B material;
(3) the mixing B material of insulation is slowly joined while stirring and mixed in A material, after fully stirring, add auxiliary agent, continue to stir 25-35 minute, be cooled to room temperature and get final product.
Excellent effect of the present invention is: the present invention adds the tensio-active agents such as Dioctyl Sodium Sulfosuccinate, on processing metal surface, form the physical adsorption top layer of long-term easy cleaning, to improve condition of surface, add auxiliary agent, have good wear-resisting, disperse, lubricated, film-forming properties, add rust-preventive agent, can form rustproof layer in metallic surface; Mixed polishing solution of the present invention, safety non-toxic, manufacture craft is simple, two-forty, easy cleaning, is applicable to Stainless Steel Products polishing.
Embodiment
Below by specific examples, the present invention is described in detail.
The etch-proof composite polishing liquid of easy to clean, by following weight part (kilogram) raw material make: cerium oxide 11, titanium dioxide 5, rust-preventive agent T747 3, ethanol 5, phosphoric acid ester 2, Virahol 5, Dioctyl Sodium Sulfosuccinate 4, sodium stearate 3, sodium alginate 2, auxiliary agent 5, deionized water 300;
Described auxiliary agent by following weight part (kilogram) raw material make: aluminium sesquioxide 4, nano titanium oxide 5, water glass 1,1-Methoxy-2-propyl acetate 3, Lauryl Alcohol ester 2, methyl acrylate 2, croscarmellose sodium 2, emulsifier BP 4, water 50; First preparation method adds aluminium sesquioxide, nano titanium oxide, croscarmellose sodium, emulsifier BP in the water of half amount, grind 1-2 hour, then slowly add all the other remaining components, slowly be heated to 70 ℃-80 ℃, stirring reaction 30-50 minute under 300-500 rev/min of condition, is cooled to room temperature and get final product.
The etch-proof composite polishing liquid of a kind of easy to clean of the present invention, by following concrete steps, made:
(1) cerium oxide, titanium dioxide, Dioctyl Sodium Sulfosuccinate are mixed, add appropriate deionized water, be heated to 30 ℃-35 ℃, grind 25-35 minute, obtain mixing A material;
(2) all the other remaining components except auxiliary agent are joined in reactor, be uniformly mixed, be slowly heated to 35 ℃-45 ℃, insulation 1-1.5 hour, obtains mixing B material;
(3) the mixing B material of insulation is slowly joined while stirring and mixed in A material, after fully stirring, add auxiliary agent, continue to stir 25-35 minute, be cooled to room temperature and get final product.
Laboratory test results: the surface of each stainless steel work-piece of visual inspection, workpiece surface outward appearance evenly, without heterochromatic or have slight aberration and without snowflake; Adopt miniature glossometer A-4430(Germany BYK company) glossiness of testing each polishing stainless steel workpiece surface, glossiness is 48 Gu.
Claims (2)
1. the etch-proof composite polishing liquid of easy to clean, it is characterized in that, by the raw material of following weight part, made: cerium oxide 11-14, titanium dioxide 5-7, rust-preventive agent T747 3-4, ethanol 5-7, phosphoric acid ester 2-4, Virahol 5-7, Dioctyl Sodium Sulfosuccinate 4-7, sodium stearate 3-5, sodium alginate 2-4, auxiliary agent 5-7, deionized water 300;
Described auxiliary agent is made by the raw material of following weight part: aluminium sesquioxide 4-6, nano titanium oxide 5-7, water glass 1-2,1-Methoxy-2-propyl acetate 3-4, Lauryl Alcohol ester 2-3, methyl acrylate 2-4, croscarmellose sodium 2-3, emulsifier BP 4-5, water 50-54; First preparation method adds aluminium sesquioxide, nano titanium oxide, croscarmellose sodium, emulsifier BP in the water of half amount, grind 1-2 hour, then slowly add all the other remaining components, slowly be heated to 70 ℃-80 ℃, stirring reaction 30-50 minute under 300-500 rev/min of condition, is cooled to room temperature and get final product.
2. the etch-proof composite polishing liquid of a kind of easy to clean according to claim 1, is characterized in that, by following concrete steps, is made:
(1) cerium oxide, titanium dioxide, Dioctyl Sodium Sulfosuccinate are mixed, add appropriate deionized water, be heated to 30 ℃-35 ℃, grind 25-35 minute, obtain mixing A material;
(2) all the other remaining components except auxiliary agent are joined in reactor, be uniformly mixed, be slowly heated to 35 ℃-45 ℃, insulation 1-1.5 hour, obtains mixing B material;
(3) the mixing B material of insulation is slowly joined while stirring and mixed in A material, after fully stirring, add auxiliary agent, continue to stir 25-35 minute, be cooled to room temperature and get final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410308876.2A CN104131292B (en) | 2014-07-01 | 2014-07-01 | Etch-proof composite polishing liquid of a kind of easy to clean and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410308876.2A CN104131292B (en) | 2014-07-01 | 2014-07-01 | Etch-proof composite polishing liquid of a kind of easy to clean and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104131292A true CN104131292A (en) | 2014-11-05 |
| CN104131292B CN104131292B (en) | 2015-10-28 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201410308876.2A Active CN104131292B (en) | 2014-07-01 | 2014-07-01 | Etch-proof composite polishing liquid of a kind of easy to clean and preparation method thereof |
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| Country | Link |
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| CN (1) | CN104131292B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114350317A (en) * | 2021-12-28 | 2022-04-15 | 广东红日星实业有限公司 | Grinding fluid and preparation method and application thereof |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH01208484A (en) * | 1988-02-15 | 1989-08-22 | Nippon Stainless Steel Co Ltd | Polished stainless steel having superior corrosion resistance and production thereof |
| JPH01219171A (en) * | 1988-01-14 | 1989-09-01 | Henkel Kgaa | Method and compound for polishing, washing and passivating metal processed member |
| US4959113A (en) * | 1989-07-31 | 1990-09-25 | Rodel, Inc. | Method and composition for polishing metal surfaces |
| JPH1074719A (en) * | 1996-07-22 | 1998-03-17 | Motorola Inc | Manufacture of element |
| US20040025444A1 (en) * | 2002-02-11 | 2004-02-12 | Ekc Technology, Inc. | Fenton's reagent composition for chemical-mechanical polishing, method of using same, and substrate treated with same |
| CN103451658A (en) * | 2013-08-23 | 2013-12-18 | 苏州长盛机电有限公司 | Environmentally-friendly metal polishing agent and preparation method thereof |
| CN103498161A (en) * | 2013-09-23 | 2014-01-08 | 无锡阳工机械制造有限公司 | Metal polishing anti-corrosion slurry |
-
2014
- 2014-07-01 CN CN201410308876.2A patent/CN104131292B/en active Active
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH01219171A (en) * | 1988-01-14 | 1989-09-01 | Henkel Kgaa | Method and compound for polishing, washing and passivating metal processed member |
| JPH01208484A (en) * | 1988-02-15 | 1989-08-22 | Nippon Stainless Steel Co Ltd | Polished stainless steel having superior corrosion resistance and production thereof |
| US4959113A (en) * | 1989-07-31 | 1990-09-25 | Rodel, Inc. | Method and composition for polishing metal surfaces |
| US4959113C1 (en) * | 1989-07-31 | 2001-03-13 | Rodel Inc | Method and composition for polishing metal surfaces |
| JPH1074719A (en) * | 1996-07-22 | 1998-03-17 | Motorola Inc | Manufacture of element |
| US20040025444A1 (en) * | 2002-02-11 | 2004-02-12 | Ekc Technology, Inc. | Fenton's reagent composition for chemical-mechanical polishing, method of using same, and substrate treated with same |
| CN103451658A (en) * | 2013-08-23 | 2013-12-18 | 苏州长盛机电有限公司 | Environmentally-friendly metal polishing agent and preparation method thereof |
| CN103498161A (en) * | 2013-09-23 | 2014-01-08 | 无锡阳工机械制造有限公司 | Metal polishing anti-corrosion slurry |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114350317A (en) * | 2021-12-28 | 2022-04-15 | 广东红日星实业有限公司 | Grinding fluid and preparation method and application thereof |
| CN114350317B (en) * | 2021-12-28 | 2023-08-15 | 广东红日星实业有限公司 | Grinding fluid and preparation method and application thereof |
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| Publication number | Publication date |
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| CN104131292B (en) | 2015-10-28 |
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Denomination of invention: Conveniently-cleaned anti-corrosion composite polishing fluid and preparation method thereof Effective date of registration: 20200612 Granted publication date: 20151028 Pledgee: Merchants Bank Bengbu branch of Limited by Share Ltd. Pledgor: BENGBU GAOHUA ELECTRONIC Co.,Ltd. Registration number: Y2020980003040 |
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Denomination of invention: A composite polishing liquid for easy cleaning and corrosion prevention and its preparation method Effective date of registration: 20220701 Granted publication date: 20151028 Pledgee: Bengbu Branch of China Everbright Bank Co.,Ltd. Pledgor: BENGBU GAOHUA ELECTRONIC Co.,Ltd. Registration number: Y2022980009667 |