CN104109430B - A kind of emulsion-type waterproof anti-corrosion acrylate paint for external wall - Google Patents
A kind of emulsion-type waterproof anti-corrosion acrylate paint for external wall Download PDFInfo
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- CN104109430B CN104109430B CN201410310476.5A CN201410310476A CN104109430B CN 104109430 B CN104109430 B CN 104109430B CN 201410310476 A CN201410310476 A CN 201410310476A CN 104109430 B CN104109430 B CN 104109430B
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Abstract
The invention discloses a kind of emulsion-type waterproof anti-corrosion acrylate paint for external wall, its raw material includes 50 60 parts of base materials, 5 15 parts of alcohol ester 12 coalescents and 30 40 parts of adjuvants by weight；The raw materials by weight of described base material includes: drying oil alkyd resin 5 10 parts, acrylic emulsion 50 60 parts, Ludox 30 40 parts, coupling agent 26 parts, sodium butylnaphthalenesulfonate 14 parts；Adjuvant includes by weight: Borax 20 25 parts, precipitated calcium carbonate 15 20 parts, titanium dioxide 15 20 parts, wollastonite in powder 18 23 parts, nano zine oxide 5 10 parts, polyvinylpyrrolidone 0.5 1 parts, defoamer 0.5 1.5 parts, sodium carboxymethyl cellulose 0.8 1.3 parts, 1,2 benzisothiazole 3 ketone 12 parts, ammonia 1 1.3 parts, 10 15 parts of water, nylon acid methyl ester 25 parts.Water resistance of the present invention is excellent, and corrosion resistance is strong, and service life is long.
Description
Technical field
The present invention relates to acrylate paint for external wall technical field, particularly relate to a kind of emulsion-type waterproof anti-corrosion
Acrylate paint for external wall.
Background technology
The Cultivar development of China's anticorrosive paint is extremely rapid, at present, has developed the anticorrosion of many function admirables
Coating, such as high-temperature anticorrosion paint, anti-static and anti-corrosive paint, high resiliency anticorrosive paint, nonpoisonous anti-corrosive paint etc.
All multi items, continually developing and applying along with High Performance Corrosion Protective Coatings, anticorrosive paint is carried out research and has
Important scientific value and social value.Although anticorrosive paint quickly grows, but the corrosion resistance of anticorrosive paint
And water resistance is the most to be further improved.
Summary of the invention
The present invention proposes a kind of emulsion-type waterproof anti-corrosion acrylate paint for external wall, and water resistance is excellent,
Corrosion resistance and good, service life is long.
A kind of emulsion-type waterproof anti-corrosion acrylate paint for external wall that the present invention proposes, its raw material is by weight
Including 50-60 part base material, 5-15 part alcohol ester 12 coalescents and 30-40 part adjuvant；
The raw materials by weight of described base material includes: drying oil alkyd resin 5-10 part, acrylic emulsion
50-60 part, Ludox 30-40 part, coupling agent 2-6 part, sodium butylnaphthalenesulfonate 1-4 part, use following work
Prepared by skill: acrylic emulsion and Ludox are placed in reactor, stir, then add at 75-80 DEG C
Enter coupling agent, sodium butylnaphthalenesulfonate and drying oil alkyd resin and be uniformly mixing to obtain base material；
Adjuvant includes by weight: Borax 20-25 part, precipitated calcium carbonate 15-20 part, titanium dioxide 15-20
Part, wollastonite in powder 18-23 part, nano zine oxide 5-10 part, polyvinylpyrrolidone 0.5-1 part, froth breaking
Agent 0.5-1.5 part, sodium carboxymethyl cellulose 0.8-1.3 part, 1,2-benzisothiazole-3-ketone 1-2 part, ammonia
Water 1-1.3 part, water 10-15 part, nylon acid methyl ester 2-5 part；
In preparation process, first base material is put in agitator, under the rotating speed of 400-500r/min successively
Put into alcohol ester 12 coalescents, polyvinylpyrrolidone, sodium carboxymethyl cellulose, 1,2-benzisothiazole
-3-ketone, ammonia and water-dispersible 10-15min, put into Borax, lightweight carbonic acid under 700-750r/min rotating speed
After calcium, titanium dioxide, wollastonite in powder and nano zine oxide, rotating speed raising is disperseed to 1300-1400r/min,
After pick test fineness is less than 50 microns, under 800-850r/min rotating speed, put into the dispersion of nylon acid methyl ester
After 8-13min, under the rotating speed of 550-600r/min add defoamer dispersion 8-13min obtain emulsion-type prevent
The corrosion-resistant acrylate paint for external wall of water.
Preferably, the weight ratio of base material, alcohol ester 12 coalescents and adjuvant is 55-60:10-15:30-35.
Preferably, the weight ratio of base material, alcohol ester 12 coalescents and adjuvant is 55:15:30.
Preferably, its adjuvant includes by weight: Borax 22-24 part, precipitated calcium carbonate 16-18 part, titanium
White lead 18-20 part, wollastonite in powder 20-22 part, nano zine oxide 8-10 part, polyvinylpyrrolidone 0.6-0.8
Part, defoamer 1-1.4 part, sodium carboxymethyl cellulose 1-1.2 part, 1,2-benzisothiazole-3-ketone 1.5-2
Part, ammonia 1-1.2 part, water 12-14 part, nylon acid methyl ester 2-4 part.
Preferably, sodium carboxymethyl cellulose and 1, the weight ratio of 2-benzisothiazole-3-ketone is 1.2:1.6.
Preferably, in preparation process, first base material is put in agitator, under the rotating speed of 450r/min
Put into alcohol ester 12 coalescents, polyvinylpyrrolidone, sodium carboxymethyl cellulose, 1,2-benzisoxa successively
Thiazole-3-ketone, ammonia and water-dispersible 12min, under 720r/min rotating speed put into Borax, precipitated calcium carbonate,
Being improved by rotating speed after titanium dioxide, wollastonite in powder and nano zine oxide and disperse to 1350r/min, sampling is examined
Test fineness less than after 50 microns, after putting into nylon acid methyl ester dispersion 12min under 820r/min rotating speed,
Add defoamer dispersion 12min under the rotating speed of 580r/min and obtain emulsion-type waterproof anti-corrosion acrylate exterior wall
Coating.
In the present invention, acrylic emulsion can overcome respective not enough generation to superpose effect with the compound action of Ludox
Should, add appropriate coupling agent and emulsifying agent can improve both interface performance, make acrylic emulsion and Ludox
Crosslinking compound phase interaction, to form close hydrophobic coating, can make complex emulsions stability more excellent, produces
Product, while isolation rainwater, can be obviously enhanced the anti-cracking performance of exterior wall base material, make base material from acid rain
Corroding, Acid Rain corrosive nature is good, with Borax, precipitated calcium carbonate, titanium dioxide, wollastonite in powder and nano oxygen
Changing zinc jointly to act on, the compactness extent of coating strengthens, and light covers efficiency height, and coupling agent has bridge formation
Effect, can be closely joined together inorganic matter with Organic substance, make product particle more tend to complete, and add
Enter appropriate 1,2-benzisothiazole-3-ketone preservative, the waterproof and Corrosion Protection of product further enhances, and
Paint film can keep primary colors not fade for a long time, the strongest to base material adhesive force, selects alcohol ester 12 coalescents
Film-formation result is good, and paint film is closely knit, even if being dried the paint film that also can reach good under disadvantageous temperature and humidity
Performance；This product waterproof property is excellent, and corrosion resistance is strong, and service life is long.
Detailed description of the invention
Embodiment 1
In the present embodiment, a kind of emulsion-type waterproof anti-corrosion acrylate paint for external wall, its raw material is by weight
Including 50 parts of base materials, 15 parts of alcohol ester 12 coalescents and 30 parts of adjuvants；
The raw materials by weight of described base material includes: drying oil alkyd resin 10 parts, acrylic emulsion 50
Part, Ludox 40 parts, coupling agent 2 parts, sodium butylnaphthalenesulfonate 4 parts, use following technique to prepare: by third
Olefin(e) acid emulsion and Ludox are placed in reactor, stir, be subsequently adding coupling agent, butyl at 75 DEG C
Sodium naphthalene sulfonate and drying oil alkyd resin are uniformly mixing to obtain base material；
Adjuvant includes by weight: Borax 25 parts, precipitated calcium carbonate 15 parts, titanium dioxide 20 parts, wollastonite
18 parts of powder, nano zine oxide 10 parts, polyvinylpyrrolidone 0.5 part, defoamer 1.5 parts, carboxymethyl
Sodium cellulosate 0.8 part, 1,2-benzisothiazole-3-ketone 2 parts, ammonia 1 part, 15 parts of water, nylon acid first
Ester 2 parts；
In preparation process, first base material is put in agitator, put into successively under the rotating speed of 500r/min
Alcohol ester 12 coalescents, polyvinylpyrrolidone, sodium carboxymethyl cellulose, 1,2-benzisothiazole-3-ketone,
Ammonia and water-dispersible 10min, put into Borax, precipitated calcium carbonate, titanium dioxide, silicon under 750r/min rotating speed
Being improved by rotating speed after limestone flour and nano zine oxide and disperse to 1300r/min, pick test fineness is less than
After 50 microns, after putting into nylon acid methyl ester dispersion 8min under 850r/min rotating speed, turning at 600r/min
The lower defoamer dispersion 8-13min that adds of speed obtains emulsion-type waterproof anti-corrosion acrylate paint for external wall.
Embodiment 2
In the present embodiment, a kind of emulsion-type waterproof anti-corrosion acrylate paint for external wall, its raw material is by weight
Including 55 parts of base materials, 10 parts of alcohol ester 12 coalescents and 35 parts of adjuvants；
The raw materials by weight of described base material includes: drying oil alkyd resin 9 parts, acrylic emulsion 53
Part, Ludox 38 parts, coupling agent 4 parts, sodium butylnaphthalenesulfonate 3 parts, use following technique to prepare: by third
Olefin(e) acid emulsion and Ludox are placed in reactor, stir, be subsequently adding coupling agent, butyl at 77 DEG C
Sodium naphthalene sulfonate and drying oil alkyd resin are uniformly mixing to obtain base material；
Adjuvant includes by weight: Borax 24 parts, precipitated calcium carbonate 17 parts, titanium dioxide 18 parts, wollastonite
20 parts of powder, nano zine oxide 8 parts, polyvinylpyrrolidone 0.6 part, defoamer 1.3 parts, carboxymethyl is fine
Dimension 1.2 parts of sodium of element, 1,2-benzisothiazole-3-ketone 1.7 parts, ammonia 1.1 parts, 14 parts of water, nylon acid
Methyl ester 3 parts；
In preparation process, first base material is put in agitator, put into successively under the rotating speed of 450r/min
Alcohol ester 12 coalescents, polyvinylpyrrolidone, sodium carboxymethyl cellulose, 1,2-benzisothiazole-3-ketone,
Ammonia and water-dispersible 12min, put into Borax, precipitated calcium carbonate, titanium dioxide, silicon under 720r/min rotating speed
Being improved by rotating speed after limestone flour and nano zine oxide and disperse to 1350r/min, pick test fineness is less than
After 50 microns, after putting into nylon acid methyl ester dispersion 12min under 820r/min rotating speed, 580r/min's
Add defoamer dispersion 12min under rotating speed and obtain emulsion-type waterproof anti-corrosion acrylate paint for external wall.
Embodiment 3
In the present embodiment, a kind of emulsion-type waterproof anti-corrosion acrylate paint for external wall, its raw material is by weight
Including 60 parts of base materials, 5 parts of alcohol ester 12 coalescents and 40 parts of adjuvants；
The raw materials by weight of described base material includes: drying oil alkyd resin 5 parts, acrylic emulsion 60
Part, Ludox 30 parts, coupling agent 6 parts, sodium butylnaphthalenesulfonate 1 part, use following technique to prepare: by third
Olefin(e) acid emulsion and Ludox are placed in reactor, stir, be subsequently adding coupling agent, butyl at 80 DEG C
Sodium naphthalene sulfonate and drying oil alkyd resin are uniformly mixing to obtain base material；
Adjuvant includes by weight: Borax 22 parts, precipitated calcium carbonate 18 parts, titanium dioxide 19 parts, wollastonite
20 parts of powder, nano zine oxide 9 parts, polyvinylpyrrolidone 0.8 part, defoamer 1 part, carboxymethyl cellulose
1.2 parts of sodium of element, 1,2-benzisothiazole-3-ketone 1.6 parts, ammonia 1.1 parts, 14 parts of water, nylon acid first
Ester 3 parts；
In preparation process, first base material is put in agitator, put into successively under the rotating speed of 400r/min
Alcohol ester 12 coalescents, polyvinylpyrrolidone, sodium carboxymethyl cellulose, 1,2-benzisothiazole-3-ketone,
Ammonia and water-dispersible 15min, put into Borax, precipitated calcium carbonate, titanium dioxide, silicon under 700r/min rotating speed
Being improved by rotating speed after limestone flour and nano zine oxide and disperse to 1400r/min, pick test fineness is less than
After 50 microns, after putting into nylon acid methyl ester dispersion 13min under 800r/min rotating speed, 550r/min's
Add defoamer dispersion 13min under rotating speed and obtain emulsion-type waterproof anti-corrosion acrylate paint for external wall.
Embodiment 4
In the present embodiment, a kind of emulsion-type waterproof anti-corrosion acrylate paint for external wall, its raw material is by weight
Including 55 parts of base materials, 15 parts of alcohol ester 12 coalescents and 30 parts of adjuvants；
The raw materials by weight of described base material includes: drying oil alkyd resin 7 parts, acrylic emulsion 57
Part, Ludox 33 parts, coupling agent 5 parts, sodium butylnaphthalenesulfonate 2 parts, use following technique to prepare: by third
Olefin(e) acid emulsion and Ludox are placed in reactor, stir, be subsequently adding coupling agent, butyl at 78 DEG C
Sodium naphthalene sulfonate and drying oil alkyd resin are uniformly mixing to obtain base material；
Adjuvant includes by weight: Borax 24 parts, precipitated calcium carbonate 16 parts, titanium dioxide 18 parts, wollastonite
22 parts of powder, nano zine oxide 8 parts, polyvinylpyrrolidone 0.6 part, defoamer 1.4 parts, carboxymethyl is fine
Dimension 1 part of sodium of element, 1,2-benzisothiazole-3-ketone 1.5 parts, ammonia 1.2 parts, 12 parts of water, nylon acid first
Ester 4 parts；
In preparation process, first base material is put in agitator, put into successively under the rotating speed of 470r/min
Alcohol ester 12 coalescents, polyvinylpyrrolidone, sodium carboxymethyl cellulose, 1,2-benzisothiazole-3-ketone,
Ammonia and water-dispersible 12min, put into Borax, precipitated calcium carbonate, titanium dioxide, silicon under 740r/min rotating speed
Being improved by rotating speed after limestone flour and nano zine oxide and disperse to 1380r/min, pick test fineness is less than
After 50 microns, after putting into nylon acid methyl ester dispersion 12min under 840r/min rotating speed, 590r/min's
Add defoamer dispersion 12min under rotating speed and obtain emulsion-type waterproof anti-corrosion acrylate paint for external wall.
The acrylate paint for external wall of emulsion-type waterproof anti-corrosion described in embodiment 1-4 is carried out performance test,
Test result is as follows:
| Performance test | Testing standard | Test result |
| Resistance to water | 168h is without exception | 168h is without exception |
| Corrosion resistance (20% aqueous sulfuric acid soaks) | 10 days without exception | 10 days without exception |
| Resistance to coating temperature degeneration can (circulate for 10 times) | Without exception | Without exception |
The above, the only present invention preferably detailed description of the invention, but protection scope of the present invention not office
Being limited to this, any those familiar with the art is in the technical scope that the invention discloses, according to this
The technical scheme of invention and inventive concept thereof in addition equivalent or change, all should contain the protection in the present invention
Within the scope of.
Claims (6)
1. an emulsion-type waterproof anti-corrosion acrylate paint for external wall, it is characterised in that its raw material includes 50-60 part base material, 5-15 part alcohol ester 12 coalescents and 30-40 part adjuvant by weight；
The raw material of described base material includes by weight: drying oil alkyd resin 5-10 part, acrylic emulsion 50-60 part, Ludox 30-40 part, coupling agent 2-6 part, sodium butylnaphthalenesulfonate 1-4 part, following technique is used to prepare: acrylic emulsion and Ludox to be placed in reactor, stir at 75-80 DEG C, be subsequently adding coupling agent, sodium butylnaphthalenesulfonate and drying oil alkyd resin and be uniformly mixing to obtain base material；
Adjuvant includes by weight: Borax 20-25 part, precipitated calcium carbonate 15-20 part, titanium dioxide 15-20 part, wollastonite in powder 18-23 part, nano zine oxide 5-10 part, polyvinylpyrrolidone 0.5-1 part, defoamer 0.5-1.5 part, sodium carboxymethyl cellulose 0.8-1.3 part, 1,2-benzisothiazole-3-ketone 1-2 part, ammonia 1-1.3 part, water 10-15 part, nylon acid methyl ester 2-5 part；
nullIn preparation process，First base material is put in agitator，Alcohol ester 12 coalescents is put into successively under the rotating speed of 400-500r/min、Polyvinylpyrrolidone、Sodium carboxymethyl cellulose、1,2-benzisothiazole-3-ketone、Ammonia and water-dispersible 10-15min，Borax is put under 700-750r/min rotating speed、Precipitated calcium carbonate、Titanium dioxide、After wollastonite in powder and nano zine oxide, rotating speed raising is disperseed to 1300-1400r/min，After pick test fineness is less than 50 microns，After putting into nylon acid methyl ester dispersion 8-13min under 800-850r/min rotating speed，Under the rotating speed of 550-600r/min, add defoamer dispersion 8-13min obtain emulsion-type waterproof anti-corrosion acrylate paint for external wall.
Emulsion-type waterproof anti-corrosion acrylate paint for external wall the most according to claim 1, it is characterised in that the weight ratio of base material, alcohol ester 12 coalescents and adjuvant is 55-60:10-15:30-35.
Emulsion-type waterproof anti-corrosion acrylate paint for external wall the most according to claim 1 and 2, it is characterised in that the weight ratio of base material, alcohol ester 12 coalescents and adjuvant is 55:15:30.
Emulsion-type waterproof anti-corrosion acrylate paint for external wall the most according to claim 1 and 2, it is characterised in that its adjuvant includes by weight: Borax 22-24 part, precipitated calcium carbonate 16-18 part, titanium dioxide 18-20 part, wollastonite in powder 20-22 part, nano zine oxide 8-10 part, polyvinylpyrrolidone 0.6-0.8 part, defoamer 1-1.4 part, sodium carboxymethyl cellulose 1-1.2 part, 1,2-benzisothiazole-3-ketone 1.5-2 part, ammonia 1-1.2 part, water 12-14 part, nylon acid methyl ester 2-4 part.
Emulsion-type waterproof anti-corrosion acrylate paint for external wall the most according to claim 1 and 2, it is characterised in that sodium carboxymethyl cellulose and 1, the weight ratio of 2-benzisothiazole-3-ketone is 1.2:1.6.
nullEmulsion-type waterproof anti-corrosion acrylate paint for external wall the most according to claim 1 and 2，It is characterized in that，In preparation process，First base material is put in agitator，Alcohol ester 12 coalescents is put into successively under the rotating speed of 450r/min、Polyvinylpyrrolidone、Sodium carboxymethyl cellulose、1,2-benzisothiazole-3-ketone、Ammonia and water-dispersible 12min，Borax is put under 720r/min rotating speed、Precipitated calcium carbonate、Titanium dioxide、After wollastonite in powder and nano zine oxide, rotating speed raising is disperseed to 1350r/min，After pick test fineness is less than 50 microns，After putting into nylon acid methyl ester dispersion 12min under 820r/min rotating speed，Under the rotating speed of 580r/min, add defoamer dispersion 12min obtain emulsion-type waterproof anti-corrosion acrylate paint for external wall.
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Cited By (1)
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| CB03 | Change of inventor or designer information | ||
| CB03 | Change of inventor or designer information |
Inventor after: Wang Lin Inventor before: Hu Changti |
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| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20171213 Address after: 410100 Hunan province Changsha County Xiang Long Street No. 6 at the He Long School of cloud Valley Di 6, 7, 3205 Patentee after: Hunan love new material Co. Ltd. Address before: Wuhu County Industrial Park, 241100 Anhui Huaqiao city in Wuhu Province Patentee before: WUHU SHUANGBAO BUILDING MATERIAL CO., LTD. |