CN104069191A - 一种水辣蓼总黄酮的提取工艺 - Google Patents
一种水辣蓼总黄酮的提取工艺 Download PDFInfo
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- CN104069191A CN104069191A CN201410303473.9A CN201410303473A CN104069191A CN 104069191 A CN104069191 A CN 104069191A CN 201410303473 A CN201410303473 A CN 201410303473A CN 104069191 A CN104069191 A CN 104069191A
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- Prior art keywords
- herba polygoni
- polygoni hydropiperis
- water
- water herba
- total flavones
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- 235000017173 flavonoids Nutrition 0.000 title abstract 5
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- 229910000278 bentonite Inorganic materials 0.000 claims abstract description 23
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims abstract description 23
- 239000000725 suspension Substances 0.000 claims abstract description 21
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- 238000000034 method Methods 0.000 claims abstract description 10
- 235000019834 papain Nutrition 0.000 claims abstract description 9
- 238000005189 flocculation Methods 0.000 claims abstract description 7
- 108090000526 Papain Proteins 0.000 claims abstract description 5
- 239000004365 Protease Substances 0.000 claims abstract description 5
- 230000016615 flocculation Effects 0.000 claims abstract description 5
- 229940055729 papain Drugs 0.000 claims abstract description 5
- 229930003944 flavone Natural products 0.000 claims description 35
- 235000011949 flavones Nutrition 0.000 claims description 35
- 150000002213 flavones Chemical class 0.000 claims description 28
- 239000000203 mixture Substances 0.000 claims description 22
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- 239000006228 supernatant Substances 0.000 claims description 10
- 108010059892 Cellulase Proteins 0.000 claims description 8
- 229940106157 cellulase Drugs 0.000 claims description 8
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- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 description 7
- 150000002212 flavone derivatives Chemical class 0.000 description 6
- 230000014759 maintenance of location Effects 0.000 description 6
- 238000010521 absorption reaction Methods 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- 230000004071 biological effect Effects 0.000 description 3
- 235000010987 pectin Nutrition 0.000 description 3
- 229920001277 pectin Polymers 0.000 description 3
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- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 208000001848 dysentery Diseases 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- -1 flavone compound Chemical class 0.000 description 1
- 229930182478 glucoside Natural products 0.000 description 1
- 150000008131 glucosides Chemical class 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 230000007803 itching Effects 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
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- 231100000614 poison Toxicity 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
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- 238000007560 sedimentation technique Methods 0.000 description 1
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- 239000001648 tannin Substances 0.000 description 1
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- 150000003648 triterpenes Chemical class 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
Landscapes
- Cosmetics (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Medicines That Contain Protein Lipid Enzymes And Other Medicines (AREA)
Abstract
Description
Claims (6)
Priority Applications (1)
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CN201410303473.9A CN104069191B (zh) | 2014-06-30 | 2014-06-30 | 一种水辣蓼总黄酮的提取工艺 |
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CN201410303473.9A CN104069191B (zh) | 2014-06-30 | 2014-06-30 | 一种水辣蓼总黄酮的提取工艺 |
Publications (2)
Publication Number | Publication Date |
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CN104069191A true CN104069191A (zh) | 2014-10-01 |
CN104069191B CN104069191B (zh) | 2016-08-17 |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105055540A (zh) * | 2015-09-10 | 2015-11-18 | 广西大学 | 大孔吸附树脂分离纯化辣蓼黄酮的工艺 |
CN105106327A (zh) * | 2015-09-10 | 2015-12-02 | 广西大学 | 酶解-超声偶联法提取辣蓼总黄酮的工艺 |
CN107569541A (zh) * | 2017-08-28 | 2018-01-12 | 付林春 | 一种水辣蓼总黄酮提取物的制备工艺 |
CN115192637A (zh) * | 2022-08-10 | 2022-10-18 | 特一药业集团股份有限公司 | 一种枫蓼肠胃康片及其制备工艺 |
-
2014
- 2014-06-30 CN CN201410303473.9A patent/CN104069191B/zh active Active
Non-Patent Citations (2)
Title |
---|
蔡玲等: "微波法提取水蓼中总黄酮的工艺研究", 《广州化学》, vol. 32, no. 4, 31 December 2007 (2007-12-31), pages 25 - 29 * |
郑友兰、张崇禧主编: "《中药化学》", 30 April 2008, article "黄酮的提取与纯化", pages: 221-222 * |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105055540A (zh) * | 2015-09-10 | 2015-11-18 | 广西大学 | 大孔吸附树脂分离纯化辣蓼黄酮的工艺 |
CN105106327A (zh) * | 2015-09-10 | 2015-12-02 | 广西大学 | 酶解-超声偶联法提取辣蓼总黄酮的工艺 |
CN105106327B (zh) * | 2015-09-10 | 2018-12-28 | 广西大学 | 酶解-超声偶联法提取辣蓼总黄酮的工艺 |
CN105055540B (zh) * | 2015-09-10 | 2019-01-25 | 广西大学 | 大孔吸附树脂分离纯化辣蓼黄酮的工艺 |
CN107569541A (zh) * | 2017-08-28 | 2018-01-12 | 付林春 | 一种水辣蓼总黄酮提取物的制备工艺 |
CN115192637A (zh) * | 2022-08-10 | 2022-10-18 | 特一药业集团股份有限公司 | 一种枫蓼肠胃康片及其制备工艺 |
WO2024031830A1 (zh) * | 2022-08-10 | 2024-02-15 | 特一药业集团股份有限公司 | 一种枫蓼肠胃康片及其制备工艺 |
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Publication number | Publication date |
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CN104069191B (zh) | 2016-08-17 |
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Address after: 528458 Guangdong province Zhongshan city mayor Shan five life water Road No. 9-13 Patentee after: GUANGDONG PHARMACEUTICAL University Address before: 528458 Guangdong province Zhongshan city mayor Shan five life water Road No. 9-13 Patentee before: Guangdong Pharmaceutical University |
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Effective date of registration: 20170522 Address after: 528400 Guangdong city of Zhongshan Province East Torch Development Zone, Road No. 9 (golden arrow District) the first floor of building R 10-12 card Patentee after: GUANGDONG BRUNDO BIO-TECHNOLOGY CO.,LTD. Address before: 528458 Guangdong province Zhongshan city mayor Shan five life water Road No. 9-13 Patentee before: Guangdong Pharmaceutical University |
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Address after: 528400 No. 11 science and Technology West Road, Torch Development Zone, Zhongshan, Guangdong Patentee after: GUANGDONG BRUNDO BIO-TECHNOLOGY CO.,LTD. Address before: 528400 Guangdong Zhongshan Torch Development Zone No. 9 Donghe Road (Jinjian District) R building 10-12 cards on the first floor. Patentee before: GUANGDONG BRUNDO BIO-TECHNOLOGY CO.,LTD. |
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Denomination of invention: Extraction Process of Total Flavonoids from Water Spicy Polygonum Effective date of registration: 20230609 Granted publication date: 20160817 Pledgee: Bank of Guangzhou Co.,Ltd. Zhongshan branch Pledgor: GUANGDONG BRUNDO BIO-TECHNOLOGY CO.,LTD. Registration number: Y2023980043423 |