CN103937366A - Anti-fouling and dustproof automobile coating and preparation method thereof - Google Patents
Anti-fouling and dustproof automobile coating and preparation method thereof Download PDFInfo
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- CN103937366A CN103937366A CN201410107202.6A CN201410107202A CN103937366A CN 103937366 A CN103937366 A CN 103937366A CN 201410107202 A CN201410107202 A CN 201410107202A CN 103937366 A CN103937366 A CN 103937366A
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- 238000002360 preparation method Methods 0.000 title claims description 7
- 238000000576 coating method Methods 0.000 title abstract description 18
- 239000011248 coating agent Substances 0.000 title abstract description 17
- 230000003373 anti-fouling effect Effects 0.000 title abstract 3
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims abstract description 39
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims abstract description 14
- ZNOKGRXACCSDPY-UHFFFAOYSA-N tungsten(VI) oxide Inorganic materials O=[W](=O)=O ZNOKGRXACCSDPY-UHFFFAOYSA-N 0.000 claims abstract description 13
- -1 polytetrafluoroethylene Polymers 0.000 claims abstract description 12
- 239000003973 paint Substances 0.000 claims abstract description 11
- 239000004793 Polystyrene Substances 0.000 claims abstract description 9
- 239000004005 microsphere Substances 0.000 claims abstract description 9
- 229920002223 polystyrene Polymers 0.000 claims abstract description 9
- CXMXRPHRNRROMY-UHFFFAOYSA-N sebacic acid Chemical compound OC(=O)CCCCCCCCC(O)=O CXMXRPHRNRROMY-UHFFFAOYSA-N 0.000 claims abstract description 8
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229920002125 Sokalan® Polymers 0.000 claims abstract description 7
- 229960001631 carbomer Drugs 0.000 claims abstract description 7
- RGPUVZXXZFNFBF-UHFFFAOYSA-K diphosphonooxyalumanyl dihydrogen phosphate Chemical compound [Al+3].OP(O)([O-])=O.OP(O)([O-])=O.OP(O)([O-])=O RGPUVZXXZFNFBF-UHFFFAOYSA-K 0.000 claims abstract description 7
- 239000003822 epoxy resin Substances 0.000 claims abstract description 7
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 claims abstract description 7
- 229920000647 polyepoxide Polymers 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 238000003756 stirring Methods 0.000 claims description 21
- 239000003595 mist Substances 0.000 claims description 7
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims description 6
- 239000004743 Polypropylene Substances 0.000 claims description 6
- 239000012752 auxiliary agent Substances 0.000 claims description 6
- CQEYYJKEWSMYFG-UHFFFAOYSA-N butyl acrylate Chemical compound CCCCOC(=O)C=C CQEYYJKEWSMYFG-UHFFFAOYSA-N 0.000 claims description 6
- 235000013399 edible fruits Nutrition 0.000 claims description 6
- 239000012467 final product Substances 0.000 claims description 6
- 229920001155 polypropylene Polymers 0.000 claims description 6
- 235000019832 sodium triphosphate Nutrition 0.000 claims description 6
- 229920002803 thermoplastic polyurethane Polymers 0.000 claims description 6
- XMNIXWIUMCBBBL-UHFFFAOYSA-N 2-(2-phenylpropan-2-ylperoxy)propan-2-ylbenzene Chemical compound C=1C=CC=CC=1C(C)(C)OOC(C)(C)C1=CC=CC=C1 XMNIXWIUMCBBBL-UHFFFAOYSA-N 0.000 claims description 3
- DXPPIEDUBFUSEZ-UHFFFAOYSA-N 6-methylheptyl prop-2-enoate Chemical group CC(C)CCCCCOC(=O)C=C DXPPIEDUBFUSEZ-UHFFFAOYSA-N 0.000 claims description 3
- ZTHYODDOHIVTJV-UHFFFAOYSA-N Propyl gallate Chemical compound CCCOC(=O)C1=CC(O)=C(O)C(O)=C1 ZTHYODDOHIVTJV-UHFFFAOYSA-N 0.000 claims description 3
- 101710194948 Protein phosphatase PhpP Proteins 0.000 claims description 3
- 239000006087 Silane Coupling Agent Substances 0.000 claims description 3
- 239000002253 acid Substances 0.000 claims description 3
- HTKFORQRBXIQHD-UHFFFAOYSA-N allylthiourea Chemical compound NC(=S)NCC=C HTKFORQRBXIQHD-UHFFFAOYSA-N 0.000 claims description 3
- WMGSQTMJHBYJMQ-UHFFFAOYSA-N aluminum;magnesium;silicate Chemical compound [Mg+2].[Al+3].[O-][Si]([O-])([O-])[O-] WMGSQTMJHBYJMQ-UHFFFAOYSA-N 0.000 claims description 3
- 238000006243 chemical reaction Methods 0.000 claims description 3
- XXMIOPMDWAUFGU-UHFFFAOYSA-N hexane-1,6-diol Chemical compound OCCCCCCO XXMIOPMDWAUFGU-UHFFFAOYSA-N 0.000 claims description 3
- ZCTXEAQXZGPWFG-UHFFFAOYSA-N imidurea Chemical compound O=C1NC(=O)N(CO)C1NC(=O)NCNC(=O)NC1C(=O)NC(=O)N1CO ZCTXEAQXZGPWFG-UHFFFAOYSA-N 0.000 claims description 3
- 229940113174 imidurea Drugs 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 3
- HWGNBUXHKFFFIH-UHFFFAOYSA-I pentasodium;[oxido(phosphonatooxy)phosphoryl] phosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O HWGNBUXHKFFFIH-UHFFFAOYSA-I 0.000 claims description 3
- 239000002002 slurry Substances 0.000 claims description 3
- 229910052708 sodium Inorganic materials 0.000 claims description 3
- 239000011734 sodium Substances 0.000 claims description 3
- UNXRWKVEANCORM-UHFFFAOYSA-I triphosphate(5-) Chemical compound [O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O UNXRWKVEANCORM-UHFFFAOYSA-I 0.000 claims description 3
- 238000001132 ultrasonic dispersion Methods 0.000 claims description 3
- 230000000694 effects Effects 0.000 abstract description 3
- 229920001343 polytetrafluoroethylene Polymers 0.000 abstract 2
- 239000004810 polytetrafluoroethylene Substances 0.000 abstract 2
- 239000004640 Melamine resin Substances 0.000 abstract 1
- 229920000877 Melamine resin Polymers 0.000 abstract 1
- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 abstract 1
- SNAAJJQQZSMGQD-UHFFFAOYSA-N aluminum magnesium Chemical compound [Mg].[Al] SNAAJJQQZSMGQD-UHFFFAOYSA-N 0.000 abstract 1
- SOROIESOUPGGFO-UHFFFAOYSA-N diazolidinylurea Chemical compound OCNC(=O)N(CO)C1N(CO)C(=O)N(CO)C1=O SOROIESOUPGGFO-UHFFFAOYSA-N 0.000 abstract 1
- 229960001083 diazolidinylurea Drugs 0.000 abstract 1
- 238000009413 insulation Methods 0.000 abstract 1
- 239000011976 maleic acid Substances 0.000 abstract 1
- 150000007974 melamines Chemical class 0.000 abstract 1
- 229920001225 polyester resin Polymers 0.000 abstract 1
- 239000004645 polyester resin Substances 0.000 abstract 1
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 abstract 1
- 230000032683 aging Effects 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000004568 cement Substances 0.000 description 1
- 230000004087 circulation Effects 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000003628 erosive effect Effects 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 230000000750 progressive effect Effects 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Landscapes
- Paints Or Removers (AREA)
Abstract
The invention relates to an anti-fouling and dustproof automobile coating, which is prepared from the following raw materials by weight part: 26-30 of methylated melamine resin, 25-30 of epoxy resin, 3-5 of maleic acid, 4-6 of polyester resin, 3-4 of polytetrafluoroethylene micropowder, 5-8 of sebacic acid, 2-3 of magnesium aluminum silicate, 1-2 of Carbomer, 2-3 of aluminum dihydrogen phosphate, 3-4 of crosslinked polystyrene microspheres, 5-7 of ethyl acetate, 1-2 of diazolidinyl urea, 8-12 of acetone, 0.01-0.02 of nano-tungsten trioxide, and 4-6 of an adhesion assistant. The coating provided by the invention has very good hardness, flexibility and outdoor weatherability. By adding the polytetrafluoroethylene micropowder, the coating can have anti-fouling and dustproof effects, and by adding the crosslinked polystyrene microspheres, the coating has good thermal insulation properties, and the cost is reduced. The coating is suitable for coil coatings and automobile paint.
Description
Technical field
The invention belongs to paint field, relate in particular to a kind of dirt-resisting dustproof car paint and preparation method thereof.
Background technology
The use field of coating is a lot of now, owing to being often exposed among atmosphere, be subject to the erosion of oxygen, moisture etc., easily cause the phenomenons such as corrosion of metal, foxy, cement weathering, along with the raising of people's living standard, requirement to coating each side all increases, especially the requirement of the aspects such as performance such as the hardness to coating, wear resistance, fullness ratio, shock-resistance, ageing resistance, anticorrosion, waterproof, grease proofing, chemicals-resistant, fast light, heatproof is more and more higher, therefore needs the more progressive coating of research to meet people's needs.
Summary of the invention
The object of the present invention is to provide a kind of dirt-resisting dustproof car paint and preparation method thereof, this coating has and has fabulous hardness, snappiness, outdoor weatherability, dirt-resisting dustproof effect, also has good heat-insulating property.
Technical scheme of the present invention is as follows:
A kind of dirt-resisting dustproof car paint, is characterized in that being made up of the raw material of following weight part: methyl-etherified melmac 26-30, epoxy resin 25-30, toxilic acid 3-5, vibrin 4-6, polytetrafluoroethyl-ne micro mist 3-4, sebacic acid 5-8, neusilin 2-3, carbomer 1-2, aluminium dihydrogen phosphate 2-3, crosslinked polystyrene microsphere 3-4, ethyl acetate 5-7, two Imidurea 1-2, acetone 8-12, nano tungsten trioxide 0.01-0.02, adhere to auxiliary agent 4-6;
The described auxiliary agent that adheres to is made up of the raw material of following weight part: thiosinamine 0.2-0.3, Silane coupling agent KH550 0.4-0.6, butyl acrylate 3-5,1,6 hexanediol diacrylate 4-7, urethane resin 6-8, chlorinated polypropylene 7-9, Tenox PG 2-3, tripoly phosphate sodium STPP 2-3, dicumyl peroxide 0.1-0.2, Isooctyl acrylate monomer 5-7, ethyl acetate 10-15, propyl carbinol 10-15, oleum lini 1-2, wet nurse fruit oily 1-2, succsinic acid 0.2-0.3; Making method is: ethyl acetate, propyl carbinol, oleum lini, wet nurse fruit oil are mixed, under 3000-4000 rev/min, add urethane resin, chlorinated polypropylene, after dissolving, add again butyl acrylate, 1,6-hexanediyl ester, stir 20-30 minute, add other remaining components, be heated to 80-90 DEG C, stirring reaction 30-50 minute, to obtain final product.
The preparation method of described dirt-resisting dustproof car paint, is characterized in that comprising the following steps:
(1) prepare A component: in encloses container, ethyl acetate, acetone are mixed, under 6000-7000 rev/min of stirring, add nano tungsten trioxide, stir 10-15 minute, add again methyl-etherified melmac, epoxy resin, vibrin, stir 1-2 hour, ultrasonic dispersion 7-10 minute, makes A component;
(2) prepare B component: toxilic acid, carbomer, aluminium dihydrogen phosphate are mixed, under 8000-10000 rev/min, add crosslinked polystyrene microsphere, polytetrafluoroethyl-ne micro mist, stir 20-30 minute, disperse and be ground to fineness≤50 μ m, make B component;
(3) other remaining components are mixed, add A component and B component, stir and grind to form slurry and get final product.
Beneficial effect of the present invention
Coating of the present invention has and has fabulous hardness, snappiness and outdoor weatherability, by adding polytetrafluoroethyl-ne micro mist, make coating there is dirt-resisting dustproof effect, by adding crosslinked polystyrene microsphere, make coating there is good heat-insulating property, reduce cost, be applicable to coil steel coating and automobile finish.
Embodiment
A kind of dirt-resisting dustproof car paint, by following weight part (kilogram) raw material make: methyl-etherified melmac 28, epoxy resin 28, toxilic acid 4, vibrin 5, polytetrafluoroethyl-ne micro mist 3.5, sebacic acid 6, neusilin 2.5, carbomer 1.5, aluminium dihydrogen phosphate 2.5, crosslinked polystyrene microsphere 3.5, ethyl acetate 6, two Imidurea 1.5, acetone 10, nano tungsten trioxide 0.01, adhere to auxiliary agent 5;
Described adhere to auxiliary agent by following weight part (kilogram) raw material make: thiosinamine 0.2, Silane coupling agent KH550 0.5, butyl acrylate 4,1,6 hexanediol diacrylate 5, urethane resin 7, chlorinated polypropylene 8, Tenox PG 2.5, tripoly phosphate sodium STPP 2.5, dicumyl peroxide 0.1, Isooctyl acrylate monomer 6, ethyl acetate 13, propyl carbinol 13, oleum lini 1.5, wet nurse fruit oil 1.5, succsinic acid 0.2; Making method is: ethyl acetate, propyl carbinol, oleum lini, wet nurse fruit oil are mixed, under 3500 revs/min, add urethane resin, chlorinated polypropylene, after dissolving, add again butyl acrylate, 1,6-hexanediyl ester, stir 25 minutes, add other remaining components, be heated to 85 DEG C, stirring reaction 40 minutes, to obtain final product.
The preparation method of described dirt-resisting dustproof car paint, comprises the following steps:
(1) prepare A component: in encloses container, ethyl acetate, acetone are mixed, under 6500 revs/min of stirrings, add nano tungsten trioxide, stir 13 minutes, then add methyl-etherified melmac, epoxy resin, vibrin, stir 1.5 hours, ultrasonic dispersion 8 minutes, makes A component;
(2) prepare B component: toxilic acid, carbomer, aluminium dihydrogen phosphate are mixed, add crosslinked polystyrene microsphere, polytetrafluoroethyl-ne micro mist under 9000 revs/min, stir 25 minutes, disperseing and being ground to fineness is 50 μ m, makes B component;
(3) other remaining components are mixed, add A component and B component, stir and grind to form slurry and get final product.
This coating artificial ageing resistance 3000 hours, coating thicknesses of layers under the prerequisite that keeps low-luster and high-wearing feature reaches more than 30 microns, and sticking power is 1 grade, resistance to impact shock >=50kgcm, snappiness is 2mm.Contamination resistance (5 circulations)≤10%.
Claims (2)
1. a dirt-resisting dustproof car paint, is characterized in that being made up of the raw material of following weight part: methyl-etherified melmac 26-30, epoxy resin 25-30, toxilic acid 3-5, vibrin 4-6, polytetrafluoroethyl-ne micro mist 3-4, sebacic acid 5-8, neusilin 2-3, carbomer 1-2, aluminium dihydrogen phosphate 2-3, crosslinked polystyrene microsphere 3-4, ethyl acetate 5-7, two Imidurea 1-2, acetone 8-12, nano tungsten trioxide 0.01-0.02, adhere to auxiliary agent 4-6;
The described auxiliary agent that adheres to is made up of the raw material of following weight part: thiosinamine 0.2-0.3, Silane coupling agent KH550 0.4-0.6, butyl acrylate 3-5,1,6 hexanediol diacrylate 4-7, urethane resin 6-8, chlorinated polypropylene 7-9, Tenox PG 2-3, tripoly phosphate sodium STPP 2-3, dicumyl peroxide 0.1-0.2, Isooctyl acrylate monomer 5-7, ethyl acetate 10-15, propyl carbinol 10-15, oleum lini 1-2, wet nurse fruit oily 1-2, succsinic acid 0.2-0.3; Making method is: ethyl acetate, propyl carbinol, oleum lini, wet nurse fruit oil are mixed, under 3000-4000 rev/min, add urethane resin, chlorinated polypropylene, after dissolving, add again butyl acrylate, 1,6-hexanediyl ester, stir 20-30 minute, add other remaining components, be heated to 80-90 DEG C, stirring reaction 30-50 minute, to obtain final product.
2. the preparation method of dirt-resisting dustproof car paint according to claim 1, is characterized in that comprising the following steps:
(1) prepare A component: in encloses container, ethyl acetate, acetone are mixed, under 6000-7000 rev/min of stirring, add nano tungsten trioxide, stir 10-15 minute, add again methyl-etherified melmac, epoxy resin, vibrin, stir 1-2 hour, ultrasonic dispersion 7-10 minute, makes A component;
(2) prepare B component: toxilic acid, carbomer, aluminium dihydrogen phosphate are mixed, under 8000-10000 rev/min, add crosslinked polystyrene microsphere, polytetrafluoroethyl-ne micro mist, stir 20-30 minute, disperse and be ground to fineness≤50 μ m, make B component;
(3) other remaining components are mixed, add A component and B component, stir and grind to form slurry and get final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410107202.6A CN103937366A (en) | 2014-03-21 | 2014-03-21 | Anti-fouling and dustproof automobile coating and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410107202.6A CN103937366A (en) | 2014-03-21 | 2014-03-21 | Anti-fouling and dustproof automobile coating and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103937366A true CN103937366A (en) | 2014-07-23 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410107202.6A Pending CN103937366A (en) | 2014-03-21 | 2014-03-21 | Anti-fouling and dustproof automobile coating and preparation method thereof |
Country Status (1)
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| CN (1) | CN103937366A (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105086719A (en) * | 2015-07-11 | 2015-11-25 | 合肥正浩机械科技有限公司 | Surface treating agent for sliding mechanical parts and preparation method therefor |
| CN105602310A (en) * | 2015-12-29 | 2016-05-25 | 浙江名匠实业股份有限公司 | Novel dustproof coating material for automotive wheel rims and preparation method thereof |
| CN110343442A (en) * | 2019-06-10 | 2019-10-18 | 安徽蓝润自动化仪表有限公司 | A kind of power control cabinet shell potent anti-aging coating and preparation method thereof |
| CN111040609A (en) * | 2019-11-29 | 2020-04-21 | 中国科学院宁波材料技术与工程研究所 | A kind of coating material for car coat film and preparation method thereof |
| CN112029374A (en) * | 2019-06-04 | 2020-12-04 | 佛山市南海区永利兴塑料丝织五金有限公司 | Preparation method of dustproof and anti-fouling fan blade of electric fan |
| CN119931446A (en) * | 2025-02-13 | 2025-05-06 | 怀化学院 | Aqueous coating for aluminum protection and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105086719A (en) * | 2015-07-11 | 2015-11-25 | 合肥正浩机械科技有限公司 | Surface treating agent for sliding mechanical parts and preparation method therefor |
| CN105602310A (en) * | 2015-12-29 | 2016-05-25 | 浙江名匠实业股份有限公司 | Novel dustproof coating material for automotive wheel rims and preparation method thereof |
| CN112029374A (en) * | 2019-06-04 | 2020-12-04 | 佛山市南海区永利兴塑料丝织五金有限公司 | Preparation method of dustproof and anti-fouling fan blade of electric fan |
| CN110343442A (en) * | 2019-06-10 | 2019-10-18 | 安徽蓝润自动化仪表有限公司 | A kind of power control cabinet shell potent anti-aging coating and preparation method thereof |
| CN111040609A (en) * | 2019-11-29 | 2020-04-21 | 中国科学院宁波材料技术与工程研究所 | A kind of coating material for car coat film and preparation method thereof |
| CN119931446A (en) * | 2025-02-13 | 2025-05-06 | 怀化学院 | Aqueous coating for aluminum protection and preparation method thereof |
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Application publication date: 20140723 |
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