CN103933173B - A kind of Chinese medicine super-micro wall-broken fine powder for the treatment of gastropathy - Google Patents

A kind of Chinese medicine super-micro wall-broken fine powder for the treatment of gastropathy Download PDF

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CN103933173B
CN103933173B CN201410167118.3A CN201410167118A CN103933173B CN 103933173 B CN103933173 B CN 103933173B CN 201410167118 A CN201410167118 A CN 201410167118A CN 103933173 B CN103933173 B CN 103933173B
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powder
fine powder
gastropathy
wall
chinese medicine
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CN103933173A (en
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王建荣
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Tianjin Zhongrui Pharmaceutical Co ltd
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HUZHOU KONCH PHARMACEUTICAL Co Ltd
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Abstract

Treat a Chinese medicine super-micro wall-broken fine powder for gastropathy, belong to technical field of Chinese medicines.Comprise the following steps: 1) Feedstock treating; 2) wall breaking pulverization; 3) wet ball grinding is pulverized; 4) decoction filtering; 5) filter vacuum thin film concentration is dry; 6) high temperature sterilize.Above-mentioned a kind of Chinese medicine super-micro wall-broken fine powder for the treatment of gastropathy, adopts the natural food materials with invigorating spleen and reinforcing stomach and medical material is composite makes, and has synergistic function to gastropathy; And adopt super-micro wall-broken to be made into fine powder, reduce the destruction of the course of processing to nutrient substance contained in product and functional component, greatly remain original bioactive ingredients and functional component, its granularity is little, good evenness and dissolution rate high, its dissolving in vivo, infiltration rate can be accelerated, improve its absorbtivity, good to the therapeutic effect of gastropathy.

Description

A kind of Chinese medicine super-micro wall-broken fine powder for the treatment of gastropathy
Technical field
The invention belongs to technical field of Chinese medicines, be specifically related to a kind of Chinese medicine super-micro wall-broken fine powder for the treatment of gastropathy.
Background technology
Gastropathy can very light also can be very heavy, modal have epigastric discomfort or pain, nausea,vomiting,diarrhea, inappetence.The symptom of gastritis and duodenal ulcer is then epigastrium burning pain, and particularly between two meals, early occur before the meal or after drinking orange juice, coffee, severe patient can have tarry stool, melena or hemafecia.Gastropathy is difficult to cure, but often treating one section can recur again, has a strong impact on physical and mental health.The Chinese medicine of existing treatment gastropathy generally adopts high-temperature water boiling standby, and in water cooking liquid, the biological activity of Chinese crude drug is easily destroyed, and dissolution rate is not high, and effective component content is not high, affects therapeutic effect.
Summary of the invention
For prior art Problems existing, the object of the invention is to design provides a kind of technical scheme for the treatment of the Chinese medicine super-micro wall-broken fine powder of gastropathy, it remains that the bioactive ingredients of Chinese crude drug, granularity are little, good evenness and dissolution rate high, its dissolving in vivo, infiltration rate can be accelerated, improve its absorbtivity, good to the therapeutic effect of gastropathy.
Described a kind of Chinese medicine super-micro wall-broken fine powder for the treatment of gastropathy, is characterized in that comprising the following steps:
1) Feedstock treating: percentage composition takes Semen Lablab Album 20-30%, sepiellae seu sepiae ink sac dry powder 15-20%, Semen Ziziphi Spinosae (parched) powder 20-27%, Radix Glycyrrhizae Preparata 9-12%, Rhizoma Atractylodis Macrocephalae 9-12%, Pericarpium Citri Reticulatae 10-15% by weight, for subsequent use; Pulverize after Semen Lablab Album, Radix Glycyrrhizae Preparata, the Rhizoma Atractylodis Macrocephalae, Pericarpium Citri Reticulatae mixing with pulverizer, cross 30-50 mesh sieve, add sepiellae seu sepiae ink sac dry powder, the mixing of Semen Ziziphi Spinosae (parched) powder;
2) wall breaking pulverization: by the mixed powder in step 1), be crushed to 50-100 μm through super micron mill, obtains breaking cellular wall fine powder;
3) wet ball grinding is pulverized: by step 2) fine powder that obtains adds ball mill wet ball grinding and pulverizes, and the weight ratio of fine powder raw material and water is 1:3-5, and drum's speed of rotation is 200-300rpm, through 2-3 hour ball milling breaking cellular wall, obtains ball milling wall cell disruption powder;
4) ball milling wall cell disruption powder in step 3) is added raw material weight 5-6 water soaking 1-2h doubly, then 100 DEG C of big fire decoct 20-30min, then use little fire decoction 10-20min instead, and cold filtration, collects filtrate;
5) by filtrate at 70-80 DEG C, vacuum is 0.09MpaMpa, and feed liquor flow velocity is 200-300mLmin -1condition under carry out vacuum film concentrate drying;
6) high temperature sterilize: dry powder step 5) obtained is short time sterilizing under the high temperature of 80 DEG C-90 DEG C, and fill, in sterilizing bottle, namely obtains finished product.
Described a kind of Chinese medicine super-micro wall-broken fine powder for the treatment of gastropathy, is characterized in that in step 1): Semen Lablab Album 23-27%, sepiellae seu sepiae ink sac dry powder 16-18%, Semen Ziziphi Spinosae (parched) powder 22-25%, Radix Glycyrrhizae Preparata 10-11%, Rhizoma Atractylodis Macrocephalae 10-11%, Pericarpium Citri Reticulatae 12-13%.
Described a kind of Chinese medicine super-micro wall-broken fine powder for the treatment of gastropathy, is characterized in that in step 1): Semen Lablab Album 25%, sepiellae seu sepiae ink sac dry powder 17%, Semen Ziziphi Spinosae (parched) powder 24%, Radix Glycyrrhizae Preparata 10%, the Rhizoma Atractylodis Macrocephalae 11%, Pericarpium Citri Reticulatae 13%.
Described a kind of Chinese medicine super-micro wall-broken fine powder for the treatment of gastropathy, is characterized in that step 2) in: wall breaking pulverization is to 70-80 μm.
Described a kind of Chinese medicine super-micro wall-broken fine powder for the treatment of gastropathy, is characterized in that in step 3): the weight ratio of fine powder raw material and water is 1:4, and drum's speed of rotation is 250rpm.
Semen Lablab Album, be the medical material of integration of edible and medicinal herbs, it is not only a kind of food, is also a kind of medicine, Semen Lablab Album put down, sweet in the mouth, effect spleen invigorating and in, removing dampness of relieving summer heat, the nourishing the stomach therapeutic method to keep the adverse QI flowing downwards.Compendium of Material Medica is recorded: " duricrust Semen Lablab Album, it is sub substantial, and Bai Erwei is yellow, and its gas raw meat is fragrant, and it is warm in nature flat, and obtain and neutralize, the paddy of spleen also ".
Sepiellae seu sepiae ink sac dry powder adopts sepiellae seu sepiae ink sac to make, and can directly buy from the market.Sepiellae seu sepiae is also known as black sepiellae seu sepiae fish, cuttle fish, and Sepiida marine products cephalopod, with Octopus and the nearly edge of squid.Sepiellae seu sepiae is distributed in each ocean, the world, mainly lives in the littoral shallow water in the torrid zone and temperate zone, often adjourns to comparatively territory, deep-sea winter.Sepiellae seu sepiae can say that whole body is precious, and not only sense of taste is fresh and crisp tasty and refreshing, has higher nutritive value, and is rich in medical value.The every hectogram meat of sepiellae seu sepiae is containing 13 grams, protein, and only 0.7 gram, fat, also containing carbohydrate and the necessary material of human body such as vitamin A, vitamin B group and calcium, phosphorus, ferrum, is a kind of high protein and low fat nourishing food.Be worth mentioning, it is the desirable health food that women moulds build and maintenance skin.Sepiellae seu sepiae shell is containing calcium carbonate, conchiolin, phlegmatic temperament and a small amount of sodium chloride, calcium phosphate, magnesium salt etc.Cuttle-fish bone juice contains a kind of mucopolysaccharide, and experiment confirms there is certain cancer suppressing action to mice.According to theory of Chinese medical science, sepiellae seu sepiae salty in the mouth, property are flat, enter liver, kidney channel; Have nourish blood, stimulate the menstrual flow, lactogenic, spleen reinforcing, kidney tonifying, YIN nourishing, regulating menstruation, leukorrhagia stopping effect; Be used for the treatment of the diseases such as women's irregular menstruation, edema, arthralgia chiefly caused by damp pathogen, hemorrhoid, beriberi.Cuttlefish meat, spine (Chinese medicine is called Endoconcha Sepiae) all can be used as medicine.Li Shizhen (1518-1593 A.D.) claims cuttlefish to be " blood system medicine ", is the good medicine for the treatment of woman anemia, blood deficiency amenorrhea.The cuisines function of food and medicines and health protection function combine by sepiellae seu sepiae.Sepiellae seu sepiae ink sac dry powder is good to the therapeutic effect of gastropathy.
Semen Ziziphi Spinosae (parched) powder adopts Semen Ziziphi Spinosae to make, Semen Ziziphi Spinosae, and another name Semen Ziziphi Spinosae, Fructus Choerospondiatis, jujube nucleus, Zizyphus jujuba is Rhamnaceae jujube.Semen Ziziphi Spinosae is said: astringing QI is calmed the nerves, and flourish muscle supports marrow, stomach function regulating activating the spleen in " book on Chinese herbal medicine converges and says ".Semen Ziziphi Spinosae is containing volume fatty oil and protein, and containing sterol, triterpenes, Semen Ziziphi Spinosae saponin, volume vitamin C, sweet in the mouth, acid, property is put down, and stomach function regulating activating the spleen, can nourish conscience, calm the nerves, arresting sweating.
Radix Glycyrrhizae Preparata is leguminous plant, and Radix Glycyrrhizae Preparata is with the honey Radix Glycyrrhizae of smoking, and is commonly called as the process of preparing Chinese medicine, is put in pot by Mel exactly and be smelt middle honey, uses slow fire instead and adds Radix Glycyrrhizae sheet and stir evenly, take the dish out of the pot, and puts taking-up when barn or baking oven are dried to tack-free, cools.Modern study, Radix Glycyrrhizae Preparata contains the number of chemical compositions such as glycyrrhizin, enoxolone, Angelica Polysaccharide, has antiinflammatory and anti-allergy action, scalable body's immunity, antitumor and analgesic effect.Therefore the primary efficacy of Radix Glycyrrhizae Preparata is and middle emergency, lung moistening, removing toxic substances, coordinating the actions of various ingredients in a prescription.Be usually used in weakness of the spleen and stomach, fatigue and weakness, severe palpitation, irregularly intermittent and regularly intermittent pulse, Radix Aconiti Lateralis Preparata poison can be separated.
The Rhizoma Atractylodis Macrocephalae, another name: small wooden raft Ji, Rhizoma Atractylodis Macrocephalae, the winter Rhizoma Atractylodis Macrocephalae, wash rice art, poplar small wooden raft, Wu Shu, sheet art, Rhizoma Atractylodis, Compositae, [WTBX herbaceos perennial, root stock nodositas.Stem is upright, the long branch from middle and lower part usually, whole Glabrous.The nice and cool weather of happiness, is used as medicine with rhizome, has multinomial medicinal function.There is spleen reinforcing, stomach reinforcing, dampness, and in, antiabortive; Control deficient QI of the spleen and stomach, anorexia, asthenia weak breath, deficiency-distension, has loose bowels, phlegm retention, edema, jaundice, arthralgia chiefly caused by damp pathogen, dysuria, dizzy, spontaneous perspiration, and nausea is uneasy.
Pericarpium Citri Reticulatae, sweet-bitter flavor, but the delicate fragrance having Fructus Citri tangerinae, be the dryness peel made after the peel drying process of Fructus Citri tangerinae, this peel, as under the condition kept dry, can place storage for a long time, therefore claims Pericarpium Citri Reticulatae.Regulating qi-flowing for strengthening spleen, in tune, dampness, reduces phlegm.Cure mainly distension and fullness in the abdomen or pain, the dyspepsia of stagnation of QI in spleen and stomach.Abdominal distention uncomfortable in chest in turbid damp resistance, indigestion and loss of appetite loose stool.Phlegm-damp stops up the cough and asthma of lung.Temperature can circulation of qi promoting, pungently can disperse, bitter and sluice.Therefore Pericarpium Citri Reticulatae has three major types effect, one is lead cold-evil in the heart, two broken stagnant gas, three strengthening the spleen stomaches.This three large on, Main Function is row QI of the spleen and stomach.
Described atomizer, ball mill directly can be buied by market.
Above-mentioned a kind of Chinese medicine super-micro wall-broken fine powder for the treatment of gastropathy, adopt there is invigorating spleen and reinforcing stomach natural food materials and medical material Semen Lablab Album, sepiellae seu sepiae ink sac dry powder, Semen Ziziphi Spinosae (parched) powder, Radix Glycyrrhizae Preparata, the Rhizoma Atractylodis Macrocephalae, Pericarpium Citri Reticulatae is composite makes, and has synergistic function to gastropathy; And adopt super-micro wall-broken to be made into fine powder, reduce the destruction of the course of processing to nutrient substance contained in product and functional component, greatly remain original bioactive ingredients and functional component, its granularity is little, good evenness and dissolution rate high, its dissolving in vivo, infiltration rate can be accelerated, improve its absorbtivity, good to the therapeutic effect of gastropathy, cure rate reaches more than 98%.
The percentage composition related in present specification unless otherwise indicated, is weight percentage.
Detailed description of the invention
Now in conjunction with embodiments of the invention and correlation test, the invention will be further described.
Embodiment 1
1) Feedstock treating: percentage composition takes Semen Lablab Album 20%, sepiellae seu sepiae ink sac dry powder 15%, Semen Ziziphi Spinosae (parched) powder 27%, Radix Glycyrrhizae Preparata 12%, the Rhizoma Atractylodis Macrocephalae 12%, Pericarpium Citri Reticulatae 14% by weight, for subsequent use; Pulverize after Semen Lablab Album, Radix Glycyrrhizae Preparata, the Rhizoma Atractylodis Macrocephalae, Pericarpium Citri Reticulatae mixing with pulverizer, cross 30 mesh sieves, add sepiellae seu sepiae ink sac dry powder, the mixing of Semen Ziziphi Spinosae (parched) powder;
2) wall breaking pulverization: by the mixed powder in step 1), is crushed to 50 μm through super micron mill, obtains breaking cellular wall fine powder;
3) wet ball grinding is pulverized: by step 2) fine powder that obtains adds ball mill wet ball grinding and pulverizes, and the weight ratio of fine powder raw material and water is 1:3, and drum's speed of rotation is 200rpm, through 2 hours ball milling breaking cellular walls, obtains ball milling wall cell disruption powder;
4) ball milling wall cell disruption powder in step 3) is added the water soaking 1h of raw material weight 5 times, then 100 DEG C of big fire decoct 20min, then use little fire decoction 10min instead, and cold filtration, collects filtrate;
5) by filtrate at 70 DEG C, vacuum is 0.09MpaMpa, and feed liquor flow velocity is 200mLmin -1condition under carry out vacuum film concentrate drying;
6) high temperature sterilize: dry powder step 5) obtained is short time sterilizing under the high temperature of 80 DEG C, and fill, in sterilizing bottle, namely obtains finished product.
Embodiment 2
1) Feedstock treating: percentage composition takes Semen Lablab Album 30%, sepiellae seu sepiae ink sac dry powder 20%, Semen Ziziphi Spinosae (parched) powder 20%, Radix Glycyrrhizae Preparata 9%, the Rhizoma Atractylodis Macrocephalae 9%, Pericarpium Citri Reticulatae 12% by weight, for subsequent use; Pulverize after Semen Lablab Album, Radix Glycyrrhizae Preparata, the Rhizoma Atractylodis Macrocephalae, Pericarpium Citri Reticulatae mixing with pulverizer, cross 50 mesh sieves, add sepiellae seu sepiae ink sac dry powder, the mixing of Semen Ziziphi Spinosae (parched) powder;
2) wall breaking pulverization: by the mixed powder in step 1), is crushed to 100 μm through super micron mill, obtains breaking cellular wall fine powder;
3) wet ball grinding is pulverized: by step 2) fine powder that obtains adds ball mill wet ball grinding and pulverizes, and the weight ratio of fine powder raw material and water is 1:5, and drum's speed of rotation is 300rpm, through 3 hours ball milling breaking cellular walls, obtains ball milling wall cell disruption powder;
4) ball milling wall cell disruption powder in step 3) is added the water soaking 2h of raw material weight 6 times, then 100 DEG C of big fire decoct 30min, then use little fire decoction 20min instead, and cold filtration, collects filtrate;
5) by filtrate at 80 DEG C, vacuum is 0.09MpaMpa, and feed liquor flow velocity is 300mLmin -1condition under carry out vacuum film concentrate drying;
6) high temperature sterilize: dry powder step 5) obtained is short time sterilizing under the high temperature of 90 DEG C, and fill, in sterilizing bottle, namely obtains finished product.
Embodiment 3
1) Feedstock treating: percentage composition takes Semen Lablab Album 25%, sepiellae seu sepiae ink sac dry powder 17%, Semen Ziziphi Spinosae (parched) powder 24%, Radix Glycyrrhizae Preparata 10%, the Rhizoma Atractylodis Macrocephalae 11%, Pericarpium Citri Reticulatae 13% by weight, for subsequent use; Pulverize after Semen Lablab Album, Radix Glycyrrhizae Preparata, the Rhizoma Atractylodis Macrocephalae, Pericarpium Citri Reticulatae mixing with pulverizer, cross 30-50 mesh sieve, add sepiellae seu sepiae ink sac dry powder, the mixing of Semen Ziziphi Spinosae (parched) powder;
2) wall breaking pulverization: by the mixed powder in step 1), is crushed to 80 μm through super micron mill, obtains breaking cellular wall fine powder;
3) wet ball grinding is pulverized: by step 2) fine powder that obtains adds ball mill wet ball grinding and pulverizes, and the weight ratio of fine powder raw material and water is 1:4, and drum's speed of rotation is 250rpm, through 2.5 hours ball milling breaking cellular walls, obtains ball milling wall cell disruption powder;
4) ball milling wall cell disruption powder in step 3) is added the water soaking 1.5h of raw material weight 5.5 times, then 100 DEG C of big fire decoct 25min, then use little fire decoction 15min instead, and cold filtration, collects filtrate;
5) by filtrate at 75 DEG C, vacuum is 0.09MpaMpa, and feed liquor flow velocity is 250mLmin -1condition under carry out vacuum film concentrate drying;
6) high temperature sterilize: dry powder step 5) obtained is short time sterilizing under the high temperature of 85 DEG C, and fill, in sterilizing bottle, namely obtains finished product.
Instructions of taking: 3 times on the one, a 4-5 gram, warm water is dissolved and is taken, and anemia of pregnant woman, infant avoid clothes.Take 8-10 days: flatulence, stomachache, symptom of diarrhea alleviate, have appetite sense.Take 15-20 days: have the hiccups, heartburn, nauseating, pantothenic acid, tripe are swollen, and phenomenon disappears substantially.Take 30 days: heal substantially in gastroenteritic ulcer face, new gastrointestinal mucosa generates, and gastrointestinal function recovers normal substantially.Within 30 days, be a course for the treatment of, take 2-3 the course for the treatment of: gastric mucosal immunity power, gastrointestinal function obviously strengthen, gastropathy cures Be very effective.
Beneficial effect of the present invention is further illustrated below by way of healing case.
Cure case 1: Zhang, female, 30 years old, clinical diagnosis bile reflux gastritis, upper abdomen persistence burning pain, pain increases the weight of after the meal, remission after drug administration, but often recur, cannot cure, do not feel like oneself more than 2 years, after taking 2 courses for the treatment of of above-mentioned super-micro wall-broken fine powder (embodiment 1), subjective symptoms disappears, and drug withdrawal, after 6 months, is felt without uncomfortable.
Cure case 2: Lee, man, 45 years old, clinical diagnosis is gastric ulcer, epigastrium pain, in burning property, nibbling property or inanition dull pain, distending pain or dull pain, remission after drug administration, but often recur, cannot cure, do not feel like oneself more than 1 year, after taking 3 courses for the treatment of of above-mentioned super-micro wall-broken fine powder (embodiment 2), subjective symptoms disappears, and drug withdrawal, after 4 months, is felt without uncomfortable.
Cure case 3: Liu, female, 60 years old, suffer from chronic superficial gastritis for many years, the conscious dull pain of upper abdomen sometimes, loss of appetite, post-prandial fullness, acid regurgitation etc., take 2 courses for the treatment of of above-mentioned super-micro wall-broken fine powder (embodiment 3), subjective symptoms disappears.
Cure case 4: thank certain, man, 36 years old, suffer from atrophic gastritis, often recur, cannot cure, do not feel like oneself 4-5, and after taking 3 courses for the treatment of of above-mentioned super-micro wall-broken fine powder (embodiment 2), subjective symptoms disappears, and drug withdrawal is after 9 months, without uncomfortable sensation.
Below by way of microbiological indicator and content of beary metal test the invention will be further described, in table 1.
Above-mentioned test determination result shows, microorganism, the content of beary metal of the super-micro wall-broken fine powder of embodiment 1 preparation are humble, meet green industry standard and green food standard.Carry out same test with embodiment 2-3, its microorganism, content of beary metal also meet green industry standard and green food standard.

Claims (5)

1. treat a Chinese medicine super-micro wall-broken fine powder for gastropathy, it is characterized in that comprising the following steps:
1) Feedstock treating: percentage composition takes Semen Lablab Album 20-30%, sepiellae seu sepiae ink sac dry powder 15-20%, Semen Ziziphi Spinosae (parched) powder 20-27%, Radix Glycyrrhizae Preparata 9-12%, Rhizoma Atractylodis Macrocephalae 9-12%, Pericarpium Citri Reticulatae 10-15% by weight, for subsequent use; Pulverize after Semen Lablab Album, Radix Glycyrrhizae Preparata, the Rhizoma Atractylodis Macrocephalae, Pericarpium Citri Reticulatae mixing with pulverizer, cross 30-50 mesh sieve, add sepiellae seu sepiae ink sac dry powder, the mixing of Semen Ziziphi Spinosae (parched) powder;
2) wall breaking pulverization: by the mixed powder in step 1), be crushed to 50-100 μm through super micron mill, obtains breaking cellular wall fine powder;
3) wet ball grinding is pulverized: by step 2) fine powder that obtains adds ball mill wet ball grinding and pulverizes, and the weight ratio of fine powder raw material and water is 1:3-5, and drum's speed of rotation is 200-300rpm, through 2-3 hour ball milling breaking cellular wall, obtains ball milling wall cell disruption powder;
4) ball milling wall cell disruption powder in step 3) is added raw material weight 5-6 water soaking 1-2h doubly, then 100 DEG C of big fire decoct 20-30min, then use little fire decoction 10-20min instead, and cold filtration, collects filtrate;
5) by filtrate at 70-80 DEG C, vacuum is 0.09MPa, and feed liquor flow velocity is 200-300mLmin -1condition under carry out vacuum film concentrate drying;
6) high temperature sterilize: dry powder step 5) obtained is short time sterilizing under the high temperature of 80 DEG C-90 DEG C, and fill, in sterilizing bottle, namely obtains finished product.
2. a kind of Chinese medicine super-micro wall-broken fine powder for the treatment of gastropathy as claimed in claim 1, is characterized in that in step 1): Semen Lablab Album 23-27%, sepiellae seu sepiae ink sac dry powder 16-18%, Semen Ziziphi Spinosae (parched) powder 22-25%, Radix Glycyrrhizae Preparata 10-11%, Rhizoma Atractylodis Macrocephalae 10-11%, Pericarpium Citri Reticulatae 12-13%.
3. a kind of Chinese medicine super-micro wall-broken fine powder for the treatment of gastropathy as claimed in claim 1, is characterized in that in step 1): Semen Lablab Album 25%, sepiellae seu sepiae ink sac dry powder 17%, Semen Ziziphi Spinosae (parched) powder 24%, Radix Glycyrrhizae Preparata 10%, the Rhizoma Atractylodis Macrocephalae 11%, Pericarpium Citri Reticulatae 13%.
4. a kind of Chinese medicine super-micro wall-broken fine powder for the treatment of gastropathy as claimed in claim 1, is characterized in that step 2) in: wall breaking pulverization is to 70-80 μm.
5. a kind of Chinese medicine super-micro wall-broken fine powder for the treatment of gastropathy as claimed in claim 1, is characterized in that in step 3): the weight ratio of fine powder raw material and water is 1:4, and drum's speed of rotation is 250rpm.
CN201410167118.3A 2014-04-24 2014-04-24 A kind of Chinese medicine super-micro wall-broken fine powder for the treatment of gastropathy Expired - Fee Related CN103933173B (en)

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