CN103911638B - 一种钴镍磷-碳化硅电镀液及电镀方法 - Google Patents
一种钴镍磷-碳化硅电镀液及电镀方法 Download PDFInfo
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- CN103911638B CN103911638B CN201410158338.XA CN201410158338A CN103911638B CN 103911638 B CN103911638 B CN 103911638B CN 201410158338 A CN201410158338 A CN 201410158338A CN 103911638 B CN103911638 B CN 103911638B
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- silicon carbide
- electroplate liquid
- cobalt nickel
- nickel phosphorus
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- 229910010271 silicon carbide Inorganic materials 0.000 title claims abstract description 25
- 239000007788 liquid Substances 0.000 title claims abstract description 23
- YFQIPGMZAZUECC-UHFFFAOYSA-N [Si].[P].[Co].[Ni] Chemical compound [Si].[P].[Co].[Ni] YFQIPGMZAZUECC-UHFFFAOYSA-N 0.000 title claims abstract description 17
- 238000009713 electroplating Methods 0.000 title claims abstract description 14
- 238000000034 method Methods 0.000 title claims abstract description 12
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims abstract description 16
- 238000007747 plating Methods 0.000 claims abstract description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 11
- 241000220317 Rosa Species 0.000 claims abstract description 8
- 239000008367 deionised water Substances 0.000 claims abstract description 8
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 8
- MLRKYSNODSLPAB-UHFFFAOYSA-N hex-1-yn-1-ol Chemical class CCCCC#CO MLRKYSNODSLPAB-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000004310 lactic acid Substances 0.000 claims abstract description 8
- 235000014655 lactic acid Nutrition 0.000 claims abstract description 8
- 150000002815 nickel Chemical class 0.000 claims abstract description 8
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000001509 sodium citrate Substances 0.000 claims abstract description 8
- ISIJQEHRDSCQIU-UHFFFAOYSA-N tert-butyl 2,7-diazaspiro[4.5]decane-7-carboxylate Chemical compound C1N(C(=O)OC(C)(C)C)CCCC11CNCC1 ISIJQEHRDSCQIU-UHFFFAOYSA-N 0.000 claims abstract description 8
- HRXKRNGNAMMEHJ-UHFFFAOYSA-K trisodium citrate Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O HRXKRNGNAMMEHJ-UHFFFAOYSA-K 0.000 claims abstract description 8
- 239000000203 mixture Substances 0.000 claims abstract description 5
- 229940038773 trisodium citrate Drugs 0.000 claims abstract description 5
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 8
- MWECWRCFCLYOTJ-UHFFFAOYSA-N [Ti+4].[O-2].[O-2].[O-2].[O-2].[O-2].[Ta+5].[Ir+3] Chemical compound [Ti+4].[O-2].[O-2].[O-2].[O-2].[O-2].[Ta+5].[Ir+3] MWECWRCFCLYOTJ-UHFFFAOYSA-N 0.000 claims description 5
- 230000000694 effects Effects 0.000 claims description 5
- -1 10-40 parts Chemical compound 0.000 claims description 4
- 235000017557 sodium bicarbonate Nutrition 0.000 claims description 4
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims description 4
- 229910001080 W alloy Inorganic materials 0.000 abstract description 7
- 238000004070 electrodeposition Methods 0.000 abstract description 6
- 238000004381 surface treatment Methods 0.000 abstract description 2
- 229910052751 metal Inorganic materials 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
- 238000003756 stirring Methods 0.000 description 12
- 239000000243 solution Substances 0.000 description 6
- 235000019263 trisodium citrate Nutrition 0.000 description 5
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- 229910052804 chromium Inorganic materials 0.000 description 4
- 239000011651 chromium Substances 0.000 description 4
- 230000007797 corrosion Effects 0.000 description 4
- 238000005260 corrosion Methods 0.000 description 4
- 239000003208 petroleum Substances 0.000 description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 229910052739 hydrogen Inorganic materials 0.000 description 3
- 239000001257 hydrogen Substances 0.000 description 3
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 3
- 229910052748 manganese Inorganic materials 0.000 description 3
- 239000011572 manganese Substances 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- 230000001105 regulatory effect Effects 0.000 description 3
- 229910052708 sodium Inorganic materials 0.000 description 3
- 239000011734 sodium Substances 0.000 description 3
- 229910001145 Ferrotungsten Inorganic materials 0.000 description 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 2
- 229910052721 tungsten Inorganic materials 0.000 description 2
- 239000010937 tungsten Substances 0.000 description 2
- 229910045601 alloy Inorganic materials 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 239000010941 cobalt Substances 0.000 description 1
- 229910017052 cobalt Inorganic materials 0.000 description 1
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 1
- 230000001276 controlling effect Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 239000005300 metallic glass Substances 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- MOWMLACGTDMJRV-UHFFFAOYSA-N nickel tungsten Chemical compound [Ni].[W] MOWMLACGTDMJRV-UHFFFAOYSA-N 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
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- Electroplating Methods And Accessories (AREA)
- Electroplating And Plating Baths Therefor (AREA)
Abstract
Description
Claims (4)
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CN103911638A CN103911638A (zh) | 2014-07-09 |
CN103911638B true CN103911638B (zh) | 2016-03-02 |
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CN104611744B (zh) * | 2014-12-15 | 2017-06-06 | 常州大学 | 一种低温水溶液电化学共沉积镍铱合金的方法 |
CN104846409A (zh) * | 2015-04-30 | 2015-08-19 | 云南民族大学 | 高钨含量且无裂纹的钨镍合金镀层及电镀液和电镀工艺 |
CN109137031B (zh) * | 2018-09-07 | 2020-04-28 | 张惠海 | 一种金属基陶瓷复合材料 |
CN109518237B (zh) * | 2019-01-24 | 2020-12-08 | 合鸿新材科技有限公司 | 锌镍磷电镀液、其制备方法及电镀方法 |
CN109797383A (zh) * | 2019-04-04 | 2019-05-24 | 山东新海表面技术科技有限公司 | 铝合金发动机缸体及其制备方法 |
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JPS6421097A (en) * | 1987-07-16 | 1989-01-24 | Riken Kk | Sliding member |
CN1025056C (zh) * | 1989-11-24 | 1994-06-15 | 中国人民解放军装甲兵工程学院 | 钴-镍-磷非晶态合金刷镀镀层及其方法 |
CN101928967B (zh) * | 2010-08-30 | 2011-08-24 | 赵汝山 | 钴-钨-镍-磷合金电镀液 |
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2014
- 2014-04-18 CN CN201410158338.XA patent/CN103911638B/zh active Active
Non-Patent Citations (3)
Title |
---|
Fabrication of porous Co–Ni–P catalysts by electrodeposition and their catalytic characteristics for the generation of hydrogen from an alkaline NaBH4 solution;Deog-Ryung Kim等;《international journal of hydrogenenergy 》;20090220;第32卷;第2622-2630页 * |
Preparation,characterization and microwave absorption properties of electroless Ni–Co–P-coated SiC powder;Yongjie Li等;《Applied Surface Science 》;20080120;第254卷;第4708-4715页 * |
电沉积镍基SiC/Si3N4纳米复合镀层及组织结构与性能研究;王法斌;《万方学位论文数据库》;20091019;第24页第2段,第4段 * |
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Denomination of invention: Cobalt nickel phosphorus-silicon carbide electroplating solution and electroplating method Effective date of registration: 20190306 Granted publication date: 20160302 Pledgee: Qi quotient bank Limited by Share Ltd. Weihai Wendeng branch Pledgor: HEHONG NEW MATERIAL SCIENCE & TECHNOLOGY CO.,LTD. Registration number: 2019370000043 |
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Denomination of invention: Cobalt nickel phosphorus silicon carbide electroplating solution and electroplating method Effective date of registration: 20210301 Granted publication date: 20160302 Pledgee: Qi quotient bank Limited by Share Ltd. Weihai Wendeng branch Pledgor: HEHONG NEW MATERIAL SCIENCE & TECHNOLOGY Co.,Ltd. Registration number: Y2021980001347 |
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