CN103833418A - Making method of white-ground colored crystal flower crystal glaze - Google Patents

Making method of white-ground colored crystal flower crystal glaze Download PDF

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Publication number
CN103833418A
CN103833418A CN201210481447.6A CN201210481447A CN103833418A CN 103833418 A CN103833418 A CN 103833418A CN 201210481447 A CN201210481447 A CN 201210481447A CN 103833418 A CN103833418 A CN 103833418A
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Prior art keywords
glaze
hours
mud
hour
raw material
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CN201210481447.6A
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Chinese (zh)
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王锡明
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CHAOZHOU YUBINGHUA CERAMIC Co Ltd
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CHAOZHOU YUBINGHUA CERAMIC Co Ltd
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Priority to CN201210481447.6A priority Critical patent/CN103833418A/en
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Abstract

A making method of a white-ground colored crystal flower crystal glaze comprises the following steps: 1, crystal glaze material preparation: mixing albite, potash feldspar, quartz, mud, calcite, barium carbonate, zinc oxide and titanium dioxide, carrying out fine grinding, sieving by a 200 mesh sieve, and removing iron to obtain a crystal glaze material for later use; 2, engobe preparation: respectively selecting one of golden brown engobe prepared by fully and uniformly mixing praseodymium yellow with vanadium-zirconium yellow and finished mud, yellowish green engobe prepared by fully and uniformly mixing vanadium-zirconium blue with the praseodymium yellow and the finished mud and pinky engobe prepared by fully and uniformly mixing manganese red with the finished mud according to the color difference; 3, applying the engobe to white adobe, drying, applying the crystal glaze to the thickness of the obtained glaze layer of about 1mm; and 4, firing to a highest temperature, and cooling to room temperature. The controllable color change of crystal flowers is realized through different engobes, so the obtained white-ground colored crystal flower crystal glaze has the advantages of brilliant, multiple and hierarchic color, simple technology, wide firing temperature range, high yield and low cost.

Description

The making method of the brilliant flower of a kind of white background color crystalline glaze
Technical field
The present invention relates to a kind of ceramic glaze preparation field, refer in particular to the making method of the brilliant flower of a kind of white background color crystalline glaze.
Background technology
Along with society is aesthetic and ceramic art is appreciated to the raising of level, people value ceramic artistic value more and more, ceramic decoration art bring to people aesthetic feeling be unique and special, people's taste is improving constantly, and requires also improving for the class of ceramic simultaneously.Since 20 century 70s, there is comprehensive innovation in the production technology of China's ceramic industry and equipment thereof, and in the 2l century developing rapidly at hi tech and new material, whole ceramic industry must have new looks.Pottery is the traditional product of China, no matter domestic ceramics or architectural pottery, and the output of China is sure to occupy the first in the world already.But still as main, assortment are few take low and middle-grade for our product, one of them major reason is just that the decoration level of product, decorative quality are not high, wherein it will be further appreciated that the impact of the brilliant floral shape of crystalline glaze and color.
In prior art, research for crystalline glaze is quite ripe, if Patent Office's disclosed publication number in 2009 is CN101481261A " a kind of titanium by name, zinc, pyroxene crystalline glaze and distribution thereof ", exist firing range for existing crystalline glaze narrow, brilliant flower growth deficiency rambunctious, on the basis of pyroxene crystalline glaze, introduce titanium oxide and zinc oxide, and mix in the basestocks of pyroxene crystalline glaze, the sintering technology of pyroxene crystalline glaze routinely, the manufacture craft of this crystalline glaze is the same with the sintering technology of conventional pyroxene crystalline glaze, do not need to process especially, brilliant flower is more easy to control and operating procedure is simple, but its brilliant flower color is comparatively single, therefore, be necessary the color of crystalline substance flower to be studied, change effort for realizing brilliant flower color controllability, this is significant to promoting ceramic art value.
Summary of the invention
The object of the invention is to overcome the deficiencies in the prior art, a kind of crystalline glaze making method that can realize to controllability brilliant flower colour-change is provided.
For achieving the above object, the technical scheme of this employing is:
(1) preparation of crystallization glaze: the weight that weighs each raw material in albite 12-20, potassium felspar sand 16-26, quartzy 23-33, the ratio of washing mud 2-4, calcite 8-15, barium carbonate 6-10, zinc oxide 20-3, titanium dioxide 4-10 is mixed, ball milling 28-32 hour, fineness be 325 mesh screen residues to 0.02-0.04, then blowing cross 200 mesh sieves and deironing.
(2) preparation of cosmetic soil, any in can be respectively below three kinds according to the difference of color:
1. golden yellow cosmetic soil: weigh after fully mixing in hollander after the weight of each raw material for subsequent use in the ratio of the yellow 4-7 of praseodymium yellow 4-7, vanadium zirconium, finished product mud 100.
2. fruit green cosmetic soil: weigh after fully mixing in hollander after the weight of each raw material for subsequent use in the ratio of vanadium zirconium blue 1-3, praseodymium yellow 5-8, finished product mud 100.
3. pink cosmetic soil: weigh after fully mixing in hollander after the weight of each raw material for subsequent use in the ratio of manganese red 6-9, finished product mud 100.
(3) cosmetic soil is imposed on white sun-dried mud brick, wait for its dry after, then impose on crystalline glaze, glaze layer thickness is controlled at 0.9-1.1mm.
(4) sintering curve is: first stage heat temperature raising, rise to 850 ℃ with 2.5 hours from room temperature, and 850 ℃ rose to 1080-1100 ℃ with 2 hours, and 1080-1100 ℃ rises to 1260-1300 ℃ with 0.5-1 hour; Subordinate phase cools, and is down to 1150-1050 ℃ with 0.5-1 hour from the highest temperature, is then incubated 3-5 hour, finally naturally cools to room temperature.
The present invention adopts after technique scheme compared with prior art tool to have the following advantages: first, the present invention has realized the colour-change of brilliant colored controllability by different cosmetic soils, have advantages of that pattern uniqueness, tire starved glaze are even, highest quality, with countless changes, bright in luster colourful and be rich in gradation sense, show better crystalline glaze and entered that kiln is of the same colour, unique quality of kiln discharge ten thousand coloured silks, effectively promoted the artistic value of ceramic product and appreciate space.
The second, sintering curve of the present invention can expand the maturing range of crystalline glaze effectively, has broken through the technical bottleneck that crystalline glaze maturing temperature is narrow, crystalline range is narrow, makes crystalline glaze as other glaze, realize suitability for industrialized production, improves yield rate.
Embodiment
Implement time of the present invention, according to can not color demand, from golden yellow cosmetic soil, fruit green cosmetic soil, pink cosmetic soil, choosing any one kind of them be respectively used in combination with crystallization glaze and realizes the crystalline substance flower of different colours.
Embodiment 1: make golden yellow brilliant flower, select golden yellow cosmetic soil.
The weight that weighs each raw material in albite 16, potassium felspar sand 20, quartz 24, the ratio of washing mud 3, calcite 12, barium carbonate 8, zinc oxide 13, titanium dioxide 4 is mixed, ball milling 30 hours, fineness is 325 mesh screen residues to 0.03, then after blowing mistake 200 mesh sieves and deironing, makes crystallization glaze for subsequent use; Weighing in the ratio of praseodymium yellow 5, vanadium zirconium Huang 5, finished product mud 100 after fully mixing in hollander after the weight of each raw material becomes golden yellow cosmetic soil for subsequent use; Golden yellow cosmetic soil is imposed on white sun-dried mud brick, wait for its dry after, then impose on crystalline glaze, glaze layer thickness is controlled at 1mm; Sintering curve is: first stage heat temperature raising, rise to 850 ℃ with 2.5 hours from room temperature, and 850 ℃ rose to 1090 ℃ with 2 hours, and 1090 ℃ rose to 1280 ℃ with 0.8 hour; Subordinate phase cools, and is down to 1100 ℃ with 0.8 hour from the highest temperature, is then incubated 4 hours, finally naturally cools to room temperature.
Embodiment 2: make the brilliant flower of fruit green, select fruit green cosmetic soil.
The weight that weighs each raw material in albite 16, potassium felspar sand 20, quartz 24, the ratio of washing mud 3, calcite 12, barium carbonate 8, zinc oxide 13, titanium dioxide 4 is mixed, ball milling 30 hours, fineness is 325 mesh screen residues to 0.03, then after blowing mistake 200 mesh sieves and deironing, makes crystallization glaze for subsequent use; Weighing in the ratio of vanadium zirconium blue 2, praseodymium yellow 6, finished product mud 100 after fully mixing in hollander after the weight of each raw material becomes golden yellow cosmetic soil for subsequent use; Golden yellow cosmetic soil is imposed on white sun-dried mud brick, wait for its dry after, then impose on crystalline glaze, glaze layer thickness is controlled at 1mm; Sintering curve is: first stage heat temperature raising, rise to 850 ℃ with 2.5 hours from room temperature, and 850 ℃ rose to 1090 ℃ with 2 hours, and 1090 ℃ rose to 1280 ℃ with 0.8 hour; Subordinate phase cools, and is down to 1100 ℃ with 0.8 hour from the highest temperature, is then incubated 4 hours, finally naturally cools to room temperature.
Embodiment 3: make the brilliant flower of pink, select pink cosmetic soil.
The weight that weighs each raw material in albite 16, potassium felspar sand 20, quartz 24, the ratio of washing mud 3, calcite 12, barium carbonate 8, zinc oxide 13, titanium dioxide 4 is mixed, ball milling 30 hours, fineness is 325 mesh screen residues to 0.03, then after blowing mistake 200 mesh sieves and deironing, makes crystallization glaze for subsequent use; Weighing in the ratio of manganese red 8, finished product mud 100 after fully mixing in hollander after the weight of each raw material becomes golden yellow cosmetic soil for subsequent use; Golden yellow cosmetic soil is imposed on white sun-dried mud brick, wait for its dry after, then impose on crystalline glaze, glaze layer thickness is controlled at 1mm; Sintering curve is: first stage heat temperature raising, rise to 850 ℃ with 2.5 hours from room temperature, and 850 ℃ rose to 1090 ℃ with 2 hours, and 1090 ℃ rose to 1280 ℃ with 0.8 hour; Subordinate phase cools, and is down to 1100 ℃ with 0.8 hour from the highest temperature, is then incubated 4 hours, finally naturally cools to room temperature.

Claims (4)

1. a making method for the brilliant flower of white background color crystalline glaze, is characterized in that:
(1) preparation of crystallization glaze: the weight that weighs each raw material in albite 12-20, potassium felspar sand 16-26, quartzy 23-33, the ratio of washing mud 2-4, calcite 8-15, barium carbonate 6-10, zinc oxide 20-3, titanium dioxide 4-10 is mixed, ball milling 28-32 hour, fineness be 325 mesh screen residues to 0.02-0.04, then blowing cross 200 mesh sieves and deironing;
(2) preparation of cosmetic soil, any in can be respectively below three kinds according to the difference of color:
1. golden yellow cosmetic soil: weigh after fully mixing in hollander after the weight of each raw material for subsequent use in the ratio of the yellow 4-7 of praseodymium yellow 4-7, vanadium zirconium, finished product mud 100;
2. fruit green cosmetic soil: weigh after fully mixing in hollander after the weight of each raw material for subsequent use in the ratio of vanadium zirconium blue 1-3, praseodymium yellow 5-8, finished product mud 100;
3. pink cosmetic soil: weigh after fully mixing in hollander after the weight of each raw material for subsequent use in the ratio of manganese red 6-9, finished product mud 100;
(3) cosmetic soil is imposed on white sun-dried mud brick, wait for its dry after, then impose on crystalline glaze, glaze layer thickness is controlled at 0.9-1.1mm;
(4) sintering curve is: first stage heat temperature raising, rise to 850 ℃ with 2.5 hours from room temperature, and 850 ℃ rose to 1080-1100 ℃ with 2 hours, and 1080-1100 ℃ rises to 1260-1300 ℃ with 0.5-1 hour; Subordinate phase cools, and is down to 1150-1050 ℃ with 0.5-1 hour from the highest temperature, is then incubated 3-5 hour, finally naturally cools to room temperature.
2. the making method of the brilliant flower of a kind of white background color according to claim 1 crystalline glaze, it is characterized in that: the weight that weighs each raw material in albite 16, potassium felspar sand 20, quartz 24, the ratio of washing mud 3, calcite 12, barium carbonate 8, zinc oxide 13, titanium dioxide 4 is mixed, ball milling 30 hours, fineness is 325 mesh screen residues to 0.03, then after blowing mistake 200 mesh sieves and deironing, makes crystallization glaze for subsequent use; Weighing in the ratio of praseodymium yellow 5, vanadium zirconium Huang 5, finished product mud 100 after fully mixing in hollander after the weight of each raw material becomes golden yellow cosmetic soil for subsequent use; Golden yellow cosmetic soil is imposed on white sun-dried mud brick, wait for its dry after, then impose on crystalline glaze, glaze layer thickness is controlled at 1mm; Sintering curve is: first stage heat temperature raising, rise to 850 ℃ with 2.5 hours from room temperature, and 850 ℃ rose to 1090 ℃ with 2 hours, and 1090 ℃ rose to 1280 ℃ with 0.8 hour; Subordinate phase cools, and is down to 1100 ℃ with 0.8 hour from the highest temperature, is then incubated 4 hours, finally naturally cools to room temperature.
3. the making method of the brilliant flower of a kind of white background color according to claim 1 crystalline glaze, it is characterized in that: the weight that weighs each raw material in albite 16, potassium felspar sand 20, quartz 24, the ratio of washing mud 3, calcite 12, barium carbonate 8, zinc oxide 13, titanium dioxide 4 is mixed, ball milling 30 hours, fineness is 325 mesh screen residues to 0.03, then after blowing mistake 200 mesh sieves and deironing, makes crystallization glaze for subsequent use; Weighing in the ratio of vanadium zirconium blue 2, praseodymium yellow 6, finished product mud 100 after fully mixing in hollander after the weight of each raw material becomes golden yellow cosmetic soil for subsequent use; Golden yellow cosmetic soil is imposed on white sun-dried mud brick, wait for its dry after, then impose on crystalline glaze, glaze layer thickness is controlled at 1mm; Sintering curve is: first stage heat temperature raising, rise to 850 ℃ with 2.5 hours from room temperature, and 850 ℃ rose to 1090 ℃ with 2 hours, and 1090 ℃ rose to 1280 ℃ with 0.8 hour; Subordinate phase cools, and is down to 1100 ℃ with 0.8 hour from the highest temperature, is then incubated 4 hours, finally naturally cools to room temperature.
4. the making method of the brilliant flower of a kind of white background color according to claim 1 crystalline glaze, it is characterized in that: the weight that weighs each raw material in albite 16, potassium felspar sand 20, quartz 24, the ratio of washing mud 3, calcite 12, barium carbonate 8, zinc oxide 13, titanium dioxide 4 is mixed, ball milling 30 hours, fineness is 325 mesh screen residues to 0.03, then after blowing mistake 200 mesh sieves and deironing, makes crystallization glaze for subsequent use; Weighing in the ratio of manganese red 8, finished product mud 100 after fully mixing in hollander after the weight of each raw material becomes golden yellow cosmetic soil for subsequent use; Golden yellow cosmetic soil is imposed on white sun-dried mud brick, wait for its dry after, then impose on crystalline glaze, glaze layer thickness is controlled at 1mm; Sintering curve is: first stage heat temperature raising, rise to 850 ℃ with 2.5 hours from room temperature, and 850 ℃ rose to 1090 ℃ with 2 hours, and 1090 ℃ rose to 1280 ℃ with 0.8 hour; Subordinate phase cools, and is down to 1100 ℃ with 0.8 hour from the highest temperature, is then incubated 4 hours, finally naturally cools to room temperature.
CN201210481447.6A 2012-11-23 2012-11-23 Making method of white-ground colored crystal flower crystal glaze Pending CN103833418A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109734320A (en) * 2019-03-27 2019-05-10 佛山市利德嘉陶瓷制釉有限公司 A kind of plasticity effect is good and the manufacture craft for convenient ceramic wall and floor bricks colorful crystal glazes of painting
CN109987843A (en) * 2019-04-24 2019-07-09 广东省大埔陶瓷工业研究所 A method of it carrying out zinc silicate positioning on ceramic flat surface and crystallizes and prepare ceramics
CN111018566A (en) * 2019-12-18 2020-04-17 江苏省宜兴彩陶工艺厂 Silk-like emerald flow kiln-change fancy glaze ceramic container and preparation method thereof
CN111362725A (en) * 2020-03-18 2020-07-03 湖南陶润会文化传播有限公司 Green-bottom crystal glaze and preparation method thereof

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109734320A (en) * 2019-03-27 2019-05-10 佛山市利德嘉陶瓷制釉有限公司 A kind of plasticity effect is good and the manufacture craft for convenient ceramic wall and floor bricks colorful crystal glazes of painting
CN109987843A (en) * 2019-04-24 2019-07-09 广东省大埔陶瓷工业研究所 A method of it carrying out zinc silicate positioning on ceramic flat surface and crystallizes and prepare ceramics
CN109987843B (en) * 2019-04-24 2022-03-15 广东省大埔陶瓷工业研究所 Method for performing zinc silicate positioning crystallization on ceramic plane and preparing ceramic
CN111018566A (en) * 2019-12-18 2020-04-17 江苏省宜兴彩陶工艺厂 Silk-like emerald flow kiln-change fancy glaze ceramic container and preparation method thereof
CN111362725A (en) * 2020-03-18 2020-07-03 湖南陶润会文化传播有限公司 Green-bottom crystal glaze and preparation method thereof

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Application publication date: 20140604