CN103833418A - Making method of white-ground colored crystal flower crystal glaze - Google Patents
Making method of white-ground colored crystal flower crystal glaze Download PDFInfo
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- CN103833418A CN103833418A CN201210481447.6A CN201210481447A CN103833418A CN 103833418 A CN103833418 A CN 103833418A CN 201210481447 A CN201210481447 A CN 201210481447A CN 103833418 A CN103833418 A CN 103833418A
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- XLOMVQKBTHCTTD-UHFFFAOYSA-N zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims abstract description 20
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 19
- AYJRCSIUFZENHW-UHFFFAOYSA-L Barium carbonate Chemical compound [Ba+2].[O-]C([O-])=O AYJRCSIUFZENHW-UHFFFAOYSA-L 0.000 claims abstract description 18
- 238000002156 mixing Methods 0.000 claims abstract description 16
- 229910052777 Praseodymium Inorganic materials 0.000 claims abstract description 10
- PUDIUYLPXJFUGB-UHFFFAOYSA-N praseodymium Chemical compound [Pr] PUDIUYLPXJFUGB-UHFFFAOYSA-N 0.000 claims abstract description 10
- -1 vanadium-zirconium Chemical compound 0.000 claims abstract description 10
- 239000011787 zinc oxide Substances 0.000 claims abstract description 10
- 229910052656 albite Inorganic materials 0.000 claims abstract description 9
- 239000004408 titanium dioxide Substances 0.000 claims abstract description 9
- 238000002360 preparation method Methods 0.000 claims abstract description 7
- 239000010453 quartz Substances 0.000 claims abstract description 7
- 229910052904 quartz Inorganic materials 0.000 claims abstract description 7
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 7
- PWHULOQIROXLJO-UHFFFAOYSA-N manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 claims abstract description 5
- 229910052748 manganese Inorganic materials 0.000 claims abstract description 5
- 239000011572 manganese Substances 0.000 claims abstract description 5
- 239000002537 cosmetic Substances 0.000 claims description 29
- 239000002689 soil Substances 0.000 claims description 29
- 239000002994 raw material Substances 0.000 claims description 20
- FFRBMBIXVSCUFS-UHFFFAOYSA-N Martius yellow Chemical compound C1=CC=C2C(O)=C([N+]([O-])=O)C=C([N+]([O-])=O)C2=C1 FFRBMBIXVSCUFS-UHFFFAOYSA-N 0.000 claims description 17
- 238000005245 sintering Methods 0.000 claims description 11
- 238000002425 crystallisation Methods 0.000 claims description 9
- 230000005712 crystallization Effects 0.000 claims description 9
- 238000000498 ball milling Methods 0.000 claims description 8
- 238000007664 blowing Methods 0.000 claims description 8
- 239000011454 mudbrick Substances 0.000 claims description 8
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 8
- 229910052700 potassium Inorganic materials 0.000 claims description 8
- 239000011591 potassium Substances 0.000 claims description 8
- 239000004576 sand Substances 0.000 claims description 8
- 238000005406 washing Methods 0.000 claims description 8
- 238000005303 weighing Methods 0.000 claims description 6
- 235000013399 edible fruits Nutrition 0.000 claims description 5
- OIQPTROHQCGFEF-QIKYXUGXSA-L Sunset Yellow FCF Chemical compound [Na+].[Na+].OC1=CC=C2C=C(S([O-])(=O)=O)C=CC2=C1\N=N\C1=CC=C(S([O-])(=O)=O)C=C1 OIQPTROHQCGFEF-QIKYXUGXSA-L 0.000 claims description 2
- YXHBBEQKMVAJOH-GLCFPVLVSA-K Tartrazine Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)C1=NN(C=2C=CC(=CC=2)S([O-])(=O)=O)C(O)=C1\N=N\C1=CC=C(S([O-])(=O)=O)C=C1 YXHBBEQKMVAJOH-GLCFPVLVSA-K 0.000 claims description 2
- 238000005516 engineering process Methods 0.000 abstract description 5
- 238000010304 firing Methods 0.000 abstract description 3
- 239000000463 material Substances 0.000 abstract description 3
- 239000011499 joint compound Substances 0.000 abstract 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract 2
- 238000001816 cooling Methods 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 239000010433 feldspar Substances 0.000 abstract 1
- 229910052742 iron Inorganic materials 0.000 abstract 1
- 229940072033 potash Drugs 0.000 abstract 1
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 abstract 1
- 235000015320 potassium carbonate Nutrition 0.000 abstract 1
- KWYUFKZDYYNOTN-UHFFFAOYSA-M potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 abstract 1
- 238000007873 sieving Methods 0.000 abstract 1
- 239000000919 ceramic Substances 0.000 description 10
- 229910052611 pyroxene Inorganic materials 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000005034 decoration Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- OGIDPMRJRNCKJF-UHFFFAOYSA-N TiO Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- 238000011030 bottleneck Methods 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 238000011017 operating method Methods 0.000 description 1
- 230000001737 promoting Effects 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910001929 titanium oxide Inorganic materials 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
Abstract
A making method of a white-ground colored crystal flower crystal glaze comprises the following steps: 1, crystal glaze material preparation: mixing albite, potash feldspar, quartz, mud, calcite, barium carbonate, zinc oxide and titanium dioxide, carrying out fine grinding, sieving by a 200 mesh sieve, and removing iron to obtain a crystal glaze material for later use; 2, engobe preparation: respectively selecting one of golden brown engobe prepared by fully and uniformly mixing praseodymium yellow with vanadium-zirconium yellow and finished mud, yellowish green engobe prepared by fully and uniformly mixing vanadium-zirconium blue with the praseodymium yellow and the finished mud and pinky engobe prepared by fully and uniformly mixing manganese red with the finished mud according to the color difference; 3, applying the engobe to white adobe, drying, applying the crystal glaze to the thickness of the obtained glaze layer of about 1mm; and 4, firing to a highest temperature, and cooling to room temperature. The controllable color change of crystal flowers is realized through different engobes, so the obtained white-ground colored crystal flower crystal glaze has the advantages of brilliant, multiple and hierarchic color, simple technology, wide firing temperature range, high yield and low cost.
Description
Technical field
The present invention relates to a kind of ceramic glaze preparation field, refer in particular to the making method of the brilliant flower of a kind of white background color crystalline glaze.
Background technology
Along with society is aesthetic and ceramic art is appreciated to the raising of level, people value ceramic artistic value more and more, ceramic decoration art bring to people aesthetic feeling be unique and special, people's taste is improving constantly, and requires also improving for the class of ceramic simultaneously.Since 20 century 70s, there is comprehensive innovation in the production technology of China's ceramic industry and equipment thereof, and in the 2l century developing rapidly at hi tech and new material, whole ceramic industry must have new looks.Pottery is the traditional product of China, no matter domestic ceramics or architectural pottery, and the output of China is sure to occupy the first in the world already.But still as main, assortment are few take low and middle-grade for our product, one of them major reason is just that the decoration level of product, decorative quality are not high, wherein it will be further appreciated that the impact of the brilliant floral shape of crystalline glaze and color.
In prior art, research for crystalline glaze is quite ripe, if Patent Office's disclosed publication number in 2009 is CN101481261A " a kind of titanium by name, zinc, pyroxene crystalline glaze and distribution thereof ", exist firing range for existing crystalline glaze narrow, brilliant flower growth deficiency rambunctious, on the basis of pyroxene crystalline glaze, introduce titanium oxide and zinc oxide, and mix in the basestocks of pyroxene crystalline glaze, the sintering technology of pyroxene crystalline glaze routinely, the manufacture craft of this crystalline glaze is the same with the sintering technology of conventional pyroxene crystalline glaze, do not need to process especially, brilliant flower is more easy to control and operating procedure is simple, but its brilliant flower color is comparatively single, therefore, be necessary the color of crystalline substance flower to be studied, change effort for realizing brilliant flower color controllability, this is significant to promoting ceramic art value.
Summary of the invention
The object of the invention is to overcome the deficiencies in the prior art, a kind of crystalline glaze making method that can realize to controllability brilliant flower colour-change is provided.
For achieving the above object, the technical scheme of this employing is:
(1) preparation of crystallization glaze: the weight that weighs each raw material in albite 12-20, potassium felspar sand 16-26, quartzy 23-33, the ratio of washing mud 2-4, calcite 8-15, barium carbonate 6-10, zinc oxide 20-3, titanium dioxide 4-10 is mixed, ball milling 28-32 hour, fineness be 325 mesh screen residues to 0.02-0.04, then blowing cross 200 mesh sieves and deironing.
(2) preparation of cosmetic soil, any in can be respectively below three kinds according to the difference of color:
1. golden yellow cosmetic soil: weigh after fully mixing in hollander after the weight of each raw material for subsequent use in the ratio of the yellow 4-7 of praseodymium yellow 4-7, vanadium zirconium, finished product mud 100.
2. fruit green cosmetic soil: weigh after fully mixing in hollander after the weight of each raw material for subsequent use in the ratio of vanadium zirconium blue 1-3, praseodymium yellow 5-8, finished product mud 100.
3. pink cosmetic soil: weigh after fully mixing in hollander after the weight of each raw material for subsequent use in the ratio of manganese red 6-9, finished product mud 100.
(3) cosmetic soil is imposed on white sun-dried mud brick, wait for its dry after, then impose on crystalline glaze, glaze layer thickness is controlled at 0.9-1.1mm.
(4) sintering curve is: first stage heat temperature raising, rise to 850 ℃ with 2.5 hours from room temperature, and 850 ℃ rose to 1080-1100 ℃ with 2 hours, and 1080-1100 ℃ rises to 1260-1300 ℃ with 0.5-1 hour; Subordinate phase cools, and is down to 1150-1050 ℃ with 0.5-1 hour from the highest temperature, is then incubated 3-5 hour, finally naturally cools to room temperature.
The present invention adopts after technique scheme compared with prior art tool to have the following advantages: first, the present invention has realized the colour-change of brilliant colored controllability by different cosmetic soils, have advantages of that pattern uniqueness, tire starved glaze are even, highest quality, with countless changes, bright in luster colourful and be rich in gradation sense, show better crystalline glaze and entered that kiln is of the same colour, unique quality of kiln discharge ten thousand coloured silks, effectively promoted the artistic value of ceramic product and appreciate space.
The second, sintering curve of the present invention can expand the maturing range of crystalline glaze effectively, has broken through the technical bottleneck that crystalline glaze maturing temperature is narrow, crystalline range is narrow, makes crystalline glaze as other glaze, realize suitability for industrialized production, improves yield rate.
Embodiment
Implement time of the present invention, according to can not color demand, from golden yellow cosmetic soil, fruit green cosmetic soil, pink cosmetic soil, choosing any one kind of them be respectively used in combination with crystallization glaze and realizes the crystalline substance flower of different colours.
Embodiment 1: make golden yellow brilliant flower, select golden yellow cosmetic soil.
The weight that weighs each raw material in albite 16, potassium felspar sand 20, quartz 24, the ratio of washing mud 3, calcite 12, barium carbonate 8, zinc oxide 13, titanium dioxide 4 is mixed, ball milling 30 hours, fineness is 325 mesh screen residues to 0.03, then after blowing mistake 200 mesh sieves and deironing, makes crystallization glaze for subsequent use; Weighing in the ratio of praseodymium yellow 5, vanadium zirconium Huang 5, finished product mud 100 after fully mixing in hollander after the weight of each raw material becomes golden yellow cosmetic soil for subsequent use; Golden yellow cosmetic soil is imposed on white sun-dried mud brick, wait for its dry after, then impose on crystalline glaze, glaze layer thickness is controlled at 1mm; Sintering curve is: first stage heat temperature raising, rise to 850 ℃ with 2.5 hours from room temperature, and 850 ℃ rose to 1090 ℃ with 2 hours, and 1090 ℃ rose to 1280 ℃ with 0.8 hour; Subordinate phase cools, and is down to 1100 ℃ with 0.8 hour from the highest temperature, is then incubated 4 hours, finally naturally cools to room temperature.
Embodiment 2: make the brilliant flower of fruit green, select fruit green cosmetic soil.
The weight that weighs each raw material in albite 16, potassium felspar sand 20, quartz 24, the ratio of washing mud 3, calcite 12, barium carbonate 8, zinc oxide 13, titanium dioxide 4 is mixed, ball milling 30 hours, fineness is 325 mesh screen residues to 0.03, then after blowing mistake 200 mesh sieves and deironing, makes crystallization glaze for subsequent use; Weighing in the ratio of vanadium zirconium blue 2, praseodymium yellow 6, finished product mud 100 after fully mixing in hollander after the weight of each raw material becomes golden yellow cosmetic soil for subsequent use; Golden yellow cosmetic soil is imposed on white sun-dried mud brick, wait for its dry after, then impose on crystalline glaze, glaze layer thickness is controlled at 1mm; Sintering curve is: first stage heat temperature raising, rise to 850 ℃ with 2.5 hours from room temperature, and 850 ℃ rose to 1090 ℃ with 2 hours, and 1090 ℃ rose to 1280 ℃ with 0.8 hour; Subordinate phase cools, and is down to 1100 ℃ with 0.8 hour from the highest temperature, is then incubated 4 hours, finally naturally cools to room temperature.
Embodiment 3: make the brilliant flower of pink, select pink cosmetic soil.
The weight that weighs each raw material in albite 16, potassium felspar sand 20, quartz 24, the ratio of washing mud 3, calcite 12, barium carbonate 8, zinc oxide 13, titanium dioxide 4 is mixed, ball milling 30 hours, fineness is 325 mesh screen residues to 0.03, then after blowing mistake 200 mesh sieves and deironing, makes crystallization glaze for subsequent use; Weighing in the ratio of manganese red 8, finished product mud 100 after fully mixing in hollander after the weight of each raw material becomes golden yellow cosmetic soil for subsequent use; Golden yellow cosmetic soil is imposed on white sun-dried mud brick, wait for its dry after, then impose on crystalline glaze, glaze layer thickness is controlled at 1mm; Sintering curve is: first stage heat temperature raising, rise to 850 ℃ with 2.5 hours from room temperature, and 850 ℃ rose to 1090 ℃ with 2 hours, and 1090 ℃ rose to 1280 ℃ with 0.8 hour; Subordinate phase cools, and is down to 1100 ℃ with 0.8 hour from the highest temperature, is then incubated 4 hours, finally naturally cools to room temperature.
Claims (4)
1. a making method for the brilliant flower of white background color crystalline glaze, is characterized in that:
(1) preparation of crystallization glaze: the weight that weighs each raw material in albite 12-20, potassium felspar sand 16-26, quartzy 23-33, the ratio of washing mud 2-4, calcite 8-15, barium carbonate 6-10, zinc oxide 20-3, titanium dioxide 4-10 is mixed, ball milling 28-32 hour, fineness be 325 mesh screen residues to 0.02-0.04, then blowing cross 200 mesh sieves and deironing;
(2) preparation of cosmetic soil, any in can be respectively below three kinds according to the difference of color:
1. golden yellow cosmetic soil: weigh after fully mixing in hollander after the weight of each raw material for subsequent use in the ratio of the yellow 4-7 of praseodymium yellow 4-7, vanadium zirconium, finished product mud 100;
2. fruit green cosmetic soil: weigh after fully mixing in hollander after the weight of each raw material for subsequent use in the ratio of vanadium zirconium blue 1-3, praseodymium yellow 5-8, finished product mud 100;
3. pink cosmetic soil: weigh after fully mixing in hollander after the weight of each raw material for subsequent use in the ratio of manganese red 6-9, finished product mud 100;
(3) cosmetic soil is imposed on white sun-dried mud brick, wait for its dry after, then impose on crystalline glaze, glaze layer thickness is controlled at 0.9-1.1mm;
(4) sintering curve is: first stage heat temperature raising, rise to 850 ℃ with 2.5 hours from room temperature, and 850 ℃ rose to 1080-1100 ℃ with 2 hours, and 1080-1100 ℃ rises to 1260-1300 ℃ with 0.5-1 hour; Subordinate phase cools, and is down to 1150-1050 ℃ with 0.5-1 hour from the highest temperature, is then incubated 3-5 hour, finally naturally cools to room temperature.
2. the making method of the brilliant flower of a kind of white background color according to claim 1 crystalline glaze, it is characterized in that: the weight that weighs each raw material in albite 16, potassium felspar sand 20, quartz 24, the ratio of washing mud 3, calcite 12, barium carbonate 8, zinc oxide 13, titanium dioxide 4 is mixed, ball milling 30 hours, fineness is 325 mesh screen residues to 0.03, then after blowing mistake 200 mesh sieves and deironing, makes crystallization glaze for subsequent use; Weighing in the ratio of praseodymium yellow 5, vanadium zirconium Huang 5, finished product mud 100 after fully mixing in hollander after the weight of each raw material becomes golden yellow cosmetic soil for subsequent use; Golden yellow cosmetic soil is imposed on white sun-dried mud brick, wait for its dry after, then impose on crystalline glaze, glaze layer thickness is controlled at 1mm; Sintering curve is: first stage heat temperature raising, rise to 850 ℃ with 2.5 hours from room temperature, and 850 ℃ rose to 1090 ℃ with 2 hours, and 1090 ℃ rose to 1280 ℃ with 0.8 hour; Subordinate phase cools, and is down to 1100 ℃ with 0.8 hour from the highest temperature, is then incubated 4 hours, finally naturally cools to room temperature.
3. the making method of the brilliant flower of a kind of white background color according to claim 1 crystalline glaze, it is characterized in that: the weight that weighs each raw material in albite 16, potassium felspar sand 20, quartz 24, the ratio of washing mud 3, calcite 12, barium carbonate 8, zinc oxide 13, titanium dioxide 4 is mixed, ball milling 30 hours, fineness is 325 mesh screen residues to 0.03, then after blowing mistake 200 mesh sieves and deironing, makes crystallization glaze for subsequent use; Weighing in the ratio of vanadium zirconium blue 2, praseodymium yellow 6, finished product mud 100 after fully mixing in hollander after the weight of each raw material becomes golden yellow cosmetic soil for subsequent use; Golden yellow cosmetic soil is imposed on white sun-dried mud brick, wait for its dry after, then impose on crystalline glaze, glaze layer thickness is controlled at 1mm; Sintering curve is: first stage heat temperature raising, rise to 850 ℃ with 2.5 hours from room temperature, and 850 ℃ rose to 1090 ℃ with 2 hours, and 1090 ℃ rose to 1280 ℃ with 0.8 hour; Subordinate phase cools, and is down to 1100 ℃ with 0.8 hour from the highest temperature, is then incubated 4 hours, finally naturally cools to room temperature.
4. the making method of the brilliant flower of a kind of white background color according to claim 1 crystalline glaze, it is characterized in that: the weight that weighs each raw material in albite 16, potassium felspar sand 20, quartz 24, the ratio of washing mud 3, calcite 12, barium carbonate 8, zinc oxide 13, titanium dioxide 4 is mixed, ball milling 30 hours, fineness is 325 mesh screen residues to 0.03, then after blowing mistake 200 mesh sieves and deironing, makes crystallization glaze for subsequent use; Weighing in the ratio of manganese red 8, finished product mud 100 after fully mixing in hollander after the weight of each raw material becomes golden yellow cosmetic soil for subsequent use; Golden yellow cosmetic soil is imposed on white sun-dried mud brick, wait for its dry after, then impose on crystalline glaze, glaze layer thickness is controlled at 1mm; Sintering curve is: first stage heat temperature raising, rise to 850 ℃ with 2.5 hours from room temperature, and 850 ℃ rose to 1090 ℃ with 2 hours, and 1090 ℃ rose to 1280 ℃ with 0.8 hour; Subordinate phase cools, and is down to 1100 ℃ with 0.8 hour from the highest temperature, is then incubated 4 hours, finally naturally cools to room temperature.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210481447.6A CN103833418A (en) | 2012-11-23 | 2012-11-23 | Making method of white-ground colored crystal flower crystal glaze |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210481447.6A CN103833418A (en) | 2012-11-23 | 2012-11-23 | Making method of white-ground colored crystal flower crystal glaze |
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| CN103833418A true CN103833418A (en) | 2014-06-04 |
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| CN201210481447.6A Pending CN103833418A (en) | 2012-11-23 | 2012-11-23 | Making method of white-ground colored crystal flower crystal glaze |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109734320A (en) * | 2019-03-27 | 2019-05-10 | 佛山市利德嘉陶瓷制釉有限公司 | A kind of plasticity effect is good and the manufacture craft for convenient ceramic wall and floor bricks colorful crystal glazes of painting |
| CN109987843A (en) * | 2019-04-24 | 2019-07-09 | 广东省大埔陶瓷工业研究所 | A method of it carrying out zinc silicate positioning on ceramic flat surface and crystallizes and prepare ceramics |
| CN111018566A (en) * | 2019-12-18 | 2020-04-17 | 江苏省宜兴彩陶工艺厂 | Silk-like emerald flow kiln-change fancy glaze ceramic container and preparation method thereof |
| CN111362725A (en) * | 2020-03-18 | 2020-07-03 | 湖南陶润会文化传播有限公司 | Green-bottom crystal glaze and preparation method thereof |
-
2012
- 2012-11-23 CN CN201210481447.6A patent/CN103833418A/en active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109734320A (en) * | 2019-03-27 | 2019-05-10 | 佛山市利德嘉陶瓷制釉有限公司 | A kind of plasticity effect is good and the manufacture craft for convenient ceramic wall and floor bricks colorful crystal glazes of painting |
| CN109987843A (en) * | 2019-04-24 | 2019-07-09 | 广东省大埔陶瓷工业研究所 | A method of it carrying out zinc silicate positioning on ceramic flat surface and crystallizes and prepare ceramics |
| CN109987843B (en) * | 2019-04-24 | 2022-03-15 | 广东省大埔陶瓷工业研究所 | Method for performing zinc silicate positioning crystallization on ceramic plane and preparing ceramic |
| CN111018566A (en) * | 2019-12-18 | 2020-04-17 | 江苏省宜兴彩陶工艺厂 | Silk-like emerald flow kiln-change fancy glaze ceramic container and preparation method thereof |
| CN111362725A (en) * | 2020-03-18 | 2020-07-03 | 湖南陶润会文化传播有限公司 | Green-bottom crystal glaze and preparation method thereof |
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Application publication date: 20140604 |