CN103815144B - Mycotoxin removal feed additive for pigs - Google Patents

Mycotoxin removal feed additive for pigs Download PDF

Info

Publication number
CN103815144B
CN103815144B CN201410094915.3A CN201410094915A CN103815144B CN 103815144 B CN103815144 B CN 103815144B CN 201410094915 A CN201410094915 A CN 201410094915A CN 103815144 B CN103815144 B CN 103815144B
Authority
CN
China
Prior art keywords
powder
ultramicro
part
refining
crab shell
Prior art date
Application number
CN201410094915.3A
Other languages
Chinese (zh)
Other versions
CN103815144A (en
Inventor
王勇飞
栾兆双
张承勇
Original Assignee
双胞胎(集团)股份有限公司
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 双胞胎(集团)股份有限公司 filed Critical 双胞胎(集团)股份有限公司
Priority to CN201410094915.3A priority Critical patent/CN103815144B/en
Publication of CN103815144A publication Critical patent/CN103815144A/en
Application granted granted Critical
Publication of CN103815144B publication Critical patent/CN103815144B/en

Links

Abstract

The invention discloses a mycotoxin removal feed additive for pigs, and belongs to the field of feed additives. The mycotoxin removal feed additive comprises the following raw materials: compound polysaccharides, refined crab shell powder, marigold residues, refined sugarcane residues, superfine ground alfalfa, superfine ground madder, superfine ground rhizoma smilacis glabrae and superfine ground medlar. According to the mycotoxin removal feed additive, mycotoxin in a feed can be effectively adsorbed, the growth of mildew can be inhibited, the mycotoxin can be prevented from being generated, the physiological influence of the mycotoxin on animals can be removed, the disease resistance of the animals can be improved, and the feed utilization rate can be remarkably increased. In addition, a production method of the additive is simple and convenient to operate.

Description

One boar detoxicating mycotoxin feed addictive

Technical field

The present invention relates to a kind of feed addictive, be specifically related to boar detoxicating mycotoxin feed addictive, belong to feed additive field.

Background technology

Mycotoxin is by mould or mycetogenetic poisonous and harmful substance, all can produce in the manufacture of the growth course of cereal, feed, storage and transportation.Worldwide, cereal and feed all also exist serious mycotoxin contamination.Mycotoxin not only can, cause the decline of its immunocompetence, reproductive performance obstacle, feed intake reduce and disease incident rise, even cause the death of livestock and poultry animal, also can be transferred to human body from animal by food chain.Some toxin can produce some toxin related compounds by metabolism in animal body, and these compounds also can produce injury through food chain to human body.Investigation result shows, and the ratio that China's feed and contamination of raw material mycotoxin exceed standard is up to 60-70%, and thus mycotoxin contamination is extremely general in China.

In recent years, mycotoxin brought huge economic loss to animal husbandry, and its harm is increasing, main manifestations is that immunity function suppresses, and premunition reduces, and feed intake reduces, the speed of growth is slow, the hematopoiesis function of hemopoietic system, the physiological function damage of internal organs, neural and endocrine disturbance, carcinogenic teratogenesis, genital disorders is as precocity, false heat, miscarriage etc., and suckling pig is had loose bowels, laying hen egg yield declines, milk quality reductions etc., therefore Mycotoxins in Feed, have the title of " stealthy killer ".Usually, the pollution of Mycotoxins in Feed is not the composite pollution of single a kind of mycotoxin but multiple toxin, and the synergy of multiple mycotoxin often makes its toxicity strengthen, and causes more serious infringement.Therefore, feed mold problem is very important and problem demanding prompt solution in feed industry and Animal husbandry production, and mycotoxin contamination problem causes extensive concern.

At present, the prevention and controls commonly used mycotoxin adds de-mould dose in feed.De-mould dose of conventional kind has clay class, yeast cell wall class, microbiology class, enzymolysis class and Chinese herbal medicine class etc.But a kind of single method also exists defect and drawback, the harm of mycotoxin effectively can not be contained; Although market also there are some composite parts take off mould dose, act on single, result of use also differs larger.

Therefore be necessary to strengthen the Study and Development that highly effective and safe takes off mould dose, to animal husbandry and food security, there is very important application.

Summary of the invention

The object of this invention is to provide boar detoxicating mycotoxin feed addictive, effectively can remove the mycotoxin in feedstuff and feed, the generation of the various diseases preventing livestock and poultry from causing because of domestic fungus endotoxin contamination feed, ensures health, the safety of cultivated animals.

The present invention is achieved through the following technical solutions:

One boar detoxicating mycotoxin feed addictive, is made up of following raw materials by weight portion: complex polysaccharide 8-16 part, refining crab shell powder 6-18 part, marigold residue 6-14 part, refining bagasse 4-12 part, clover Ultramicro-powder 2-8 part, madder Ultramicro-powder mince 2-6 part, matrimony vine Ultramicro-powder of 3-6 part, smilax Ultramicro-powder that mince that mince minces 3-8 part;

Described complex polysaccharide by Auricularia polysaccharide, LBP-X, bark of official magnolia polysaccharide and moutan bark polysaccharide in mass ratio 2-5:1-4:3-6:1-3 form;

Preferably, one boar detoxicating mycotoxin feed addictive, is made up of following raw materials by weight portion: complex polysaccharide 12-14 part, refining crab shell powder 6-18 part, marigold residue 6-14 part, refining bagasse 4-12 part, clover Ultramicro-powder 2-8 part, madder Ultramicro-powder mince 2-6 part, matrimony vine Ultramicro-powder of 3-6 part, smilax Ultramicro-powder that mince that mince minces 3-8 part;

Described complex polysaccharide by Auricularia polysaccharide, LBP-X, bark of official magnolia polysaccharide and moutan bark polysaccharide in mass ratio 2-5:1-4:3-6:1-3 form;

The preparation method of described refining crab shell powder is: cleaned up by crab shell, dry, pulverize 30 mesh sieves, obtain crab shell powder; Crab shell powder is put in sterilizing 30-60 minute under 125-130 DEG C of condition, by solid-to-liquid ratio 1:(4-6 after sterilizing terminates) add the ethanol of 50-55%, boiling 1-2 hour under 50-70 DEG C of condition, filter, by filter residue and drying, then by solid-to-liquid ratio 1:(3-5) add the sodium chloride solution of 15-20%, 2-4 days is soaked under 20-25 DEG C of condition, immersion terminates rear filtration, by filter residue and drying, pulverizes 60 mesh sieves and namely obtains refining crab shell powder;

Described marigold residue is the byproduct after marigold extracts lutein, is dried pulverizing, crosses 60 mesh sieves;

The preparation method of described refining bagasse is: after sugar cane crushing, get bagasse, add distilled water by solid-to-liquid ratio 1:5-10, soaks 1-2h, filters, gets filter residue; Filter residue 100 DEG C of steam are steamed 1-2h, carries out drying after having steamed, make its water content lower than 20%, pulverize, cross 30 mesh sieves; In the bagasse after pulverizing, add the ethanol of 55-75% by solid-to-liquid ratio 1:4-8, at 45-60 DEG C, boil 2-4h, filter, get filter residue, by filter residue and drying, make its water content lower than 12%, pulverize, cross 60 mesh sieves, obtain refining bagasse;

The preparation method that described clover Ultramicro-powder minces is: clover is dry, adopts ultramicro grinding;

The preparation method that described madder Ultramicro-powder minces is: madder is dry, adopts ultramicro grinding;

The preparation method that described smilax Ultramicro-powder minces is: smilax is dry, adopts ultramicro grinding;

The preparation method that described matrimony vine Ultramicro-powder minces is: matrimony vine is dry, adopts ultramicro grinding;

Present invention also offers the preparation method of this feed mycotoxin detoxification agent, it comprises the steps:

(1) raw material is taken according to following weight portion: complex polysaccharide 8-16 part, refining crab shell powder 6-18 part, marigold residue 6-14 part, refining bagasse 4-12 part, clover Ultramicro-powder 2-8 part, madder Ultramicro-powder mince 2-6 part, matrimony vine Ultramicro-powder of 3-6 part, smilax Ultramicro-powder that mince that mince minces 3-8 part;

(2) complex polysaccharide is mixed with marigold residue, refining bagasse, stand-by;

(3) minced by clover Ultramicro-powder, madder Ultramicro-powder minces, smilax Ultramicro-powder minces and matrimony vine Ultramicro-powder minces mixes, at 50-60 DEG C, temperature fries 1-1.5h, stand-by;

(4) gains in (2) and (3) are mixed with refining crab shell powder, get product.

Boar detoxicating mycotoxin feed addictive in the present invention, its addition in feed is 600-1000 gram/ton.

Beneficial effect

Additive of the present invention adopts rational component to prepare, can mycotoxin effectively in adsorption feed as aflatoxin, zearalenone, vomitoxin, T-2 toxin, FT and conspicuous aspertoxin etc., simultaneously can also the growth of mould fungus inhibition, prevent the generation of mycotoxin, eliminate mycotoxin to the impact of animal physiological, improve animal to the resistance of disease, can the price of deed be significantly improved.And the production method of additive of the present invention is simple, easy to operate.Additive component of the present invention is natural products, has the feature such as safety, nutrition in addition, meets the needs of animal husbandry development.

Specific embodiment

By the following specific examples further illustrate the invention.

Embodiment 1

One boar detoxicating mycotoxin feed addictive, is made up of following raw materials by weight portion: complex polysaccharide 8 parts, refining 6 parts, crab shell powder, marigold residue 6 parts, refining bagasse 4 parts, clover Ultramicro-powder mince 2 parts, madder Ultramicro-powder mince 3 parts, smilax Ultramicro-powder mince 2 parts, matrimony vine Ultramicro-powder minces 3 parts;

Described complex polysaccharide by Auricularia polysaccharide, LBP-X, bark of official magnolia polysaccharide and moutan bark polysaccharide in mass ratio 2:1:3:1 form;

The preparation method of described refining crab shell powder is: cleaned up by crab shell, dry, pulverize 30 mesh sieves, obtain crab shell powder; Crab shell powder to be put under 125 DEG C of conditions sterilizing 30 minutes, add the ethanol of 50% by solid-to-liquid ratio 1:4 after sterilizing terminates, boiling 1 hour under 50 DEG C of conditions, filter, by filter residue and drying, then add the sodium chloride solution of 15% by solid-to-liquid ratio 1:3, soak 2 days under 20 DEG C of conditions, immersion terminates rear filtration, by filter residue and drying, pulverizes 60 mesh sieves and namely obtains refining crab shell powder;

Described marigold residue is the byproduct after marigold extracts lutein, is dried pulverizing, crosses 60 mesh sieves;

The preparation method of described refining bagasse is: after sugar cane crushing, get bagasse, add distilled water by solid-to-liquid ratio 1:5, soaks 1h, filters, gets filter residue; Filter residue 100 DEG C of steam are steamed 1h, carries out drying after having steamed, make its water content lower than 20%, pulverize, cross 30 mesh sieves; In the bagasse after pulverizing, add the ethanol of 55% by solid-to-liquid ratio 1:4, at 45 DEG C, boil 2h, filter, get filter residue, by filter residue and drying, make its water content lower than 12%, pulverize, cross 60 mesh sieves, obtain refining bagasse;

The preparation method that described clover Ultramicro-powder minces is: clover is dry, adopts ultramicro grinding;

The preparation method that described madder Ultramicro-powder minces is: madder is dry, adopts ultramicro grinding;

The preparation method that described smilax Ultramicro-powder minces is: smilax is dry, adopts ultramicro grinding;

The preparation method that described matrimony vine Ultramicro-powder minces is: matrimony vine is dry, adopts ultramicro grinding;

Present invention also offers the preparation method of this feed mycotoxin detoxification agent, it comprises the steps:

(1) take raw material according to following weight portion: complex polysaccharide 8 parts, refining 6 parts, crab shell powder, marigold residue 6 parts, refining bagasse 4 parts, clover Ultramicro-powder mince 2 parts, madder Ultramicro-powder mince 3 parts, smilax Ultramicro-powder mince 2 parts, matrimony vine Ultramicro-powder minces 3 parts;

(2) complex polysaccharide is mixed with marigold residue, refining bagasse, stand-by;

(3) minced by clover Ultramicro-powder, madder Ultramicro-powder minces, smilax Ultramicro-powder minces and matrimony vine Ultramicro-powder minces mixes, at 50 DEG C, temperature fries 1h, stand-by;

(4) gains in (2) and (3) are mixed with refining crab shell powder, get product.

Boar detoxicating mycotoxin feed addictive in the present invention, its addition in feed is 600 grams/ton.

Embodiment 2

One boar detoxicating mycotoxin feed addictive, is made up of following raw materials by weight portion: complex polysaccharide 12 parts, refining 12 parts, crab shell powder, marigold residue 10 parts, refining bagasse 8 parts, clover Ultramicro-powder mince 5 parts, madder Ultramicro-powder mince 5 parts, smilax Ultramicro-powder mince 4 parts, matrimony vine Ultramicro-powder minces 6 parts;

Described complex polysaccharide by Auricularia polysaccharide, LBP-X, bark of official magnolia polysaccharide and moutan bark polysaccharide in mass ratio 3:3:5:2 form;

The preparation method of described refining crab shell powder is: cleaned up by crab shell, dry, pulverize 30 mesh sieves, obtain crab shell powder; Crab shell powder to be put under 127 DEG C of conditions sterilizing 45 minutes, add the ethanol of 53% by solid-to-liquid ratio 1:5 after sterilizing terminates, boiling 1.5 hours under 60 DEG C of conditions, filter, by filter residue and drying, then add the sodium chloride solution of 18% by solid-to-liquid ratio 1:4, soak 3 days under 23 DEG C of conditions, immersion terminates rear filtration, by filter residue and drying, pulverizes 60 mesh sieves and namely obtains refining crab shell powder;

Described marigold residue is the byproduct after marigold extracts lutein, is dried pulverizing, crosses 60 mesh sieves;

The preparation method of described refining bagasse is: after sugar cane crushing, get bagasse, add distilled water by solid-to-liquid ratio 1:8, soaks 1.5h, filters, gets filter residue; Filter residue 100 DEG C of steam are steamed 1.5h, carries out drying after having steamed, make its water content lower than 20%, pulverize, cross 30 mesh sieves; In the bagasse after pulverizing, add the ethanol of 65% by solid-to-liquid ratio 1:6, at 55 DEG C, boil 3h, filter, get filter residue, by filter residue and drying, make its water content lower than 12%, pulverize, cross 60 mesh sieves, obtain refining bagasse;

The preparation method that described clover Ultramicro-powder minces is: clover is dry, adopts ultramicro grinding;

The preparation method that described madder Ultramicro-powder minces is: madder is dry, adopts ultramicro grinding;

The preparation method that described smilax Ultramicro-powder minces is: smilax is dry, adopts ultramicro grinding;

The preparation method that described matrimony vine Ultramicro-powder minces is: matrimony vine is dry, adopts ultramicro grinding;

Present invention also offers the preparation method of this feed mycotoxin detoxification agent, it comprises the steps:

(1) take raw material according to following weight portion: complex polysaccharide 12 parts, refining 12 parts, crab shell powder, marigold residue 10 parts, refining bagasse 8 parts, clover Ultramicro-powder mince 5 parts, madder Ultramicro-powder mince 5 parts, smilax Ultramicro-powder mince 4 parts, matrimony vine Ultramicro-powder minces 6 parts;

(2) complex polysaccharide is mixed with marigold residue, refining bagasse, stand-by;

(3) minced by clover Ultramicro-powder, madder Ultramicro-powder minces, smilax Ultramicro-powder minces and matrimony vine Ultramicro-powder minces mixes, at 55 DEG C, temperature fries 1.3h, stand-by;

(4) gains in (2) and (3) are mixed with refining crab shell powder, get product.

Boar detoxicating mycotoxin feed addictive in the present invention, its addition in feed is 800 grams/ton.

Embodiment 3

One boar detoxicating mycotoxin feed addictive, is made up of following raw materials by weight portion: complex polysaccharide 16 parts, refining 18 parts, crab shell powder, marigold residue 14 parts, refining bagasse 12 parts, clover Ultramicro-powder mince 8 parts, madder Ultramicro-powder mince 6 parts, smilax Ultramicro-powder mince 6 parts, matrimony vine Ultramicro-powder minces 8 parts;

Described complex polysaccharide by Auricularia polysaccharide, LBP-X, bark of official magnolia polysaccharide and moutan bark polysaccharide in mass ratio 5:4:6:3 form;

The preparation method of described refining crab shell powder is: cleaned up by crab shell, dry, pulverize 30 mesh sieves, obtain crab shell powder; Crab shell powder to be put under 130 DEG C of conditions sterilizing 60 minutes, add the ethanol of 55% by solid-to-liquid ratio 1:6 after sterilizing terminates, boiling 2 hours under 70 DEG C of conditions, filter, by filter residue and drying, then add the sodium chloride solution of 20% by solid-to-liquid ratio 1:5, soak 4 days under 25 DEG C of conditions, immersion terminates rear filtration, by filter residue and drying, pulverizes 60 mesh sieves and namely obtains refining crab shell powder;

Described marigold residue is the byproduct after marigold extracts lutein, is dried pulverizing, crosses 60 mesh sieves;

The preparation method of described refining bagasse is: after sugar cane crushing, get bagasse, add distilled water by solid-to-liquid ratio 1:10, soaks 2h, filters, gets filter residue; Filter residue 100 DEG C of steam are steamed 2h, carries out drying after having steamed, make its water content lower than 20%, pulverize, cross 30 mesh sieves; In the bagasse after pulverizing, add the ethanol of 75% by solid-to-liquid ratio 1:8, at 60 DEG C, boil 4h, filter, get filter residue, by filter residue and drying, make its water content lower than 12%, pulverize, cross 60 mesh sieves, obtain refining bagasse;

The preparation method that described clover Ultramicro-powder minces is: clover is dry, adopts ultramicro grinding;

The preparation method that described madder Ultramicro-powder minces is: madder is dry, adopts ultramicro grinding;

The preparation method that described smilax Ultramicro-powder minces is: smilax is dry, adopts ultramicro grinding;

The preparation method that described matrimony vine Ultramicro-powder minces is: matrimony vine is dry, adopts ultramicro grinding;

Present invention also offers the preparation method of this feed mycotoxin detoxification agent, it comprises the steps:

(1) take raw material according to following weight portion: complex polysaccharide 16 parts, refining 18 parts, crab shell powder, marigold residue 14 parts, refining bagasse 12 parts, clover Ultramicro-powder mince 8 parts, madder Ultramicro-powder mince 6 parts, smilax Ultramicro-powder mince 6 parts, matrimony vine Ultramicro-powder minces 8 parts;

(2) complex polysaccharide is mixed with marigold residue, refining bagasse, stand-by;

(3) minced by clover Ultramicro-powder, madder Ultramicro-powder minces, smilax Ultramicro-powder minces and matrimony vine Ultramicro-powder minces mixes, at 60 DEG C, temperature fries 1.5h, stand-by;

(4) gains in (2) and (3) are mixed with refining crab shell powder, get product.

Boar detoxicating mycotoxin feed addictive in the present invention, its addition in feed is 1000 grams/ton.

Embodiment 4 product result of use one

Carry out the embodiment of the present invention 2 feed mycotoxin detoxification agent to test the detoxification efficiency of mycotoxin in laboratory, and select certain brand mold toxin sorbent commercially available as a control group.Mycotoxin is respectively zearalenone, AFB1 (AFB1), vomitoxin, T-2 toxin, fumonisin B1, get centrifuge tube and add more than 10ml mycotoxin standard liquid (specifically in table 1), in centrifuge tube, add feed mycotoxin detoxification agent sample 25mg of the present invention again, make detoxification sample concentration in the solution be 2.5mg/ml.Arrange blank group (not adding detoxifying agent) and control group (certain brand mold toxin sorbent commercially available), all samples establishes 2 repetitions simultaneously.All samples adsorbs 2h with 150r/min vibration in 37 DEG C of water bath with thermostatic control oscillators.Then, with the centrifugal 10min of 3000r/min, collect supernatant, measure the content of each mycotoxin in supernatant.By following formulae discovery adsorbance Q (ng/mg) and adsorption rate Y (%).Then in residue, add the PBS cushioning liquid of 10ml pH 7.0, in 37 DEG C, vibrate in the constant temperature oscillation water-bath of 150r/min desorb 30min, the centrifugal 10min of 3000r/min, collects supernatant, and the same method measures the content of each mycotoxin in supernatant.Accumulation desorption efficiency R (%) is asked after correcting with control group.

Formula one Q=V (C0-C1)/M

Formula two Y=100 × (C0-C1)/C0

Formula three R=C2/ (C0-C1) × 100%

Wherein: V is the volume (ml) of solution; M is the consumption (mg) of feed mycotoxin detoxification agent of the present invention; C0 is the concentration (ng/ml) of each mycotoxin before absorption; C1 is the concentration (ng/ml) of each mycotoxin after absorption; C2 is the concentration (ng/ml) of each mycotoxin after desorb.

Measuring result is specifically in table 1.Result shows that feed mycotoxin detoxification agent of the present invention is all fine to the removal effect of zearalenone, AFB1, vomitoxin, T-2 toxin, fumonisin B1, and is combined with toxin closely, and detoxification is more thorough.The successful of product of the present invention is better than the removal effect of commercially available mold toxin sorbent to each mycotoxin in addition.

Embodiment 5 product result of use two

The embodiment of the present invention 2 feed addictive result of use is tested.

Test method: select twins (group) limited company subordinate pig farm, select age in days, healthy sow that body weight is close, piglet and each 80 of growing and fattening pigs, be divided into all at random 2 groups (test group and control groups), test group add 800 grams of embodiments 2 obtained invention product, control group does not add product of the present invention; Feed continuously 60 days; Daily observation and detection are carried out to test pig.

Compared with control group, use invention feed addictive can obtain following effect:

(1) number born of sow on average increases by 0.8, and piglet Birth weight on average increases 15-20%g;

(2) sow produces mummy, stillborn foetus, weak young number minimizing more than 40%;

(3), before and after childbirth, prevention of sow constipation number of times reduces 30-40%;

(4) the diarrhea rate test group of piglet fewer than control group more than 30%;

(5) feed intake of growing and fattening pigs test group pig comparatively control group obviously increases, and about increases by 10%;

(6) growing and fattening pigs test group adds more than 10% than the weight average of control group;

(7) stink of the column home of test group is obviously light than control group.

Claims (5)

1. boar detoxicating mycotoxin feed addictive, is characterized in that being made up of following raw materials by weight portion: complex polysaccharide 8-16 part, refining crab shell powder 6-18 part, marigold residue 6-14 part, refining bagasse 4-12 part, clover Ultramicro-powder 2-8 part, madder Ultramicro-powder mince 2-6 part, matrimony vine Ultramicro-powder of 3-6 part, smilax Ultramicro-powder that mince that mince minces 3-8 part;
Described complex polysaccharide by Auricularia polysaccharide, LBP-X, bark of official magnolia polysaccharide and moutan bark polysaccharide in mass ratio
2-5:1-4:3-6:1-3 forms;
The preparation method of described refining crab shell powder is: cleaned up by crab shell, dry, pulverize 30 mesh sieves, obtain crab shell powder; Crab shell powder is put in sterilizing 30-60 minute under 125-130 DEG C of condition, by solid-to-liquid ratio 1:(4-6 after sterilizing terminates) add the ethanol of 50-55%, boiling 1-2 hour under 50-70 DEG C of condition, filter, by filter residue and drying, then by solid-to-liquid ratio 1:(3-5) add the sodium chloride solution of 15-20%, 2-4 days is soaked under 20-25 DEG C of condition, immersion terminates rear filtration, by filter residue and drying, pulverizes 60 mesh sieves and namely obtains refining crab shell powder;
The preparation method of described refining bagasse is: after sugar cane crushing, get bagasse, add distilled water by solid-to-liquid ratio 1:5-10, soaks 1-2h, filters, gets filter residue; Filter residue 100 DEG C of steam are steamed 1-2h, carries out drying after having steamed, make its water content lower than 20%, pulverize, cross 30 mesh sieves; In the bagasse after pulverizing, add the ethanol of 55-75% by solid-to-liquid ratio 1:4-8, at 45-60 DEG C, boil 2-4h, filter, get filter residue, by filter residue and drying, make its water content lower than 12%, pulverize, cross 60 mesh sieves, obtain refining bagasse.
2. boar detoxicating mycotoxin feed addictive according to claim 1, is characterized in that being made up of following raw materials by weight portion: complex polysaccharide 12-14 part, refining crab shell powder 6-18 part, marigold residue 6-14 part, refining bagasse 4-12 part, clover Ultramicro-powder 2-8 part, madder Ultramicro-powder mince 2-6 part, matrimony vine Ultramicro-powder of 3-6 part, smilax Ultramicro-powder that mince that mince minces 3-8 part;
Described complex polysaccharide by Auricularia polysaccharide, LBP-X, bark of official magnolia polysaccharide and moutan bark polysaccharide in mass ratio 2-5:1-4:3-6:1-3 form.
3. boar detoxicating mycotoxin feed addictive according to claim 1, is characterized in that being made up of following raw materials by weight portion: complex polysaccharide 12 parts, refining 12 parts, crab shell powder, marigold residue 10 parts, refining bagasse 8 parts, clover Ultramicro-powder mince 5 parts, madder Ultramicro-powder mince 5 parts, smilax Ultramicro-powder mince 4 parts, matrimony vine Ultramicro-powder minces 6 parts;
Described complex polysaccharide by Auricularia polysaccharide, LBP-X, bark of official magnolia polysaccharide and moutan bark polysaccharide in mass ratio 3:3:5:2 form;
The preparation method of described refining crab shell powder is: cleaned up by crab shell, dry, pulverize 30 mesh sieves, obtain crab shell powder; Crab shell powder to be put under 127 DEG C of conditions sterilizing 45 minutes, add the ethanol of 53% by solid-to-liquid ratio 1:5 after sterilizing terminates, boiling 1.5 hours under 60 DEG C of conditions, filter, by filter residue and drying, then add the sodium chloride solution of 18% by solid-to-liquid ratio 1:4, soak 3 days under 23 DEG C of conditions, immersion terminates rear filtration, by filter residue and drying, pulverizes 60 mesh sieves and namely obtains refining crab shell powder;
The preparation method of described refining bagasse is: after sugar cane crushing, get bagasse, add distilled water by solid-to-liquid ratio 1:8, soaks 1.5h, filters, gets filter residue; Filter residue 100 DEG C of steam are steamed 1.5h, carries out drying after having steamed, make its water content lower than 20%, pulverize, cross 30 mesh sieves; In the bagasse after pulverizing, add the ethanol of 65% by solid-to-liquid ratio 1:6, at 55 DEG C, boil 3h, filter, get filter residue, by filter residue and drying, make its water content lower than 12%, pulverize, cross 60 mesh sieves, obtain refining bagasse.
4., according to the arbitrary described boar detoxicating mycotoxin feed addictive of claim 1-3, it is characterized in that described marigold residue is the byproduct after marigold extracts lutein.
5. boar detoxicating mycotoxin feed addictive according to claim 1, its spy is that its preparation method is:
(1) raw material is taken according to following weight portion: complex polysaccharide 8-16 part, refining crab shell powder 6-18 part, marigold residue 6-14 part, refining bagasse 4-12 part, clover Ultramicro-powder 2-8 part, madder Ultramicro-powder mince 2-6 part, matrimony vine Ultramicro-powder of 3-6 part, smilax Ultramicro-powder that mince that mince minces 3-8 part;
(2) complex polysaccharide is mixed with marigold residue, refining bagasse, stand-by;
(3) minced by clover Ultramicro-powder, madder Ultramicro-powder minces, smilax Ultramicro-powder minces and matrimony vine Ultramicro-powder minces mixes, at 50-60 DEG C, temperature fries 1-1.5h, stand-by;
(4) gains in (2) and (3) are mixed with refining crab shell powder, get product.
CN201410094915.3A 2014-03-17 2014-03-17 Mycotoxin removal feed additive for pigs CN103815144B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410094915.3A CN103815144B (en) 2014-03-17 2014-03-17 Mycotoxin removal feed additive for pigs

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201410094915.3A CN103815144B (en) 2014-03-17 2014-03-17 Mycotoxin removal feed additive for pigs

Publications (2)

Publication Number Publication Date
CN103815144A CN103815144A (en) 2014-05-28
CN103815144B true CN103815144B (en) 2015-03-25

Family

ID=50750673

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201410094915.3A CN103815144B (en) 2014-03-17 2014-03-17 Mycotoxin removal feed additive for pigs

Country Status (1)

Country Link
CN (1) CN103815144B (en)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104489408A (en) * 2014-12-30 2015-04-08 瑞金双胞胎饲料有限公司 Porcine feed additive for effectively improving intestinal health and enhancing immunity
CN106615643A (en) * 2016-09-28 2017-05-10 临沂大学 Antimycotoxicgenic feed additive for poultry as well as preparation method and application of antimycotoxicgenic feed additive
CN106615776A (en) * 2016-11-16 2017-05-10 临沂大学 Anti-mycotoxin feed additive for pigs as well as preparation method and application of anti-mycotoxin feed additive
CN106901137A (en) * 2016-12-31 2017-06-30 安徽宏亮饲料科技有限公司 A kind of detoxicating mycotoxin feed addictive
CN106942498A (en) * 2017-04-28 2017-07-14 巴马原种香猪农牧实业有限公司 A kind of efficient BaMa miniature pig feed for pregnant sows
CN107821823A (en) * 2017-12-01 2018-03-23 无为县雨露生态农业有限公司 Improve the pig detoxified feed additive of intestinal health

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1104047A (en) * 1993-12-22 1995-06-28 黄明和 High-efficient detoxifying agent for fried-flour cake
CN101669574A (en) * 2008-09-10 2010-03-17 陈健雄 Feed additive for detoxicating mycotoxin and production method thereof
CN103141685A (en) * 2013-03-12 2013-06-12 北京翰赛柯生物科技有限公司 Mycotoxin detoxication agent for swine feed
CN103583823A (en) * 2013-11-07 2014-02-19 北京大北农科技集团股份有限公司 Mold removal agent for feed and preparation method and feed additive thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1104047A (en) * 1993-12-22 1995-06-28 黄明和 High-efficient detoxifying agent for fried-flour cake
CN101669574A (en) * 2008-09-10 2010-03-17 陈健雄 Feed additive for detoxicating mycotoxin and production method thereof
CN103141685A (en) * 2013-03-12 2013-06-12 北京翰赛柯生物科技有限公司 Mycotoxin detoxication agent for swine feed
CN103583823A (en) * 2013-11-07 2014-02-19 北京大北农科技集团股份有限公司 Mold removal agent for feed and preparation method and feed additive thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
饲料中霉菌毒素与脱毒剂的研究进展;卢永红等;《种业研究》;20050930(第9期);46-49 *

Also Published As

Publication number Publication date
CN103815144A (en) 2014-05-28

Similar Documents

Publication Publication Date Title
CN103141710B (en) Compound feed for weaned pigs and preparation method of feed
CN103518992B (en) A kind of alfalfa chicken feed and preparation method thereof
CN103652479B (en) A kind of carp feed
CN104171725B (en) A kind of raising is laid eggs the Chinese medicine chicken feed of quality and processing method thereof
CN1219451C (en) Additive for farm animal feed
CN102318744B (en) Natural plant feed additive and preparation method thereof
CN100421575C (en) Anti-stress health-care agent for shrimp and crab
CN103704485A (en) Clarias fuscus feed and preparation method thereof
CN103518987B (en) Corn protein chicken feed and preparation method thereof
CN103478457B (en) Safe feed for truogx sinensis
CN104824346A (en) Compound pig feed and preparation method thereof
CN103960530B (en) A kind of put condition in a suitable place to breed under the ecological feed of traditional black pig fattening period
CN103262961B (en) Feed additive specially used for tilapia
CN103494001A (en) Laying hen forage and preparation method thereof
CN106071351A (en) A kind of feed of grass carp and preparation method thereof
CN101548728B (en) Chinese herbal medicine additive for improving meat quality of java tilapia
CN104286593B (en) A kind of silver carp rearing feed additive special
CN104543459A (en) Feeding method for producing high-quality goose meat
CN102845638B (en) Duck feed capable of preventing and treating avian influenza and Chinese herbal additive used therein
CN103494013A (en) Chinese toon forage for broilers and preparation method thereof
CN102028129A (en) Novel mycotoxin detoxification agent for feed and preparation method and feed additive thereof
CN103202411B (en) Compound feed for high-density cultivation of grass carps
CN102630816B (en) Camphor tree branch and leave extracting feed additive and preparation method thereof
CN102100318B (en) Chicken feed
CN102940131B (en) Novel mycotoxin detoxification agent and preparation method thereof

Legal Events

Date Code Title Description
PB01 Publication
C06 Publication
SE01 Entry into force of request for substantive examination
C10 Entry into substantive examination
GR01 Patent grant
C14 Grant of patent or utility model
EE01 Entry into force of recordation of patent licensing contract

Application publication date: 20140528

Assignee: Yichang twin Feed Co., Ltd.

Assignor: Twins (Group) Co., Ltd.

Contract record no.: 2015360000143

Denomination of invention: Mycotoxin removal feed additive for pigs

Granted publication date: 20150325

License type: Exclusive License

Record date: 20151117

LICC Enforcement, change and cancellation of record of contracts on the licence for exploitation of a patent or utility model
EC01 Cancellation of recordation of patent licensing contract

Assignee: Yichang twin Feed Co., Ltd.

Assignor: Twins (Group) Co., Ltd.

Contract record no.: 2015360000143

Date of cancellation: 20160321

LICC Enforcement, change and cancellation of record of contracts on the licence for exploitation of a patent or utility model
TR01 Transfer of patent right

Effective date of registration: 20160519

Address after: 525027 Guangdong Province, Maoming City Maogang District East sixteen

Patentee after: Maoming twin Feed Co., Ltd.

Address before: 330096 Nanchang high tech Zone, torch street, No. 999, twins group, Jiangxi

Patentee before: Twins (Group) Co., Ltd.

C41 Transfer of patent application or patent right or utility model