CN103788691A - Method for preparing and producing bright cyan wheat straw dye - Google Patents

Method for preparing and producing bright cyan wheat straw dye Download PDF

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CN103788691A
CN103788691A CN 201410074048 CN201410074048A CN103788691A CN 103788691 A CN103788691 A CN 103788691A CN 201410074048 CN201410074048 CN 201410074048 CN 201410074048 A CN201410074048 A CN 201410074048A CN 103788691 A CN103788691 A CN 103788691A
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wheat straw
solution
alum
dye
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CN 201410074048
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马文侠
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哈尔滨市工艺美术有限责任公司
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Abstract

The invention discloses a method for preparing and producing bright cyan wheat straw dye. According to the method, leaves and stalk of an indigo plant, echinacea flowers, hyacinth flowers, sericite powder, alum, an antimony ionic compound solution and mineral water are used as main raw materials. The main technological process of the production method comprises sorting, cutting, drying, soaking, boiling, mixing, settling, dyeing and forming of a finished product. The bright cyan wheat straw dye is purely natural, free of pollution, environmentally friendly, and free of toxic and side effects on a human body, and is made from purely natural plants through preparation.

Description

一种制备亮青色麦秸秆染料及生产方法 A process for preparing light cyan dyes and producing wheat straw

[0001] 技术领域: [0001] Technical Field:

本发明涉一种植物染料,特别是涉及一种制备亮青色麦稻杆染料及生产方法。 The present invention relates to a plant dyes, particularly cyan dyes and wheat and rice stems relates to a method for the preparation of light production.

[0002] 背景技术: [0002] BACKGROUND:

工艺美术是指日常生活用品经过艺术化处理以后,使之具有强烈的审美价值的产品。 Arts and Crafts daily necessities through means of art after treatment, so that it has a strong aesthetic value of the product. 我们一般把工艺美术分为实用工艺美术和陈设欣赏的工艺美术。 We generally put into practical Arts and Crafts Arts and Crafts furnishings and appreciation of arts and crafts. 实用工艺美术是整个工艺美术的主体和基础,包括衣、食、化、行、用的工艺品类,实用价值是这类工艺品的主要价值,审美价值是作为辅助价值存在的。 Arts and practical basis for the overall process is the subject of the art, including clothing, food, chemical, transportation, use of crafts, the main practical value of such crafts, aesthetic value is present as an auxiliary value. 这类工艺品包括经过装饰加工的茶餐具、灯具、木器家具、绣花制品、草竹编织品等。 Such crafts including refurbished processing of tea utensils, lamps, wood furniture, embroidered products, such as bamboo weaving grass. 陈设欣赏工艺品是指那些以摆设、观赏功能为主的工艺品,这类工艺品以审美为其首要价值,手工技艺性很强,如玉器、金银首饰、象牙雕刻、景泰蓝、漆器、壁挂、陶艺等。 Enjoy crafts furnishings are those with furnishings, ornamental function-based products, such as its primary Crafts aesthetic value, highly manual skills, such as jade, gold and silver jewelry, ivory carvings, cloisonné, lacquer ware, wall hangings, pottery, etc. .

[0003] 中国工艺美术的历史悠久,是我国文化宝库中一颗璀璨的明珠,在国际上素负盛名。 [0003] a long history of Chinese arts and crafts, cultural treasure is our jewel, the prestigious in the world. 工艺美术起源于人类开始制造工具的时代。 Arts and Crafts originated in the era of humans began to make tools. 工艺美术大多是劳动人民直接创造的,同人们的物质生活和精神生活密切相关。 Most of arts and crafts created by working people directly, closely related to people's material life and spiritual life. 它的产生,常因历史时期、地理环境、经济条件、文化技术水平、民族风尚和审美观点不同而表现出不同的风格特色。 Its production, often due to different historical periods and geographical environment, economic conditions, cultural and technical level, ethnic fashion and aesthetic point of view and show different style characteristics.

[0004]现有技术中,将制作麦秸画的主要原料麦秸杆染成亮青色的方法有很多种,但多数染料均为化学染料,染出的亮青色不纯正,容易退色,不仅不环保,部分染料在染制的过程中甚至会产生有毒气体,危害人体的健康。 [0004] prior art, would have produced the main raw material wheat straw paintings in brilliant blue straw method are many, but most are dyes chemical dye, dyed bright blue is not pure, easy to fade, not only environmentally friendly , part of the dye may even produce toxic gases in the process of dyed, the harm to human health.

[0005]因而,在麦秸画制作领域缺乏一种将麦秸杆染成不同颜色的植物染料,特别是将麦秸杆染成亮青色的纯天然植物染料,它染出的亮青色麦秸杆不仅色彩纯正,用其材料制出的麦秸画光鲜亮丽,不易退色,而且绿色环保,作品长时间散发出植物清香,有易人的身心健康,程度不同的解决了其它有毒有害化学染料在染制过程中对人们身体造成的危害。 [0005] Thus, the lack of a straw in the production of wheat straw art Videos dyed different colors vegetable dyes, in particular the wheat straw in brilliant blue natural plant dye and dyed bright blue wheat straw not only pure color, with its materials out of the straw painting glamorous, easy to fade, and the green, works long exudes fragrance of plants, physical and mental health have changed hands, with varying degrees of resolve other toxic chemical dyes in dyed harm to people during the body.

[0006] 发明内容: [0006] SUMMARY OF THE INVENTION:

本发明的目的在于提供一种纯天然、无污染、绿色环保、对人身体无毒副作用的用纯天然植物配制成的一种制备亮青色麦秸杆染料及生产方法。 Object of the present invention is to provide a natural, non-polluting, green, wheat straw preparing a light cyan dye formulation and production method of a natural plant into a toxic side effects on the human body.

[0007] 本发明的目的是这样实现的。 Objective [0007] The present invention is achieved. 它是由下述重量配的原料制成的,寥蓝叶杆25-40份、锥花5-15份、风信子花10-25份、絹云母粉20-35份、白矾5_15份、锑离子化合物溶液5-15份、矿泉水30-80份。 It is composed of the following weight distribution of the raw materials, very few blue leaves pole parts 25-40, 5-15 parts echinacea, hyacinth flowers 10-25 parts, 20-35 parts of sericite powder, alum 5_15 parts, antimony 5-15 parts of a solution of the ionic compound, 30-80 parts of mineral water.

[0008] 制备本发明亮青色麦秸杆染料优选重量配比范围是,其中各种原料的重量配比是,寥蓝叶杆25-35份、锥花5-10份、风信子花10-20份、絹云母粉20-29份、白矾5_10份、锑离子化合物溶液5-10份、矿泉水30-70份。 [0008] The present invention was prepared bright cyan dye is preferably wheat straw weight ratio range, wherein the weight ratio of the various raw materials is 25-35 parts by blue leaves very few bars, echinacea 5-10 parts, hyacinth flowers 10- 20 parts, 20-29 parts of sericite powder, alum 5_10 parts, 5-10 parts of a solution of a compound of antimony ions, 30-70 parts mineral.

[0009] 制备本发明亮青色麦秸杆染料的最佳重量配比范围是,其中各种原料的重量配比是:寥蓝叶杆30份、锥花8份、风信子花15份、絹云母粉24份、白矾8份、锑离子化合物溶液7份、矿泉水60份。 [0009] The optimum range of the ratio by weight of the present invention prepared bright cyan dyes are wheat straw, wherein the weight ratio of the various starting materials are: blue leaves very few parts of the lever 30, echinacea 8 parts, 15 parts hyacinth flowers, silk 24 parts of mica, alum 8 parts, 7 parts of antimony ions compound solution, 60 parts of mineral water.

[0010] 将上述各组份制成本发明亮青色麦秸杆染料的生产方法,主要工艺流程为:选料、切料、烘干、浸泡、热煮、混合、沉淀、染色、成品,具体操作方法依次按下列步骤:A、选料、按原料重量配比,挑选符合国家卫生和质量标准的寥蓝叶杆、锥花、风信子花、絹云母粉、白矾、锑离子化合物溶液、矿泉水备用;B、切料、将选出的原料除絹云母粉、白矾、锑离子化合物溶液、矿泉水分别切成块状;C、烘干、将切成块状原料分别置于烘干炉中干化,温度控制在100-120°C,时间30分钟,蒸发原料水份、灭菌;D、浸泡、将烘干后的原料置于装有矿泉水的储槽中浸泡,并加入絹云母粉,温度为室20°C,时间2 - 4小时;E、热煮、将泡过的原料从水中捞出,放到陶器里热煮,时间6小时,煮出色素溶液;F、混合、将色素液侵入20%锑离子化合物溶液里,时间4-8小时 [0010] The above components were made of the cost of wheat straw made bright cyan dye production process, the main process are: choice of materials, cutting, drying, soaking, heat cooking, mixing, sedimentation, dyed and finished products, particularly the method of operation of the following steps in sequence: a, choice of materials, the ratio by weight of the material, very few blue leaves selection lever compliance with national health and quality standards, echinacea, hyacinth flowers, sericite, alum, a solution of a compound of antimony ions, mineral water reserve; B, blanking the selected raw materials other sericite powder, alum, antimony ions compound solution, respectively, cut into pieces of mineral water; C, and drying the cut block material were placed in a drying oven the drying temperature was controlled at 100-120 ° C, for 30 minutes, water was evaporated feedstock, sterilization; D, soaking, after drying the raw material placed in the reservoir with the mineral water immersion, and addition of silk mica, chamber temperature was 20 ° C, time 2 - 4 hours; E, boiled with water, soaked feedstock remove from the water, into the hot cooking of pottery, 6 hours, cook dye solution; F, mixed , 20 percent of an antimony compound solution ionic liquid dye intrusion, the time 4-8 hours 制成混合溶液;G、沉淀、将混合溶液凉至20°C,沉淀出纯净亮青色素溶液;H、染色、将100升纯净亮青色素溶液的温度渐渐升到80°C以上,将经过杀菌、脱硫、蒸煮处理后的麦秸杆浸泡其中,恒温静置12-14小时,期间将麦秸杆上下翻动,使麦秸杆充分吸收亮青色素溶液,均匀染色;1、固色、将染色后的麦秸杆放入加入白矾粉沫的溶液中,浸泡3-6小时,使麦秸杆充分固色后捞出,淋干,在室温中慢慢干燥成亮青色麦秸杆成品。 To prepare a mixed solution; G, the precipitate, the mixed solution to cool to 20 ° C, the precipitated bright pure blue dye solution; H, dyeing, 100 liters of purified dye solution is bright green temperature gradually raised to above 80 ° C, after the sterilization, desulfurization, after retorting soaked wheat straw wherein temperature was allowed to stand 12-14 hours, during which the turning down of wheat straw, wheat straw to fully absorb the light that the blue dye solution, dyeing uniformity; 1, fixing the wheat straw dyed powder into a solution of alum was added, soaked 3-6 hours, the wheat straw was sufficiently fixing the fish, pouring dry slowly dried into a finished light cyan wheat straw at room temperature.

[0011] 本发明的优点在于:1、选择原料,配方科学,色彩纯正;2、产品中不添加防腐剂,化工原料,纯天然,对人体无任何伤害,用其原料制成的麦秸画作品不仅散发植物香气,而且抗腐蚀;3原料来源广泛,加工艺线路短,产品易加工制造。 [0011] advantages of the present invention is that: 1, selection of raw materials, formulation science, pure color; 2, the product does not add preservatives, chemicals, natural, without any harm to the human body, with wheat straw paintings made its raw materials not only sporadic plant aroma, and corrosion resistance; 3 wide range of sources of raw materials, plus short-circuit the process, the product is easy to manufacturing.

具体实施方式 detailed description

[0012] 下面结合具体实施例对本发明作进一步的说明: [0012] The following embodiments in conjunction with specific embodiments of the present invention is further described:

实施例1: Example 1:

制备本发明亮青色麦秸杆染料重量配比范围是:寥蓝叶杆25-40份、锥花5-15份、风信子花10-25份、絹云母粉20-3 5份、白矾5-15份、锑离子化合物溶液5_15份、矿泉水30-80份。 Preparation of wheat straw present bright cyan dye weight ratio range: 25-40 bar blue leaves very few parts, 5-15 parts echinacea, hyacinth flowers 10-25 parts, 20-35 parts of sericite powder, alum 5 -15 parts, parts of antimony ions 5_15 compound solution, 30 to 80 parts of mineral water.

[0013] 实施例2: [0013] Example 2:

制备本发明亮青色麦秸杆染料优选重量配比范围是:寥蓝叶杆25-35份、锥花5-10份、风信子花10-20份、絹云母粉20-29份、白矾5-10份、锑离子化合物溶液5_10份、矿泉水30-70 份。 Preparation of wheat straw present bright cyan dye is preferably in the range of weight ratio: 25-35 bar blue leaves very few parts, 5-10 parts echinacea, hyacinth flowers 10-20 parts, 20-29 parts of sericite powder, alum 5 -10 parts, parts of antimony ions 5_10 compound solution, 30-70 parts of mineral water.

[0014] 实施例3: [0014] Example 3:

制备本发明亮青色麦秸杆染料最佳重量配比范围是:寥蓝叶杆30份、锥花8份、风信子花15份、絹云母粉24份、白矾8份、锑离子化合物溶液7份、矿泉水60份。 Prepared bright cyan present wheat straw is the best range of the ratio by weight of dye: blue leaves very few parts of the lever 30, 8 parts of echinacea, hyacinth flowers 15 parts, 24 parts of sericite powder, 8 parts of alum, a solution of Compound 7 antimony ions parts, 60 parts of mineral water.

[0015] 将上述各组份制成本发明亮青色麦秸杆染料的生产方法,主要工艺流程为:选料、切料、烘干、浸泡、热煮、混合、沉淀、染色、成品,具体操作方法依次按下列步骤:A、选料、按原料重量配比,挑选符合国家卫生和质量标准的寥蓝叶杆、锥花、风信子花、絹云母粉、白矾、锑离子化合物溶液、矿泉水备用;B、切料、将选出的原料除絹云母粉、白矾、锑离子化合物溶液、矿泉水分别切成块状;C、烘干、将切成块状原料分别置于烘干炉中干化,温度控制在100-120°C,时间30分钟,蒸发原料水份、灭菌;D、浸泡、将烘干后的原料置于装有矿泉水的储槽中浸泡,并加入絹云母粉,温度为室20°C,时间2 - 4小时;E、热煮、将泡过的原料从水中捞出,放到陶器里热煮,时间6小时,煮出色素溶液;F、混合、将色素液侵入20%锑离子化合物溶液里,时间4-8小时 [0015] The above components were made of the cost of wheat straw made bright cyan dye production process, the main process are: choice of materials, cutting, drying, soaking, heat cooking, mixing, sedimentation, dyed and finished products, particularly the method of operation of the following steps in sequence: a, choice of materials, the ratio by weight of the material, very few blue leaves selection lever compliance with national health and quality standards, echinacea, hyacinth flowers, sericite, alum, a solution of a compound of antimony ions, mineral water reserve; B, blanking the selected raw materials other sericite powder, alum, antimony ions compound solution, respectively, cut into pieces of mineral water; C, and drying the cut block material were placed in a drying oven the drying temperature was controlled at 100-120 ° C, for 30 minutes, water was evaporated feedstock, sterilization; D, soaking, after drying the raw material placed in the reservoir with the mineral water immersion, and addition of silk mica, chamber temperature was 20 ° C, time 2 - 4 hours; E, boiled with water, soaked feedstock remove from the water, into the hot cooking of pottery, 6 hours, cook dye solution; F, mixed , 20 percent of an antimony compound solution ionic liquid dye intrusion, the time 4-8 hours 制成混合溶液;G、沉淀、将混合溶液凉至20°C,沉淀出纯净亮青色素溶液;H、染色、将100升纯净亮青色素溶液的温度渐渐升到80°C以上,将经过杀菌、脱硫、蒸煮处理后的麦秸杆浸泡其中,恒温静置12-14小时,期间将麦秸杆上下翻动,使麦秸杆充分吸收亮青色素溶液,均匀染色;1、固色、将染色后的麦秸杆放入加入白矾粉沫的溶液中,浸泡3-6小时,使麦秸杆充分固色后捞出,淋干,在室温中慢慢干燥成亮青色麦秸杆成品。 To prepare a mixed solution; G, the precipitate, the mixed solution to cool to 20 ° C, the precipitated bright pure blue dye solution; H, dyeing, 100 liters of purified dye solution is bright green temperature gradually raised to above 80 ° C, after the sterilization, desulfurization, after retorting soaked wheat straw wherein temperature was allowed to stand 12-14 hours, during which the turning down of wheat straw, wheat straw to fully absorb the light that the blue dye solution, dyeing uniformity; 1, fixing the wheat straw dyed powder into a solution of alum was added, soaked 3-6 hours, the wheat straw was sufficiently fixing the fish, pouring dry slowly dried into a finished light cyan wheat straw at room temperature.

Claims (4)

  1. 1.一种制备亮青色麦秸杆染料,其特征在于:它是由下述重量配比的原料制成的,寥蓝叶杆25-40份、锥花5-15份、风信子花10-25份、絹云母粉20-35份、白矾5_15份、锑离子化合物溶液5-15份、矿泉水30-80份。 1. A process for preparing a bright cyan dye wheat straw, characterized in that: it is made by the following ratio by weight of the raw material, blue leaves very few parts 25-40 bar, echinacea 5-15 parts, hyacinth flowers 10 -25 parts, 20-35 parts of sericite powder, alum 5_15 parts, 5-15 parts of a solution of a compound of antimony ions, 30-80 parts of mineral water.
  2. 2.一种制备亮青色麦秸杆染料,其特征在于:其中各种原料的重量配比是,寥蓝叶杆25-35份、锥花5-10份、风信子花10-20份、絹云母粉20-29份、白矾5_10份、锑离子化合物溶液5-10份、矿泉水30-70份。 A process for preparing a bright cyan dye wheat straw, characterized in that: wherein the weight ratio of the various raw materials, the lever 25-35 leaves very few parts of the blue, echinacea 5-10 parts, 10-20 parts hyacinth flowers, 20-29 parts of sericite powder, alum 5_10 parts, 5-10 parts of a solution of a compound of antimony ions, 30-70 parts mineral.
  3. 3.一种制备亮青色麦秸杆染料,其特征在于:其中各种原料的重量配比是,寥蓝叶杆30份、锥花8份、风信子花15份、絹云母粉24份、白矾8份、锑离子化合物溶液7份、矿泉水60份。 3. A process for preparing a bright cyan dye wheat straw, characterized in that: wherein the weight ratio of the various raw materials, the blue leaves very few parts of the rod 30, 8 parts of echinacea, hyacinth flowers 15 parts, 24 parts of sericite powder, alum 8 parts, 7 parts of antimony ions compound solution, 60 parts of mineral water.
  4. 4.根据权利要求1-3所述的一种制备亮青色麦秸杆染料的生产方法,其特征在于:主要工艺流程为:选料、切料、烘干、浸泡、热煮、混合、沉淀、染色、成品,具体操作方法依次按下列步骤:A、选料、按原料重量配比,挑选符合国家卫生和质量标准的寥蓝叶杆、锥花、风信子花、絹云母粉、白矾、锑离子化合物溶液、矿泉水备用、切料、将选出的原料除絹云母粉、白矾、锑离子化合物溶液、矿泉水分别切成块状;C、烘干、将切成块状原料分别置于烘干炉中干化,温度控制在100-120°C,时间30分钟,蒸发原料水份、灭菌;D、浸泡、将烘干后的原料置于装有矿泉水的储槽中浸泡,并加入絹云母粉,温度为室20°C,时间2 - 4小时;E、热煮、将泡过的原料从水中捞出,放到陶器里热煮,时间6小时,煮出色素溶液;F、混合、将色素液侵入20%锑离子化合物溶液里, The one of the production methods 1 to 3 for preparing a cyan dye bright wheat straw as claimed in claim wherein: Main process: material selection, cutting, drying, soaking, heat cooking, mixing, sedimentation , dyeing and finished products, specific methods of operation press the following steps: a, choice of materials, according to the weight ratio of raw materials, very few blue leaf selection lever in line with national health and quality standards, cone flowers, hyacinth flowers, sericite powder, alum, antimony ions compound solution, mineral reserve, cutting, the selected raw materials other sericite powder, alum, antimony ions compound solution, respectively, cut into pieces of mineral water; C, drying the bulk material are cut into opposing drying in the drying oven temperature was controlled at 100-120 ° C, for 30 minutes, water was evaporated feedstock, sterilization; D, soaking, after drying the raw material placed in the reservoir with the mineral water immersion and sericite was added, room temperature 20 ° C, time 2 - 4 hours; E, boiled with water, soaked feedstock remove from the water, into the hot cooking of pottery, 6 hours, cook dye solution ; F, mixing, the pigment was 20% antimony ions invade compound solution, and 间4-8小时,制成混合溶液;G、沉淀、将混合溶液凉至20°C,沉淀出纯净亮青色素溶液;H、染色、将100升纯净亮青色素溶液的温度渐渐升到80°C以上,将经过杀菌、脱硫、蒸煮处理后的麦秸杆浸泡其中,恒温静置12-14小时,期间将麦秸杆上下翻动,使麦秸杆充分吸收亮青色素溶液,均匀染色;1、固色、将染色后的麦秸杆放入加入白矾粉沫的溶液中,浸泡3-6小时,使麦秸杆充分固色后捞出,淋干,在室温中慢慢干燥成亮青色麦秸杆成品。 Between 4-8 hours, to prepare a mixed solution; G, the precipitate, the mixed solution to cool to 20 ° C, the precipitated bright pure blue dye solution; H, dyeing, 100 liters of purified dye solution is bright green temperature gradually rose to 80 above ° C, the pasteurized, desulfurization, after retorting soaked wheat straw wherein temperature was allowed to stand 12-14 hours, during which the turning down of wheat straw, wheat straw to fully absorb the light that the blue dye solution, dyeing uniformity; 1, fixing, the dyed wheat straw were added into a solution of alum powder, soaked 3-6 hours, the wheat straw was sufficiently fixing the fish, pouring dry to dry slowly at room temperature into the light green wheat straw products.
CN 201410074048 2014-03-03 2014-03-03 Method for preparing and producing bright cyan wheat straw dye CN103788691A (en)

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