CN103652922A - Application of Kaempferia galanga L. extract in health food - Google Patents

Application of Kaempferia galanga L. extract in health food Download PDF

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Publication number
CN103652922A
CN103652922A CN201310683338.7A CN201310683338A CN103652922A CN 103652922 A CN103652922 A CN 103652922A CN 201310683338 A CN201310683338 A CN 201310683338A CN 103652922 A CN103652922 A CN 103652922A
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husky ginger
extract
oral liquid
ginger extract
add
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CN201310683338.7A
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Chinese (zh)
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CN103652922B (en
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梁木鸿
梁木林
梁楠
梁滨
江小元
何彩霞
莫丽春
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广东长兴生物科技股份有限公司
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A23B - A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/105Plant extracts, their artificial duplicates or their derivatives
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

Abstract

The invention discloses application of Kaempferia galanga L. extract in health food. The Kaempferia galanga L. extract is specifically applied to preparation of an oral liquid with the female immunity enhancing function. The oral liquid with the female immunity enhancing function can be prepared from the following components: angelica, medlar, mulberry, astragalus root, arillus longan, poria cocos, yam, jujube, honey and Kaempferia galanga L. extract, and the content of the Kaempferia galanga L. extract in the oral liquid with the female immunity enhancing function is 0.08-0.15%. The formula of the oral liquid mainly adapts to physiological characteristics of women, focuses on reinforcing qi and nourishing blood, achieves the function of enhancing body immunity through reinforcing qi and nourishing blood, mainly uses angelica, medlar, mulberry, arillus longan and jujube to nourish blood, matches with poria cocos, astragalus root and yam to reinforce qi, and uses Kaempferia galanga L. to warm middle, thereby facilitating playing the health-keeping effect of the product and rapidly enhancing the body immunity; the honey mainly plays the role of seasoning, so that the product has sweet and comfortable mouthfeel.

Description

The application of a kind of husky ginger extract on health food
Technical field
The present invention relates to a kind of application of extract, the specifically application of a kind of husky ginger extract on health food, belongs to health products preparing technical field.
Background technology
Husky ginger, has another name called kaempferia galamga, is the dry rhizome of zingiberaceous plant kaempferia galamga (Kaempferia galanga L.), has in promoting the circulation of qi temperature, the effect of the pain relieving that helps digestion, and is one of south of the Five Ridges traditional medicine.Being famous Chinese medicine, is again conventional non-staple foodstuff seasoning matter.In husky ginger, main chemical compositions has: volatile oil, Flavonoid substances, Diphenylheptane class material, trace element etc.Husky Rhizoma Zingiberis Recens volatile oil content is higher, it as its pungent fragrance taste of pungent temperature class medicinal material, is one of index of the husky ginger quality good or not of judgement, Ethyl p-methoxy-silicate in oil is the significant compound of the husky ginger of medicinal material and the index components of quality control, also be the compound that relative amount is the highest, there is antitumor, antibacterial and sun-proof effect, can be used for medicine, cosmetics and flavorant.
The effects such as the flavonols compound of Sha Jiangzhong is as antitumor, anti-infective in Kaempferol, Kaempferol have, reducing blood lipid, wherein the strong anti-oxidation of the material such as Kaempferol is active and cardiovascular pharmacotoxicological effect has been caused widely and paid close attention to.Research about husky ginger both at home and abroad mainly concentrates on following three aspects: 1, separated to the extraction of essential oil activity or active ingredient in husky ginger.2, the Analysis and Identification to chemical composition contained in the husky ginger essential oil in the different places of production.3, study physiological and pharmacological effect or the application aspect food additives of each composition.In the scope of the claims also relevant for the relevant report of husky ginger extracts active ingredients.For example, patent CN101919534A discloses a kind of sand ginger paste and preparation method thereof, sand ginger paste is to take husky ginger as primary raw material, coordinates and forms according to certain ratio with auxiliary material such as garlic, white wine, granulated sugar, glucose, light-coloured vinegar, salt, soy sauce, sesame oil, citric acid, CMCs.Patent application 200310112027.1 discloses a kind of method that enzymolysis-steam distillation method extracts husky ginger essential oil and p-methoxy-ethyl-Cinnamate, comprise the steps: (1) to fresh husky ginger or dry husky Jiang Jinhang select materials, purify, fragmentation, the granularity after fragmentation is at 0.1-3mm; (2) 50-100 ℃ and solid-to-liquid ratio 1: 1-1: in the time of under 3 weight conditions, adopt amylase or carbohydrase to carry out enzymolysis 30-150 minute to slurries, the concentration of enzyme is the 0.2-2.0% of gross weight; (3) in solid-to-liquid ratio, be 1: 3-1: during 7 weight, carry out steam distillation 3-7 hour, in 100 Ke Shajiang, quantity of steam is converted into liquid volume and is about 200-700g/h; (4) with water-oil separating method and filtration method, obtain essential oil and p-methoxy-ethyl-Cinnamate.Patent application 200410051384.6 discloses a kind of method that two enzymes method is extracted the active ingredient in separated husky ginger.Patent application CN 103005438 A disclose a kind of the application and have used supercritical CO 2the method of extraction and steam distillation coupling is extracted the Ethyl p-methoxy-silicate in husky ginger, has obtained the higher husky ginger extract of Ethyl p-methoxy-silicate relative amount.
Women is due to physiological structure, and its immunity is easily subject to the impacts such as mood, weather or environmental change, production.Patent application 201210512440.6 discloses a kind of female health tea, is by 20 grams of red dates, 20 grams, donkey-hide gelatin, 5 grams of peanuts, 5 grams, red bean, 5 grams of matrimony vines, 30 grams, brown sugar, 20 grams of longan, is prepared from.Patent CN100444862C disclose a kind of strengthen women's immunity take Chinese herbal medicine as main Halth-care composition, it is mainly by the Poria cocos, peach kernel, the feverfew that are food and medicine, with glossy ganoderma, Reishi sporule, the Radix Astragali, pearl, the red sage root, Radix Glycyrrhizae, the bighead atractylodes rhizome, Radix Angelicae Sinensis, Ligusticum wallichii, safflower, radix rehmanniae recen, root of herbaceous peony Chinese herbal medicine, also have imvite, be prepared from according to a certain weight ratio.200710010697.0 disclose a kind of brown sugar health product that can improve immunity of puerpera, consist of: brown sugar: donkey-hide gelatin: red date: lily=82-96: 3-4: 2-10: 0.1-10 is mainly used in improving puerpera's immunity following component by following portions by weight.
Prior art does not have and husky ginger extract is applied to preparation has the health products that strengthen women's immunity function.
Summary of the invention
The object of the invention is for the deficiencies in the prior art, provide a kind of husky ginger extract to there is the application in the oral liquid that strengthens women's immunity function in preparation, this oral liquid with enhancing women's immunity function is to be prepared by following component: Radix Angelicae Sinensis, matrimony vine, mulberries, the Radix Astragali, first meat, Poria cocos, Chinese yam, date, honey, husky ginger extract, the content that husky ginger extract has in the oral liquid that strengthens women's immunity function at this is 0.8-1.5 ‰.
Another object of the present invention is to provide a kind of and utilizes husky ginger extract preparation to have the method for the oral liquid that strengthens women's immunity function.
For addressing the above problem, the technical solution adopted in the present invention is: the application of a kind of husky ginger extract on health food is to be applied to preparation to have the oral liquid that strengthens women's immunity function; The described oral liquid with enhancing women's immunity function is prepared by following component: Radix Angelicae Sinensis, matrimony vine, mulberries, the Radix Astragali, first meat, Poria cocos, Chinese yam, date, honey, husky ginger extract, the content that described husky ginger extract has in the oral liquid that strengthens women's immunity function at this is 0.8-1.5 ‰.
The described consumption proportion with each component in the oral liquid that strengthens women's immunity function is as follows: Radix Angelicae Sinensis 40-80g, matrimony vine 30-70g, mulberries 30-70g, first meat 20-60g, date 8-40g, Poria cocos 20-60g, Radix Astragali 20-60g, Chinese yam 20-60g, honey 30-70g, husky ginger extract 0.005-0.02ml.
Described has in the oral liquid that strengthens women's immunity function, and preferably the consumption proportion of each component is as follows: Radix Angelicae Sinensis 50-70g, matrimony vine 40-60g, mulberries 40-60g, first meat 30-50g, date 10-30g, Poria cocos 30-50g, Radix Astragali 30-50g, Chinese yam 30-50g, honey 40-60g, husky ginger extract 0.008-0.015ml.
The husky ginger extract of faint yellow oily that described husky ginger extract preferably adopts the extraction of molecular clock technology to obtain, the relative amount of its Ethyl p-methoxy-silicate is 90-98%.
A kind of husky ginger extract is prepared according to the following steps when being applied to prepare the oral liquid with enhancing women's immunity function:
(1) adopt following raw material preparation: the husky ginger extract 0.005-0.02ml that Radix Angelicae Sinensis 40-80g, matrimony vine 30-70g, mulberries 30-70g, first meat 20-60g, date 8-40g, Poria cocos 20-60g, Radix Astragali 20-60g, Chinese yam 20-60g, honey 30-70g, the molecular clock technology of take extraction obtain and the relative amount of Ethyl p-methoxy-silicate is 90-98%;
(2) preparation of Chinese medicine extract: by Radix Angelicae Sinensis, matrimony vine, mulberries, the Radix Astragali, first meat, Poria cocos, Chinese yam, date totally eight taste medicinal materials, choose respectively the removal of impurity, clean; Add the decocting of 8 times of amounts of quality of medicinal material to boil 3 hours, decoction process supplements the water yield evaporating in time; Decoct completely, filter, the decocting that filter residue adds 5 times of amounts again boils 2 hours, and decoction process supplements the water yield evaporating in time; Decoct completely, filter, merges twice filtrate, be condensed into thick paste, thick paste is naturally cooling after, add the edible alcohol of 2 times of amounts of thick paste quality, stir, in 0-4 ℃ of refrigeration, placement 12-24 hour spends the night; Get supernatant recovered alcohol, concentrate adds the cold boiling water of 3 times of amounts, fully stirs, and in 0-4 ℃ of refrigeration, spends the night, and filters, and gets filtrate for later use;
(3) get above-mentioned Chinese medicine extract, add and should prepare half the water yield of oral liquid cumulative volume, boil, add honey, stir evenly, add water to total amount, with square frame filter press, filter while hot, add husky ginger extract, stir, make oral liquid; Packing after the assay was approved, capping, at 1kg/cm 2under pressure, high pressure sterilizing in 20 minutes, after lamp inspection is qualified, packing, hands over storehouse.
The husky ginger extract of faint yellow oily that the preparation method of husky ginger extract of the present invention preferably adopts the extraction of molecular clock technology to obtain, the relative amount of its Ethyl p-methoxy-silicate is 90-98%.
Further preferred scheme is to adopt the disclosed method of patent application CN 103005438 A, specifically comprises the following steps:
The first step: get appropriate husky ginger, wash away sandy soil, remove coring, impurity, chopping, with the juice extractor pulverizing of squeezing the juice,
Second step: get the husky ginger juice slag through the pulverizing of squeezing the juice of making by first step step and be positioned over CO 2in supercritical extraction reactor, carry out supercritical CO 2extraction, starts equipment, and parameters starts extraction, and extraction process parameter is as follows: pressure of storage tank 2-6Mpa, extraction kettle pressure 5-25MPa, extraction-container pressure are 5-10MPa, 30-55 ℃ of extraction kettle temperature, CO 2flow 5-30kg/h, extraction-container temperature are 30-50 ℃, cooling water temperature 3-10 ℃, extraction time 60-180min;
The 3rd step: extraction finishes, and obtains husky ginger supercritical extract, is brown color, oily liquids, and yield is 5-15%;
The 4th step: husky ginger supercritical extract is joined in molecular distillation equipment, start equipment, setup parameter, distillation pressure 50-100Pa, knifing speed 200-400r/min, condensation temperature 15-30 ℃, preheat temperature 30-50 ℃, material flow 1.5-2.5ml/min, vapo(u)rizing temperature 35-55 ℃, carry out molecular clock, control each parameter well, distillation finishes, the husky ginger molecular clock of gained brown color oily extract, yield is about 50-97%, the relative amount 80-90% of Ethyl p-methoxy-silicate; The 5th step: continue the 4th extract of step by step suddenly making to carry out molecular clock, setup parameter, distillation pressure 20-70Pa, knifing speed 200-400r/min, condensation temperature 15-30 ℃, preheat temperature 30-50 ℃, material flow 1.5-2.5ml/min, vapo(u)rizing temperature 50-80 ℃, the husky ginger extract of the faint yellow oily of last gained, the relative amount 90-98% of Ethyl p-methoxy-silicate.
The present invention with respect to the beneficial effect of prior art is:
(1) effective component of husky ginger is Ethyl p-methoxy-silicate, belongs to ethereal oil, adopts traditional water boiling method, and effective ingredient has been volatilized totally; In the present invention's formula, the husky ginger extract adopting is for extracting and obtain with molecular clock technology, the relative amount 90-98% of Ethyl p-methoxy-silicate, when preparing health products, husky ginger extract is directly added in the semi-finished product of the oral liquid before filling and capping, can better makes the significant composition Ethyl p-methoxy-silicate in husky ginger extract bring into play its useful effect;
(2) in the present invention's formula, take and adapt to physiology characteristics as main, bias toward nourishing qi and blood, pass through nourishing qi and blood, by nourishing qi and blood, reach and strengthen body immunity function, it is main that Radix Angelicae Sinensis, matrimony vine, mulberries, first meat, date nourish blood, be equipped with Poria cocos, the Radix Astragali, Chinese yam benefit gas, in Sha Jiangwen, thereby make this product bring into play faster its health-care efficacy, strengthen rapidly immunity of organisms.Honey mainly plays seasoning effect, makes this product mouthfeel sweet comfortable.
The specific embodiment
Below by embodiment, the present invention is described in further details, these embodiment are only used for illustrating the present invention, do not limit the scope of the invention.
Embodiment 1 the present embodiment is to adopt the disclosed method of patent application CN 103005438 A to prepare a kind of husky ginger extract, the health food that strengthens women's immunity function that has by husky ginger extract for the preparation of a kind of oral liquid formulation, specifically comprises the following steps.
1, the preparation of husky ginger extract:
(1) get husky ginger, wash away sandy soil, remove coring, impurity, chopping, with the juice extractor pulverizing of squeezing the juice, the husky ginger juice slag that pulverizing is obtained is positioned over CO 2in supercritical extraction reactor, carry out supercritical CO 2extraction, starts equipment, and parameters starts extraction, and extraction process parameter is as follows: pressure of storage tank 2Mpa, extraction kettle pressure 5MPa, extraction-container pressure are 5MPa, 40 ℃ of extraction kettle temperature, CO 2flow 10kg/h, extraction-container temperature are 30 ℃, 3 ℃ of cooling water temperatures, extraction time 60min, and extraction finishes, and obtains husky ginger supercritical extract, is brown color, oily liquids, and yield is 15%;
(2) husky ginger supercritical extract is joined in molecular distillation equipment, start equipment, setup parameter, distillation pressure 50-100Pa, knifing speed 300r/min, 22 ℃ of condensation temperatures, 40 ℃ of preheat temperatures, material flow 2ml/min, 45 ℃ of vapo(u)rizing temperatures, carry out molecular clock, control each parameter well, distillation finishes, the husky ginger molecular clock of gained brown color oily extract, yield is 90%, the relative amount 85% of Ethyl p-methoxy-silicate;
(3) extract that continuation makes step (2) carries out molecular clock, setup parameter, distillation pressure 50Pa, knifing speed 300r/min, 22 ℃ of condensation temperatures, 40 ℃ of preheat temperatures, material flow 2ml/min, 65 ℃ of vapo(u)rizing temperatures, the husky ginger extract of the faint yellow oily of last gained, the relative amount 95% of Ethyl p-methoxy-silicate.
2, oral liquid preparation
(1) get Radix Angelicae Sinensis 60g; Matrimony vine 50g; Mulberries 50g; The meat 40g of unit; Date 20g; Poria cocos 40g; Radix Astragali 40g; Chinese yam 40g; Honey 50g; The above-mentioned husky ginger extract 0.01ml making;
(2), by Radix Angelicae Sinensis, matrimony vine, mulberries, the Radix Astragali, first meat, Poria cocos, Chinese yam, date totally eight taste medicinal materials, choose respectively the removal of impurity, clean; Add the decocting of 8 times of amounts of quality of medicinal material to boil 3 hours, decoction process supplements the water yield evaporating in time; Decoct completely, filter, the decocting that filter residue adds 5 times of amounts again boils 2 hours, and decoction process supplements the water yield evaporating in time; Decoct completely, filter, merges twice filtrate, be condensed into thick paste, thick paste is naturally cooling after, add the edible alcohol of 2 times of amounts of thick paste quality, stir, in 0-4 ℃ of refrigeration, the placement 18 hours of spending the night; Get supernatant recovered alcohol, concentrate adds the cold boiling water of 3 times of amounts, fully stirs, and in 0-4 ℃ of refrigeration, spends the night, and filters, and gets filtrate for later use;
(3) get above-mentioned Chinese medicine extract, add and should prepare half the water yield of total amount, boil, add honey, stir evenly, add water to total amount, with square frame filter press, filter while hot, add husky ginger essential oil to stir, make oral liquid; Packing after the assay was approved, capping, at 1kg/cm 2under pressure, high pressure sterilizing in 20 minutes, after lamp inspection is qualified, packing, hands over storehouse.
Embodiment 2 the present embodiment are to adopt the disclosed method of patent application CN 103005438 A to prepare a kind of husky ginger extract, the health food that strengthens women's immunity function that has by husky ginger extract for the preparation of a kind of oral liquid formulation, specifically comprises the following steps.
1, the preparation of husky ginger extract:
(1) get husky ginger, wash away sandy soil, remove coring, impurity, chopping, with the juice extractor pulverizing of squeezing the juice, the husky ginger juice slag that pulverizing is obtained is positioned over CO 2in supercritical extraction reactor, carry out supercritical CO 2extraction, starts equipment, and parameters starts extraction, and extraction process parameter is as follows: pressure of storage tank 4Mpa, extraction kettle pressure 20MPa, extraction-container pressure are 8MPa, extraction kettle temperature 45 C, CO 2flow 30kg/h, extraction-container temperature are 30 ℃, 5 ℃ of cooling water temperatures, extraction time 120min, and extraction finishes, and obtains husky ginger supercritical extract, is brown color, oily liquids, and yield is 12%;
(2) husky ginger supercritical extract is joined in molecular distillation equipment, start equipment, setup parameter, distillation pressure 80Pa, knifing speed 400r/min, 20 ℃ of condensation temperatures, 50 ℃ of preheat temperatures, material flow 1.8ml/min, 50 ℃ of vapo(u)rizing temperatures, carry out molecular clock, control each parameter well, distillation finishes, the husky ginger molecular clock of gained brown color oily extract, yield is 60%, the relative amount 90% of Ethyl p-methoxy-silicate;
(3) extract that continuation makes step (2) carries out molecular clock, setup parameter, distillation pressure 70Pa, knifing speed 400r/min, 30 ℃ of condensation temperatures, 50 ℃ of preheat temperatures, material flow 2.5ml/min, 80 ℃ of vapo(u)rizing temperatures, the husky ginger extract of the faint yellow oily of last gained, the relative amount 90% of Ethyl p-methoxy-silicate.
2, oral liquid preparation:
(1) get Radix Angelicae Sinensis 40g, matrimony vine 30g, mulberries 30g, first meat 60g, date 40g, Poria cocos 20, Radix Astragali 20g, Chinese yam 60g, honey 30g, the above-mentioned husky ginger extract 0.005ml making;
(2), by Radix Angelicae Sinensis, matrimony vine, mulberries, the Radix Astragali, first meat, Poria cocos, Chinese yam, date totally eight taste medicinal materials, choose respectively the removal of impurity, clean; Add the decocting of 8 times of amounts of quality of medicinal material to boil 3 hours, decoction process supplements the water yield evaporating in time; Decoct completely, filter, the decocting that filter residue adds 5 times of amounts again boils 2 hours, and decoction process supplements the water yield evaporating in time; Decoct completely, filter, merges twice filtrate, be condensed into thick paste, thick paste is naturally cooling after, add the edible alcohol of 2 times of amounts of thick paste quality, stir, in 0-4 ℃ of refrigeration, the placement 12 hours of spending the night; Get supernatant recovered alcohol, concentrate adds the cold boiling water of 3 times of amounts, fully stirs, and in 0-4 ℃ of refrigeration, spends the night, and filters, and gets filtrate for later use;
(2) filtrate is put in concentration tank and concentrate, when 60 ℃ of relative densities 1.2, stop concentrating, make Chinese medical concrete liquid, let cool, standby;
(3) get above-mentioned Chinese medicine extract, add and should prepare half the water yield of total amount, boil, add honey, stir evenly, add water to total amount, with square frame filter press, filter while hot, add husky ginger essential oil to stir, make oral liquid; Packing after the assay was approved, capping, at 1kg/cm 2under pressure, high pressure sterilizing in 20 minutes, after lamp inspection is qualified, packing, hands over storehouse.
Embodiment 3 the present embodiment are to adopt the disclosed method of patent application CN 103005438 A to prepare a kind of husky ginger extract, the health food that strengthens women's immunity function that has by husky ginger extract for the preparation of a kind of oral liquid formulation, specifically comprises the following steps.
1, the preparation of husky ginger extract:
(1) get husky ginger, wash away sandy soil, remove coring, impurity, chopping, with the juice extractor pulverizing of squeezing the juice, the husky ginger juice slag that pulverizing is obtained is positioned over CO 2in supercritical extraction reactor, carry out supercritical CO 2extraction, starts equipment, and parameters starts extraction, and extraction process parameter is as follows: pressure of storage tank 2Mpa, extraction kettle pressure 5MPa, extraction-container pressure are 5MPa, 40 ℃ of extraction kettle temperature, CO 2flow 20kg/h, extraction-container temperature are 40 ℃, 10 ℃ of cooling water temperatures, extraction time 180min, and extraction finishes, and obtains husky ginger supercritical extract, is brown color, oily liquids, and yield is 11%;
(2) husky ginger supercritical extract is joined in molecular distillation equipment, start equipment, setup parameter, distillation pressure 50Pa, knifing speed 200r/min, 15 ℃ of condensation temperatures, 30 ℃ of preheat temperatures, material flow 1.5ml/min, 35 ℃ of vapo(u)rizing temperatures, carry out molecular clock, control each parameter well, distillation finishes, the husky ginger molecular clock of gained brown color oily extract, yield is 82%, the relative amount 80% of Ethyl p-methoxy-silicate;
(3) extract that continuation makes step (2) carries out molecular clock, setup parameter, distillation pressure 20Pa, knifing speed 200r/min, 15 ℃ of condensation temperatures, 30 ℃ of preheat temperatures, material flow 1.5ml/min, 50 ℃ of vapo(u)rizing temperatures, the husky ginger extract of the faint yellow oily of last gained, the relative amount 98% of Ethyl p-methoxy-silicate.
2, oral liquid preparation:
(1) get Radix Angelicae Sinensis 80g, matrimony vine 40g, mulberries 70g, first meat 20g, date 8g, Poria cocos 60g, Radix Astragali 60g, Chinese yam 20, honey 70g, the above-mentioned husky ginger extract 0.012ml making;
(2), by Radix Angelicae Sinensis, matrimony vine, mulberries, the Radix Astragali, first meat, Poria cocos, Chinese yam, date totally eight taste medicinal materials, choose respectively the removal of impurity, clean; Add the decocting of 8 times of amounts of quality of medicinal material to boil 3 hours, decoction process supplements the water yield evaporating in time; Decoct completely, filter, the decocting that filter residue adds 5 times of amounts again boils 2 hours, and decoction process supplements the water yield evaporating in time; Decoct completely, filter, merges twice filtrate, be condensed into thick paste, thick paste is naturally cooling after, add the edible alcohol of 2 times of amounts of thick paste quality, stir, in 0-4 ℃ of refrigeration, the placement 24 hours of spending the night; Get supernatant recovered alcohol, concentrate adds the cold boiling water of 3 times of amounts, fully stirs, and in 0-4 ℃ of refrigeration, spends the night, and filters, and gets filtrate for later use;
(3) get above-mentioned Chinese medicine extract, add and should prepare half the water yield of total amount, boil, add honey, stir evenly, add water to total amount, with square frame filter press, filter while hot, add husky ginger essential oil to stir, make oral liquid; Packing after the assay was approved, capping, at 1kg/cm 2under pressure, high pressure sterilizing in 20 minutes, after lamp inspection is qualified, packing, hands over storehouse.
Embodiment 4 the present embodiment are to adopt the disclosed method of patent application CN 103005438 A to prepare a kind of husky ginger extract, the health food that strengthens women's immunity function that has by husky ginger extract for the preparation of a kind of oral liquid formulation, specifically comprises the following steps.
1, the preparation of husky ginger extract:
(1) get husky ginger, wash away sandy soil, remove coring, impurity, chopping, with the juice extractor pulverizing of squeezing the juice, the husky ginger juice slag that pulverizing is obtained is positioned over CO 2in supercritical extraction reactor, carry out supercritical CO 2extraction, starts equipment, and parameters starts extraction, and extraction process parameter is as follows: pressure of storage tank 2Mpa, extraction kettle pressure 5MPa, extraction-container pressure are 5MPa, 40 ℃ of extraction kettle temperature, CO 2flow 20kg/h, extraction-container temperature are 40 ℃, 10 ℃ of cooling water temperatures, extraction time 180min, and extraction finishes, and obtains husky ginger supercritical extract, is brown color, oily liquids, and yield is 11%;
(2) husky ginger supercritical extract is joined in molecular distillation equipment, start equipment, setup parameter, distillation pressure 50Pa, knifing speed 200r/min, 15 ℃ of condensation temperatures, 30 ℃ of preheat temperatures, material flow 1.5ml/min, 35 ℃ of vapo(u)rizing temperatures, carry out molecular clock, control each parameter well, distillation finishes, the husky ginger molecular clock of gained brown color oily extract, yield is 82%, the relative amount 80% of Ethyl p-methoxy-silicate;
(3) extract that continuation makes step (2) carries out molecular clock, setup parameter, distillation pressure 20Pa, knifing speed 200r/min, 15 ℃ of condensation temperatures, 30 ℃ of preheat temperatures, material flow 1.5ml/min, 50 ℃ of vapo(u)rizing temperatures, the husky ginger extract of the faint yellow oily of last gained, the relative amount 98% of Ethyl p-methoxy-silicate.
2, oral liquid preparation:
(1) get Radix Angelicae Sinensis 50g, matrimony vine 60g, mulberries 60g, first meat 30g, date 30g, Poria cocos 50g, Radix Astragali 30g, Chinese yam 30, honey 40g, the above-mentioned husky ginger extract 0.02ml making;
(2), by Radix Angelicae Sinensis, matrimony vine, mulberries, the Radix Astragali, first meat, Poria cocos, Chinese yam, date totally eight taste medicinal materials, choose respectively the removal of impurity, clean; Add the decocting of 8 times of amounts of quality of medicinal material to boil 3 hours, decoction process supplements the water yield evaporating in time; Decoct completely, filter, the decocting that filter residue adds 5 times of amounts again boils 2 hours, and decoction process supplements the water yield evaporating in time; Decoct completely, filter, merges twice filtrate, be condensed into thick paste, thick paste is naturally cooling after, add the edible alcohol of 2 times of amounts of thick paste quality, stir, in 0-4 ℃ of refrigeration, the placement 24 hours of spending the night; Get supernatant recovered alcohol, concentrate adds the cold boiling water of 3 times of amounts, fully stirs, and in 0-4 ℃ of refrigeration, spends the night, and filters, and gets filtrate for later use;
(3) get above-mentioned Chinese medicine extract, add and should prepare half the water yield of total amount, boil, add honey, stir evenly, add water to total amount, with square frame filter press, filter while hot, add husky ginger essential oil to stir, make oral liquid; Packing after the assay was approved, capping, at 1kg/cm 2under pressure, high pressure sterilizing in 20 minutes, after lamp inspection is qualified, packing, hands over storehouse.
Embodiment 5 the present embodiment are to adopt the disclosed method of patent application CN 103005438 A to prepare a kind of husky ginger extract, the health food that strengthens women's immunity function that has by husky ginger extract for the preparation of a kind of oral liquid formulation, specifically comprises the following steps.
1, the preparation of husky ginger extract:
(1) get husky ginger, wash away sandy soil, remove coring, impurity, chopping, with the juice extractor pulverizing of squeezing the juice, the husky ginger juice slag that pulverizing is obtained is positioned over CO 2in supercritical extraction reactor, carry out supercritical CO 2extraction, starts equipment, and parameters starts extraction, and extraction process parameter is as follows: pressure of storage tank 3.5Mpa, extraction kettle pressure 7MPa, extraction-container pressure are 5MPa, 42 ℃ of extraction kettle temperature, CO 2flow 18kg/h, extraction-container temperature are 40 ℃, 8 ℃ of cooling water temperatures, extraction time 120min, and extraction finishes, and obtains husky ginger supercritical extract, is brown color, oily liquids, and yield is 10.8%;
(2) husky ginger supercritical extract is joined in molecular distillation equipment, start equipment, setup parameter, distillation pressure 80Pa, knifing speed 300r/min, 22 ℃ of condensation temperatures, 35 ℃ of preheat temperatures, material flow 2ml/min, 45 ℃ of vapo(u)rizing temperatures, carry out molecular clock, control each parameter well, distillation finishes, the husky ginger molecular clock of gained brown color oily extract, yield is 83.8%, the relative amount 82% of Ethyl p-methoxy-silicate;
(3) extract that continuation makes step (2) carries out molecular clock, setup parameter, distillation pressure 35Pa, knifing speed 200r/min, 15 ℃ of condensation temperatures, 40 ℃ of preheat temperatures, material flow 2ml/min, 50 ℃ of vapo(u)rizing temperatures, the husky ginger extract of the faint yellow oily of last gained, the relative amount 93.5% of Ethyl p-methoxy-silicate.
2, oral liquid preparation:
(1) get Radix Angelicae Sinensis 70g, matrimony vine 70g, mulberries 40g, first meat 50g, date 10g, Poria cocos 30g, Radix Astragali 50g, Chinese yam 50, honey 60g, the above-mentioned husky ginger extract 0.015ml making;
(2), by Radix Angelicae Sinensis, matrimony vine, mulberries, the Radix Astragali, first meat, Poria cocos, Chinese yam, date totally eight taste medicinal materials, choose respectively the removal of impurity, clean; Add the decocting of 8 times of amounts of quality of medicinal material to boil 3 hours, decoction process supplements the water yield evaporating in time; Decoct completely, filter, the decocting that filter residue adds 5 times of amounts again boils 2 hours, and decoction process supplements the water yield evaporating in time; Decoct completely, filter, merges twice filtrate, be condensed into thick paste, thick paste is naturally cooling after, add the edible alcohol of 2 times of amounts of thick paste quality, stir, in 0-4 ℃ of refrigeration, the placement 12 hours of spending the night; Get supernatant recovered alcohol, concentrate adds the cold boiling water of 3 times of amounts, fully stirs, and in 0-4 ℃ of refrigeration, spends the night, and filters, and gets filtrate for later use;
(3) get above-mentioned Chinese medicine extract, add and should prepare half the water yield of total amount, boil, add honey, stir evenly, add water to total amount, with square frame filter press, filter while hot, add husky ginger essential oil to stir, make oral liquid; Packing after the assay was approved, capping, at 1kg/cm 2under pressure, high pressure sterilizing in 20 minutes, after lamp inspection is qualified, packing, hands over storehouse.
Embodiment 6 the present embodiment are to adopt the disclosed method of patent application CN 103005438 A to prepare a kind of husky ginger extract, the health food that strengthens women's immunity function that has by husky ginger extract for the preparation of a kind of oral liquid formulation, specifically comprises the following steps.
1, the preparation of husky ginger extract:
(1) get husky ginger, wash away sandy soil, remove coring, impurity, chopping, with the juice extractor pulverizing of squeezing the juice, the husky ginger juice slag that pulverizing is obtained is positioned over CO 2in supercritical extraction reactor, carry out supercritical CO 2extraction, starts equipment, and parameters starts extraction, and extraction process parameter is as follows: pressure of storage tank 4Mpa, extraction kettle pressure 10MPa, extraction-container pressure are 6MPa, 35 ℃ of extraction kettle temperature, CO 2flow 10kg/h, extraction-container temperature are 40 ℃, 5 ℃ of cooling water temperatures, extraction time 180min, and extraction finishes, and obtains husky ginger supercritical extract, is brown color, oily liquids, and yield is 13.8%;
(2) husky ginger supercritical extract is joined in molecular distillation equipment, start equipment, setup parameter, distillation pressure 60Pa, knifing speed 200r/min, 18 ℃ of condensation temperatures, 30 ℃ of preheat temperatures, material flow 1.5ml/min, 45 ℃ of vapo(u)rizing temperatures, carry out molecular clock, control each parameter well, distillation finishes, the husky ginger molecular clock of gained brown color oily extract, yield is 88%, the relative amount 81.7% of Ethyl p-methoxy-silicate;
(3) extract that continuation makes step (2) carries out molecular clock, setup parameter, distillation pressure 30Pa, knifing speed 200r/min, 18 ℃ of condensation temperatures, 30 ℃ of preheat temperatures, material flow 1.5ml/min, 50 ℃ of vapo(u)rizing temperatures, the husky ginger extract of the faint yellow oily of last gained, the relative amount 92.6% of Ethyl p-methoxy-silicate.
2, oral liquid preparation:
(1) get Radix Angelicae Sinensis 65g, matrimony vine 45g, mulberries 50g, first meat 40g, date 25g, Poria cocos 40g, Radix Astragali 45g, Chinese yam 45, honey 55g, the above-mentioned husky ginger extract 0.01ml making;
(2), by Radix Angelicae Sinensis, matrimony vine, mulberries, the Radix Astragali, first meat, Poria cocos, Chinese yam, date totally eight taste medicinal materials, choose respectively the removal of impurity, clean; Add the decocting of 8 times of amounts of quality of medicinal material to boil 3 hours, decoction process supplements the water yield evaporating in time; Decoct completely, filter, the decocting that filter residue adds 5 times of amounts again boils 2 hours, and decoction process supplements the water yield evaporating in time; Decoct completely, filter, merges twice filtrate, be condensed into thick paste, thick paste is naturally cooling after, add the edible alcohol of 2 times of amounts of thick paste quality, stir, in 0-4 ℃ of refrigeration, the placement 12 hours of spending the night; Get supernatant recovered alcohol, concentrate adds the cold boiling water of 3 times of amounts, fully stirs, and in 0-4 ℃ of refrigeration, spends the night, and filters, and gets filtrate for later use;
(3) get above-mentioned Chinese medicine extract, add and should prepare half the water yield of total amount, boil, add honey, stir evenly, add water to total amount, with square frame filter press, filter while hot, add husky ginger essential oil to stir, make oral liquid; Packing after the assay was approved, capping, at 1kg/cm 2under pressure, high pressure sterilizing in 20 minutes, after lamp inspection is qualified, packing, hands over storehouse.

Claims (5)

1. the application of husky ginger extract on health food, is characterized in that: be applied to preparation and have the oral liquid that strengthens women's immunity function; The described oral liquid with enhancing women's immunity function is prepared by following component: Radix Angelicae Sinensis, matrimony vine, mulberries, the Radix Astragali, first meat, Poria cocos, Chinese yam, date, honey, husky ginger extract, the content that described husky ginger extract has in the oral liquid that strengthens women's immunity function at this is 0.8-1.5 ‰.
2. according to power, require the application on health food of husky ginger extract described in 1, it is characterized in that: the described consumption proportion with each component in the oral liquid that strengthens women's immunity function is as follows: Radix Angelicae Sinensis 40-80g, matrimony vine 30-70g, mulberries 30-70g, first meat 20-60g, date 8-40g, Poria cocos 20-60g, Radix Astragali 20-60g, Chinese yam 20-60g, honey 30-70g, husky ginger extract 0.005-0.02ml.
3. according to power, require the application on health food of husky ginger extract described in 1 or 2, it is characterized in that: the described consumption proportion with each component in the oral liquid that strengthens women's immunity function is as follows: Radix Angelicae Sinensis 50-70g, matrimony vine 40-60g, mulberries 40-60g, first meat 30-50g, date 10-30g, Poria cocos 30-50g, Radix Astragali 30-50g, Chinese yam 30-50g, honey 40-60g, husky ginger extract 0.008-0.015ml.
4. according to power, require 1 or 2 or the application on health food of described husky ginger extract, it is characterized in that: described husky ginger extract is the husky ginger extract of faint yellow oily that adopts the extraction of molecular clock technology to obtain, and the relative amount of its Ethyl p-methoxy-silicate is 90-98%.
5. the application of husky ginger extract on health food, is characterized in that: be applied to preparation and have the oral liquid that strengthens women's immunity function, described oral liquid adopts following steps preparation:
(1) adopt following raw material preparation: the husky ginger extract 0.005-0.02ml that Radix Angelicae Sinensis 40-80g, matrimony vine 30-70g, mulberries 30-70g, first meat 20-60g, date 8-40g, Poria cocos 20-60g, Radix Astragali 20-60g, Chinese yam 20-60g, honey 30-70g, the molecular clock technology of take extraction obtain and the relative amount of Ethyl p-methoxy-silicate is 90-98%;
(2) preparation of Chinese medicine extract: by Radix Angelicae Sinensis, matrimony vine, mulberries, the Radix Astragali, first meat, Poria cocos, Chinese yam, date totally eight taste medicinal materials, choose respectively the removal of impurity, clean; Add the decocting of 8 times of amounts of quality of medicinal material to boil 3 hours, decoction process supplements the water yield evaporating in time; Decoct completely, filter, the decocting that filter residue adds 5 times of amounts again boils 2 hours, and decoction process supplements the water yield evaporating in time; Decoct completely, filter, merges twice filtrate, be condensed into thick paste, thick paste is naturally cooling after, add the edible alcohol of 2 times of amounts of thick paste quality, stir, in 0-4 ℃ of refrigeration, placement 12-24 hour spends the night; Get supernatant recovered alcohol, concentrate adds the cold boiling water of 3 times of amounts, fully stirs, and in 0-4 ℃ of refrigeration, spends the night, and filters, and gets filtrate for later use;
(3) get above-mentioned Chinese medicine extract, add and should prepare half the water yield of oral liquid cumulative volume, boil, add honey, stir evenly, add water to total amount, with square frame filter press, filter while hot, add husky ginger extract, stir, make oral liquid; Packing after the assay was approved, capping, at 1kg/cm 2under pressure, high pressure sterilizing in 20 minutes, after lamp inspection is qualified, packing, hands over storehouse.
CN201310683338.7A 2013-12-16 2013-12-16 Application of Kaempferia galanga L extract in health food CN103652922B (en)

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