CN103651494A - Insecticide composition - Google Patents

Insecticide composition Download PDF

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Publication number
CN103651494A
CN103651494A CN201310622548.5A CN201310622548A CN103651494A CN 103651494 A CN103651494 A CN 103651494A CN 201310622548 A CN201310622548 A CN 201310622548A CN 103651494 A CN103651494 A CN 103651494A
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CN
China
Prior art keywords
percent
thiacloprid
insecticide composition
carrier
capillary
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Pending
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CN201310622548.5A
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Chinese (zh)
Inventor
房伟
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Individual
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Individual
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Priority to CN201310622548.5A priority Critical patent/CN103651494A/en
Publication of CN103651494A publication Critical patent/CN103651494A/en
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Abstract

The invention discloses an insecticide composition which comprises the following components: 1 to 50 percent of thiacloprid, 6 percent to 80 percent of chlorfenapyr, 2 percent to 12 percent of a dispersant, 1 percent to 6 percent of a wetting agent, 2 percent to 6 percent of a disintegrant, 1 percent to 5 percent of astragalus polysaccharide, 1 percent to 5 percent of carboxymethyl cellulose sodium and the balance of carrier. The carrier is plateau soil or bentonite. The synergistic insecticide composition disclosed by the invention is suitable for preventing and treating piercing-sucking mouthpart pests on rice, vegetables, fruit trees, flowers, lawn and the like. Compounding of two effective ingredients of the insecticide composition has an obvious synergistic effect and improves preventing and treating effects; the use amount of the pesticide is reduced, and popularization and application of the insecticide composition have relatively large economic benefits and social benefits.

Description

A kind of Pesticidal combination
 
Technical field:
The present invention relates to the preparation method of Pesticidal combination, a kind of preparation method of the Synergistic insecticidal compositions that contains thiacloprid and capillary specifically, for preventing and treating the suckings pest such as paddy rice, vegetables, fruit tree, flowers, lawn.
 
Background technology:
Thiacloprid is a kind ofly new sucking pest to be had to efficient broad spectrum pesticide, and different according to crop, insect and method of application, its consumption is 50.4~100.8g a.i./hm2.Field trial shows, thiacloprid has excellent control efficiency to the important pests on tea tree, pomaceous fruits fruit, cotton, vegetables and potato.Except to aphid, aleyrodid, thrips effectively, it to various beetles (as colorado potato beetle, apple weevil, Lissorhoptrus oryzophilus Kuschel) and lepidoptera pest as the leaf miner on apple tree and codling moth also effective, and corresponding all crops are all suitable for.
Thiacloprid acts on nicotinic acid acetylcholinergic receptor.It and common insecticides do not have cross resistance as pyrethroid, organic phosphates and carbamates, thereby can be used for resistance management.Thiacloprid has interior absorption and has acute contact toxicity and stomach poison function.The soil half life period of thiacloprid is short, to birds, fish and multiple beneficial arthropods safety.It is very safe to honeybee, at flowering phase of crop, can use equally.Due to thiacloprid low toxicity, efficient, by numerous users, liked.
Capillary is new pyrrole class Insecticidal and acaricidal agent.Various pests, mite are had to stomach toxicity and action of contace poison, to crop safety, be applicable to prevent and treat brassicaceous vegetable diamond-back moth, beet armyworm, tea tree tea lesser leafhopper, looper, mite, citrus red mites etc., have the advantages such as preventive effect is high, the lasting period is long, dosage is low.
In recent years, the sucking pest on crops is caused harm seriously, and peasant uses the medicines such as Imidacloprid, Biphenthrin, chlopyrifos to produce serious resistance for a long time, occurs strengthening dosage, the poor problem of control efficiency, and it is serious that environmental pollution is also tending towards.
Being mixed of different pesticide species is the common methods of the agriculture resistant insect of control.By formulation of pesticide, screening, filter out rational formula, can effectively improve actual control efficiency, reduce dosage, reduce costs, delay the generation of pest resistance to insecticide, extend the service life of medicament, is the important means of integrated pest management.The inventor is on the basis of a large amount of indoor virulence screenings and field medicine effect test, and discovery thiacloprid and capillary are mixed the suckings pest such as aphid are had to synergistic function.
Water dispersible granular is disintegration dispersion rapidly in water, forming can be for suspension or the solution of spraying, its major advantage is without dust or there is few dust to produce when producing and using, to using and producer's safety, and have the advantage of aqueous emulsion and wetting powder concurrently, thereby become the fashion trend formulation of the most potential on international market and development prospect.
Summary of the invention:
The object of the invention is to overcome the shortcoming existing in prior art, provide using method simple, the object of the invention is of using is mixed different thiacloprid and the capillaries of the mechanism of action, make full use of the synergistic effect that both are mixed and produce, provide a kind of efficient, low toxicity, agricultural insecticide composition cheaply, for preventing and treating the suckings pest such as paddy rice, vegetables, fruit tree, flowers, lawn.
Technical scheme of the present invention:
A Pesticidal combination, is characterized in that, comprises following component:
Thiacloprid 1~50%, capillary 6%~80%, dispersant 2%~12%, wetting agent 1%~6%, disintegrant 2%~6%, astragalus polyose 1%~5%, sodium cellulose glycolate 1%~5%, surplus are carrier.
Or, comprise following component:
Thiacloprid 1~30%, capillary 6%~40%, dispersant 2%~6%, wetting agent 1%~3%, disintegrant 2%~4%, astragalus polyose 1%~3%, sodium cellulose glycolate 1%~2%, surplus are carrier.
Described carrier is upland soil or bentonite.
The preparation method of Pesticidal combination, take thiacloprid and capillary as active ingredient, and in composition, the weight percentage of thiacloprid is 1~50%, the weight percentage of capillary is 5%~80%.
Pesticidal combination of the present invention adds suitable auxiliary agent to make water dispersible granules.
Described auxiliary agent is: dispersant 2%~12%, wetting agent 1%~6%, disintegrant 2%~6%, adhesive 1%~5%, sodium cellulose glycolate 1%~5%, surplus are carrier.
Wherein, dispersant is selected from one or more in alkylbenzenesulfonate, two naphthyl sulfonate, acrylic acid polymers sodium salt, ethoxylated dodecyl alcohol; Wetting agent is selected from lauryl sodium sulfate, pulls open powder, one or more in wetting and penetrating agent F, spaonin powder; Disintegrant is selected from one or more in bentonite, ammonium sulfate, aluminium chloride, citric acid, succinic acid, carbonic hydroammonium; Carrier is selected from one or more in kaolin, diatomite, white carbon.
Its preparation method carries out as follows.
(1) thiacloprid 1~50%, capillary 6%~80%, dispersant 2%~12%, wetting agent 1%~6%, disintegrant 2%~6%, astragalus polyose 1%~5%, sodium cellulose glycolate 1%~5%, surplus are carrier; Except astragalus polyose, other raw material mixes and obtains mixture.
(2) mixture after carrying out ultramicro grinding, airslide disintegrating mill is obtained to female powder.
(3) the female powder obtaining after ultramicro grinding is taken to certain amount and put into revolving fluid bed.
(4) open revolving fluid bed and slowly toward it, add the aqueous solution of astragalus polyose to carry out granulation.
(5) after completing, granulation dries.
(6) shot-like particle of oven dry sieved, obtain water dispersible granules after analytical control.
Beneficial effect of the present invention is.
(1) Pesticidal combination of the present invention can effectively be prevented and treated the suckings pest such as resistance aphid, thrips, rice fulgorid and Bemisia tabaci, remarkably productive, to crop safety; (2) Pesticidal combination dust of the present invention is few, to the producer, user and Environmental security; (3) in the present invention, do not contain organic solvent, environmental pollution is little, is convenient to accumulating and use; (4) preventive effect of the present invention is compared single dose and is had obvious synergistic effect, reduces dosage, alleviates pest resistance to insecticide and produces.
Embodiment:
Below in conjunction with embodiment, content of the present invention is described in further detail, in embodiment, mentioned content is not limitation of the invention, material prescription select to suit measures to local conditions and on result without substantial impact.In these embodiments, unless otherwise indicated, all percentage is all weight percentage.
Embodiment 1:30% thiacloprid acarid nitrile water dispersion granula.
Take the former medicine 10% of thiacloprid, capillary 20%, spaonin powder 1%, sodium lignin sulfonate 5%, ammonium sulfate 5%, precipitated calcium carbonate 5%, above raw material is mixed, stir and obtain female powder by airslide disintegrating mill, female powder is mixed with 2% polyvinylpyrrolidone, with kaolin, mend to 100%, then granulation, oven dry, screening obtain 30% thiacloprid acarid nitrile water dispersion granula again.Through check active constituent content, be thiacloprid 10%, capillary 20%, suspension Shuai≤75% Shui Fen≤2.5%, pH is 7.2, particle size range (225~800um)≤98%, Fen San≤85%, moistening Shi Jian≤90s, (by 75um, sieve)≤98, ()≤12ml after 1min, acceleration heat storage stability is qualified for lasting foaming characteristic in wet screening test.
The 30% thiacloprid acarid nitrile water dispersion granula of this embodiment is used for preventing and treating tea tree tea lesser leafhopper.In the Sheng phase dispenser of nymph beginning, 60 grams of usage amounts (active ingredient)/hectare, is watered even spraying, and after medicine, 3 days preventive effects are 99.8%; Contrast medicament 48% 80 grams of thiacloprid suspending agent usage amounts (active ingredient)/hectare, 10% 90 grams of capillary suspending agent usage amounts (active ingredient)/hectare, adopt same method dispenser, and after medicine, 3 days preventive effects are respectively 76.8% and 85.2%.
 
Embodiment 2:50% thiacloprid acarid nitrile water dispersion granula.
Take thiacloprid 20%, capillary 30%, pulls open powder 3%, carboxymethyl cellulose 5%, carbonic hydroammonium 12%, white carbon 25%; Above raw material is mixed, stir and obtain female powder by airslide disintegrating mill, female powder is mixed with 3% polyvinylpyrrolidone, then mend to 100% with soluble starch, then granulation, oven dry, screening obtain 50% thiacloprid acarid nitrile water dispersion granula.Through check active constituent content, be thiacloprid 20%, capillary 30%, suspension Shuai≤75% Shui Fen≤2.5%, pH is 7.2, particle size range (225~800um)≤98%, Fen San≤85%, moistening Shi Jian≤90s, (by 75um, sieve)≤98, ()≤12ml after 1min, acceleration heat storage stability is qualified for lasting foaming characteristic in wet screening test.
The 50% thiacloprid acarid nitrile water dispersion granula of this embodiment is used for preventing and treating water rice hopper.In the phase dispenser of rice fulgorid nymph beginning Sheng, 50 grams of usage amounts (active ingredient)/hectare, is watered even spraying, and after medicine, 3 days preventive effects are 97.3%; Contrast medicament 48% 80 grams of thiacloprid suspending agent usage amounts (active ingredient)/hectare, 10% 90 grams of capillary suspending agent usage amounts (active ingredient)/hectare, adopt same method dispenser, and after medicine, 3 days preventive effects are respectively 67.1% and 86.8%.

Claims (3)

1. a Pesticidal combination, is characterized in that, comprises following component:
Thiacloprid 1~50%, capillary 6%~80%, dispersant 2%~12%, wetting agent 1%~6%, disintegrant 2%~6%, astragalus polyose 1%~5%, sodium cellulose glycolate 1%~5%, surplus are carrier.
2. Pesticidal combination according to claim 1, is characterized in that, comprises following component:
Thiacloprid 1~30%, capillary 6%~40%, dispersant 2%~6%, wetting agent 1%~3%, disintegrant 2%~4%, astragalus polyose 1%~3%, sodium cellulose glycolate 1%~2%, surplus are carrier.
3. according to Pesticidal combination described in claim 1 or 2, it is characterized in that, described carrier is upland soil or bentonite.
CN201310622548.5A 2013-11-30 2013-11-30 Insecticide composition Pending CN103651494A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201310622548.5A CN103651494A (en) 2013-11-30 2013-11-30 Insecticide composition

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201310622548.5A CN103651494A (en) 2013-11-30 2013-11-30 Insecticide composition

Publications (1)

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CN103651494A true CN103651494A (en) 2014-03-26

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105076185A (en) * 2015-08-21 2015-11-25 山东农业大学 Insecticide composition with chlorfenapyr and neonicotinoid insecticides, and preparation and application of insecticide composition

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105076185A (en) * 2015-08-21 2015-11-25 山东农业大学 Insecticide composition with chlorfenapyr and neonicotinoid insecticides, and preparation and application of insecticide composition
CN105076185B (en) * 2015-08-21 2017-04-05 山东农业大学 The Pesticidal combination and its preparation and application of a kind of capillary and anabasine insecticide

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Application publication date: 20140326