CN103549084A - Houttuynia extract and method for preparing herbal tea and effervescent tablets from houttuynia extract - Google Patents
Houttuynia extract and method for preparing herbal tea and effervescent tablets from houttuynia extract Download PDFInfo
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- CN103549084A CN103549084A CN201310527308.7A CN201310527308A CN103549084A CN 103549084 A CN103549084 A CN 103549084A CN 201310527308 A CN201310527308 A CN 201310527308A CN 103549084 A CN103549084 A CN 103549084A
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Abstract
The invention discloses a houttuynia extract, and a method for preparing herbal tea and effervescent tablets from the houttuynia extract. The houttuynia, Hubei begonia leaves and momordica grosvenori serving as raw materials are subjected to heating reflux extraction, and volatile oil is collected by an oil-water separator to obtain an extract and the volatile oil; the houttuynia herbal tea is prepared by performing filtration, enzymolysis and the like on the extract; the volatile oil can be prepared into the effervescent tablets. By the method for preparing the herbal tea provided by the invention, main nutritional ingredients of the houttuynia are preserved, and moreover, the problem that houttuynia herbal tea is likely to precipitate is solved by the process measures of volatile oil separation, chitosan clarification and enzymolysis. The defect that the flavor of conventional houttuynia beverage is not obvious is overcome by an inclusion process measure of the volatile oil, the drinking forms of the houttuynia herbal tea are enriched, and the drinking pleasure of customers is enhanced.
Description
Technical field
The present invention relates to the processing of a kind of cordate houttuynia, be specifically related to a kind of houttuynia extract and utilize houttuynia extract to prepare the method for cold tea and effervescent tablet.
Background technology
Cordate houttuynia (Houttuynia Cordata Thumb.) has another name called heartleaf houttuynia, Cen grass, the root of picking up the ears, smelly raw meat grass etc., is the herb of Saururaceae heartleaf houttuynia platymiscium, is herbaceos perennial, rubs with the hands after broken and has a fish like smell, therefore named cordate houttuynia because of its cauline leaf.Often be grown in the shade hillside, limit, village ridge, in small stream limit, riverside and wetland thick grass.Cordate houttuynia contains rich in protein, fat carbohydrate, calcium, phosphorus, iron and VC, VP, VB1, VB6, VE, with abundant dietary fiber, in addition, cordate houttuynia also has heat-clearing, removing toxic substances, anti-inflammatory, antibiotic, antiviral, diuresis is gushed pouring, the effect of detumescence row's gland and enhanced machine body immunity function.Cordate houttuynia is formally defined as " being food, is again medicine " by health ministry, become a kind of medicinal, health care and the more edible resource of edibility.The beverage that at present relevant cordate houttuynia is made, because clarity is bad, easily precipitates, and mouthfeel is owed harmony, and cordate houttuynia local flavor is not obvious, and ordinary consumer is difficult for accepting.This method be take dry cordate houttuynia as raw material, take Momordica grosvenori, Malus spectabilis leaf is auxiliary material, be processed into cordate houttuynia cold tea, both retained Nutritive Compsition from Houttuynia cordata Thunb, there is again cordate houttuynia local flavor, and clear, mouthfeel are coordinated, and are a kind of strong local characteristic and exclusive popular local flavors of having embodied, and integrate the natural beverage of health-care effect nutritive value simultaneously.
Summary of the invention
For the deficiencies in the prior art, the object of this invention is to provide a kind of houttuynia extract and utilize houttuynia extract to prepare the method for cold tea and effervescent tablet, this method be take dry cordate houttuynia as raw material, take Momordica grosvenori, Malus spectabilis leaf is auxiliary material, be processed into cordate houttuynia cold tea, both retained Nutritive Compsition from Houttuynia cordata Thunb, and there is again cordate houttuynia local flavor, and clear, mouthfeel are coordinated
The object of the present invention is achieved like this: a kind of preparation method of houttuynia extract, comprises the following steps:
1) selection: raw material used is dry cordate houttuynia, Hubei Chinese flowering crabapple leaf and Momordica grosvenori, and raw material is cleaned up;
2) heating and refluxing extraction: cordate houttuynia, Momordica grosvenori, Hubei Chinese flowering crabapple leaf are placed in to 80～100 ℃ of hot water and extract, extraction time is 1～3 h, raw material and water are by quality ratio: 1:4-12, by oil water separator, collect volatile oil, obtain extract and volatile oil is houttuynia extract.
The addition of described cordate houttuynia, Hubei Chinese flowering crabapple leaf and Momordica grosvenori is by quality ratio: 2-4:1:1.
Utilize right houttuynia extract to prepare the method for cold tea, comprise the following steps:
1) filter: with diatomite filter, by extracting liquid filtering, obtain the filtered fluid of Herba Houttuyniae extract;
2) enzymolysis: add alpha amylase and Glucoamylase hydrolysis in filtered fluid.Alpha amylase consumption used is 0.1%～0.3% of filtered fluid quality; Carbohydrase consumption used is 0.05%～0.2% of filtered fluid quality;
3) enzyme that goes out: the extract after enzymolysis is at 85～120 ℃ of deactivation 30-60min;
4) preparation: complete the water dilution that the filtered fluid going out after enzyme adds 2～3 times, and add flavoring; Add sugar and honey, addition is 5%～7% of extract quality, obtains preparing liquid;
5) clarification: first the acetum with 0.3%～3% is made shitosan to 0.5%～5% shitosan liquid, then the shitosan liquid configuring is added preparation liquid to carry out clarifying treatment, shitosan liquid addition for press that obtaining liq amasss 2%～4%, settling time is 1h～1.5h, and clarifying temp is 50 ℃～70 ℃;
6) coarse filtration and essence filter: clarify complete preparation liquid through coarse filtration and essence filter, after 105-121 ℃ of sterilizing 30-60min, obtain cordate houttuynia cold tea.
Utilize houttuynia extract to prepare the method for effervescent tablet, comprise the following steps:
1) prepare inclusion compound: by volatile oil: hydroxypropylβ-cyclodextrin=1:7～9(ml:g) take hydroxypropyl beta cyclodextrin, add suitable quantity of water and be ground to dissolving, grinding limit, limit adds volatile oil, and dissolve with appropriate ethanol, grind 1～1.5h, solution after grinding is put into refrigerator and cooled and is frozen by freeze drying 20～24h, obtains inclusion compound powder;
2) prepare effervescent tablet: formula: inclusion compound powder 35%; Citric acid: sodium acid carbonate (1:3.5) 40%; Lactose 25%; Technique: inclusion compound is divided into two parts, and portion mixes with citric acid, lactose, simple syrup, as adhesive, is granulated, dry; Another part mixes with sodium acid carbonate, and simple syrup, as adhesive, is granulated, dry; Two kinds of dried particles are mixed, add 0.5% dolomol, mix, compressing tablet, obtains the effervescent tablet containing houttuynia extract.
Described cordate houttuynia is dry or bright cordate houttuynia herb or root of Herba Houttuyniae.
The invention provides production method due to the steps such as volatile oil, enzymolysis, shitosan precipitation that adopted refluxing extraction separation, the cold tea obtaining has not only well kept the natural nutrient component of cordate houttuynia, and clear, good stability.In production stage of the present invention, inclusion essential oil is processed and made effervescent tablet, drinking front consumer can put it in cold water or other tea, after its rapid disintegration, can discharge unique cordate houttuynia local flavor, overcome the unconspicuous defect of traditional houttuynia beverage cordate houttuynia local flavor.
The specific embodiment
Embodiment 1: prepare houttuynia extract:
1) selection: raw material used is cordate houttuynia, Hubei Chinese flowering crabapple leaf and Momordica grosvenori, and raw material is cleaned up;
2) heating and refluxing extraction: 2Kg cordate houttuynia, 1Kg Momordica grosvenori, 1Kg Hubei Chinese flowering crabapple leaf are placed in to 80～100 ℃ of hot water and extract, extraction time is 1～3 h, raw material and water are by quality ratio: 1:4-12, by oil water separator, collect volatile oil, obtain extract and volatile oil is houttuynia extract.
Embodiment 2: prepare houttuynia extract:
1) selection: raw material used is cordate houttuynia, Hubei Chinese flowering crabapple leaf and Momordica grosvenori, and raw material is cleaned up;
2) heating and refluxing extraction: 3Kg cordate houttuynia, 1Kg Momordica grosvenori, 1Kg Hubei Chinese flowering crabapple leaf are placed in to 80～100 ℃ of hot water and extract, extraction time is 1～3 h, raw material and water are by quality ratio: 1:4-12, by oil water separator, collect volatile oil, obtain extract and volatile oil is houttuynia extract.
Embodiment 3: prepare houttuynia extract:
1) selection: raw material used is cordate houttuynia, Hubei Chinese flowering crabapple leaf and Momordica grosvenori, and raw material is cleaned up;
2) heating and refluxing extraction: 4Kg cordate houttuynia, 1Kg Momordica grosvenori, 1Kg Hubei Chinese flowering crabapple leaf are placed in to 80～100 ℃ of hot water and extract, extraction time is 1～3 h, raw material and water are by quality ratio: 1:4-12, by oil water separator, collect volatile oil, obtain extract and volatile oil is houttuynia extract.
Cordate houttuynia in above-described embodiment 1-3 is dry or bright cordate houttuynia herb or root of Herba Houttuyniae.
Embodiment 4: utilize right houttuynia extract to prepare cold tea:
1) filter: by obtaining filtering with diatomite filter of extract in above-described embodiment 1-3, obtain the filtered fluid of Herba Houttuyniae extract; During filtration, filter paper, with after wet with solvent, is opened water pump, allows filter paper be adsorbed on tightly on funnel, adds the diatomite that 1～2cm is thick, spreads evenly as far as possible, after adding a small amount of wet with solvent, pours extract suction filtration into;
2) enzymolysis: add alpha amylase and Glucoamylase hydrolysis in filtered fluid.Alpha amylase consumption used is 0.1%～0.3% of filtered fluid quality; Carbohydrase consumption used is 0.05%～0.2% of filtered fluid quality; Under 60 ℃ of conditions, enzymolysis is 1.5 hours;
3) enzyme that goes out: the extract after enzymolysis is at 85～120 ℃ of deactivation 30-60min;
4) preparation: complete the filtered fluid going out after enzyme and add 2-3 water dilution doubly, and add flavoring; Add sugar and honey, addition is 5%～7% of extract quality, obtains preparing liquid;
5) clarification: first shitosan is made to 0.5%～5% shitosan liquid with 0.3%～3% acetum, then the shitosan liquid configuring is added preparation liquid to carry out clarifying treatment, shitosan liquid addition for press that obtaining liq amasss 2%～4%, settling time is 1h～1.5h, and clarifying temp is 50 ℃～70 ℃;
6) coarse filtration and essence filter: clarify complete preparation liquid through coarse filtration and essence filter, after 105-121 ℃ of sterilizing 30-60min, obtain cordate houttuynia cold tea.
Embodiment 5: utilize houttuynia extract to prepare effervescent tablet:
1) prepare inclusion compound: get the volatile oil in embodiment 1-3, by volatile oil: hydroxypropylβ-cyclodextrin=1:7-9(ml:g) take hydroxypropyl beta cyclodextrin, add suitable quantity of water and be ground to dissolving, grinding limit, limit adds volatile oil, and dissolve with appropriate ethanol, grind 1～1.5h, the solution after grinding is put into refrigerator and cooled and is frozen by freeze drying 20～24h, obtains inclusion compound powder;
2) prepare effervescent tablet: formula: inclusion compound powder 35%; Citric acid: sodium acid carbonate (1:3.5) 40%; Lactose 25%; Technique: inclusion compound is divided into two parts, and portion mixes with citric acid, lactose, simple syrup, as adhesive, is granulated, dry; Another part mixes with sodium acid carbonate, and simple syrup, as adhesive, is granulated, dry; Two kinds of dried particles are mixed, add 0.5% dolomol, mix, compressing tablet, obtains the effervescent tablet containing houttuynia extract.
When adding cordate houttuynia cold tea, effervescent tablet can make cold tea cordate houttuynia local flavor more obvious.
Claims (6)
1. a preparation method for houttuynia extract, is characterized in that, comprises the following steps:
1) selection: raw material used is cordate houttuynia, Hubei Chinese flowering crabapple leaf and Momordica grosvenori, and raw material is cleaned up;
2) heating and refluxing extraction: cordate houttuynia, Momordica grosvenori, Hubei Chinese flowering crabapple leaf are placed in to 80～100 ℃ of hot water and extract, extraction time is 1～3 h, raw material and water are by quality ratio: 1:4～12, by oil water separator, collect volatile oil, obtain extract and volatile oil is houttuynia extract.
2. the preparation method of houttuynia extract according to claim 1, is characterized in that: the addition of cordate houttuynia, Hubei Chinese flowering crabapple leaf and Momordica grosvenori is by quality ratio: 2～4:1:1.
3. utilize houttuynia extract described in claim 1 or 2 to prepare the method for cold tea, it is characterized in that: comprise the following steps:
1) filter: with diatomite filter, by extracting liquid filtering, obtain the filtered fluid of Herba Houttuyniae extract;
2) enzymolysis: add alpha amylase and Glucoamylase hydrolysis in filtered fluid, alpha amylase consumption used is 0.1%～0.3% of filtrate quality; Carbohydrase consumption used is 0.05%～0.2% of filtered fluid quality;
3) enzyme that goes out: the extract after enzymolysis is at 85～120 ℃ of deactivation 30-60min;
4) preparation: complete the water dilution that the filtered fluid going out after enzyme adds 2～3 times, and add sugar or honey, obtain preparing liquid;
5) clarification: first shitosan is made to 0.5%～5% shitosan liquid with 0.3%～3% acetum, then the shitosan liquid configuring is added preparation liquid to carry out clarifying treatment, shitosan liquid addition for press that obtaining liq amasss 2%～4%, settling time is 1h～1.5h, and clarifying temp is 50 ℃～70 ℃;
6) coarse filtration and essence filter: clarify complete preparation liquid through coarse filtration and essence filter, after 105-121 ℃ of sterilizing 30-60min, obtain cordate houttuynia cold tea.
4. utilize Herba Houttuyniae volatile oil described in claim 1 or 2 to prepare the method for effervescent tablet, it is characterized in that, comprise the following steps:
1) prepare inclusion compound: by volatile oil: hydroxypropylβ-cyclodextrin=1:7-9(ml:g) take hydroxypropyl beta cyclodextrin, add suitable quantity of water and be ground to dissolving, grinding limit, limit adds volatile oil, and dissolve with appropriate ethanol, grind 1～1.5h, solution after grinding is put into refrigerator and cooled and is frozen by freeze drying 20～24h, obtains inclusion compound powder;
2) prepare effervescent tablet: formula: inclusion compound powder 35%; Citric acid: sodium acid carbonate (1:3.5) 40%; Lactose 25%; Technique: inclusion compound is divided into two parts, and portion mixes with citric acid, lactose, simple syrup, as adhesive, is granulated, dry; Another part mixes with sodium acid carbonate, and simple syrup, as adhesive, is granulated, dry; Two kinds of dried particles are mixed, add 0.5% dolomol, mix, compressing tablet, obtains the effervescent tablet containing houttuynia extract.
5. the method for utilizing houttuynia extract to prepare cold tea according to claim 3, is characterized in that: described batching is sugar or honey, and addition is 5%～7% of extract quality.
6. the preparation method of houttuynia extract according to claim 1, is characterized in that: described cordate houttuynia is dry or bright cordate houttuynia herb or root of Herba Houttuyniae.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104522801A (en) * | 2014-12-22 | 2015-04-22 | 百花医药集团股份有限公司 | Health-care beverage and preparation method thereof |
| CN105505648A (en) * | 2015-12-25 | 2016-04-20 | 青岛海特新蓝生物科技有限公司 | Liquid detergent |
| CN105707326A (en) * | 2016-03-21 | 2016-06-29 | 张俊辉 | Preparation method of purple grass and juncus effuses instant tea powder |
| CN108175017A (en) * | 2018-01-24 | 2018-06-19 | 荆州市俏佳人生物科技有限公司 | One kind is relieved inflammation or internal heat beverage and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH06133744A (en) * | 1992-10-27 | 1994-05-17 | Sumiko Sawabe | Adlay healthy tea and its production |
| CN1528283A (en) * | 2003-10-16 | 2004-09-15 | 晏四平 | Non-injection pharmaceutical product containing novel houttuynine sodium bisulfite |
| CN101011096A (en) * | 2007-01-26 | 2007-08-08 | 彭定有 | Hubei Malus spectabilis tea |
| CN101077114A (en) * | 2007-06-27 | 2007-11-28 | 修正药业集团股份有限公司 | Lung-clearing tea and preparation method thereof |
| CN101766725A (en) * | 2010-03-09 | 2010-07-07 | 四川省中医药科学院 | Anti-inflammatory and antiviral medicine |
-
2013
- 2013-10-31 CN CN201310527308.7A patent/CN103549084B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH06133744A (en) * | 1992-10-27 | 1994-05-17 | Sumiko Sawabe | Adlay healthy tea and its production |
| CN1528283A (en) * | 2003-10-16 | 2004-09-15 | 晏四平 | Non-injection pharmaceutical product containing novel houttuynine sodium bisulfite |
| CN101011096A (en) * | 2007-01-26 | 2007-08-08 | 彭定有 | Hubei Malus spectabilis tea |
| CN101077114A (en) * | 2007-06-27 | 2007-11-28 | 修正药业集团股份有限公司 | Lung-clearing tea and preparation method thereof |
| CN101766725A (en) * | 2010-03-09 | 2010-07-07 | 四川省中医药科学院 | Anti-inflammatory and antiviral medicine |
Non-Patent Citations (2)
| Title |
|---|
| 刘冰，等: "含羟丙基-环糊精鱼腥草注射液的制备方法研究", 《云南中医中药杂志》 * |
| 刘冰，等: "含羟丙基-环糊精鱼腥草注射液的制备方法研究", 《云南中医中药杂志》, vol. 30, no. 6, 31 December 2009 (2009-12-31), pages 58 - 59 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104522801A (en) * | 2014-12-22 | 2015-04-22 | 百花医药集团股份有限公司 | Health-care beverage and preparation method thereof |
| CN105505648A (en) * | 2015-12-25 | 2016-04-20 | 青岛海特新蓝生物科技有限公司 | Liquid detergent |
| CN105707326A (en) * | 2016-03-21 | 2016-06-29 | 张俊辉 | Preparation method of purple grass and juncus effuses instant tea powder |
| CN108175017A (en) * | 2018-01-24 | 2018-06-19 | 荆州市俏佳人生物科技有限公司 | One kind is relieved inflammation or internal heat beverage and preparation method thereof |
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