CN103509474B - Book and periodical side glue - Google Patents
Book and periodical side glue Download PDFInfo
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- CN103509474B CN103509474B CN201310426837.8A CN201310426837A CN103509474B CN 103509474 B CN103509474 B CN 103509474B CN 201310426837 A CN201310426837 A CN 201310426837A CN 103509474 B CN103509474 B CN 103509474B
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- side glue
- jade powder
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Abstract
The invention discloses book and periodical side glue which is prepared by the following raw materials in parts by weight: 3-5 parts of paraffin, 1-2 parts of nano carbon, 0.6-1.5 parts of antioxygen 626, 0.2-0.4 parts of antioxygen 1135, 0.8-1.5 parts of butyl acrylate, 1-10 parts of polypropylene (PP), 5-7 parts of rosin resin, 5-7 parts of petroleum resin, 40-50 parts of Japan Asahi Kasei EF1531 EVA (ethylene vinyl acetate), 6-7 parts of polyethylene, 5-8 parts of hydrogenated rosin, 0.2-0.4 parts of antistatic agent ASA (acrylonitrile styrene acrylate), and 3-5 parts of composite bowlder powder. According to the side glue, a special filler, namely the composite bowlder powder is added, so that the side glue is high in binding power and firm in binding, and the side glue is good in effect and firm in binding serving as unsewn book binding back glue.
Description
Technical field
The present invention relates to hot melt adhesive field, is exactly a kind of book side glue.
Background technology
Hot melt adhesive is a kind of plastic tackiness agent, and in certain temperature range, its physical condition changes with temperature change, and chemical property is constant, and it is nonpoisonous and tasteless, belongs to environmental-protecting chemical product.
By the way such as blending, grafting, modification is carried out to improve the performance of hot melt adhesive to existing kind.Such as stablizer is used for anti-oxidation; Tackifier improve bonding strength; Paraffin reduces viscosity-modifying surface properties; Various filler can improve viscosity, fusing point and bonding strength etc.Study the kind of various Synergist S-421 95, consumption, and carry out formulation optimization with satisfied different demand.
Summary of the invention
The object of the present invention is to provide a kind of book side glue.
Above-mentioned purpose is realized by following scheme:
A kind of book side glue, it is characterized in that: it is obtained by the raw material of following weight parts: paraffin 3-5, nano-sized carbon 1-2, oxidation inhibitor 626 0.6-1.5, oxidation inhibitor 1135 0.2-0.4, butyl acrylate 0.8-1.5, polypropylene PP 1-10, Gum Rosin 5-7, petroleum resin 5-7, Japanese Asahi Chemical Industry EF1531EVA 40-50, polyethylene 6-7, staybelite 5-8, static inhibitor ASA 0.2-0.4, compound jade powder 3-5;
Compound jade powder is made up of the raw material of following weight part:
Jade powder 15-20, diatomite 8-14, hydrotalcite powder 4-8, clorafin 3-5, starch 4-5, chitosan 1-2, dimethyl phthalate 0.7-1.5, Tritolyl Phosphate 0.1-0.2;
The preparation method of described compound jade powder:
(1), by jade powder, diatomite, hydrotalcite powder concentration be the sodium hydroxide bubble of 5-10% after 2-3 hour, then with deionized water wash to neutral, dry, the powder that must process is for subsequent use;
(2), by the powder processed at 500-600 DEG C, calcine 2-4 hour, obtain the powder after calcining for subsequent use;
(3) add all the other raw materials and suitable quantity of water in powder, after firing, stir 10-20 minute under 1000-1200 rev/min after, dry after pulverizing, adding 10-15% hydrochloric acid soln adjusts PH to be 4-5, after ground slurry to 600-800 order, repeated hydrogenation sodium oxide is adjusted to neutrality, is drying to obtain.
Described a kind of book side glue, is characterized in that:
Preparation method comprises the following steps:
(1) by weight by Japanese Asahi Chemical Industry EF1531EVA, compound jade powder, polyethylene, mixing, under 1600-1700 rev/min, stir 10-20 minute, put into kneader at 190-210 DEG C, mediate 18-22min, take out cooling;
(2) by the cooled sizing material of step (1) gained and all the other raw material blendings, twin screw extruder granulation at 180-200 DEG C, takes out and cools and get final product.
Beneficial effect of the present invention is: the present invention is by adding particular fillers compound jade powder, and make cohesive force of the present invention strong, bonding is firmly, effective as books unsewn binding gum, and bonding firmly.
Embodiment
A kind of book side glue, it is obtained by the raw material of following weight kg: paraffin 3, nano-sized carbon 2, oxidation inhibitor 626 1.5, oxidation inhibitor 1,135 0.2, butyl acrylate 0.8, polypropylene PP 5, Gum Rosin 6, petroleum resin 5, Japanese Asahi Chemical Industry EF1531EVA 50, polyethylene 6, staybelite 5, static inhibitor ASA 0.4, compound jade powder 5;
Compound jade powder is made up of the raw material of following weight kg:
Jade powder 20, diatomite 8, hydrotalcite powder 8, clorafin 5, starch 4, chitosan 1, dimethyl phthalate 1.5, Tritolyl Phosphate 0.2;
The preparation method of described compound jade powder:
(1), by jade powder, diatomite, hydrotalcite powder concentration be 5% sodium hydroxide steep 3 hours after, then with deionized water wash to neutral, dry, the powder that must process is for subsequent use;
(2), by the powder processed calcine 4 hours at 580 DEG C, obtain the powder after calcining for subsequent use;
(3) add all the other raw materials and suitable quantity of water in powder, after firing, stir after 15 minutes, dry after pulverizing under 1200 revs/min, add 15% hydrochloric acid soln and adjust PH to be 4, after ground slurry to 800 order, repeated hydrogenation sodium oxide is adjusted to neutrality, is drying to obtain.
Described a kind of book side glue,
Preparation method comprises the following steps:
(1) by weight proportion by Japanese Asahi Chemical Industry EF1531EVA, compound jade powder, polyethylene, mixing, stir 20 minutes under 1600 revs/min, put into kneader at 210 DEG C, mediate 20min, take out cooling;
(2) by the cooled sizing material of step (1) gained and all the other raw material blendings, twin screw extruder granulation at 200 DEG C, takes out and cools and get final product.
The apparent viscosity of the binding agent of the present embodiment is 5400MPa.s, stripping strength 57N/2.5cm, and initial bonding strength reaches No. 5 steel balls, open hour 40s, and within 24 hours, thermally-stabilised proterties is stablized.
Claims (1)
1. a book side glue, it is characterized in that: it is obtained by the raw material of following weight parts: paraffin 3-5, nano-sized carbon 1-2, oxidation inhibitor 626 0.6-1.5, oxidation inhibitor 1135 0.2-0.4, butyl acrylate 0.8-1.5, polypropylene PP 1-10, Gum Rosin 5-7, petroleum resin 5-7, Japanese Asahi Chemical Industry EF1531EVA 40-50, polyethylene 6-7, staybelite 5-8, static inhibitor ASA 0.2-0.4, compound jade powder 3-5;
Compound jade powder is made up of the raw material of following weight part:
Jade powder 15-20, diatomite 8-14, hydrotalcite powder 4-8, clorafin 3-5, starch 4-5, chitosan 1-2, dimethyl phthalate 0.7-1.5, Tritolyl Phosphate 0.1-0.2;
The preparation method of described compound jade powder:
(1), by jade powder, diatomite, hydrotalcite powder concentration be the sodium hydroxide bubble of 5-10% after 2-3 hour, then with deionized water wash to neutral, dry, the powder that must process is for subsequent use;
(2), by the powder processed at 500-600 DEG C, calcine 2-4 hour, obtain the powder after calcining for subsequent use;
(3) add all the other raw materials and suitable quantity of water in powder, after firing, stir 10-20 minute under 1000-1200 rev/min after, dry after pulverizing, adding 10-15% hydrochloric acid soln adjusts pH to be 4-5, after ground slurry to 600-800 order, repeated hydrogenation sodium oxide is adjusted to neutrality, is drying to obtain;
Described a kind of book side glue, preparation method comprises the following steps:
(1) by weight by Japanese Asahi Chemical Industry EF1531EVA, compound jade powder, polyethylene, mixing, under 1600-1700 rev/min, stir 10-20 minute, put into kneader at 190-210 DEG C, mediate 18-22min, take out cooling;
(2) by the cooled sizing material of step (1) gained and all the other raw material blendings, twin screw extruder granulation at 180-200 DEG C, takes out and cools and get final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310426837.8A CN103509474B (en) | 2013-09-18 | 2013-09-18 | Book and periodical side glue |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310426837.8A CN103509474B (en) | 2013-09-18 | 2013-09-18 | Book and periodical side glue |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103509474A CN103509474A (en) | 2014-01-15 |
| CN103509474B true CN103509474B (en) | 2015-07-01 |
Family
ID=49892918
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310426837.8A Active CN103509474B (en) | 2013-09-18 | 2013-09-18 | Book and periodical side glue |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103509474B (en) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104119835A (en) * | 2014-06-26 | 2014-10-29 | 安徽图强文具股份有限公司 | Non-toxic hot-melt adhesive containing bone glue and for bookbinding of notebook |
| CN104119818A (en) * | 2014-06-26 | 2014-10-29 | 安徽图强文具股份有限公司 | Vermiculite powder-containing quick-drying hot melt adhesive for notebook bonding |
| KR102116545B1 (en) | 2015-06-30 | 2020-05-28 | (주)아모레퍼시픽 | Composite Powder of Porous Polymer Impregnated with Jade Powder Particle, Cosmetic Composition Comprising the Same and the Manufacturing Method Thereof |
| CN106244104A (en) * | 2016-08-28 | 2016-12-21 | 欧振云 | A kind of low-cost hot-melt adhesive |
| CN107815292A (en) * | 2017-11-22 | 2018-03-20 | 苏州市宽道模具机械有限公司 | A kind of wax-based binder based on nano material doping and preparation method thereof |
| CN108546521A (en) * | 2018-03-28 | 2018-09-18 | 杨帮燕 | A kind of preparation method of heat-resistant moisture-proof type tape |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS60221474A (en) * | 1984-04-18 | 1985-11-06 | Toyo Soda Mfg Co Ltd | Adhesive resin composition |
| CN1197475A (en) * | 1995-09-26 | 1998-10-28 | 阿托·芬德利公司 | Hot-melt pressure sensitive adhesive for ahdesive strips |
| CN101092101A (en) * | 2007-08-14 | 2007-12-26 | 李红军 | Method for preparing artware of synthesized jade with drawing of wheat straw hood |
| CN102838949A (en) * | 2012-09-27 | 2012-12-26 | 浙江固特热熔胶有限公司 | Back glue for books and magazines and production method thereof |
-
2013
- 2013-09-18 CN CN201310426837.8A patent/CN103509474B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS60221474A (en) * | 1984-04-18 | 1985-11-06 | Toyo Soda Mfg Co Ltd | Adhesive resin composition |
| CN1197475A (en) * | 1995-09-26 | 1998-10-28 | 阿托·芬德利公司 | Hot-melt pressure sensitive adhesive for ahdesive strips |
| CN101092101A (en) * | 2007-08-14 | 2007-12-26 | 李红军 | Method for preparing artware of synthesized jade with drawing of wheat straw hood |
| CN102838949A (en) * | 2012-09-27 | 2012-12-26 | 浙江固特热熔胶有限公司 | Back glue for books and magazines and production method thereof |
Non-Patent Citations (1)
| Title |
|---|
| "如何正确使用EVA热熔胶开好无线胶订机";王淮珠;《印刷杂志》;20030131(第1期);第81-84页 * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103509474A (en) | 2014-01-15 |
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| C14 | Grant of patent or utility model | ||
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