CN103498386A - Pearlescent pigment anti-fake cigarette paper and manufacturing method thereof - Google Patents
Pearlescent pigment anti-fake cigarette paper and manufacturing method thereof Download PDFInfo
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- CN103498386A CN103498386A CN201310483399.9A CN201310483399A CN103498386A CN 103498386 A CN103498386 A CN 103498386A CN 201310483399 A CN201310483399 A CN 201310483399A CN 103498386 A CN103498386 A CN 103498386A
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Abstract
The invention discloses pearlescent pigment anti-fake cigarette paper and a manufacturing method thereof. Visually-visible pearlescent pigments are uniformly distributed on the front or on the front and the back of the pearlescent pigment anti-fake cigarette paper, and have scattered twinkling lightspots. The method includes adding the pearlescent pigments after chemical pretreatment into fiber size or filler which is a main raw material for production of the cigarette paper, and executing normal papermaking processes to enable the pearlescent pigments to be added in the cigarette paper; or adding the pearlescent pigments after chemical pretreatment into a surface sizing agent, and forming a pearlescent pigment anti-fake marker on the front of the cigarette paper. By pretreating the pearlescent pigments, the technical quality problem that the pearlescent pigments are low in retention rate, uniform in distribution, poor in binding force and the like is solved; the pearlescent pigments enable the cigarette paper to present pearlescent visual effect in bits and pieces and in various colors, and form the anti-fake marker which is obvious and attractive, so that anti-fake effect of the cigarette paper is realized; the pearlescent pigment anti-fake cigarette paper is manufactured mainly by utilizing existing cigarette paper production processes and equipment, thereby being low in cost.
Description
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Technical field
The present invention relates to Anti-counterfeiting cigarette paper, be specifically related to a kind of pearlescent pigment Anti-counterfeiting cigarette paper and preparation method thereof.
Background technology
Simple, the feasible representative false proof measure of paper is mainly the anti-counterfeiting coating white card paper patented technology that adopts colored fiber, be about to wholely cut well-graded colored fiber water and be uniformly dispersed, be chosen in bottom (or sandwich layer) beater floor or paper machine bottom (or sandwich layer) stream send section that colored fiber is joined in paper pulp, and it is uniformly dispersed, obtain bottom (or sandwich layer) slurry, then deliver to the paper machine and manufactured paper with pulp together with surface layer, thereby form the anti-counterfeiting coating white card paper that bottom (or sandwich layer) is evenly distributed with colored fiber.This technology provides a kind of investment less, is applicable to the wrapping anti-counterfeiting coating white card paper of general merchandise and production technology thereof.The anti-counterfeiting technology of colored fiber is to add a small amount of colored fiber in the bottom paper of art post paperboard, makes the art post paperboard bottom surface have macroscopic, the dispergated colored fiber of any angle, has affected the purity of the original true qualities in page bottom surface; Colored fiber is normally used organic dye dyeing, has the safe and sanitary defect problem.
Pearlescent pigment, consist of several metal thin oxide layer Wrapping sheet shape base material.Change thin layer of metal oxide, just can produce different pearl effects.Pearlescent pigment is compared with other pigment, and its distinctive soft pearly luster has unrivaled effect.The pearlescent pigment content of beary metal is low, meets the associated safety technical standard.
Due to the factor such as laminated structure, surface electrical negativity and the proportion of pearlescent pigment is larger, mix and add in paper or the paper surface if simple, will cause pearlescent pigment exist retention in paper low, the paper skewness and with the technical quality problems such as the paper fibrous binding force is poor.Retention is low causes the pearlescent pigment that needs to add more pearlescent pigment and loss can affect the paper machine system of manufacturing paper with pulp; Skewness also will cause using more pearlescent pigment, and cost improves; Poor with the paper fibrous binding force is that pearlescent pigment easily comes off from paper, affects the quality of antifalse effect and paper.
At present, pearlescent pigment not yet is disclosed or reports for Anti-counterfeiting cigarette paper.
Summary of the invention
The shortcoming that the object of the invention is to overcome prior art, with not enough, provides a kind of pearlescent pigment Anti-counterfeiting cigarette paper.
Another object of the present invention is to provide the preparation method of above-mentioned pearlescent pigment Anti-counterfeiting cigarette paper.
Purpose of the present invention is achieved through the following technical solutions:
A kind of pearlescent pigment Anti-counterfeiting cigarette paper, its front (after the packing cigarette, being exposed to outer one side) or positive and negative (obverse and reverse) are uniformly distributed the visible pearlescent pigment of vision, make cigarette paper there is flicker bright spot fragmentarily, and form anti-fake mark, reach the antifalse effect of cigarette paper; Can, according to client's different requirements, by changing the kind of pearlescent pigment, realize different gloss and interference colours.
In described pearlescent pigment, the content of beary metal such as lead, arsenic meet state food packing body paper sanitary standard (GB11680-89).
Described pearlescent pigment is preferably optic metachromatic pearlescent pigment (OVP), and when adopting the optic metachromatic pearlescent pigment, the cigarette paper front can produce the changeable colors along with angle optical effect.
The particle size range of described pearlescent pigment is preferably 5～2000 microns; The consumption of described pearlescent pigment is preferably 0.0001～0.2g/m
2(pearlescent pigment weight and finished cigarettes paper Area Ratio).
The preparation method of above-mentioned pearlescent pigment Anti-counterfeiting cigarette paper, comprising the steps: that the pearlescent pigment that will process with chemical treatments adds in the pulping of having pulled an oar mixes, stirs with fibre stuff, carry out again machine hand's process flow, make pearlescent pigment can add in cigarette paper, at the cigarette paper positive and negative, form the pearlescent pigment anti-fake mark;
Maybe the pearlescent pigment of processing with chemical treatments is added in copy paper filler preparation facilities and mixes, stirs with filler, by machine hand's process flow, pearlescent pigment is added in cigarette paper together in company with filler, at the cigarette paper positive and negative, form the pearlescent pigment anti-fake mark;
The pearlescent pigment that maybe will process with chemical treatments mixes, stirs with Cypres, by surface sizing device paint cigarette paper front, at the positive formation of cigarette paper pearlescent pigment anti-fake mark.
Described chemical treatments comprises calgon, polyacrylate, carboxymethyl cellulose, quaternary ammonium salt cationic starch.
Preferably, the preparation method of described pearlescent pigment Anti-counterfeiting cigarette paper, comprise the steps: to adopt in advance quaternary ammonium salt cationic starch and calgon to process pearlescent pigment, again the pearlescent pigment after processing is added in the pulping of having pulled an oar and mixes, stirs with fibre stuff, carry out again machine hand's process flow, make pearlescent pigment can add in cigarette paper, at the cigarette paper positive and negative, form the pearlescent pigment anti-fake mark;
Or adopt in advance quaternary ammonium salt cationic starch, calgon to process pearlescent pigment, again the pearlescent pigment after processing is added in copy paper filler preparation facilities and mixes, stirs with filler, by machine hand's process flow, pearlescent pigment is added in cigarette paper together in company with filler, at the cigarette paper positive and negative, form the pearlescent pigment anti-fake mark;
Or adopt in advance Sodium Polyacrylate and carboxymethyl cellulose to process pearlescent pigment, again the pearlescent pigment after processing is mixed, stirs with Cypres, by surface sizing device paint cigarette paper front, at the positive formation of cigarette paper pearlescent pigment anti-fake mark.
The pearlescent pigment Anti-counterfeiting cigarette paper is cigarette packaging material, when adopting pearlescent pigment to add in slurry or filler, due to the reasons such as papermaking process factor that cigarette paper is quantitatively little, paper is thin and intrinsic, make the positive and negative of pearlescent pigment Anti-counterfeiting cigarette paper be distributed with the pearlescent pigment anti-counterfeiting mark, but positive pearlescent pigment sign is more than reverse side; To thering is the cigarette paper production of surface sizing technique requirement, adopt pearlescent pigment to add in Cypres, only pearlescent pigment directly is applied over to the cigarette recto, can reduce the consumption of pearlescent pigment.During the packing cigarette; pearlescent pigment Anti-counterfeiting cigarette paper reverse side is interior, front outside, along with the be visible to the naked eye pearlescent pigment anti-counterfeiting mark of different color effect of the rotation of finished product cigarette; play the protection manufacturer rights and interests, prevent the effect of counterfeit goods, also have aesthetic function simultaneously.
The present invention has following advantage and effect:
The present invention carries out Chemical Pretreatment to pearlescent pigment, the retention of pearlescent pigment, the cohesive force on surface and dispersiveness and the dispersion stabilization in water have been improved, the pearlescent pigment that relative usage does not deal with, its pearlescent pigment exists the retention in paper can bring up to 76% by 48%; Pearlescent pigment distribution evenness difference is reduced to 25% by 68%; Pearlescent pigment and paper fiber bonding strength are brought up to 0.6m/s by 0.3m/s; Solved that the pearlescent pigment retention is low, skewness and the technical quality problems such as adhesion is poor.
Pearlescent pigment Anti-counterfeiting cigarette paper front of the present invention or positive and negative are uniformly distributed the visible pearlescent pigment of vision, and, according to the different series pearlescent pigment, present pearly-lustre visual effect fragmentarily of all kinds, form anti-fake mark, anti-fake mark is obviously attractive in appearance, reaches the anti-fake effect of cigarette paper.Pearlescent pigment anti-fake mark characteristics: when with the custom angle, observing paper surface and common paper without any difference, but at inclination angle (when light source equals paper to the angle of reflection of eyes to the incidence angle of paper) while observing, naked eyes can be easy to see pearly-lustre point of scintillation (especially successful under spot light), anti-counterfeiting mark has certain disguise (also easily causing people's curiosity and mystique), does not affect the purity of the original true qualities in paper surface; During perusal, along with the variation of angle, different pearlescent pigments can present different colours flicker bright spot, is easy to identification and has again a beautification function; The color effect of pearlescent pigment is produced by its physical arrangement, nontoxic.
The preparation of pearlescent pigment Anti-counterfeiting cigarette paper of the present invention mainly utilizes ready-made cigarette paper production procedure and equipment, only need add one approximately 1 cubic metre of volume there is the preliminary treatment tank of stirring, heating function, anti-counterfeiting technology is simple, with low cost.
The specific embodiment
Below in conjunction with embodiment, the present invention is done to further detailed description, but embodiments of the present invention are not limited to this.If do not specialize, the conventional means that in embodiment, technological means used is well known to those skilled in the art.
The production embodiment of pearlescent pigment Anti-counterfeiting cigarette paper of the present invention, to add the commodity pearlescent pigment in the existing cigarette paper technological process of production, respectively the pearlescent pigment suspension through Chemical Pretreatment is added in fibre stuff or copy paper filler or Cypres, further disperse pearlescent pigment by the facility in existing procedure, by copy paper technique, realize the technology of the present invention.
Pearlescent pigment exists the measurement of the retention in paper to adopt " mensuration of paper making raw material, paper pulp, paper and cardboard ash content " method, GB/T 742-2008.Pearlescent pigment distribution evenness difference is: the granule number in A4 area sample in the most intensive one square centimeter of pearlescent pigment particle with the most sparse one square centimeter in granule number poor, with respect to the percentage of average grain number of every square centimeter in sample.The measurement of pearlescent pigment and paper fiber bonding strength adopts " mensuration of paper and cardboard printing surface strength " method, GB/T 22365-2008.
Embodiment 1
Select approximately 5 microns of pearlescent pigment average grain diameters, the pearlescent pigment consumption is 0.0001g/m
2.Pearlescent pigment Chemical Pretreatment mode is, adds 2 parts of 100 parts, water and carboxymethyl celluloses in the preliminary treatment tank by mass fraction, adds 0.02 part of 1 part of pearlescent pigment and calgon after stirring and dissolving, stirring at normal temperature 90 minutes again; The addition manner of pearlescent pigment is, to join in the Cypres preparation facilities by the pearlescent pigment suspension of consumption requirement metering, mix with Cypres, press surface sizing technique and implement the top sizing to the cigarette paper front, make pearlescent pigment can be evenly distributed on the cigarette paper front.Measure of merit: than under junior, the pearlescent pigment molecule bright spot that at the bottom of paper, (instead) face can may be seen indistinctly and be evenly distributed; Pearlescent pigment and paper fiber bonding strength are 0.6m/s.According to the described method of the present embodiment, if pearlescent pigment does not have through Chemical Pretreatment, pearlescent pigment and paper fiber bonding strength are 0.4m/s.
Embodiment 2
Select approximately 2000 microns of pearlescent pigment average grain diameters, the pearlescent pigment consumption is 0.2g/m
2.Pearlescent pigment Chemical Pretreatment mode is, adds 1.2 parts of 100 parts, water and quaternary ammonium salt cationic starch in the preliminary treatment tank by mass fraction, is warmed up to 90 ℃ of gelatinizations, adds 0.01 part of 1 part of pearlescent pigment and calgon after gelatinization completes again, and Yu Wen stirs 50 minutes; The addition manner of pearlescent pigment is, pearlescent pigment suspension by consumption requirement metering is added in the machine chest of having pulled an oar, and the agitator in machine chest stirs, and pearlescent pigment is mixed with fibre stuff, carry out again machine hand's process flow, make pearlescent pigment add in cigarette paper.Measure of merit: the high-visible pearlescent pigment bulky grain of (instead) face bright spot at the bottom of paper; Pearlescent pigment average grain number is 12/cm
2; Pearlescent pigment distribution evenness difference is 42%; Pearlescent pigment and paper fiber bonding strength are 0.35m/s; The retention of pearlescent pigment in paper is 76%.According to the described method of the present embodiment, if pearlescent pigment does not have through Chemical Pretreatment, pearlescent pigment average grain number is 9/cm
2; Pearlescent pigment distribution evenness difference is 56%; Pearlescent pigment and paper fiber bonding strength are 0.3m/s; The retention of pearlescent pigment in paper is 57%.
Embodiment 3
Select approximately 500 microns of pearlescent pigment average grain diameters, the pearlescent pigment consumption is 0.03g/m
2.Pearlescent pigment Chemical Pretreatment mode is, adds 1.5 parts of 100 parts, water and quaternary ammonium salt cationic starch in the preliminary treatment tank by mass fraction, is warmed up to 90 ℃ of gelatinizations, adds 0.01 part of 1 part of pearlescent pigment and calgon after gelatinization completes again, and Yu Wen stirs 60 minutes; The addition manner of pearlescent pigment is, pearlescent pigment suspension by consumption requirement metering is added in the machine chest of having pulled an oar, and the agitator in machine chest stirs, and pearlescent pigment is mixed with fibre stuff, carry out again machine hand's process flow, make pearlescent pigment add in cigarette paper.Measure of merit: the high-visible pearlescent pigment particle bright spot of (instead) face energy at the bottom of paper; Pearlescent pigment average grain number is 21/cm
2; Pearlescent pigment distribution evenness difference is 29%; Pearlescent pigment and paper fiber bonding strength are 0.45m/s; The retention of pearlescent pigment in paper is 73%.According to the described method of the present embodiment, if pearlescent pigment does not have through Chemical Pretreatment, pearlescent pigment average grain number is 15/cm
2; Pearlescent pigment distribution evenness difference is 60%; Pearlescent pigment and paper fiber bonding strength are 0.33m/s; The retention of pearlescent pigment in paper is 52%.
Embodiment 4
Select approximately 650 microns of pearlescent pigment average grain diameters, the pearlescent pigment consumption is 0.02g/m
2.Pearlescent pigment Chemical Pretreatment mode is, adds 2 parts of 100 parts, water and quaternary ammonium salt cationic starch in the preliminary treatment tank by mass fraction, is warmed up to 90 ℃ of gelatinizations, adds 0.01 part of 1 part of pearlescent pigment and Sodium Polyacrylate after gelatinization completes again, and Yu Wen stirs 80 minutes; The addition manner of pearlescent pigment is, pearlescent pigment suspension by consumption requirement metering is added in copy paper filler preparation facilities, mix, stir with filler by the agitator in the filler preparation facilities, then by the filler adding technology, pearlescent pigment is added in cigarette paper together in company with filler.Measure of merit: the pearlescent pigment particle bright spot at the bottom of paper on (instead) face is high-visible; Pearlescent pigment average grain number is 12/cm
2; Pearlescent pigment distribution evenness difference is 33%; Pearlescent pigment and paper fiber bonding strength are 0.4m/s; The retention of pearlescent pigment in paper is 76%.According to the described method of the present embodiment, if pearlescent pigment does not have through Chemical Pretreatment, pearlescent pigment average grain number is 9/cm
2; Pearlescent pigment distribution evenness difference is 56%; Pearlescent pigment and paper fiber bonding strength are 0.32m/s; The retention of pearlescent pigment in paper is 57%.
Embodiment 5
Select approximately 400 microns of pearlescent pigment average grain diameters, the pearlescent pigment consumption is 0.004g/m
2.Pearlescent pigment Chemical Pretreatment mode is, adds 1.5 parts of 100 parts, water and carboxymethyl celluloses in the preliminary treatment tank by mass fraction, adds 0.01 part of 1 part of pearlescent pigment and calgon after stirring and dissolving, stirring at normal temperature 70 minutes again; The addition manner of pearlescent pigment is, to join in the Cypres preparation facilities by the pearlescent pigment suspension of consumption requirement metering, mix with Cypres, press surface sizing technique and implement the top sizing to the cigarette paper front, make pearlescent pigment can be evenly distributed on the cigarette paper front.Measure of merit: at the bottom of paper, (instead) face can be shown in pearlescent pigment particle bright spot clearly; Pearlescent pigment average grain number is 4/cm
2; Pearlescent pigment distribution evenness difference is 25%; Pearlescent pigment and paper fiber bonding strength are 0.6m/s.According to the described method of the present embodiment, if pearlescent pigment does not have through Chemical Pretreatment, pearlescent pigment average grain number is 4/cm
2; Pearlescent pigment distribution evenness difference is 50%; Pearlescent pigment and paper fiber bonding strength are 0.5m/s.
Above-described embodiment is preferably embodiment of the present invention; but embodiments of the present invention are not restricted to the described embodiments; other any do not deviate from change, the modification done under Spirit Essence of the present invention and principle, substitutes, combination, simplify; all should be equivalent substitute mode, within being included in protection scope of the present invention.
Claims (7)
1. a pearlescent pigment Anti-counterfeiting cigarette paper, it is characterized in that: its front or positive and negative are uniformly distributed the visible pearlescent pigment of vision, make cigarette paper have flicker bright spot fragmentarily.
2. pearlescent pigment Anti-counterfeiting cigarette paper according to claim 1, is characterized in that: by changing the kind of pearlescent pigment, realize different gloss and interference colours.
3. pearlescent pigment Anti-counterfeiting cigarette paper according to claim 1 is characterized in that: in described pearlescent pigment, content of beary metal meets state food packing body paper sanitary standard.
4. pearlescent pigment Anti-counterfeiting cigarette paper according to claim 1, it is characterized in that: described pearlescent pigment is the optic metachromatic pearlescent pigment.
5. pearlescent pigment Anti-counterfeiting cigarette paper according to claim 1, it is characterized in that: the particle size range of described pearlescent pigment is 5～2000 microns, the consumption of pearlescent pigment is 0.0001～0.2g/m
2.
6. the preparation method of the described pearlescent pigment Anti-counterfeiting cigarette paper of claim 1～5 any one, it is characterized in that comprising the steps: that the pearlescent pigment that will process with chemical treatments adds in the pulping of having pulled an oar with fibre stuff, mixes, stirs, carry out again machine hand's process flow, make pearlescent pigment can add in cigarette paper, at the cigarette paper positive and negative, form the pearlescent pigment anti-fake mark;
Maybe the pearlescent pigment of processing with chemical treatments is added in copy paper filler preparation facilities and mixes, stirs with filler, by machine hand's process flow, pearlescent pigment is added in cigarette paper together in company with filler, at the cigarette paper positive and negative, form the pearlescent pigment anti-fake mark;
The pearlescent pigment that maybe will process with chemical treatments mixes, stirs with Cypres, by surface sizing device paint cigarette paper front, at the positive formation of cigarette paper pearlescent pigment anti-fake mark;
Described chemical treatments comprises calgon, polyacrylate, carboxymethyl cellulose, quaternary ammonium salt cationic starch.
7. the preparation method of pearlescent pigment Anti-counterfeiting cigarette paper according to claim 6, it is characterized in that: adopt in advance quaternary ammonium salt cationic starch and calgon to process pearlescent pigment, again the pearlescent pigment after processing is added in the pulping of having pulled an oar and mixes, stirs with fibre stuff, carry out again machine hand's process flow, make pearlescent pigment can add in cigarette paper, at the cigarette paper positive and negative, form the pearlescent pigment anti-fake mark;
Or adopt in advance quaternary ammonium salt cationic starch, calgon to process pearlescent pigment, again the pearlescent pigment after processing is added in copy paper filler preparation facilities and mixes, stirs with filler, by machine hand's process flow, pearlescent pigment is added in cigarette paper together in company with filler, at the cigarette paper positive and negative, form the pearlescent pigment anti-fake mark;
Or adopt in advance Sodium Polyacrylate and carboxymethyl cellulose to process pearlescent pigment, again the pearlescent pigment after processing is mixed, stirs with Cypres, by surface sizing device paint cigarette paper front, at the positive formation of cigarette paper pearlescent pigment anti-fake mark.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310483399.9A CN103498386B (en) | 2013-10-16 | 2013-10-16 | Pearlescent pigment anti-fake cigarette paper and manufacturing method thereof |
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| CN201310483399.9A CN103498386B (en) | 2013-10-16 | 2013-10-16 | Pearlescent pigment anti-fake cigarette paper and manufacturing method thereof |
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| CN103498386A true CN103498386A (en) | 2014-01-08 |
| CN103498386B CN103498386B (en) | 2015-06-24 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106418686A (en) * | 2016-11-01 | 2017-02-22 | 湖北中烟工业有限责任公司 | Pearly luster coating membrane material of blasting beads for cigarette and preparation method of pearly luster blasting beads for cigarette |
| CN109072562A (en) * | 2016-02-01 | 2018-12-21 | 考代诺斯集团股份有限公司 | Pearly-lustre metal effect paper wood material and relative manufacturing process with high-light-fastness |
| CN115467189A (en) * | 2022-09-16 | 2022-12-13 | 万邦特种材料股份有限公司 | Method for manufacturing yellow high-transparency formed paper |
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| CN1082080A (en) * | 1992-07-30 | 1994-02-16 | 河南省新乡市印刷厂 | Temp-controlled antiforge agent for printing |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106418686A (en) * | 2016-11-01 | 2017-02-22 | 湖北中烟工业有限责任公司 | Pearly luster coating membrane material of blasting beads for cigarette and preparation method of pearly luster blasting beads for cigarette |
| CN115467189A (en) * | 2022-09-16 | 2022-12-13 | 万邦特种材料股份有限公司 | Method for manufacturing yellow high-transparency formed paper |
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