CN103478738B - A kind of composition with fat-reducing body shaping and Weight management effect - Google Patents

A kind of composition with fat-reducing body shaping and Weight management effect Download PDF

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CN103478738B
CN103478738B CN201310426107.8A CN201310426107A CN103478738B CN 103478738 B CN103478738 B CN 103478738B CN 201310426107 A CN201310426107 A CN 201310426107A CN 103478738 B CN103478738 B CN 103478738B
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composition
water
fat
navy bean
extract
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CN103478738A (en
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冯开东
梁卫文
余孝云
张蕴
刘娟
南春旺
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JIANKANGYUAN PHARMACEUTICAL GROUP CO Ltd
SHENZHEN TAITAI PHARMACEUTICAL INDUSTRY Co Ltd
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JIANKANGYUAN PHARMACEUTICAL GROUP CO Ltd
SHENZHEN TAITAI PHARMACEUTICAL INDUSTRY Co Ltd
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A23B - A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/385Concentrates of non-alcoholic beverages
    • A23L2/39Dry compositions
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A23B - A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L29/00Foods or foodstuffs containing additives; Preparation or treatment thereof
    • A23L29/30Foods or foodstuffs containing additives; Preparation or treatment thereof containing carbohydrate syrups; containing sugars; containing sugar alcohols, e.g. xylitol; containing starch hydrolysates, e.g. dextrin
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A23B - A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/20Reducing nutritive value; Dietetic products with reduced nutritive value
    • A23L33/21Addition of substantially indigestible substances, e.g. dietary fibres
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

Abstract

The present invention relates to a kind of composition with fat-reducing body shaping and Weight management effect.Said composition forms primarily of 30% ~ 80% water-soluble dietary fiber, 5% ~ 60% navy bean extract, 5% ~ 50% oligomeric Icing Sugar and 1% ~ 20% haw berry extract by weight percentage, it is for fat or overweight and not reach fat crowd all effective, can effectively lose weight, reduce fat percentage, contribute to reducing body fat, and can significantly improve its waistline, hip circumference, strengthen muscle, improve the bodily form, make stature more have curve, and can be used for Weight management; The crowd of said composition to hyperglycaemia and high fat of blood also has auxiliary therapeutic action; All right regulating intestinal canal flora in addition, improves human body intestinal canal beneficial bacteria breeding environment, promotes vivotoxin and metabolic waste excretion, reaches the effect of toxin-expelling and face nourishing; Composition taking convenience of the present invention, meets the fast pace life requirement of modern, and safe and effective, without any side effects.

Description

A kind of composition with fat-reducing body shaping and Weight management effect
Technical field
The present invention relates to a kind of composition, be specifically related to a kind of composition with fat-reducing body shaping and Weight management effect.
Background technology
Along with the development of society, the requirement of people to stature is more and more higher, fat or overweight and do not reach obese degree, has that strong desire is reduced weight, the moulding personage that likes to be beautiful can be found everywhere, and the market demand is extremely huge.The motion mode of going on a diet, can not adhere to for a long time of blindness is given on the contrary needs the people of weight reducing to bring reverse effect.The object that people are badly in need of a kind of convenience, safe and effective mode reaches body shaping and Weight management, the body shaping that current people commonly use and method for weight management mainly contain to be taken slimming medicine or diet food and wears body modelling dress etc.
At present, the slimming medicine on market has a lot, and its mode of action mainly contains appetite and controls, suppresses pipe intestinal digesting to absorb, increases energy ezpenditure etc.Appetite controlling agent can affect the nerves medium vigor, by central nervous system effect, realizes fat-reducing effect, but actual effect is limited and individual difference is larger.Suppress pipe intestinal digesting absorbent to mainly contain lipase inhibitor, glucosidase inhibitor and fat replacer, but these medicines have the gastrointestinal side effects such as certain intestinal tympanites, stomachache, diarrhoea.Increase energy ezpenditure agent can stimulate fat oxidation, increase energy ezpenditure, but patient easily produces the bad reactions such as anxiety, excitement, insomnia.
Diet food in the market comes with some shortcomings: some composition adds chemical composition in violation of rules and regulations, comprise sibutramine, phenolphthalein, melbine, insoral etc., and sibutramine is as a kind of depressor of nerve centre, may to cause elevation of the blood pressure, the serious side effects such as apocleisis, dysfunction of liver.
On the other hand, body-shaping slimming is also not equal to simple loss of weight, the weight of human body substantially by skeleton, muscle, fat and moisture four major part form, and be form by certain standard proportional, and common people too fat be because fat exceed standard, instead of due to muscle and moisture overweight.So only deduct fat, reduce the fat ratio in body weight, just can be really thin.If deducted the most muscle of health and moisture by some loss in weights, do not reach the object of fat-reducing so at all.And more seriously, if what cut is muscle and moisture, what bounce-back was returned is but fat, among that will be absorbed in and subtract more fat and more fat vicious circle.Meanwhile, due to the speed of the fat-reducing that covets, and ignore the necessary health slimming process of human body, unfavorable to health; And " bounce-back " is obvious, loses weight when taking, after withdrawing, body weight is recovered very soon; In addition, after fat-reducing, cutis laxa, wrinkle increases.
On market, another kind of body-shaping slimming mode wears body modelling dress, but the material of body modelling dress is ventilative not, affects skin perspiration, and body shaping underwear braces waist for a long time again, so easy extruding internal organs, hinders blood circulation, non-health body shaping mode.
Summary of the invention
For the problems referred to above, one object of the present invention is to provide a kind of composition.Said composition can lose weight effectively, reduce fat percentage, contribute to reducing body fat, strengthen muscle, have significant slimming effect, and intestinal beneficial flora in body can be improved, can be used for Weight management, and to the patient of hyperglycaemia, high fat of blood, there is auxiliary therapeutic action, be easy to as absorption of human body, long-term taking is without any side effects.
Another object of the present invention is to provide above-mentioned composition to have the purposes of losing weight in the composition of body shaping and Weight management effect in preparation.
Another object of the present invention is to provide above-mentioned composition preparing the purposes in the composition with hypoglycemic or reducing blood lipid auxiliary therapeutic action.
Another object of the present invention is the preparation method providing a kind of above-mentioned composition.
The object of the invention is to realize by the following technical solutions and solve.
Composition of the present invention forms primarily of 30% ~ 80% water-soluble dietary fiber, 5% ~ 60% navy bean extract, 5% ~ 50% oligomeric Icing Sugar and 1% ~ 20% haw berry extract by weight percentage.
Preferably, composition of the present invention forms primarily of 30% ~ 70% water-soluble dietary fiber, 5% ~ 50% navy bean extract, 5% ~ 20%L-arabinose, 5% ~ 50% oligomeric Icing Sugar and 1% ~ 20% haw berry extract by weight percentage.
Preferably, described oligomeric Icing Sugar is the mixture of xylo-oligosaccharide and FOS, and in described mixture, the ratio of xylo-oligosaccharide and FOS is 1:4 ~ 1:9.
Preferably, above-mentioned composition forms primarily of 40% ~ 60% water-soluble dietary fiber, 8% ~ 30% navy bean extract, 6% ~ 8%L-arabinose, 8% ~ 40% FOS, 2% ~ 5% xylo-oligosaccharide and 1% ~ 5% haw berry extract by weight percentage.
Preferably, described water-soluble dietary fiber is maize peel or wheat bran water-soluble dietary fiber.
Preferably, described water-soluble dietary fiber is maize peel water-soluble dietary fiber.
Preferably, described navy bean extract is through supercritical CO 2extract removal of impurities; Preferred employing water is as Extraction solvent, and in described navy bean extract, organic solvent-free remains;
Preferably, the AMS inhibit activities of described navy bean extract is greater than 3000AAIU/g.
Preferably, described navy bean extract is that commodity are called product.
More preferably, described composition is by weight percentage by 50% water-soluble dietary fiber, 10% navy bean extract 8%L-arabinose, 26% FOS, 4% xylo-oligosaccharide and 2% haw berry extract form.
Preferably, the pH value of 10g dissolution of solid in 100ml water of described composition is 3 ~ 7, and preferable ph is 3-5, and more preferably pH value is 4-5; Solution temperature is 20 ~ 80 DEG C, preferably 20 ~ 60 DEG C, is more preferably 30 ~ 40 DEG C.
Composition of the present invention, can be made into various formulation and takes orally, as tablet, capsule, granule, electuary, solid beverage, oral liquid or beverage etc.
Preferably, above-mentioned composition can be made into solid beverage.Optionally, above-mentioned composition can be added in coffee or fruit juice and drink.
Composition of the present invention not only contributes to reducing body fat, effectively loses weight, and has and significantly mould waist, mould the slimming effects such as stern, for fat or overweight and not reach the crowd of obesity all effective, also can be used for support weight management.Composition of the present invention can suppress the absorption of starch in food, and then reduce the absorption of heat, reach the object reducing fat and hoard, and improve intestinal beneficial flora in body, to ensure in body shaping process without any side effects and sense of discomfort (not hungry, do not suffer from diarrhoea, not weak, not apocleisis, do not rebound, not thirsty dizziness, do not affect sleep), antiobesity action is extremely healthy gentle, is suitable for any crowd of men and women, old and young and eats.
On the other hand, present invention also offers above-mentioned composition and there is in preparation the purposes of losing weight in the composition of body shaping and Weight management effect.
On the other hand, present invention also offers above-mentioned composition and prepare the purposes in the composition with hypoglycemic or reducing blood lipid auxiliary therapeutic action.
On the other hand, the invention provides a kind of preparation method of above-mentioned composition, described composition is solid beverage, and described preparation method comprises the steps:
1) each raw material is weighed by formulation weight;
2) each raw material is crossed 30 ~ 60 mesh sieves;
3) mixed by raw material batch mixer, incorporation time is 20 ~ 40min, and rotating speed is 20 ~ 30 revs/min;
4) quantitative package.
Below respectively the function of mentioned component is discussed:
Navy bean extract: navy bean (whitekidneybeans), formal name used at school scarlet runner bean, namely Kidney bean (PhaseolusVulgarisL.), calls white waist beans etc., belongs to pulse family, Papillionoideae, Phaseoleae Phaseolus.Navy bean originates in Mexico from America and Argentina, has adapted to by artificial cultivation domestication the moist area, plateau that cools.The country that cultivated area is larger is the Britain in Argentina in America, the U.S., Mexico, Europe, the China, Japan etc. in Asia.Navy bean rich in nutritive value, containing protein 19.9% ~ 20.0% in the dry beans of every 100g, fat 1.6% ~ 2.1%, carbohydrate 37.6% ~ 48.5%, calcium 120mg, iron l0mg.In addition, also containing Cobastab 11.56mg and Cobastab 21.02mg.Now there are some researches show, the alpha-amylase inhibitor containing greater activity in navy bean, navy bean extract extracts and obtains from navy bean, and its main component is alpha-amylase inhibitor.
Alpha-amylase inhibitor (α-amylaseinhibitor is called for short α-AI) is a kind of pure-natural biological active material, belongs to the one of glycoside hydrolase inhibitor, is abroad referred to as " starchblocker ".It is the activity by suppressing ptyalin and pancreaticα-amylase, hinders starch and the digestion of other carbohydrate in enteron aisle in food, thus reduces body to the absorption of sugar.Be characterized in, excrete through intestines and stomach, therefore blood circulation system need not be entered, do not act on brain centres, not appetite-suppressing while fat-reducing, do not affect absorption and the metabolism of other nutriment such as protein, vitamin, have no side effect when using dosage is very high yet, meet the fat-reducing principle of the World Health Organization.Asian dietary structure, based on starch, is therefore started with from the activity controlling body key enzyme, selects navy bean extract to have one of principal component of the composition of body shaping and Weight management effect as the present invention.
Water-soluble dietary fiber: be a kind of high-effect dietary fiber.Its on the one hand can make people have satiety and lower appetite and reach fat-reducing effect, on the other hand can food and extend time of staying in stomach, and sugared absorbed speed is slowed down.Its major physiological function comprises: recuperating gastrointestinal tract, reduction cholesterol, suppression blood sugar raise, prevention of obesity disease.
Arabinose: its function mainly contains two aspects, one is the enzyme that can suppress to be hydrolyzed disaccharide, the blood sugar caused because taking in sucrose therefore being suppressed to raise, being called for short the blood sugar reducing function suppressing disaccharide hydrolysis; Two is because Arabinose is to the inhibitory action of disaccharide hydrolase, the sucrose be not decomposed in small intestine is decomposed by the microorganisms in large intestine and produces a large amount of organic acids, this organic acid has inhibitory action to liver synthctic fat, add Arabinose to the inhibitory action absorbing sucrose in small intestine, thus reduce the generation of new fats in body.
Oligomeric Icing Sugar: be all heavy compound sugar, can not digest and assimilate in vivo, directly large intestine is entered after edible, had inhibitory action to harmful bacteria by beneficial bacteria in large intestine utilizes, fermentation produces organic acid, synthetic vitamin simultaneously, promote mineral absorption, suppress spoilage organisms growth, stimulating animal immunity function, plays trophism by immunization route simultaneously.
Oligomeric Icing Sugar in the present invention is mainly FOS and xylo-oligosaccharide, and it directly can improve gut flora, promotes profitable strain propagation, is beneficial to host health; And the absorption of the elements such as calcium, magnesium, iron, zinc can be promoted; The hydrochloric acid in gastric juice in its not digested road and enzymic digestion, can, by the flora Bifidobacterium selective absorbing useful to human body, make the profitable strain Bifidobacterium of human body breed rapidly; Suppress the growth of pernicious bacteria simultaneously, play the effect of removing enteron aisle rubbish; Pure natural, has no side effect; In addition, suitable proportioning between FOS and xylo-oligosaccharide is selected can to reach the effect of better adjustment blood sugar and can not waste be caused.
Haw berry extract: hawthorn is the dry fruit of rosaceous plant hawthorn (RosaceaecrataegusL.), taste is sour, property is sweet, tepor, returns spleen, stomach, Liver Channel.Have food digesting stomach fortifying, promoting the circulation of qi is fallen apart effect of the stasis of blood.Hawthorn, mainly containing flavonoids, oligomeric flavanoids, organic acid and trace element, also contains the compositions such as triterpenes, steroid and organic amine in addition.The flavone compound of haw thorn extract has prevention and cure of cardiovascular disease, hemangiectasis, increase CF, improve heart vigor, stimulating central nervous system system, reduce blood pressure and cholesterol, softening blood vessel and diuresis and sedation.Often take for patients such as diabetes, coronary heart disease, hypertension, hyperlipemia, there is the effect of prevention and therapy.In addition, containing malic acid, vitamin C, citric acid and pectin in hawthorn, can prevent pigment particles from accumulating in subcutaneous, the elasticity of vascular wall can also be protected, therefore also have beauty functions to skin.
Beneficial effect of the present invention is as follows:
1. composition of the present invention is for fat or overweight and not reach fat crowd all effective, it not only can lose weight effectively, reduce fat percentage, contribute to reducing body fat, and can significantly improve its waistline, hip circumference, strengthen muscle, improve the bodily form, make stature more have curve, and can be used for Weight management.
2. the crowd of composition of the present invention to hyperglycaemia and high fat of blood also has auxiliary therapeutic action.
3. composition of the present invention, all right regulating intestinal canal flora, improves human body intestinal canal beneficial bacteria breeding environment, promotes vivotoxin and metabolic waste excretion, can reach the effect of toxin-expelling and face nourishing.
4. composition of the present invention, can be made into solid beverage, and available warm water is taken after mixing it with water, and pH value when taking is 4-5, effectively ensure that the activity of alpha-amylase inhibitor in navy bean extract.
5. composition of the present invention, can be made into solid beverage, takes very convenient, meets the fast pace life requirement of modern, and safe and effective, without any side effects.
6. composition of the present invention, preparation technology is simple, easy to operate, is applicable to industrial production.
Accompanying drawing explanation
Fig. 1 is the changes of weight situation map of laying particular stress on experimenter in clinical testing;
Fig. 2 is the fat percentage situation of change figure laying particular stress on experimenter in clinical testing;
Fig. 3 is the waistline situation of change figure laying particular stress on experimenter in clinical testing;
Fig. 4 is the hip circumference situation of change figure laying particular stress on experimenter in clinical testing;
Fig. 5 is medium body weight experimenter mean variation situation map in clinical testing;
Fig. 6 is medium body weight experimenter maximum situation of change figure in clinical testing;
The AMS inhibit activities of Fig. 7 is pH value when being 3 present composition;
The AMS inhibit activities of Fig. 8 is pH value when being 5 present composition;
The AMS inhibit activities of Fig. 9 is pH value when being 7 present composition;
Figure 10 is preparation technology's flow chart of navy bean extract in the present composition;
The production technological process that Figure 11 is the present composition when being solid beverage.
Detailed description of the invention
Further illustrate the present invention below by way of specific embodiment, but following examples are only for illustration of the present invention but not for limiting the present invention.
Experimental technique in following embodiment, if no special instructions, is conventional method.Raw material used in following embodiment, reagent material etc., if no special instructions, be commercially available purchase product.
Below respectively the preparation method of each composition of composition of the present invention is illustrated.
Navy bean extract, adopts following technique to prepare: navy bean grinds after 1.5 ~ 2.0 hours through the 1.5%NaCl water soaking of 80 DEG C, and the navy bean through grinding is by supercritical CO 2extracting removal of impurities must containing the soya-bean cake of alpha-amylase inhibitor, and soya-bean cake extracts by deionized water again, and filtration, collection filtrate, Vacuum Concentration, pasteurization, spraying dry or freeze drying obtain navy bean extract.Navy bean extract preparation technology flow chart refers to Figure 10.The quality control index of the preferred navy bean extract of the present invention is in table 1.
The quality control index of table 1 navy bean extract
Wherein:
FTIR: infrared spectrum
KarlFischer: Karl_Fischer method
ICP:InductivelyCoupledPlasma inductively coupled plasma
AA: atomic absorption spectrophotometer
AOAC: AOAC
FDA-BAM:FoodandDrugAdministration-BecteriologicalAnalyticculManual
U.S. food Drug Administration microbiological analysis handbook
Veratox:Veratox aflatoxins kit
AAIU: α-amylaseinhibitorunit, AMS inhibit activities.
Navy bean extract also can with reference to PurificationandPropertiesofPhaseolamin, anInhibitorof α-amylase, fromtheKidneyBean, Phaseolusvulgaris (J.JohnMarmen, M.Lauda, JournalofBiologicalChemistry, Vol.250, No.20, IssueofOctober25, P8030 ~ 8037,1975) preparation.Also (American-European import) navy bean extract can be bought from Shanghai Tong Yuan food technology Co., Ltd or it is by name directly to buy commodity navy bean extract.
Wheat bran water-soluble dietary fiber, can be prepared by following technique: wheat bran is carried out drying and processing at 60 DEG C, add the hot water (wheat: hot water=1:10) of 70 ~ 80 DEG C, add hydrochloric acid, NaOH, AMS and carbohydrase and be hydrolyzed, then wash, centrifugal dehydration, high temperature goes out enzyme (110 DEG C), dry (110 DEG C, 2h), bleaching, extrusion cooking and ultramicro grinding, obtain the wheat bran dietary fiber refined.Also can buy from French Roquette Freres.
Maize peel water-soluble dietary fiber, can be prepared by following technique: soaked by maize peel, and washing removing impurity, then adopts endogenous enzyme process to remove phytic acid (temperature 60 C, pH5.0, reaction 4h), remove starch, remove albumen, dry, pulverize, sieve, obtain maize peel water-soluble dietary fiber powder.Also can buy from Shanghai Tong Yuan food technology Co., Ltd, be the loose paddy chemical products of Japan.
Oligomeric Icing Sugar: purchased from Jiangmen Quantum High-tech Biology Co., Ltd.
FOS, can be prepared by following technique: sucrose through water-soluble solution (containing sucrose concentration: 50% ~ 60%), inject immobilization bed bioreactor inside holding (50 DEG C ~ 60 DEG C) maintenance and obtain liquid glucose in 24 hours, liquid glucose is through activated carbon decolorizing, lead to the desalination of sodium filter membrane again by ion exchange resin (liquid glucose: resin=6:1) and obtain FOS liquid, FOS liquid obtains concentrate through Vacuum Concentration, obtains FOS powder after concentrate is spray-dried.Also can buy from Jiangmen Quantum High-tech Biology Co., Ltd.
Xylo-oligosaccharide, can be prepared by following technique: pulverized by corncob and mix with water, add weak acid catalyst and carry out cracking, by the xylan stripping in corncob; The pH value regulating the xylan aqueous solution is 4.5 ~ 6.5, adds zytase and carries out enzymolysis, under the high temperature of 90 DEG C ~ 100 DEG C, carry out deactivation to zytase; Slag also discards by filtering maize cob meal, then carries out active carbon and ion exchange resin removal of impurities decolouring to xylan liquid glucose; And sodium filter membrane concentrating and desalinating; Be thick pale yellow shape syrup by xylo-oligosaccharide liquid glucose Vacuum Concentration, xylo-oligosaccharide syrup is dried to xylo-oligosaccharide powder through excipient or Direct spraying.Also can buy from Shandong Longli Biology Science and Technology Co., Ltd.
Haw berry extract, can be prepared by following technique: uctus Crataegi is dropped in extractor, add 6 times amount of medicinal material amount, 4 times of water gagings extract 2 times altogether, obtain extract, then by extract filtration, removing impurities, obtain hawthorn concentrate through concentrated, hawthorn concentrate is spray-dried obtains haw berry extract.Also can buy from flying dragon bio tech ltd, Henan.
Arabinose, can be prepared by following technique: after corncob or the bagasse through squeezing sugar being pulverized, first with hot water (70 DEG C ~ 80 DEG C) lixiviate 4 ~ 6 hours, extracting concentrate, then extracting araban through the ethanol precipitating of 75% concentration; Then the hydrochloric acid solution enzyme hydrolysis araban of 1.5% concentration is adopted to prepare Arabinose.Also can buy from Shandong Fook Tin Technologies Ltd..
The key component screening experiment of the present composition:
1. the screening of navy bean extract:
Navy bean is suitable in temperate zone and the growth of tropical high altitude localities, and property happiness is warm, not resistance to frost.Suitable geographical environmental condition makes to suppress the active constituent content of alpha-amylase activity higher in navy bean.Therefore the navy bean of our preferred original producton location north America region is main material.
The alpha-amylase inhibitor obtained in some navy bean extract, without purification, comprises toxic components (as phytolectin), impurity or pollutant.These impurity are actually solvent residue and inactive component, can cause active ingredient reduced activity.When adding in the food such as solid beverage, bland, residual impurity and pollutant easily cause disagreeable taste, make these food not cause appetite.
Therefore we are further preferably through the purer navy bean extract of purification process, preferably through supercritical CO 2extract the navy bean extract of removal of impurities; Preferred employing water is as Extraction solvent, and in navy bean extract, organic solvent-free remains.
We screen discovery further, the indexs such as the ratio of the just extraction of mark raw material and finished product on the product specification list of current some navy bean extract are on the market (as 10:1,12:1 etc.), and what really work in navy bean extract is to the inhibited composition of amylase activity, AMS suppresses the activity of composition to be applicable to AAIU(α-amylaseinhibitorunit) evaluate, lack this efficiency index of AAIU, the AMS inhibit activities of navy bean extract can be caused unstable, and the effect of such product cannot ensure.
Result shows, and the active unit of navy bean extract is for having the effect of fat-reducing body shaping more significantly by the effective guarantee present composition when being greater than 3000AAIU/g.
Therefore the active unit of further preferably navy bean extract is for being greater than 3000AAIU/g.
Further preferably, the navy bean extract that the present invention chooses is that commodity are called navy bean (Phaseolusvulgaris) extract.
navy bean (Phaseolusvulgaris) extract is researched and developed by Pharmachem company of the U.S., is current first effective Starch blockers through complete toxicity, human clinical trial's checking in the world, and by U.S. GRAS certification.At present in the world existing 14 independently clinical report confirm the security of product and validity.This product is the new resource food that ministry of Health of China approval in 2011 enters China's Mainland.
2. the screening of water-soluble dietary fiber:
By by 20 health adults tested corn source and wheat bran source water-soluble dietary fiber 2 weeks respectively, compare the change of capacity.
Result shows, and the people taking corn dietary fiber reacts aerogenesis hardly, and the people taking wheat bran dietary fiber reacts enteron aisle and has flatulence.Therefore, in order to be suitable for crowd widely, its work and life is not affected, the water-soluble dietary fiber of our preferred corn source.
3. the screening of compound sugar:
Different types of compound sugar, the difference of its structure, composition and glycosidic bond can be different to the suppression of the increment of beneficial bacterium in body and harmful bacteria.
We find through research, xylo-oligosaccharide, FOS and galactooligosaccharide can be utilized by beneficial bacterium (mainly Bifidobacterium and lactic acid bacteria), but galactooligosaccharide is excessive ingest after can cause what is called " osmotic diarrhea ", therefore in order to be suitable for crowd widely, our preferred FOS and xylo-oligosaccharide.Xylo-oligosaccharide and FOS by enteric bacteria utilization power in table 2.
Table 2 xylo-oligosaccharide and FOS are by enteric bacteria utilization power
Pseudomonas FOS Xylo-oligosaccharide
Bifidobacterium adolescentis
Bifidobacterium infantis
Bifidobacterium longum
Bifidobacterium breve
Lactobacillus acidophilus
Saliva Bacillus acidi lactici
Comprehensive xylo-oligosaccharide and FOS are by factors such as enteric bacteria utilization power and products tastes, and in our preferred composition, the proportioning of xylo-oligosaccharide and FOS is in 1:4 to 1:9 scope.
Be below specific embodiments of the invention.
embodiment 1the preparation of navy bean extract
1000g navy bean is put into grinder through the 1.5%NaCl water soaking of 80 DEG C after 1.5 ~ 2.0 hours grind, the navy bean after grinding is imported in extractor, adopt supercritical CO 2extract 3 hours at 60 DEG C, obtain the soya-bean cake containing alpha-amylase inhibitor after removal of impurities, soya-bean cake deionized water is extracted 5 hours at 50 DEG C, after filtration, collection filtrate, Vacuum Concentration, obtain navy bean extract 120g after pasteurization and spraying dry.Navy bean extract preparation technology flow chart refers to Figure 10.
Table 3 lists the testing result of the navy bean extract of above-mentioned preparation, and as seen from Table 3, the indices of the navy bean extract of preparation all meets standard-required.
The testing result of table 3 navy bean extract
The navy bean extract that the composition of following examples 2,4,7,9,11 adopts above-mentioned technique to prepare; Embodiment 3,5,6,8,10 buys (American-European import) navy bean extract from Shanghai Tong Yuan food technology Co., Ltd
embodiment 2the preparation of composition (tablet)
A kind of composition, the percentage by weight of its each component is respectively: 30% corn water-soluble dietary fiber, 5% navy bean extract, 5%L-arabinose, 45% FOS, 5% xylo-oligosaccharide and 10% haw berry extract.
Preparation method: get after the water-soluble dietary fiber of recipe quantity, FOS powder, navy bean extract, Arabinose, xylo-oligosaccharide powder and haw berry extract cross 30 mesh sieves, obtain mixed material after mixing 20 minutes by automatic lifting mixer under 20 revs/min.Then in mixed material, add dolomol, compressing tablet after mixing, obtains tablet.
embodiment 3the preparation of composition (capsule)
A kind of composition, the percentage by weight of its each component is respectively: 40% wheat bran water-soluble dietary fiber, 6% navy bean extract, 20%L-arabinose, 25% FOS, 5% xylo-oligosaccharide and 4% haw berry extract.
Preparation method: get after the water-soluble dietary fiber of recipe quantity, FOS powder, navy bean extract, Arabinose, xylo-oligosaccharide powder and haw berry extract cross 40 mesh sieves, obtain mixed material after mixing 30 minutes by automatic lifting mixer under 20 revs/min.Then in mixed material, add dolomol and starch mixing, incapsulate, obtain capsule.
embodiment 4the preparation of composition (granule)
A kind of composition, the percentage by weight of its each component is respectively: 50% wheat bran water-soluble dietary fiber, 8% navy bean extract, 7%L-arabinose, 25% FOS, 5% xylo-oligosaccharide and 5% haw berry extract.
Preparation method: get after the water-soluble dietary fiber of recipe quantity, FOS powder, navy bean extract, Arabinose, xylo-oligosaccharide powder and haw berry extract cross 50 mesh sieves, obtain mixed material after mixing 20 minutes by automatic lifting mixer under 30 revs/min.Then granulate with ethanol wet, wet granular is dry, and whole grain, obtains granule.
embodiment 5the preparation of composition (solid beverage)
A kind of composition, the percentage by weight of its each component is respectively: 50% corn water-soluble dietary fiber, 10% navy bean extract, 8%L-arabinose, 26% FOS, 4% xylo-oligosaccharide and 2% haw berry extract.
Preparation method: get after the water-soluble dietary fiber of recipe quantity, FOS powder, navy bean extract, Arabinose, xylo-oligosaccharide powder and haw berry extract cross 60 mesh sieves, obtain mixed material after mixing 30 minutes by automatic lifting mixer under 30 revs/min.Quantitative package, obtains solid beverage.The production technological process of solid beverage is shown in Figure 11.
embodiment 6the preparation of composition (electuary)
A kind of composition, the percentage by weight of its each component is respectively: 60% corn water-soluble dietary fiber, 15% navy bean extract, 9%L-arabinose, 12% FOS, 3% xylo-oligosaccharide and 1% haw berry extract.
Preparation method: get after the water-soluble dietary fiber of recipe quantity, FOS powder, navy bean extract, Arabinose, xylo-oligosaccharide powder and haw berry extract cross 50 mesh sieves, obtain mixed material after mixing 40 minutes by automatic lifting mixer under 20 revs/min.Quantitative package, obtains electuary.
embodiment 7the preparation of composition (oral liquid)
A kind of composition, the percentage by weight of its each component is respectively: 70% corn water-soluble dietary fiber, 10% navy bean extract, 8%L-arabinose, 8% FOS, 2% xylo-oligosaccharide and 2% haw berry extract.
Preparation method: get after the water-soluble dietary fiber of recipe quantity, FOS powder, navy bean extract, Arabinose, xylo-oligosaccharide powder and haw berry extract cross 60 mesh sieves, obtain mixed material after mixing 20 minutes by automatic lifting mixer under 30 revs/min.Then in mixed material, add sorbierite, purified water, heating is boiled, and stirs, and leaves standstill 24 hours, and filter, embedding becomes bottle, and sterilizing obtains oral liquid.
embodiment 8the preparation of composition (fruit drink)
A kind of composition, the percentage by weight of its each component is respectively: 80% corn water-soluble dietary fiber, 9% navy bean extract, 10% oligomeric Icing Sugar (purchased from Jiangmen Quantum High-tech Biology Co., Ltd) and 1% haw berry extract.
Preparation method: get after the water-soluble dietary fiber of recipe quantity, navy bean extract, oligomeric Icing Sugar and haw berry extract cross 60 mesh sieves, obtain mixed material after mixing 30 minutes by automatic lifting mixer under 30 revs/min.Quantitative package, obtains solid beverage.Optionally add in fruit juice and can obtain fruit drink.
embodiment 9the preparation of composition (chewable tablets)
A kind of composition, the percentage by weight of its each component is respectively: 30% corn water-soluble dietary fiber, 60% navy bean extract, 5% oligomeric Icing Sugar (purchased from Jiangmen Quantum High-tech Biology Co., Ltd) and 5% haw berry extract.
Preparation method: get after the water-soluble dietary fiber of recipe quantity, navy bean extract, oligomeric Icing Sugar and haw berry extract cross 60 mesh sieves, obtain mixed material after mixing 40 minutes by automatic lifting mixer under 20 revs/min.Then in mixed material, add dolomol, after mixing, compressing tablet obtains chewable tablets.
embodiment 10the preparation of composition (coffee solid beverage)
A kind of composition, the percentage by weight of its each component is respectively: 30% wheat bran water-soluble dietary fiber, 50% navy bean extract, 9%L-arabinose, 8% FOS, 2% xylo-oligosaccharide and 1% haw berry extract.
Preparation method: get after the water-soluble dietary fiber of recipe quantity, FOS powder, navy bean extract, Arabinose, xylo-oligosaccharide powder and haw berry extract cross 60 mesh sieves, obtain mixed material after mixing 30 minutes by automatic lifting mixer under 30 revs/min.Then mixed material is mixed with appropriate coffee, quantitative package, obtain containing coffee solid beverage.
embodiment 11the preparation of composition (solid beverage)
A kind of composition, the percentage by weight of its each component is respectively: 30% wheat bran water-soluble dietary fiber, 40% navy bean extract, 8% FOS, 2% xylo-oligosaccharide and 20% haw berry extract.
Preparation method: get after the water-soluble dietary fiber of recipe quantity, FOS powder, navy bean extract, xylo-oligosaccharide powder and haw berry extract cross 60 mesh sieves, obtain mixed material after mixing 30 minutes by automatic lifting mixer under 30 revs/min.Then by mixed material quantitative package, solid beverage is obtained.
embodiment 12the thermally-stabilised research of the present composition and pH screening experiment:
In order to ensure the AMS inhibit activities of product, we have carried out thermally-stabilised and pH research to composition of the present invention.
Experimental products: the 10g dissolution of solid respectively getting three parts of embodiments 5 preparations respectively, in 100ml water, measures its pH value and is about 5, and a copy of it keeps pH value to be 5, and a adjust ph is 3, and another part of adjust ph is 7, tests respectively by following condition:
Experimental technique: doelhert design matrix
Experiment condition: pH:2 ~ 7;
Temperature: 20 ~ 100 DEG C continue;
Time: 0 ~ 20min;
The AMS inhibit activities of testing product.
Testing result is shown in Fig. 7, Fig. 8 and Fig. 9; Result shows:
When pH value is 3,
1, product 20 ~ 40 DEG C, keep in 0 ~ 20min 95 ~ 100% activity;
2, temperature 20 ~ 100 DEG C, in any case heating in 0 ~ 20min, activity is all greater than 60%;
When pH value is 5,
1, product heats the activity that 10min still keeps 90 ~ 100% below 80 DEG C, highly stable; Even if heating 15 ~ 20min, still keeps the activity of 70 ~ 90%;
2, product is 90 ~ 100 DEG C of heating of Activated declines, and activity is reduced to 50 ~ 70%.
When pH value is 7,
1, product is greater than 65% the activity of 20 ~ 40 DEG C, and in 15min, the activity of 40 ~ 100 DEG C is 90 ~ 100%, more stable at 40 ~ 100 DEG C.
Therefore the pH value that 10g solid product is dissolved in 100ml water is preferably 3 ~ 7; More preferably pH value is 3 ~ 5, and further preferable ph is 4 ~ 5; Solution temperature is preferably 20 ~ 80 DEG C, preferably 20 ~ 60 DEG C, is more preferably 30 ~ 40 DEG C.
The pH value of product 10g dissolution of solid of the present invention in 100ml water is 4 ~ 5; Advise that 30 ~ 40 DEG C of warm water are taken after mixing it with water, fully can ensure the inhibit activities of its AMS.
embodiment 13fat-reducing and slimming effect test
In order to verify the beneficial effect of technical solution of the present invention further, the product of embodiment 2-11 is adopted to do following research:
One, test method
Openly collect volunteer, selection principle is the personage of the starchy food such as personage or preference bread, wheaten food, potato taking notice of body.
With 320 experimenters for subjects (comprising BMI(body-mass index), body fat, waistline the higher person), through two weeks neutral gear after dates, start to carry out to test (data are subdivided into higher (laying particular stress on) person of body fat and normal subjects (medium body reinvent body person) again, and the higher person of body fat is males fat >=20% and women's body fat >=30%).320 experimenters are divided into 10 groups, often organize 32 people (lay particular stress on woman 17 people, lay particular stress on man 9 people and medium body person 6 people that reinvents body), 10 groups of experimenters absorb 10 set products (namely each group of experimenter absorbs the product of different embodiment respectively) of embodiment 2-11 respectively, often eat and absorb product 15 ~ 20 minutes ante cibum, warm water is taken after mixing it with water, one day breakfast, lunch and dinner.Test carries out 12 weeks altogether, monthly notes down the indexs such as body weight, body fat, waistline, a hip circumference.Change relatively before and after picked-up product.
Remarks: 1. neutral gear phase and the preparatory stage, stop going on a diet, keep normal diet and movable adjustment period.
2., if tested products form is solid powder Bao Ze without the need to 20min in advance, directly take before the meal.
Two, experimenter's points for attention:
1. often eat picked-up product 15 ~ 20 minutes ante cibum (specification: 10g), coordinate one glass of warm plain boiled water or soup to take.
2. tested period dinner is tried one's best before arrangement 7 and is eaten, and does not eat food.
3. if forget before the meal and take, please at mealtime solid powder bag is opened, powder is sprinkled upon on food and uses.
If sensation is hungry after 4. taking product, more edible fresh, the low sugar fruit of suggestion, snack of trying not.
5. if coordinate appropriate motion every day during taking product, then more contribute to product and play effect.
Three, observation index
Body weight (batheroom scale), body fat (Omron body fat instrument), waistline (tape measure), hip circumference (tape measure).
Four, result
The data recorded are divided into and lay particular stress on woman's group, lay particular stress on man's group and medium body and reinvent body group and carry out statistical analysis process, before the experiment of effective (people), efficient (%), maximum wherein in statistics, average deduction item, numerical value is all set to 0, its statistics is the result of 320 people (10 groups) integration test, in table 4, table 5 and table 6, final average statistics the results are shown in Table 7, table 8 and table 9.
Table 4 is laid particular stress on woman and is organized statistics
Table 5 is laid particular stress on man and is organized statistics
Table 6 medium body reinvents body group statistics
Table 7 is laid particular stress on woman and is organized final average statistics result
Table 8 is laid particular stress on man and is organized final average statistics result
Table 9 medium body reinvents the final average statistics result of body group
Fig. 1-4 shows in clinical testing the body weight, fat percentage, waistline and the hip circumference situation of change that lay particular stress on experimenter, and Fig. 5-6 shows the situation of change of medium body weight experimenter mean value and maximum in clinical testing.Find out from table 4-9 and Fig. 1-6, totally 10 set products are efficient in body weight, fat percentage, waistline and the hip circumference statistics of 12 weeks all almost reaches 100% for embodiment of the present invention 2-11, illustrate that 10 set products all have significant fat-reducing and slimming effect.In addition, according to result of the test, in the product of embodiment 2-11, after experimenter takes the product of embodiment 5, achieve best fat-reducing and slimming effect.
To sum up, after the inclined severe one of body weight eats the technical program product for a long time, body weight obviously alleviates, and waistline and hip circumference obviously reduce, and fat percentage takes a turn for the better to some extent.And medium body severe one for a long time after edible the technical program product waistline and hip circumference also obviously reduce, make body more be added with curve.Prove that product of the present invention has significant fat-reducing and slimming effect thus, especially for minimizing waistline and hip circumference the most remarkable, and without any side effects.And a lot of experimenter reacts its skin also than originally more smooth, illustrates that the technical program product also has certain toxin-expelling and face nourishing effect.

Claims (18)

1. a composition, it is made up of 50% water-soluble dietary fiber, 10% navy bean extract, 8%L-arabinose, 26% FOS, 4% xylo-oligosaccharide and 2% haw berry extract by weight percentage.
2. composition according to claim 1, is characterized in that, described water-soluble dietary fiber is maize peel or wheat bran water-soluble dietary fiber.
3. composition according to claim 1, is characterized in that, described water-soluble dietary fiber is maize peel water-soluble dietary fiber.
4. composition according to claim 1, is characterized in that, described navy bean extract is through supercritical CO 2extract removal of impurities.
5. composition according to claim 1, is characterized in that, described navy bean extract adopts water as Extraction solvent, and in described navy bean extract, organic solvent-free remains.
6. composition according to claim 1, is characterized in that, the AMS inhibit activities of described navy bean extract is greater than 3000AAIU/g.
7. composition according to claim 1, is characterized in that, the pH value of 10g dissolution of solid in 100ml water of described composition is 3 ~ 7.
8. composition according to claim 7, is characterized in that, the pH value of 10g dissolution of solid in 100ml water of described composition is 3 ~ 5.
9. composition according to claim 7, is characterized in that, the pH value of 10g dissolution of solid in 100ml water of described composition is 4 ~ 5.
10. composition according to claim 7, is characterized in that, described solution temperature is 20 ~ 80 DEG C.
11. compositions according to claim 7, is characterized in that, described solution temperature is 20 ~ 60 DEG C.
12. compositions according to claim 7, is characterized in that, described solution temperature is 30 ~ 40 DEG C.
13. compositions according to claim 1, is characterized in that, described composition is tablet, capsule, granule, electuary, solid beverage or oral liquid.
14. compositions according to claim 1, is characterized in that, described composition is solid beverage.
15. composition according to claim 1, is characterized in that, described composition is added in coffee or fruit juice and drinks.
16. 1 kinds of compositions according to any one of claim 1 to 15 are preparing the purposes in the composition with body shaping and Weight management effect.
17. 1 kinds of compositions according to any one of claim 1 to 15 are preparing the purposes in the composition with hypoglycemic or reducing blood lipid auxiliary therapeutic action.
The preparation method of 18. 1 kinds of compositions according to any one of claim 1 to 14, described composition is solid beverage, it is characterized in that, described preparation method comprises the steps:
1) each raw material is weighed by formulation weight;
2) each raw material is crossed 30 ~ 60 mesh sieves;
3) mixed by raw material batch mixer, incorporation time is 20 ~ 40min, and rotating speed is 20 ~ 30 revs/min;
4) quantitative package.
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