CN103388223B - A kind of high-strength Fanglun l414 long filament/flame-retardant cotton fiber blended yarn woven fabric and preparation method thereof - Google Patents
A kind of high-strength Fanglun l414 long filament/flame-retardant cotton fiber blended yarn woven fabric and preparation method thereof Download PDFInfo
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- CN103388223B CN103388223B CN201210139304.7A CN201210139304A CN103388223B CN 103388223 B CN103388223 B CN 103388223B CN 201210139304 A CN201210139304 A CN 201210139304A CN 103388223 B CN103388223 B CN 103388223B
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- 229920000742 Cotton Polymers 0.000 title claims abstract description 71
- 239000003063 flame retardant Substances 0.000 title claims abstract description 33
- 238000002360 preparation method Methods 0.000 title claims abstract description 20
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 title claims abstract description 18
- 239000002759 woven fabric Substances 0.000 title claims abstract description 18
- 239000004744 fabric Substances 0.000 claims abstract description 17
- 230000009970 fire resistant effect Effects 0.000 claims abstract description 11
- 239000012530 fluid Substances 0.000 claims abstract description 11
- 238000000034 method Methods 0.000 claims description 24
- 239000000835 fiber Substances 0.000 claims description 19
- 239000007788 liquid Substances 0.000 claims description 19
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
- 239000000203 mixture Substances 0.000 claims description 9
- 239000002270 dispersing agent Substances 0.000 claims description 8
- 102000004190 Enzymes Human genes 0.000 claims description 6
- 108090000790 Enzymes Proteins 0.000 claims description 6
- 229940088598 enzyme Drugs 0.000 claims description 6
- 238000002203 pretreatment Methods 0.000 claims description 6
- 239000003795 chemical substances by application Substances 0.000 claims description 5
- 230000000149 penetrating effect Effects 0.000 claims description 5
- 238000009970 yarn dyeing Methods 0.000 claims description 5
- 239000004382 Amylase Substances 0.000 claims description 3
- 102000013142 Amylases Human genes 0.000 claims description 3
- 108010065511 Amylases Proteins 0.000 claims description 3
- 108010059892 Cellulase Proteins 0.000 claims description 3
- 235000019418 amylase Nutrition 0.000 claims description 3
- 229940106157 cellulase Drugs 0.000 claims description 3
- 101710180316 Protease 2 Proteins 0.000 claims description 2
- 238000001035 drying Methods 0.000 claims description 2
- 238000005470 impregnation Methods 0.000 claims description 2
- 230000035699 permeability Effects 0.000 abstract description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 6
- 238000012360 testing method Methods 0.000 description 6
- 229920000271 Kevlar® Polymers 0.000 description 5
- 230000008595 infiltration Effects 0.000 description 5
- 238000001764 infiltration Methods 0.000 description 5
- 239000004761 kevlar Substances 0.000 description 5
- 238000002156 mixing Methods 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 3
- 239000000975 dye Substances 0.000 description 3
- -1 ester compound Chemical class 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 2
- 238000004132 cross linking Methods 0.000 description 2
- 238000005238 degreasing Methods 0.000 description 2
- 239000008367 deionised water Substances 0.000 description 2
- 229910021641 deionized water Inorganic materials 0.000 description 2
- 238000007598 dipping method Methods 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 239000004753 textile Substances 0.000 description 2
- 229920000433 Lyocell Polymers 0.000 description 1
- 108091005804 Peptidases Proteins 0.000 description 1
- 239000004365 Protease Substances 0.000 description 1
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000002657 fibrous material Substances 0.000 description 1
- 229920006253 high performance fiber Polymers 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 238000000643 oven drying Methods 0.000 description 1
- 229940051841 polyoxyethylene ether Drugs 0.000 description 1
- 229920000056 polyoxyethylene ether Polymers 0.000 description 1
- 230000000750 progressive effect Effects 0.000 description 1
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- 239000002994 raw material Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
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- 229910052710 silicon Inorganic materials 0.000 description 1
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- 230000000087 stabilizing effect Effects 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
Landscapes
- Chemical Or Physical Treatment Of Fibers (AREA)
- Yarns And Mechanical Finishing Of Yarns Or Ropes (AREA)
- Woven Fabrics (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The present invention relates to a kind of high-strength Fanglun l414 long filament/flame-retardant cotton fiber blended yarn woven fabric and preparation method thereof.The key step of preparation method of the present invention is: cotton yarn immerses in fire resistant fluid and infiltrates by (1), dries, makes retardant cotton; (2) Fanglun 1414's long filament is twisted line with adding after the retardant cotton Split Down of flame treatment, the twist is in 280-350T/M scope, twist with the fingers and twist with the fingers to for Z, the percentage by weight of described Fanglun 1414's long filament and retardant cotton is 2: 3; (3) weaved cotton cloth as warp and parallel by the line after twisting, warp count is 200-250 root/10cm, and weft count is 180-220 root/10cm.The high-strength Fanglun l414 long filament/flame-retardant cotton fiber blended yarn woven fabric prepared by the present invention, has the features such as high strength, fire-retardant, high temperature resistant, breathable moisture permeability is good, and electrostatic is little, and wearability is good.
Description
Technical field
The present invention relates to a kind of fabric lining and preparation method thereof, particularly relate to a kind of high-strength Fanglun l414 long filament/flame-retardant cotton fiber blended yarn woven fabric and preparation method thereof.
Background technology
The development of high-performance fiber is the symbol of modern fiber science progress, and be the technological innovation of traditional textile industry, the conversion to high-tech industry creates advantage, for mankind's growth in the living standard contributes.Functional fibre refers to except the physical and mechanical properties that general fiber has, and also has the tencel of certain specific function.
High strength Fanglun l414 fiber refers to that intensity is greater than the 20g/ dawn, stands in the long period chemical fibre that high temperature (such as more than 200 DEG C) still can keep its original physical and mechanical properties substantially.Not softening under high temperature, still to maintain General Mechanics character special fibre.This fibrid has following basic characteristics: 1. fusing point and softening point high; 2. fiber at high temperature dimensionally stable; 3. macromolecular structure not easily degrades (Long-Time Service temperature is more than 200 DEG C); 4. there is the performance such as good hydrolysis and chemically-resistant medicament; 5. fire-retardant.
High strength Fanglun l414 long filament can not be all-round fibre, and it has advantage in some performance, and in other respects may with regard to existing defects, and such as hygroscopicity is poor, electrostatic is strong.
Cotton fiber is natural fabric, have moisture absorption, softness, feature that taking is good, but cotton fiber does not have anti-flammability.
In order to improve a kind of limitation of fibrous material, the method of multiple fiber blend can be adopted, blending product is carried out by the fiber finding some suitable, each fiber properties is retained, several functions superposes, maximize favourable factors and minimize unfavourable ones, to adapt to the requirement of environment for use to material property, or perhaps widen the range of application of material.
The high-strength Fanglun l414 long filament/flame-retardant cotton fiber blended yarn woven fabric of the one prepared by the present invention, has the features such as high strength, fire-retardant, high temperature resistant, breathable moisture permeability is good, and electrostatic is little, and wearability is good.
Summary of the invention
For above shortcomings in prior art, the preparation method that one of technical problem to be solved by this invention provides a kind of high-strength Fanglun l414 long filament and cotton yarn blending to weave cotton cloth, wherein also comprises the flame treatment of cotton yarn.Two of technical problem to be solved by this invention provides a kind of fabric prepared by said method, and this fabric has high fracture strength, excellent fire resistance and good taking and comfortableness.
The present invention seeks to be achieved through the following technical solutions:
A preparation method for high-strength Fanglun l414 long filament/flame-retardant cotton fiber blended yarn woven fabric, comprises following steps:
(1) cotton yarn is immersed in fire resistant fluid infiltrate, dry, make retardant cotton;
(2) Fanglun 1414's long filament (be called for short kevlar long filament) is twisted line with adding after the retardant cotton Split Down of flame treatment, the twist is 280-350T/M, twist with the fingers and twist with the fingers to for Z, the percentage by weight of described Fanglun 1414's long filament and retardant cotton is 2: 3;
(3) weaved cotton cloth as warp and parallel by the line after twisting, warp count is 200-250 root/10cm, and weft count is 180-220 root/10cm.
Wherein, described fire resistant fluid is made up of following compositions in weight percentage: fire retardant FPK80023-8%, WA dispersant 0.1-0.5%, penetrating agent JFC 0.1-0.3%, surplus is water.
Described fire retardant FPK8002 main component is nitrogenous organophosphorus ester compound, can buy from He Te global group (Shenzhen) Co., Ltd.
Described dispersant WA is the high-effect dispersant of a kind of organic silicon type, discloses the preparation method of this dispersant WA, can buy from Shanghai auxiliary reagent factory in " dyestuff and dyeing " 03 phase in 1975 " synthesis of dispersant WA and application thereof ".
Described penetrating agent JFC, full name is fatty alcohol-polyoxyethylene ether, belongs to non-ionic surface active agent, can buy from Shanghai auxiliary reagent factory.
Fire-retardant step: clean cotton yarn is put into yarn dyeing machine, then the fire resistant fluid configured stirring adds, for making fire resistant fluid infiltrate equably in cotton fiber, relating to process and comprising and be not limited to infiltrate technique, process for stabilizing, crosslinking process.
Infiltration technique concrete steps of the present invention are: after cotton yarn infiltrates 15-45 minute in fire resistant fluid, rotate 1-10 minute with the rotating speed of 10-20 rev/min, then rotate 20-30 minute with the rotating speed of 50-70 rev/min, de-liquid 1-10 minute.
The object infiltrating technique makes fiber surface fully absorb fire retardant, reaches each fiber surface and all covered by uniform fire retardant.
The important indicator parameter infiltrated in technique is the upper liquid rate controlling fiber, and preferably result controls the 5-15% in fibre weight.
Another technological parameter infiltrated in technique is the speed of gyration of cylinder, and in whole impregnation process, speed of gyration is a progressively high process, and by the programme-control of variable-frequency motor, wherein the maximum speed of final stage determines the upper liquid rate of fiber.The linear velocity that preferably the highest speed of gyration produces is 100-200m/min, and according to solubility and the attached outstanding power of infiltrate, after ensureing de-liquid, the upper liquid rate of material can ensure the required value in 5-15% scope.
Drying process key element in aforementioned stable technique, can do together with cross-linking process step, can adopt oven drying, and preferably method adopts radio frequency to dry, energy-efficient.
First can carry out pre-treatment to cotton yarn before step (1) flame treatment, pre-treatment step comprises degreasing process, cleaning etc.Wherein, described yarn degreasing, the concrete steps of cleaning and condition can adopt the pre-treatment process of existing continuous yarn dyeing to complete in dye beck, and preferred pre-treating method is:
(1) prepare cotton yarn pretreatment liquid, pretreatment liquid is made up of following compositions in weight percentage: 2-4% biology enzyme, 10-15% hydrogen peroxide, surplus are water;
(2) at 40-70 DEG C, cotton yarn is immersed pretreatment liquid 40-60 minute;
(3) with after 40-95 DEG C of hot wash, radio frequency is dried.
Pretreatment liquid is preferably made up of following compositions in weight percentage: 3wt% biology enzyme, 13wt% hydrogen peroxide, and surplus is water.
Described biology enzyme is scutching cotton teacher 100T, and scutching cotton teacher 100T is made up of following compositions in weight percentage: pectase 78%, cellulase 13%, amylase 7%, protease 2%.
Raw material of the present invention and equipment all commercially or customization can obtain.
The present invention also provides a kind of high-strength Fanglun l414 long filament/flame-retardant cotton fiber blended yarn woven fabric, adopts the preparation method of above-mentioned high-strength Fanglun l414 long filament/flame-retardant cotton fiber blended yarn woven fabric to be prepared from.
Positive progressive effect of the present invention is: the fiber adopting difference in functionality, the fabric that blending weaves, and has high fracture strength, excellent fire resistance and good taking and comfortableness.The user demand of special occasions protective clothing can be met.
Detailed description of the invention
Below in conjunction with embodiment, the invention will be further described.
Embodiment 1
For the preparation of 135 dawn kevlar long filaments and flame-retardant cotton fiber blended yarn woven fabric.
(1) cotton yarn: customize 26 cotton yarns
Cotton yarn pretreatment liquid is prepared: 3wt% scutching cotton teacher 100T, 13wt% hydrogen peroxide, all the other are water.
Treatment process condition: 60 DEG C, 50 minutes.
(2) wash: 95 DEG C of hot water wash.
(3) radio frequency is dried.
(4) cotton yarn preparation method: adopt fire retardant FPK8002(main component to be nitrogenous organophosphorus ester compound, He Te global group (Shenzhen) Co., Ltd produces) 5kg, add WA dispersant (production of Shanghai auxiliary reagent factory) 0.3Kg, penetrating agent JFC (production of Shanghai auxiliary reagent factory) 0.2Kg, add deionized water and be diluted to 100Kg, with the existing cylinder mediation running 5-10 minute that sizes mixing, the fire resistant fluid of formation is fully mixed.
(5) cotton yarn of 26 after pre-treatment is put into the yarn dyeing machine that fire retardant is housed, carry out infiltration processing.Cotton yarn, after infiltrating 45 minutes, with the rotating speed low speed rotation 5 minutes of 15 revs/min, rotates 30 minutes with the rotating speed middling speed of 60 revs/min, de-liquid 10 minutes.Infiltrate other infiltration or dipping means that technique also can use this area routine.
(6) adopt radio frequency to dry and be cross-linked.
(7) by 135 dawn kevlar long filaments and fire-retardant after 26 cotton yarn Split Down after add and stick into line, twist 300T/M, twist with the fingers to being that Z twists with the fingers.
(8) weaved cotton cloth as warp and parallel by the line after twisting, warp count is 250/10cm, and weft count is 220/10cm.
(9) adopt GB/TGB/T3923 standard testing, the warp-wise ultimate strength of this fabric is 3500N, and broadwise ultimate strength is 3650N; Adopt GB/TGB/T5455 standard testing, the fire resistance of this fabric is: glow 0 second, afterflame 0 second, char length 3mm.Adopt GB/T6503 standard testing, the regain of this fabric is 4.8%.
Embodiment 2
For the preparation of 200 dawn kevlar long filaments and flame-retardant cotton fiber blended yarn woven fabric.
(1) cotton yarn: commercial 16 cotton yarns
Cotton yarn pretreatment liquid is prepared: 3wt% scutching cotton teacher 100T, 13wt% hydrogen peroxide, all the other are water.
Treatment process condition: 60 DEG C, 50 minutes.
(2) wash: 95 DEG C of hot water wash.
(3) radio frequency is dried.
(4) cotton yarn preparation method: adopt fire retardant FPK8002(main component to be nitrogenous organophosphorus ester compound, He Te global group (Shenzhen) Co., Ltd produces) 5kg, add WA dispersant (production of Shanghai auxiliary reagent factory) 0.3Kg, penetrating agent JFC (production of Shanghai auxiliary reagent factory) 0.2Kg, add deionized water and be diluted to 100Kg, with the existing cylinder mediation running 5-10 minute that sizes mixing, the fire resistant fluid of formation is fully mixed.
(5) cotton yarn of 16 after pre-treatment is put into the dye beck that fire retardant is housed, carry out infiltration processing.Cotton yarn, after infiltrating 30 minutes, with the rotating speed low speed rotation 5 minutes of 15 revs/min, rotates 20 minutes with the rotating speed middling speed of 60 revs/min, de-liquid 10 minutes.Infiltrate other infiltration or dipping means that technique also can use this area routine.
(6) adopt radio frequency to dry and be cross-linked.
(7) by 200 dawn kevlar long filaments and fire-retardant after cotton yarn Split Down after add and stick into line, twist 280T/M, twist with the fingers to being that Z twists with the fingers.
(8) weaved cotton cloth as warp and parallel by the line after twisting, warp count is 200/10cm, and weft count is 180 10/cm.
(9) adopt GB/T3923 standard testing, the warp-wise ultimate strength of this fabric is 3600N, and broadwise ultimate strength is 3660N; Adopt GB/T5455 standard testing, the fire resistance of this fabric is: glow 0 second, afterflame 0 second, char length 3mm.Adopt GB/T6503 standard testing, the regain of this fabric is 5%.
The concrete formula of the scutching cotton teacher 100T described in embodiment 1-2 is: pectase 78wt%, cellulase 13wt%, amylase 7wt%, protease 2wt%, by Shanghai Textile, research institute provides.
Claims (6)
1. a preparation method for high-strength Fanglun l414 long filament/flame-retardant cotton fiber blended yarn woven fabric, is characterized in that, comprise following steps:
(1) cotton yarn is immersed in fire resistant fluid infiltrate, dry, make retardant cotton;
(2) be twisted line by adding after Fanglun 1414's long filament and above-mentioned retardant cotton Split Down, the twist is 280-350T/M, and twist with the fingers and twist with the fingers to for Z, the percentage by weight of described Fanglun 1414's long filament and retardant cotton is 2:3;
(3) weaved cotton cloth as warp and parallel by the line after twisting, warp count is 200-250 root/10cm, and weft count is 180-220 root/10cm;
Described in step (1), fire resistant fluid is made up of following compositions in weight percentage: fire retardant FPK80023-8%, WA dispersant 0.1-0.5%, penetrating agent JFC 0.1-0.3%, and surplus is water;
Before step (1), first carry out pre-treatment to cotton yarn, pre-treating method is:
(1) prepare cotton yarn pretreatment liquid, pretreatment liquid is made up of following compositions in weight percentage: 2-4% biology enzyme, 10-15% hydrogen peroxide, surplus are water;
(2) at 40-70 DEG C, cotton yarn is immersed pretreatment liquid 40-60 minute;
(3) with after 40-95 DEG C of hot wash, radio frequency is dried;
Described biology enzyme is scutching cotton teacher 100T, and described scutching cotton teacher 100T is made up of following compositions in weight percentage: pectase 78%, cellulase 13%, amylase 7%, protease 2%.
2. the preparation method of high-strength Fanglun l414 long filament/flame-retardant cotton fiber blended yarn woven fabric according to claim 1, is characterized in that: described pretreatment liquid is made up of following compositions in weight percentage: 3% biology enzyme, 13% hydrogen peroxide, surplus are water.
3. the preparation method of high-strength Fanglun l414 long filament/flame-retardant cotton fiber blended yarn woven fabric according to claim 1, it is characterized in that: the impregnation process described in step (1) carries out in yarn dyeing machine, after cotton yarn infiltrates 15-45 minute in fire resistant fluid, 1-10 minute is rotated with the rotating speed of 10-20 rev/min, 20-30 minute is rotated again, de-liquid 1-10 minute with the rotating speed of 50-70 rev/min.
4. the preparation method of high-strength Fanglun l414 long filament/flame-retardant cotton fiber blended yarn woven fabric according to claim 3, it is characterized in that: the linear velocity that the highest speed of gyration of the cylinder of described yarn dyeing machine produces is 100-200m/min, and the upper liquid rate of fiber is the 5-15% of total weight of fiber.
5. the preparation method of high-strength Fanglun l414 long filament/flame-retardant cotton fiber blended yarn woven fabric according to claim 1, is characterized in that: the furnace drying method described in step (1) is that radio frequency is dried and is cross-linked.
6. high-strength Fanglun l414 long filament/flame-retardant cotton fiber blended yarn woven fabric, is characterized in that: adopt the preparation method of the high-strength Fanglun l414 long filament/flame-retardant cotton fiber blended yarn woven fabric according to any one of claim 1-5 to be prepared from.
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| CN103806196A (en) * | 2014-02-18 | 2014-05-21 | 如皋市安国织造有限公司 | Flame retarding cotton bag special for cotton packaging and manufacturing method thereof |
| CN104480617A (en) * | 2014-12-12 | 2015-04-01 | 常熟市凯博尔纺织品有限公司 | Flame-retardant fabric |
| CN104611801A (en) * | 2015-02-12 | 2015-05-13 | 南通美铭锦纶有限公司 | Aramid fiber 1313 blended high-temperature-resistant and flame-resistant material |
| CN104757717B (en) * | 2015-03-27 | 2016-08-24 | 陕西锦澜科技有限公司 | Cotton/the Tencel Blended Fabric of the grease proofing water repellent of a kind of anti-static inflaming-retarding and preparation method |
| CN105483905A (en) * | 2015-12-01 | 2016-04-13 | 惠安华晨贸易有限公司 | Process for manufacturing waterproof, flame-retardant and breathable fabric |
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| CN107557966A (en) * | 2017-10-17 | 2018-01-09 | 蓝星（成都）新材料有限公司 | A kind of composite flame-proof material and preparation method |
| CN109267351B (en) * | 2018-09-26 | 2021-01-29 | 南京拓丽时装有限公司 | High-flame-retardant fireproof breathable fabric and preparation process thereof |
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