CN103290496A - Spinning technology applied to semi-continuous high-speed spinning machine with spinning roller arranged horizontally - Google Patents

Spinning technology applied to semi-continuous high-speed spinning machine with spinning roller arranged horizontally Download PDF

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CN103290496A
CN103290496A CN2013102667354A CN201310266735A CN103290496A CN 103290496 A CN103290496 A CN 103290496A CN 2013102667354 A CN2013102667354 A CN 2013102667354A CN 201310266735 A CN201310266735 A CN 201310266735A CN 103290496 A CN103290496 A CN 103290496A
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spinning
strand
viscose glue
viscose
glue
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CN103290496B (en
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李蓉玲
唐金钟
夏长林
邵方琼
范贤珍
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Yibin Grace Group Co Ltd
Yibin Grace Co Ltd
Yibin Haisite Fiber Co Ltd
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Yibin Grace Group Co Ltd
Yibin Grace Co Ltd
Yibin Haisite Fiber Co Ltd
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Abstract

The invention relates to a spinning technology applied to a semi-continuous high-speed spinning machine with a spinning roller arranged horizontally. The spinning technology comprises glue measurement and supply, pre-spinning filtering, yarn strip forming, spinning and winding. The spinning technology aims at the specific semi-continuous high-speed spinning machine with the spinning roller arranged horizontally, under the mutual action of all processes and control of technological parameters, the spinning speed is ensured to be improved, independent walking of single yarn strips can be achieved, operations are simplified, the problems of doubling, burrs, breakage and the like are solved, the yarn strips are fully reacted and good in uniformity, the product quality is guaranteed, meanwhile, operations of workers are facilitated, and equipment maintenance is easy, overhaul costs are low, so that product costs are greatly reduced while the production efficiency is effectively improved.

Description

Be applicable to the spinning technique of the semicontinuous high-speed spinning machine of spinning roller horizontally set
Technical field
The present invention relates to a kind of spinning technique, particularly a kind of spinning technique that is applicable to the semicontinuous high-speed spinning machine of spinning roller horizontally set belongs to the semicontinuous production technical field of spinning of viscose filament yarn.
Background technology
Extract pure methylcellulose by cellulosic material, be called pulp.Handle with caustic soda, carbon disulfide, obtain orange-yellow sodium cellulose xanthate, be dissolved in again in the diluted sodium hydroxide solution, become the spinning solution of thickness, be called viscose glue.Viscose glue after filtration, after the maturation, deaeration, carry out wet spinning, coagulating bath is made up of sulfuric acid, sodium sulphate and zinc sulfate.Sodium cellulose xanthate in the viscose glue and the effect of sulfuric acid in the coagulating bath and decompose, cellulose regenerated and separate out, the gained cellulose fibre becomes viscose after washing, desulfurization, bleaching, drying.Viscose filament yarn is a kind of of viscose, also is to be made by above-mentioned technology.
In spinning and spinning last handling process, the selection of spinning machine has semicontinuous weaving loom and continuous weaving loom, and from technology and equipment two aspects, there is following difference in these two kinds of spinning machines:
1, from view of production technology, semi-continuous spinning machine is that spinning and post processing (post processing comprises washing, oven dry, become step such as tube) separately, are finished separately, and semi-continuous spinning machine mainly is responsible for the spinning part; And continuous spinning machine is that spinning and post processing (post processing comprises washing, oven dry, become step such as tube) operation is concentrated in together and finishes continuously, continuous spinning be responsible for from the spinning to the post processing institute in steps.
2, from the angle of device structure, semi-continuous spinning machine comprises glue feed mechanism, thread spraying structure, strand shaping mechanism, spinning roller mechanism, wiper mechanism and winding mechanism, and the product that obtains is the spinning cake that falls into centrifugal cylinder; And continuous spinning machine has glue feed mechanism, thread spraying structure, strand shaping mechanism, spinning roller mechanism, wiper mechanism, does not have winding mechanism, and strand directly enters mechanisms such as drip washing, oven dry, obtains the silk tube of coiling and molding at last.
Based on the difference of above two kinds of spinning machines, its pluses and minuses separately are as follows:
1, semi-continuous spinning machine (as shown in Figure 1-Figure 3):
Advantage: because the post-processing step that carries out is separately arranged, and also have the process of low-temp desulfurization, low temperature long time drying in the post-processing step, product has intensity height, whiteness height, the characteristics that strand is soft beautiful;
Shortcoming: it is low to spin speed, and post processing expense height increases production cost.
2, continuous spinning machine:
Advantage: it is high to spin speed, and output improves; Spinning and post processing concentrate in together to be carried out, and production cost reduces;
Shortcoming: because strand is namely to wash i.e. baking, strand intensity is low, and whiteness is low, and strand is coarse, and quality is not as the product of semi-continuous spinning machine; For increasing strand obvolvent starching, slurry need be removed during floss silk dyeing, increases the downstream product production cost; To raw material (viscose glue) quality requirement height.
In the prior art modal semi-continuous spinning machine be the R535 semi-continuous spinning machine (as shown in Figure 1-Figure 3, comprise frame 1, glue feeder 2, strand shaped device 3, device for spinning 4 and coiler device 5, the spinning roller is vertically setting with respect to the operating surface 102 that spins face 101 in the device for spinning 4), the main flow process of its spinning is:
Viscose glue sprays in the acid bath groove with spinning head by filter filtration back and is shaped to strand through reaction, strand by the drawing-off of drawing-off dish to solidifying roller, strand carries out rising head again to twisting with the fingers the face acid removing roller after the reaction of a period of time solidifying the reel distance of a fixing turn of roller, the acid removing roller top adopts the mode of the drip washing of dripping that strand is carried out the disacidify washing, strand imports centrifugal cylinder again in the distance of acid removing roller coiling one fixing turn, obtains spinning cake at last.
Wherein, the spinning roll body mainly is divided into acid removing roller and solidifies roller, each ingot position of spinning machine is used a pair of roller and a pair of acid removing roller of solidifying respectively, solidify roller and be installed in the face of spinning, acid removing roller is installed in the sth. made by twisting face, deviate from mutually, the fixed form of roll body is an end and fixes, and installation direction becomes vertically to install with respect to the operating surface position that spinning machine spins face.Now three cylinder air drafts of R535 three cylinder silk spinning machines adopt three cylinders with air channel air draft mode in addition.
Existing its strand moulding section of R535A semi-continuous spinning machine and spinning roll structure and mounting means can't carry out high speed spinning, and its spinning is spun speed about 70-90m/min.Simultaneously its device structure and mounting means etc. cause that the spinning machine equipment floor space is big, energy consumption is high, technological process is complicated, maintenance point is many, shortcomings such as accessory consumption is big, product cost height.Three cylinders, three cylinders of R535 three cylinder silks form mutually in the air draft process with air channel air draft mode and disturb in addition, cause the air draft weak effect.
Modal continuous spinning machine structure such as Fig. 4 in the prior art-shown in Figure 6, its first half comprises frame 1, glue feeder 2, strand shaped device 3 and device for spinning 4, the spinning roller also is vertically setting with respect to the operating surface 102 that spins face 101 in the device for spinning 4.The continuous spinning machine of Soviet Union's system improves for the spinning roller segment, but because its production obtains is tow, can not obtain spinning cake, so can not directly be applied in the semi-continuous spinning machine.
It is CN1356409 that State Intellectual Property Office discloses a publication number in 2000.12.6, name is called the patent of invention of " the single channel multifibres is centrifugal to be spun and semi-continuous spinning machine and rayon spinning technology thereof ", this disclosure of the Invention a kind of centrifugal semi-continuous spinning machine, it comprises viscose glue induction system, swing tube assembly, scrape acid, the drawing-off dish, solidify roller, acid removing roller, crane and funnel, centrifugal cylinder and electric ingot system, and multichannel viscose glue pipe and supporting mechanism thereof that the viscose glue induction system is advanced glue simultaneously by head and tail two ends are formed; The swing tube assembly is made up of measuring pump, worry cover, curved tube and the shower nozzle of the multi-channel parallel that is connected in series with the multichannel sebific duct; Two solidify roller above the strand walking path be provided with up and down the acid removing roller assembly of installing of being formed by two acid removing rollers; On the machine crane, the funnel of device and the same number of synchronization action of strand; Its centrifugal cylinder, electric ingot system are set to the many centrifugal cylinders of every ingot and electric ingot and the controlling organization supporting with it.
Foregoing invention can be produced multi-filament simultaneously, increased substantially the output of viscose filament yarn, but this invention is because each ingot position of its spinning machine is used a pair of roller and a pair of acid removing roller of solidifying respectively, solidify roller and be installed in the face of spinning, acid removing roller is installed in the sth. made by twisting face, deviate from mutually, the fixed form of roll body is an end and fixes, and installation direction becomes vertically to install with respect to spinning machine operating surface position.The problem that said structure brings is as follows:
1, said structure has limited the length of roller, viscose filament yarn is short in the time that roller is walked, and the viscose filament yarn curring time is short, if carry high-speed spinning, will inevitably cause the viscose filament yarn reaction time to reduce product quality inadequately, so adopt traditional semi-continuous spinning machine efficient to reduce;
2, in order to raise the efficiency, can process the multi-filament bar simultaneously usually, but many viscose filament yarns hank knotting easily again when being wrapped on the existing spinning roller causes the viscose filament yarn fracture, influences the product quality of viscose filament yarn;
3, in addition, the fixed form of described spinning roller is that an end is fixed, and such fixed form is cantilevered, when the spinning roller rotates, is in a kind of unsure state, breaks down easily;
4, all spinning rollers all are that an end is fixed, certainly will need the extremely complicated transmission mechanism of structure to drive the rotation of spinning roller, so also can cause the rising of fault rate, and changing the silk thread kind, when changing velocity of rotation, need to stop, carry out the replacing of transmission system middle gear again, make production efficiency reduce like this, production cost increases.
It is CN2292097 that State Intellectual Property Office discloses a publication number in 1998.9.23, name is called the utility model patent of " continuous viscose filament spinning machine ", this patent relates to a kind of continuous viscose filament spinning machine, can finish spinning, washing continuously, dry, oil, coiling etc., it spins scooter 120m/min, the utility model arranges the viscose filtration device before the spinning machine board, utilize the spinning machine pump shaft to drive the measuring pump running, it is simple in structure, clean easy to maintenancely, filtered the impurity in the viscose glue effectively; In the spinning bath box spinning head is placed the swing pipe end, guaranteed the concentricity of spinning head and glass tube, can avoid producing lousiness, flexible operation, work efficiency height; The strand twin-steer is adopted in the glass tube exit, has reduced the frictional force between strand and the godet roller, and draw ratio is distributed rationally, becomes the yarn quality height.
Above-mentioned because strand is namely to wash i.e. baking, and strand intensity is low, and whiteness is low, and strand is coarse, quality is not as the product of semi-continuous spinning machine; For increasing strand obvolvent starching, slurry need be removed during floss silk dyeing, increases the downstream product production cost; To raw material (viscose glue) quality requirement height.In addition, the spinning roller of above-mentioned continuous spinning machine still is vertically to arrange with respect to workman's operating area, fixes so its mounting means also is an end, still has first piece of problem in the prior art patent.
It is CN201089811 that State Intellectual Property Office discloses a publication number in 2008.7.23, name is called " the dark bath of viscose rayon spun continuous spinning machine ", this patent disclosure dark bath of a kind of viscose rayon spin continuous spinning machine, solve the problem that existing continuous spinning machine strand residue fat degree height brings.The scheme that the utility model adopts is to be provided with acid bath groove between moulding pipe and the spinning pony roll, and the strand that stretches out from the moulding pipe falls into and walks to the spinning pony roll in the acid bath groove that acid solution is housed behind the dipping bath again.The utility model increases dark the bath and spins, and strengthens the extent of reaction of strand, reduces residue fat degree, guarantor's silk quality, and be applicable to the production of floss silk.
This technology belongs to " secondary bath " technology, and it is dense, sour warm lower than one bathing that secondary is bathed acid, so need to increase the independent acid bath of cover system, the sour station of increase input cost.In addition, the spinning roller of above-mentioned continuous spinning machine still is vertically to arrange with respect to workman's operating area, fixes so its mounting means also is an end, still has first piece of problem in the prior art patent.
It is CN2721660 that State Intellectual Property Office discloses a publication number in 2005.8.31, name is called the utility model patent of " be applicable to viscose filament yarn one ingot position spin three semi-continuous centrifugal spinning machine simultaneously ", the utility model discloses a kind of continuous centrifugal spinning machine that on an ingot position of semi-continuous centrifugal spinning machine, spins three rhizoid bars simultaneously that is applicable to, can produce the spinning machine of 18 spinning cakes in every joint of this semi-continuous centrifugal spinning machine simultaneously.By the parts of 18 electric ingots, 18 centrifugal cylinders are installed at every joint of semi-continuous centrifugal spinning machine, can be under the situation that does not increase table of equipment number, public operating cost, floor space and investment, save the maintenance time of spinning machine, reduce the production cost of single spinning cake, improve the utilization rate of spinning machine, and plant maintenance and easy to operate makes its production capacity reach former designed capacity after system equipment improves and reaches 18 spinning cakes from 6 spinning cakes of original every joint or 12 spinning cakes; Satisfy quality of production requirement simultaneously.
Though the output of the every joint of unit is owing to the electric ingot of increase, centrifugal cylinder device can improve output, the speed of spinning of this spinning machine is appointed the right raising that do not have, and spins speed if improved, and can react insufficient quality that influences final products because of strand again.In addition, the spinning roller of above-mentioned semi-continuous spinning machine still is vertically to arrange with respect to workman's operating area, fixes so its mounting means also is an end, still has first piece of problem in the prior art patent.
And for example application number is 89217293.2, the applying date is 1989-09-23, name is called " moulding high-speed spinning device in the viscose glue fiber tube ", and its technical scheme is: the utility model belongs to the viscose high-speed spinning device, mainly is made up of carrier pipe, spinning head, moulding pipe, bath.Being communicated with the moulding pipe of a thin diameter between coagulating basin and liquid return trough, being installed on the relevant position of moulding pipe import front with the supporting Conic nozzle of moulding pipe, is a thread guide near the outlet of moulding pipe, only establishes a spinning disc between thread guide and the spinning funnel.Forming technique is applied to semi-continuous centrifugal formula spinning machine in the pipe that above-mentioned utility model adopts, though said structure can be brought up to 120 meters of per minutes with spinning speed, but the strand of final molding causes strand reaction time deficiency owing to spin fast too fast meeting, does not react inadequate problem so this patent still has to solve owing to spinning the too fast strand that brings of speed.
In sum, existing processes control can't be satisfied the requirement after spinning roller horizontally set is carried high-speed spinning, also can't satisfy kind that the single control of spinning roller to horizontally set brings or the specification requirement of specifications vary.
Summary of the invention
The present invention aims to provide a kind of spinning technique of the semicontinuous high-speed spinning machine at specific spinning roller horizontally set, reaching spinning machine can be when carrying high-speed spinning, guarantee the strand sufficient reacting, and then ensure the quality of products the purpose of enhancing productivity, reducing cost.
For achieving the above object, the technical solution used in the present invention is as follows:
A kind of spinning technique that is applicable to the semicontinuous high-speed spinning machine of spinning roller horizontally set, its operation comprise the viscose glue metering and supply glue, spin preceding filtration, strand moulding, spinning and coiling, it is characterized in that:
The A viscose glue measures and supplies glue
Described viscose glue measures and supplies in the glue process, and the gauge pressure of viscose glue pipe is 0.1~0.5MPa;
B spins preceding filtration
Filter in the operation viscose ripening degree NH before described the spinning 4Cl value control is at 7.0~13ml, falling ball viscosity 28~38 mPas, and the fine content 8.0~8.2% of viscose glue first, viscose glue contains alkali 5.8~6.1%, 500ml viscose gas bubble≤25, viscose glue surface tension 50~55dyne/cm, the following viscose glue particle of 10 μ m≤100/ml;
The moulding of C strand
In the described strand molding procedure, the consisting of of acid bath: sulfuric acid concentration 135~145g/L, sodium sulfate concentration 230~245g/L, zinc sulfate concentration 11.0~12.5g/L, 55~57 ℃ of acid bath temperature, the acid bath surface tension is less than the viscose glue surface tension; Moulding bore Φ 5 ± 0.1mm, moulding pipe range 800~1200mm; The aperture of spinning head is 0.06~0.09mm, and shape is " one " font, fan-shaped or circular;
The D spinning
Described spinning process comprises the solidifying of strand, drawing-off and disacidify, spinning roller length 700~1800mm, diameter of phi 50~500mm, the wire ring number of every rhizoid bar on the spinning roller is 1 circle, spinning roller upper filament space 1~120mm, spinning roller rotating speed is 30~1300 rev/mins, and 0.1~0.2 second/root of coagulation reaction time, the degree of draft of strand are 10~25%; Water temperature in the washing disacidify is: 35~60 ℃, the pH value is: 7~8;
Described through solidify, strand behind the disacidify, washing, its acid content is 5~30%, raw silk bar residue esterification degree is less than 3%.
E reels
In the described coiling operation, strand imports in the funnel through support, and is wound into spinning cake in the centrifugal cylinder by electric ingot control, and the angle of strand and support is 0~90 degree, and the rotating speed of electric ingot is 7450~8900 rev/mins, and the rotating speed of centrifugal cylinder is 7200~8400r/min.
Attainable the key technical indexes is as follows behind the strand coiling and molding of the present invention:
1, does fracture strength (CN/dtex): 〉=1.85
2, wet breaking strength (CN/dtex): 〉=0.85
3, dried extension at break: 〉=17.0-24.0%
4, the dried extension at break coefficient of variation (CV value) :≤6.00%
5, line density (fiber number) deviation: ± 2.0%
6, the line density coefficient of variation (CV value) :≤2.00%
7, the twist coefficient of variation (CV value) :≤13.00%
8, monofilament radical deviation :≤1.0%
9, residual sulfur content (Mg/100g fiber) :≤10.0
10, dye uniformity (ash card) level: 〉=4
Semicontinuous high-speed spinning machine of the present invention comprises frame, glue feeder, strand shaped device, device for spinning and coiler device, it is characterized in that: the spinning roller is with respect to the operating surface horizontally set that spins face in the described device for spinning.
The described operating surface that spins face is to be positioned at the horizontal operation face that spins the face zone; Describedly refer to that with respect to the operating surface horizontally set that spins face the spinning roller is laterally to install with respect to the spinning workman as spinning workman during over against coiler device.
Described spinning roller comprises to be realized drawing-off, solidifies and/or the roller of disacidify function.
The two ends of described every spinning roller are separately fixed at the top of frame both sides, are connected rotation with drive unit.
Described every spinning roller is connected with drive unit respectively, can realize that independence and real-time speed regulating rotate.
At least comprise a help roll in the described device for spinning.
Described help roll is parallel with the spinning roller.
The invention has the advantages that:
1, spinning roller of the present invention is with respect to the operating surface horizontally set that spins face, spinning roller two ends behind the horizontally set are fixed, so can realize spinning the raising of speed on the basis of semi-continuous spinning machine (comprising the semi-continuous centrifugal spinning machine), and guarantee the rotation that the spinning roller can be stable, can not shake, strand is owing to the spinning roller rocks problems such as producing mutual winding, fracture of wire when having avoided spinning.Even also can guarantee the strand sufficient reacting owing to carry high-speed spinning behind the spinning roller horizontally set simultaneously, strand can not produce problems such as burr, also guarantee the uniformity of strand in spinning process, guaranteed spinning quality and carrying under the prerequisite of high-speed spinning that production efficiency is improved.The present invention since the spinning roller with respect to the operating surface horizontally set that spins face, so the structure of spinning roller with and drive mechanism obtain simplifying, make things convenient for the operation of workman to the spinning roller, made the technological parameter of semi-continuous spinning machine, as: the easier controls such as rotating speed of a plurality of spinning rollers.The present invention does not change the structure of spinning machine, but directly transforms on existing R535 semi-continuous spinning machine, low cost of manufacture, thus provide convenience for the upgrading of equipment.
2, the spinning roller horizontally set of semicontinuous high-speed spinning machine of the present invention is convenient to each spinning roller is independently controlled, and more conveniently raises speed separately for each spinning roller.
3, the spinning roller horizontally set of semicontinuous high-speed spinning machine of the present invention, be convenient to adjust real-time the specification of the strand of producing, be replaced by production 60D, 120D, 150D, 200D etc. as the strand that will produce 40D, also be convenient to adjust real-time the strand kind of producing, as compound silk, shaped filaments, flat filament etc.When speed-raising or conversion kind, do not need to shut down the replacing travelling gear.
3, the present invention is by measuring viscose glue and supplying glue, spin preceding filtration, the strand moulding, the sequential control of spinning and each operation of reeling and parameter control, especially guaranteeing that spinning roller rotating speed is 30~1300 rev/mins, spinning roller length 700~1800mm, diameter of phi 50~500mm, the wire ring number of every rhizoid bar on the spinning roller is 1 circle, spinning roller upper filament space 1~120mm, 0.1~0.2 second/root of coagulation reaction time, the degree of draft of strand be the control of 10~25% parameter condition down, can realize the single independent ambulation of strand, simplify the operation, for reducing doubling, burr, fracture of wires etc. have special good technical effect, and can realize spinning speed and reach 120~170 meters/minute, for a person skilled in the art, this effect is better than the vertically spinning roller of setting, is non-obvious.Spinning technique provided by the invention is except guaranteeing that the spinning function reaches the high-speed spinning, and more outstanding is also to have guaranteed product quality, and workman's operation is more easy, plant maintenance is easier, recondition expense is low, and this makes that product cost reduces greatly when effectively enhancing productivity.Be embodied in following each process:
1) in the viscose glue metering and in the glue process, the control of the gauge pressure of viscose glue pipe has fully guaranteed uniformity and spinning speed for glue at 0.1~0.5MPa.
2) before spinning, filter in the operation, with viscose ripening degree NH 4The control of Cl value is at 7.0~13ml, falling ball viscosity 28~38 mPas, the fine content 8.0~8.2% of viscose glue first, viscose glue contains alkali 5.8~6.1%, 500ml viscose gas bubble≤25, viscose glue surface tension 50~55dyne/cm, the following viscose glue particle of 10 μ m≤100/ml, under the condition low at the viscose ripening degree, that glue is old, guaranteed the raising of strand intensity.
3) in the strand molding procedure, adopt the acid bath technology that is complementary with the viscose ripening degree, be that peracid less salt, peracid temperature are adopted in acid bath, specific targets: the consisting of of acid bath: sulfuric acid concentration 135~145g/L, sodium sulfate concentration 230~245g/L, zinc sulfate concentration 11.0~12.5g/L, 55~57 ℃ of acid bath temperature, the acid bath surface tension is less than the viscose glue surface tension, moulding bore Φ 5 ± 0.1mm, moulding pipe range 800~1200mm, the aperture of spinning head is 0.06~0.09mm, can guarantee when realizing violent acid bath reaction, to accelerate the strand reaction speed.
4) in the solidifying of spinning process, drawing-off and disacidify process, because the stroke of strand on the spinning roller lengthen, thereby disacidify is more thorough, the good uniformity of strand, and lousiness is few, is difficult for fracture of wire, can guarantee follow-up dyeing.
5) in the moulding, adopt internal diameter Φ 5 ± 0.1mm in pipe, the moulding pipe of long 800~1200mm can effectively be avoided the monofilament drift phenomenon, guarantees the uniformity of every synnema bar monofilament radical, is beneficial to the raising of spinning speed.
6) in described coiling operation, the rotating speed of electric ingot is controlled at 7450~8900 rev/mins, and the rotating speed of centrifugal cylinder is controlled at 7200~8400r/min, and the spinning cake forming has fully guaranteed the uniformity of follow-up cake dyeing.
7) in whole technology of the present invention, because the interaction of each process, and the determining of temperature, spinning roller wire ring number, spinning roller upper filament space, moulding bore and the length of the temperature of the performance parameters of the rotating speed of spinning roller, viscose glue, acid bath, washing, make and under high-speed spinning, not only have better operability, and the spinning cake quality is good, and follow-up Color is good.
Obviously, according to foregoing of the present invention, according to ordinary skill and the customary means of this area, not breaking away under the above-mentioned basic fundamental thought of the present invention prerequisite, can also make modification, replacement or the change of other various ways.
Description of drawings
The side view of the existing semi-continuous centrifugal spinning machine of Fig. 1.
The front view of the existing semi-continuous centrifugal spinning machine of Fig. 2.
The existing semi-continuous centrifugal spinning machine of Fig. 3 spins the vertical view of face.
The side view of the existing continuous centrifugal spinning machine of Fig. 4.
The front view of the existing continuous centrifugal spinning machine of Fig. 5.
The existing continuous centrifugal spinning machine of Fig. 6 spins the vertical view of face.
The structural representation of the side-looking of Fig. 7 semi-continuous centrifugal spinning machine of the present invention.
The structural representation that the master of Fig. 8 semi-continuous centrifugal spinning machine of the present invention looks.
Fig. 9 semi-continuous centrifugal spinning machine of the present invention spins the structural representation of face.
Figure 10 process flow diagram of the present invention
In the accompanying drawing: frame 1, glue feeder 2, strand shaped device 3, device for spinning 4, coiler device 5, strand 8 spins face 101, operating surface 102, spinning roller 40, water washing device 42, air exhausting device 52.
Form by the following examples is described in further detail foregoing of the present invention again.But this should be interpreted as that the scope of the above-mentioned theme of the present invention only limits to following example, all technology that realizes based on foregoing of the present invention all belong to scope of the present invention.
The specific embodiment
Embodiment 1
A kind of spinning technique that is applicable to the semicontinuous high-speed spinning machine of spinning roller horizontally set, its operation comprise that viscose glue measures and supplies glue, spins preceding filtration, strand moulding, spinning and coiling,
The A viscose glue measures and supplies glue
In viscose glue metering and confession glue process, the gauge pressure of viscose glue pipe is 0.1MPa;
B spins preceding filtration
Before spinning, filter in the operation viscose ripening degree NH 4Cl value control is at 7.0ml, falling ball viscosity 30 mPas, and the fine content 8.0% of viscose glue first, viscose glue contains alkali 6.0%, 500ml viscose gas bubble≤25, viscose glue surface tension 50dyne/cm, the following viscose glue particle of 10 μ m≤100/ml;
The moulding of C strand
In the strand molding procedure, the consisting of of acid bath: sulfuric acid concentration 135g/L, sodium sulfate concentration 230g/L, zinc sulfate concentration 12.0g/L, 55 ℃ of acid bath temperature, the acid bath surface tension is less than the viscose glue surface tension; Moulding bore Φ 5 ± 0.1mm, moulding pipe range 800mm; The aperture of spinning head is 0.06mm, and shape is fan-shaped;
The D spinning
Spinning process comprises the solidifying of strand, drawing-off and disacidify, spinning roller length 1530mm, diameter of phi 100mm, the wire ring number of every rhizoid bar on the spinning roller is 1 circle, spinning roller upper filament space 20~50mm, 500 rev/mins of spinning roller rotating speeds, 0.1~0.2 second/root of coagulation reaction time, the degree of draft of strand are 10%; Water temperature in the washing disacidify is: 35~40 ℃, the pH value is: 7;
Described through solidify, strand behind the disacidify, washing, its acid content is 5~10%, raw silk bar residue esterification degree is less than 3%.
E reels
In the coiling operation, strand imports in the funnel through support, and is wound into spinning cake in the centrifugal cylinder by electric ingot control, and the angle of strand and support is 15 degree, and the rotating speed of electric ingot is 8000 rev/mins, and the rotating speed of centrifugal cylinder is 7800r/min.
Same above-mentioned technology can be disposed the strand of different size (as 40D, 60D, 120D, 150D, 200D etc.), different cultivars (as bright yarn, dull yarn contains the compound silks of cotton, bamboo, fiber crops etc., shaped filaments, flat filament etc.).
Embodiment 2
A kind of spinning technique that is applicable to the semicontinuous high-speed spinning machine of spinning roller horizontally set, its operation comprise that viscose glue measures and supplies glue, spins preceding filtration, strand moulding, spinning and coiling,
The A viscose glue measures and supplies glue
In viscose glue metering and confession glue process, the gauge pressure of viscose glue pipe is 0.3MPa;
B spins preceding filtration
Before spinning, filter in the operation viscose ripening degree NH 4Cl value control is at 13.0ml, falling ball viscosity 35mPas, and the fine content 8.1% of viscose glue first, viscose glue contains alkali 6.1%, 500ml viscose gas bubble≤25, viscose glue surface tension 55dyne/cm, the following viscose glue particle of 10 μ m≤100/ml;
The moulding of C strand
In the strand molding procedure, the consisting of of acid bath: sulfuric acid concentration 140g/L, sodium sulfate concentration 240g/L, zinc sulfate concentration 11.0g/L, 57 ℃ of acid bath temperature, the acid bath surface tension is less than the viscose glue surface tension; Moulding bore Φ 5 ± 0.1mm, moulding pipe range 1000mm; The aperture of institute's spinning head is 0.08mm, and shape is rounded.
The D spinning
Spinning process comprises the solidifying of strand, drawing-off and disacidify, spinning roller length 700mm, diameter of phi 500mm, the wire ring number of every rhizoid bar on the spinning roller is 1 circle, spinning roller upper filament space 1~5mm, 30 rev/mins of spinning roller rotating speeds, 0.1~0.2 second/root of coagulation reaction time, the degree of draft of strand are 25%; Water temperature in the washing disacidify is 40~50 ℃, and the pH value is: 7.5;
Described through solidify, strand behind the disacidify, washing, its acid content is 10~20%, raw silk bar residue esterification degree is less than 3%.
E reels
In the coiling operation, strand imports in the funnel through support, and is wound into spinning cake in the centrifugal cylinder by electric ingot control, and the angle of strand and support is 30 degree, and the rotating speed of electric ingot is 7450 rev/mins, and the rotating speed of centrifugal cylinder is 7200r/min.
Same above-mentioned technology can be disposed the strand of different size (as 40D, 60D, 120D, 150D, 200D etc.), different cultivars (as bright yarn, dull yarn contains the compound silks of cotton, bamboo, fiber crops etc., shaped filaments, flat filament etc.).
Embodiment 3
A kind of spinning technique that is applicable to the semicontinuous high-speed spinning machine of spinning roller horizontally set, its operation comprise that viscose glue measures and supplies glue, spins preceding filtration, strand moulding, spinning and coiling,
The A viscose glue measures and supplies glue
In viscose glue metering and confession glue process, the gauge pressure of viscose glue pipe is 0.5MPa;
B spins preceding filtration
Before spinning, filter in the operation viscose ripening degree NH 4Cl value control is at 10.0ml, falling ball viscosity 38mPas, and the fine content 8.2% of viscose glue first, viscose glue contains alkali 5.8%, 500ml viscose gas bubble≤25, viscose glue surface tension 53dyne/cm, the following viscose glue particle of 10 μ m≤100/ml;
The moulding of C strand
In the strand molding procedure, the consisting of of acid bath: sulfuric acid concentration 145g/L, sodium sulfate concentration 245g/L, zinc sulfate concentration 12.5g/L, 56 ℃ of acid bath temperature, the acid bath surface tension is less than the viscose glue surface tension; Moulding bore Φ 5 ± 0.1mm, moulding pipe range 1200mm; The aperture of spinning head is 0.09mm, and shape is " one " font;
The D spinning
Spinning process comprises the solidifying of strand, drawing-off and disacidify, spinning roller length 1800mm, diameter of phi 50mm, the wire ring number of every rhizoid bar on the spinning roller is 1 circle, spinning roller upper filament space 100~120mm, 1300 rev/mins of spinning roller rotating speeds, 0.1~0.2 second/root of coagulation reaction time, the degree of draft of strand are 15%; Water temperature in the washing disacidify is 50~60 ℃, and the pH value is: 8;
Described through solidify, strand behind the disacidify, washing, its acid content is 20~30%, raw silk bar residue esterification degree is less than 3%.
E reels
In the coiling operation, strand imports in the funnel through support, and is wound into spinning cake in the centrifugal cylinder by electric ingot control, and the angle of strand and support is 45 degree, and the rotating speed of electric ingot is 8900 rev/mins; The rotating speed of centrifugal cylinder is 8400r/min.
Same above-mentioned technology can be disposed the strand of different size (as 40D, 60D, 120D, 150D, 200D etc.), different cultivars (as bright yarn, dull yarn contains the compound silks of cotton, bamboo, fiber crops etc., shaped filaments, flat filament etc.).
Embodiment 4
A kind of spinning technique that is applicable to the semicontinuous high-speed spinning machine of spinning roller horizontally set, its operation comprise that viscose glue measures and supplies glue, spins preceding filtration, strand moulding, spinning and coiling,
The A viscose glue measures and supplies glue
In viscose glue metering and confession glue process, the gauge pressure of viscose glue pipe is 0.4MPa;
B spins preceding filtration
Before spinning, filter in the operation viscose ripening degree NH 4Cl value control is at 8.0ml, falling ball viscosity 28mPas, and the fine content 8.2% of viscose glue first, viscose glue contains alkali 5.9%, 500ml viscose gas bubble≤25, viscose glue surface tension 52dyne/cm, the following viscose glue particle of 10 μ m≤100/ml;
The moulding of C strand
In the strand molding procedure, the consisting of of acid bath: sulfuric acid concentration 138g/L, sodium sulfate concentration 241g/L, zinc sulfate concentration 11.5g/L, 57 ℃ of acid bath temperature, the acid bath surface tension is less than the viscose glue surface tension; Moulding bore Φ 5 ± 0.1mm, moulding pipe range 900mm; The aperture of spinning head is 0.07mm, and shape is rounded;
The D spinning
Spinning process comprises the solidifying of strand, drawing-off and disacidify, spinning roller length 1000mm, diameter of phi 300mm, the wire ring number of every rhizoid bar on the spinning roller is 1 circle, spinning roller upper filament space 10~20mm, 100 rev/mins of spinning roller rotating speeds, 0.1~0.2 second/root of coagulation reaction time, the degree of draft of strand are 20%; Water temperature in the washing disacidify is 45~55 ℃, and the pH value is: 7.3;
Described through solidify, strand behind the disacidify, washing, its acid content is 25~35%, raw silk bar residue esterification degree is less than 3%.
E reels
In the coiling operation, strand imports in the funnel through support, and is wound into spinning cake in the centrifugal cylinder by electric ingot control, and the angle of strand and support is 60 degree, and the rotating speed of electric ingot is 7800 rev/mins; The rotating speed of centrifugal cylinder is 7600r/min.
Same above-mentioned technology can be disposed the strand of different size (as 40D, 60D, 120D, 150D, 200D etc.), different cultivars (as bright yarn, dull yarn contains the compound silks of cotton, bamboo, fiber crops etc., shaped filaments, flat filament etc.).
The key technical indexes after the described strand moulding of above-described embodiment 1-4 sees the following form:
Figure 548626DEST_PATH_IMAGE001
Embodiment 5 (basic identical with embodiment 1-4)
A kind of spinning technique that is applicable to the semicontinuous high-speed spinning machine of spinning roller horizontally set filters in the operation viscose ripening degree NH before spinning 4Cl value control is at 7.0ml, falling ball viscosity 29mPas, and the fine content 8.0% of viscose glue first, viscose glue contains alkali 5.8%, 500ml viscose gas bubble≤25, viscose glue surface tension 50dyne/cm, the following viscose glue particle of 10 μ m≤100/ml.
Embodiment 6(and embodiment 1-4 are basic identical)
A kind of spinning technique that is applicable to the semicontinuous high-speed spinning machine of spinning roller horizontally set filters in the operation viscose ripening degree NH before spinning 4Cl value control is at 9.0ml, falling ball viscosity 33mPas, and the fine content 8.1% of viscose glue first, viscose glue contains alkali 5.9%, 500ml viscose gas bubble≤25, viscose glue surface tension 50dyne/cm, the following viscose glue particle of 10 μ m≤100/ml.
Embodiment 7(and embodiment 1-4 are basic identical)
A kind of spinning technique that is applicable to the semicontinuous high-speed spinning machine of spinning roller horizontally set, in the strand molding procedure, the consisting of of acid bath: sulfuric acid concentration 137g/L, sodium sulfate concentration 235g/L, zinc sulfate concentration 11.8g/L, 56.5 ℃ of acid bath temperature, the acid bath surface tension is less than the viscose glue surface tension; Moulding bore Φ 5 ± 0.1mm, moulding pipe range 950mm; The aperture of spinning head is 0.06mm, and shape is fan-shaped.
Embodiment 8(and embodiment 1-4 are basic identical)
A kind of spinning technique that is applicable to the semicontinuous high-speed spinning machine of spinning roller horizontally set, in the strand molding procedure, the consisting of of acid bath: sulfuric acid concentration 142g/L, sodium sulfate concentration 240g/L, zinc sulfate concentration 12.3g/L, 56.5 ℃ of acid bath temperature, the acid bath surface tension is less than the viscose glue surface tension; Moulding bore Φ 5 ± 0.1mm, moulding pipe range 1050mm.
Embodiment 9(and embodiment 1-4 are basic identical)
A kind of spinning technique that is applicable to the semicontinuous high-speed spinning machine of spinning roller horizontally set, in spinning process, spinning roller length 1550mm, diameter of phi 138mm, the wire ring number of every rhizoid bar on the spinning roller is 1 circle, spinning roller upper filament space 70~80mm, 700 rev/mins of spinning roller rotating speeds, 0.1~0.2 second/root of coagulation reaction time, the degree of draft of strand are 20%; Water temperature in the washing disacidify is 38~43 ℃, and the pH value is: 7.7.
Embodiment 10(and embodiment 1-4 are basic identical)
A kind of spinning technique that is applicable to the semicontinuous high-speed spinning machine of spinning roller horizontally set, in spinning process, spinning roller length 1535mm, diameter of phi 200mm, the wire ring number of every rhizoid bar on the spinning roller are 1 circle; Spinning roller upper filament space 50~60mm, 300 rev/mins of spinning roller rotating speeds, 0.1~0.2 second/root of coagulation reaction time, the degree of draft of strand are 23%; Water temperature in the washing disacidify is 40~46 ℃, and the pH value is: 7.8.
Embodiment 11(and embodiment 1-4 are basic identical)
A kind of spinning technique that is applicable to the semicontinuous high-speed spinning machine of spinning roller horizontally set, in the coiling operation, strand imports in the funnel through support, and is wound into spinning cake in the centrifugal cylinder by electric ingot control, and the angle of described strand and support is 0 degree; The rotating speed of electricity ingot is 7450 rev/mins; The rotating speed of centrifugal cylinder is 7200r/min.
Embodiment 12(and embodiment 1-4 are basic identical)
A kind of spinning technique that is applicable to the semicontinuous high-speed spinning machine of spinning roller horizontally set, in the coiling operation, strand imports in the funnel through support, and is wound into spinning cake in the centrifugal cylinder by electric ingot control, and the angle of described strand and support is 90 degree; The rotating speed of electricity ingot is 8500 rev/mins; The rotating speed of centrifugal cylinder is 8000r/min.
Embodiment 13
Semicontinuous high-speed spinning machine comprises frame 1, glue feeder 2, strand shaped device 3, device for spinning 4 and coiler device 5, and spinning roller 40 is with respect to operating surface 102 horizontally sets that spin face 101 in the described device for spinning 4, and strand 8 is wrapped on the spinning roller 40.The described operating surface 102 that spins face 101 is to be positioned at the horizontal operation face that spins the face zone; Describedly refer to that with respect to operating surface 102 horizontally sets that spin face 101 spinning roller 40 is laterally to install with respect to the spinning workman as spinning workman during over against coiler device 5.
Embodiment 14
Semicontinuous high-speed spinning machine comprises frame 1, glue feeder 2, strand shaped device 3, device for spinning 4 and coiler device 5, and spinning roller 40 is with respect to operating surface 102 horizontally sets that spin face 101 in the described device for spinning 4, and strand 8 is wrapped on the spinning roller 40.The described operating surface 102 that spins face 101 is to be positioned at the horizontal operation face that spins the face zone; Describedly refer to that with respect to operating surface 102 horizontally sets that spin face 101 spinning roller 40 is laterally to install with respect to the spinning workman as spinning workman during over against coiler device 5.Spinning roller 40 comprises to be realized drawing-off, solidifies and/or the roller of disacidify function.The two ends of every spinning roller 40 are separately fixed at the top of frame 1 both sides, are connected rotation with drive unit.Every spinning roller 40 is connected with drive unit respectively, can realize that independence and real-time speed regulating rotate.At least comprise a help roll 401 in the device for spinning 4.Help roll 401 is parallel with spinning roller 40.Device for spinning 4 also comprises water washing device 42, and coiler device 5 comprises air exhausting device 52.

Claims (14)

1. spinning technique that is applicable to the semicontinuous high-speed spinning machine of spinning roller horizontally set, its operation comprise the viscose glue metering with for glue, spin preceding filtration, strand moulding, spinning and coiling, it is characterized in that:
The A viscose glue measures and supplies glue
Described viscose glue measures and supplies in the glue process, and the gauge pressure of viscose glue pipe is 0.1~0.5MPa;
B spins preceding filtration
Filter in the operation viscose ripening degree NH before described the spinning 4Cl value control is at 7.0~13ml, falling ball viscosity 28~38 mPas, and the fine content 8.0~8.2% of viscose glue first, viscose glue contains alkali 5.8~6.1%, 500ml viscose gas bubble≤25, viscose glue surface tension 50~55dyne/cm, the following viscose glue particle of 10 μ m≤100/ml;
The moulding of C strand
In the described strand molding procedure, the consisting of of acid bath: sulfuric acid concentration 135~145g/L, sodium sulfate concentration 230~245g/L, zinc sulfate concentration 11.0~12.5g/L, 55~57 ℃ of acid bath temperature, the acid bath surface tension is less than the viscose glue surface tension; Moulding bore Φ 5 ± 0.1mm, moulding pipe range 800~1200mm; The aperture of spinning head is 0.06~0.09mm, and shape is " one " font, fan-shaped or circular;
The D spinning
Described spinning process comprises the solidifying of strand, drawing-off and disacidify, spinning roller length 700~1800mm, diameter of phi 50~500mm, the wire ring number of every rhizoid bar on the spinning roller is 1 circle, spinning roller upper filament space 1~120mm, spinning roller rotating speed is 30~1300 rev/mins, and 0.1~0.2 second/root of coagulation reaction time, the degree of draft of strand are 10~25%; Water temperature in the washing disacidify is: 35~60 ℃, the pH value is: 7~8;
Described through solidify, strand behind the disacidify, washing, its acid content is 5~30%, raw silk bar residue esterification degree is less than 3%;
E reels
In the described coiling operation, strand imports in the funnel through support, and is wound into spinning cake in the centrifugal cylinder by electric ingot control, and the angle of strand and support is 0~90 degree, and the rotating speed of electric ingot is 7450~8900 rev/mins, and the rotating speed of centrifugal cylinder is 7200~8400r/min.
2. the spinning technique that is applicable to the semicontinuous high-speed spinning machine of spinning roller horizontally set according to claim 1, its operation comprise the viscose glue metering with for glue, spin preceding filtration, strand moulding, spinning and coiling, it is characterized in that:
The A viscose glue measures and supplies glue
In viscose glue metering and confession glue process, the gauge pressure of viscose glue pipe is 0.1MPa;
B spins preceding filtration
Before spinning, filter in the operation viscose ripening degree NH 4Cl value control is at 7.0ml, falling ball viscosity 30 mPas, and the fine content 8.0% of viscose glue first, viscose glue contains alkali 6.0%, 500ml viscose gas bubble≤25, viscose glue surface tension 50dyne/cm, the following viscose glue particle of 10 μ m≤100/ml;
The moulding of C strand
In the strand molding procedure, the consisting of of acid bath: sulfuric acid concentration 135g/L, sodium sulfate concentration 230g/L, zinc sulfate concentration 12.0g/L, 55 ℃ of acid bath temperature, the acid bath surface tension is less than the viscose glue surface tension; Moulding bore Φ 5 ± 0.1mm, moulding pipe range 800mm; The aperture of spinning head is 0.06mm, and shape is fan-shaped;
The D spinning
Spinning process comprises the solidifying of strand, drawing-off and disacidify, spinning roller length 1530mm, diameter of phi 100mm, the wire ring number of every rhizoid bar on the spinning roller is 1 circle, spinning roller upper filament space 20~50mm, 500 rev/mins of spinning roller rotating speeds, 0.1~0.2 second/root of coagulation reaction time, the degree of draft of strand are 10%; Water temperature in the washing disacidify is: 35~40 ℃, the pH value is: 7;
Described through solidify, strand behind the disacidify, washing, its acid content is 5~10%, raw silk bar residue esterification degree is less than 3%;
E reels
In the coiling operation, strand imports in the funnel through support, and is wound into spinning cake in the centrifugal cylinder by electric ingot control, and the angle of strand and support is 15 degree, and the rotating speed of electric ingot is 8000 rev/mins, and the rotating speed of centrifugal cylinder is 7800r/min.
3. the spinning technique that is applicable to the semicontinuous high-speed spinning machine of spinning roller horizontally set according to claim 1, its operation comprise the viscose glue metering with for glue, spin preceding filtration, strand moulding, spinning and coiling, it is characterized in that:
The A viscose glue measures and supplies glue
In viscose glue metering and confession glue process, the gauge pressure of viscose glue pipe is 0.3MPa;
B spins preceding filtration
Before spinning, filter in the operation viscose ripening degree NH 4Cl value control is at 13.0ml, falling ball viscosity 35mPas, and the fine content 8.1% of viscose glue first, viscose glue contains alkali 6.1%, 500ml viscose gas bubble≤25, viscose glue surface tension 55dyne/cm, the following viscose glue particle of 10 μ m≤100/ml;
The moulding of C strand
In the strand molding procedure, the consisting of of acid bath: sulfuric acid concentration 140g/L, sodium sulfate concentration 240g/L, zinc sulfate concentration 11.0g/L, 57 ℃ of acid bath temperature, the acid bath surface tension is less than the viscose glue surface tension; Moulding bore Φ 5 ± 0.1mm, moulding pipe range 1000mm; The aperture of institute's spinning head is 0.08mm, and shape is rounded;
The D spinning
Spinning process comprises the solidifying of strand, drawing-off and disacidify, spinning roller length 700mm, diameter of phi 500mm, the wire ring number of every rhizoid bar on the spinning roller is 1 circle, spinning roller upper filament space 1~5mm, 30 rev/mins of spinning roller rotating speeds, 0.1~0.2 second/root of coagulation reaction time, the degree of draft of strand are 25%; Water temperature in the washing disacidify is 40~50 ℃, and the pH value is: 7.5;
Described through solidify, strand behind the disacidify, washing, its acid content is 10~20%, raw silk bar residue esterification degree is less than 3%;
E reels
In the coiling operation, strand imports in the funnel through support, and is wound into spinning cake in the centrifugal cylinder by electric ingot control, and the angle of strand and support is 30 degree, and the rotating speed of electric ingot is 7450 rev/mins, and the rotating speed of centrifugal cylinder is 7200r/min.
4. the spinning technique that is applicable to the semicontinuous high-speed spinning machine of spinning roller horizontally set according to claim 1, its operation comprise the viscose glue metering with for glue, spin preceding filtration, strand moulding, spinning and coiling, it is characterized in that:
The A viscose glue measures and supplies glue
In viscose glue metering and confession glue process, the gauge pressure of viscose glue pipe is 0.5MPa;
B spins preceding filtration
Before spinning, filter in the operation viscose ripening degree NH 4Cl value control is at 10.0ml, falling ball viscosity 38mPas, and the fine content 8.2% of viscose glue first, viscose glue contains alkali 5.8%, 500ml viscose gas bubble≤25, viscose glue surface tension 53dyne/cm, the following viscose glue particle of 10 μ m≤100/ml;
The moulding of C strand
In the strand molding procedure, the consisting of of acid bath: sulfuric acid concentration 145g/L, sodium sulfate concentration 245g/L, zinc sulfate concentration 12.5g/L, 56 ℃ of acid bath temperature, the acid bath surface tension is less than the viscose glue surface tension; Moulding bore Φ 5 ± 0.1mm, moulding pipe range 1200mm; The aperture of spinning head is 0.09mm, and shape is " one " font;
The D spinning
Spinning process comprises the solidifying of strand, drawing-off and disacidify, spinning roller length 1800mm, diameter of phi 50mm, the wire ring number of every rhizoid bar on the spinning roller is 1 circle, spinning roller upper filament space 100~120mm, 1300 rev/mins of spinning roller rotating speeds, 0.1~0.2 second/root of coagulation reaction time, the degree of draft of strand are 15%; Water temperature in the washing disacidify is 50~60 ℃, and the pH value is: 8;
Described through solidify, strand behind the disacidify, washing, its acid content is 20~30%, raw silk bar residue esterification degree is less than 3%;
E reels
In the coiling operation, strand imports in the funnel through support, and is wound into spinning cake in the centrifugal cylinder by electric ingot control, and the angle of strand and support is 45 degree, and the rotating speed of electric ingot is 8900 rev/mins; The rotating speed of centrifugal cylinder is 8400r/min.
5. the spinning technique that is applicable to the semicontinuous high-speed spinning machine of spinning roller horizontally set according to claim 1, its operation comprise the viscose glue metering with for glue, spin preceding filtration, strand moulding, spinning and coiling, it is characterized in that:
The A viscose glue measures and supplies glue
In viscose glue metering and confession glue process, the gauge pressure of viscose glue pipe is 0.4MPa;
B spins preceding filtration
Before spinning, filter in the operation viscose ripening degree NH 4Cl value control is at 8.0ml, falling ball viscosity 28mPas, and the fine content 8.2% of viscose glue first, viscose glue contains alkali 5.9%, 500ml viscose gas bubble≤25, viscose glue surface tension 52dyne/cm, the following viscose glue particle of 10 μ m≤100/ml;
The moulding of C strand
In the strand molding procedure, the consisting of of acid bath: sulfuric acid concentration 138g/L, sodium sulfate concentration 241g/L, zinc sulfate concentration 11.5g/L, 57 ℃ of acid bath temperature, the acid bath surface tension is less than the viscose glue surface tension; Moulding bore Φ 5 ± 0.1mm, moulding pipe range 900mm; The aperture of spinning head is 0.07mm, and shape is rounded;
The D spinning
Spinning process comprises the solidifying of strand, drawing-off and disacidify, spinning roller length 1000mm, diameter of phi 300mm, the wire ring number of every rhizoid bar on the spinning roller is 1 circle, spinning roller upper filament space 10~20mm, 100 rev/mins of spinning roller rotating speeds, 0.1~0.2 second/root of coagulation reaction time, the degree of draft of strand are 20%; Water temperature in the washing disacidify is 45~55 ℃, and the pH value is: 7.3;
Described through solidify, strand behind the disacidify, washing, its acid content is 25~35%, raw silk bar residue esterification degree is less than 3%;
E reels
In the coiling operation, strand imports in the funnel through support, and is wound into spinning cake in the centrifugal cylinder by electric ingot control, and the angle of strand and support is 60 degree, and the rotating speed of electric ingot is 7800 rev/mins; The rotating speed of centrifugal cylinder is 7600r/min.
6. the spinning technique that is applicable to the semicontinuous high-speed spinning machine of spinning roller horizontally set according to claim 1, its operation comprises the viscose glue metering and supplies glue, spins preceding filtration, strand moulding, spinning and coiling, it is characterized in that: before spinning, filter in the operation viscose ripening degree NH 4Cl value control is at 7.0ml, falling ball viscosity 29mPas, and the fine content 8.0% of viscose glue first, viscose glue contains alkali 5.8%, 500ml viscose gas bubble≤25, viscose glue surface tension 50dyne/cm, the following viscose glue particle of 10 μ m≤100/ml.
7. the spinning technique that is applicable to the semicontinuous high-speed spinning machine of spinning roller horizontally set according to claim 1, its operation comprises the viscose glue metering and supplies glue, spins preceding filtration, strand moulding, spinning and coiling, it is characterized in that: before spinning, filter in the operation viscose ripening degree NH 4Cl value control is at 9.0ml, falling ball viscosity 33mPas, and the fine content 8.1% of viscose glue first, viscose glue contains alkali 5.9%, 500ml viscose gas bubble≤25, viscose glue surface tension 50dyne/cm, the following viscose glue particle of 10 μ m≤100/ml.
8. the spinning technique that is applicable to the semicontinuous high-speed spinning machine of spinning roller horizontally set according to claim 1, its operation comprises the viscose glue metering and supplies glue, spins preceding filtration, strand moulding, spinning and coiling, it is characterized in that:, in the strand molding procedure, consisting of of acid bath: sulfuric acid concentration 137g/L, sodium sulfate concentration 235g/L, zinc sulfate concentration 11.8g/L, 56.5 ℃ of acid bath temperature, the acid bath surface tension is less than the viscose glue surface tension; Moulding bore Φ 5 ± 0.1mm, moulding pipe range 950mm; The aperture of spinning head is 0.06mm, and shape is fan-shaped.
9. the spinning technique that is applicable to the semicontinuous high-speed spinning machine of spinning roller horizontally set according to claim 1, its operation comprises the viscose glue metering and supplies glue, spins preceding filtration, strand moulding, spinning and coiling, it is characterized in that: in the strand molding procedure, consisting of of acid bath: sulfuric acid concentration 142g/L, sodium sulfate concentration 240g/L, zinc sulfate concentration 12.3g/L, 56.5 ℃ of acid bath temperature, the acid bath surface tension is less than the viscose glue surface tension; Moulding bore Φ 5 ± 0.1mm, moulding pipe range 1050mm.
10. the spinning technique that is applicable to the semicontinuous high-speed spinning machine of spinning roller horizontally set according to claim 1, its operation comprises the viscose glue metering and supplies glue, spins preceding filtration, strand moulding, spinning and coiling, it is characterized in that: in spinning process, spinning roller length 1550mm, diameter of phi 138mm, the wire ring number of every rhizoid bar on the spinning roller are 1 circle, spinning roller upper filament space 70~80mm, 700 rev/mins of spinning roller rotating speeds, 0.1~0.2 second/root of coagulation reaction time, the degree of draft of strand are 20%; Water temperature in the washing disacidify is 38~43 ℃, and the pH value is: 7.7.
11. the spinning technique that is applicable to the semicontinuous high-speed spinning machine of spinning roller horizontally set according to claim 1, its operation comprises the viscose glue metering and supplies glue, spins preceding filtration, strand moulding, spinning and coiling, it is characterized in that: in spinning process, spinning roller length 1535mm, diameter of phi 200mm, the wire ring number of every rhizoid bar on the spinning roller are 1 circle; Spinning roller upper filament space 50~60mm, 300 rev/mins of spinning roller rotating speeds, 0.1~0.2 second/root of coagulation reaction time, the degree of draft of strand are 23%; Water temperature in the washing disacidify is 40~46 ℃, and the pH value is: 7.8.
12. the spinning technique that is applicable to the semicontinuous high-speed spinning machine of spinning roller horizontally set according to claim 1, its operation comprises the viscose glue metering and supplies glue, spins preceding filtration, strand moulding, spinning and coiling, it is characterized in that: in the coiling operation, strand imports in the funnel through support, and in the centrifugal cylinder by electric ingot control, being wound into spinning cake, the angle of described strand and support is 0 degree; The rotating speed of electricity ingot is 7450 rev/mins; The rotating speed of centrifugal cylinder is 7200r/min.
13. the spinning technique that is applicable to the semicontinuous high-speed spinning machine of spinning roller horizontally set according to claim 1, its operation comprises the viscose glue metering and supplies glue, spins preceding filtration, strand moulding, spinning and coiling, it is characterized in that: in the coiling operation, strand imports in the funnel through support, and in the centrifugal cylinder by electric ingot control, being wound into spinning cake, the angle of described strand and support is 90 degree; The rotating speed of electricity ingot is 8500 rev/mins; The rotating speed of centrifugal cylinder is 8000r/min.
14. according to each described spinning technique that is applicable to the semicontinuous high-speed spinning machine of spinning roller horizontally set of claim 1-13, it is characterized in that: attainable the key technical indexes is as follows behind the described strand coiling and molding:
Do fracture strength (CN/dtex): 〉=1.85;
Wet breaking strength (CN/dtex): 〉=0.85;
Dried extension at break: 〉=17.0-24.0%;
The dried extension at break coefficient of variation (CV value) :≤6.00%;
Line density (fiber number) deviation: ± 2.0%;
The line density coefficient of variation (CV value) :≤2.00%;
The twist coefficient of variation (CV value) :≤13.00%;
Monofilament radical deviation :≤1.0%;
Residual sulfur content (Mg/100g fiber) :≤10.0;
Dye uniformity (ash card) level: 〉=4.
CN201310266735.4A 2013-06-29 2013-06-29 Spinning technology applied to semi-continuous high-speed spinning machine with spinning roller arranged horizontally Expired - Fee Related CN103290496B (en)

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CN103603073A (en) * 2013-12-04 2014-02-26 宜宾丝丽雅集团有限公司 Spinning technology suitable for spinning machine with external winding device
CN103628153A (en) * 2013-12-04 2014-03-12 宜宾丝丽雅集团有限公司 Spinning technology of spinning machine provided with novel single-spindle passive winding device
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CN103643314A (en) * 2013-12-04 2014-03-19 宜宾丝丽雅集团有限公司 Spinning process of spinning machine with external winding device
CN103643313A (en) * 2013-12-04 2014-03-19 宜宾丝丽雅集团有限公司 Spinning process suitable for novel spinning machine with external winding device
CN103643312A (en) * 2013-12-04 2014-03-19 宜宾丝丽雅集团有限公司 Spinning process of spinning machine with external winding device
CN103643322A (en) * 2013-12-04 2014-03-19 宜宾丝丽雅集团有限公司 Spinning technology of spinning machine provided with three-spindle passive winding device
CN103643328A (en) * 2013-12-04 2014-03-19 宜宾丝丽雅集团有限公司 Spinning technology of spinning machine with yarn twisting function
CN103643315A (en) * 2013-12-04 2014-03-19 宜宾丝丽雅集团有限公司 Spinning process suitable for high-speed spinning machine with external winding device
CN103643329A (en) * 2013-12-04 2014-03-19 宜宾丝丽雅集团有限公司 Spinning process of high-speed spinning machine with external winding device
CN103643311A (en) * 2013-12-04 2014-03-19 宜宾丝丽雅集团有限公司 Spinning process suitable for novel high-speed spinning machine with external winding device
CN103643323A (en) * 2013-12-04 2014-03-19 宜宾丝丽雅集团有限公司 Spinning technology of spinning machine with single-spindle passive winding device
CN103774257A (en) * 2013-12-04 2014-05-07 宜宾丝丽雅集团有限公司 Spinning process suitable for novel spinning machine with external winding device
WO2014206161A1 (en) * 2013-06-29 2014-12-31 宜宾海丝特纤维有限责任公司 Novel semi-continuous high-speed spinning machine
CN105200589A (en) * 2014-06-27 2015-12-30 如皋市利富织造有限公司 Hand-made process for silk yarn

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CN1590605A (en) * 2004-02-12 2005-03-09 湖北金环股份有限公司 High strength viscose long filament spinning technology and equipment
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WO2014206161A1 (en) * 2013-06-29 2014-12-31 宜宾海丝特纤维有限责任公司 Novel semi-continuous high-speed spinning machine
CN103628151A (en) * 2013-12-02 2014-03-12 宜宾丝丽雅股份有限公司 Production process of fluorescent whitening flat filament
CN103628151B (en) * 2013-12-02 2016-02-10 宜宾丝丽雅股份有限公司 Production process of fluorescent whitening flat filament
CN103643313A (en) * 2013-12-04 2014-03-19 宜宾丝丽雅集团有限公司 Spinning process suitable for novel spinning machine with external winding device
CN103643323B (en) * 2013-12-04 2016-04-06 宜宾丝丽雅集团有限公司 Spinning technology of spinning machine with single-spindle passive winding device
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CN103628154A (en) * 2013-12-04 2014-03-12 宜宾丝丽雅集团有限公司 Spinning technology of spinning machine provided with through shaft passive winding device
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CN103643314A (en) * 2013-12-04 2014-03-19 宜宾丝丽雅集团有限公司 Spinning process of spinning machine with external winding device
CN103603077A (en) * 2013-12-04 2014-02-26 宜宾丝丽雅集团有限公司 Spinning process suitable for spinning machine with external winding device
CN103643312A (en) * 2013-12-04 2014-03-19 宜宾丝丽雅集团有限公司 Spinning process of spinning machine with external winding device
CN103643322A (en) * 2013-12-04 2014-03-19 宜宾丝丽雅集团有限公司 Spinning technology of spinning machine provided with three-spindle passive winding device
CN103643328A (en) * 2013-12-04 2014-03-19 宜宾丝丽雅集团有限公司 Spinning technology of spinning machine with yarn twisting function
CN103643315A (en) * 2013-12-04 2014-03-19 宜宾丝丽雅集团有限公司 Spinning process suitable for high-speed spinning machine with external winding device
CN103643329A (en) * 2013-12-04 2014-03-19 宜宾丝丽雅集团有限公司 Spinning process of high-speed spinning machine with external winding device
CN103643311A (en) * 2013-12-04 2014-03-19 宜宾丝丽雅集团有限公司 Spinning process suitable for novel high-speed spinning machine with external winding device
CN103643323A (en) * 2013-12-04 2014-03-19 宜宾丝丽雅集团有限公司 Spinning technology of spinning machine with single-spindle passive winding device
CN103774257A (en) * 2013-12-04 2014-05-07 宜宾丝丽雅集团有限公司 Spinning process suitable for novel spinning machine with external winding device
CN103628153A (en) * 2013-12-04 2014-03-12 宜宾丝丽雅集团有限公司 Spinning technology of spinning machine provided with novel single-spindle passive winding device
CN103628164A (en) * 2013-12-04 2014-03-12 宜宾丝丽雅集团有限公司 Novel spinning machine
CN103643315B (en) * 2013-12-04 2017-01-18 宜宾丝丽雅集团有限公司 Spinning process suitable for high-speed spinning machine with external winding device
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CN103628164B (en) * 2013-12-04 2016-02-10 宜宾丝丽雅集团有限公司 Novel spinning machine
CN103603073A (en) * 2013-12-04 2014-02-26 宜宾丝丽雅集团有限公司 Spinning technology suitable for spinning machine with external winding device
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CN103603077B (en) * 2013-12-04 2016-02-10 宜宾丝丽雅集团有限公司 Spinning process suitable for spinning machine with external winding device
CN103643322B (en) * 2013-12-04 2016-01-20 宜宾丝丽雅集团有限公司 Spinning technology of spinning machine provided with three-spindle passive winding device
CN103643314B (en) * 2013-12-04 2016-05-25 宜宾丝丽雅集团有限公司 Spinning process of spinning machine with external winding device
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CN103774257B (en) * 2013-12-04 2016-05-25 宜宾丝丽雅集团有限公司 Spinning technology suitable for spinning machine with external winding device
CN103628162B (en) * 2013-12-04 2016-05-25 宜宾丝丽雅集团有限公司 Spinning process suitable for novel high-speed spinning machine with external winding device
CN103643313B (en) * 2013-12-04 2016-06-22 宜宾丝丽雅集团有限公司 Spinning process suitable for spinning machine with external winding device
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CN105200589A (en) * 2014-06-27 2015-12-30 如皋市利富织造有限公司 Hand-made process for silk yarn

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