CN102978030B - Multifunctional detergent and preparation method thereof - Google Patents

Multifunctional detergent and preparation method thereof Download PDF

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Publication number
CN102978030B
CN102978030B CN201210523511.2A CN201210523511A CN102978030B CN 102978030 B CN102978030 B CN 102978030B CN 201210523511 A CN201210523511 A CN 201210523511A CN 102978030 B CN102978030 B CN 102978030B
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detergent
sodium sulfate
preparation
multifunctional
formula
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Expired - Fee Related
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CN201210523511.2A
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Chinese (zh)
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CN102978030A (en
Inventor
李祖敏
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Zhejiang Yuanmin Science & Technology Co Ltd
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Zhejiang Yuanmin Science & Technology Co Ltd
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Abstract

The invention provides a multifunctional detergent and a preparation method thereof. The formula of the multifunctional detergent comprises fatty alcohol ether sodium sulfate, fatty acid methyl ester sulfonate and glycine betaine at a weight ratio of 4-7:2-5:1-3. The formula also can comprise dodecylbenzene sulfonic acid, alpha-alkenyl sulphonate and an addition agent. The detergent provided by the invention has the double advantages of forming by adding water and good washing effect and is comparative to more than 10 times of liquid detergent on the market in terms of effect; and the detergent provided by the invention can be dissolved under any conditions when encountering water, has low simulation and can be degraded, thus the environmental pollution and damage are reduced and the detergent is an environment-friendly product. The preparation method of the detergent is simple, low in cost and suitable for industrial production.

Description

Multifunctional detergent and preparation method thereof
Technical field
The present invention relates to washing composition technical field, refer to especially a kind of multifunctional detergent and preparation method thereof.
Background technology
On market, have the washing composition that generally has three kinds of powderies now, a kind of is pure tensio-active agent powdery monomer, bad as the effect of product application.The second is the civilian industry powdered detergent of everybody more clearly as similar washing powder, and it is to take inorganic salt as main, a kind of powdered detergent of tensio-active agent for assisting.Also have part in the formula of its product, have the biological limitation that adds materials and cannot be as being widely used and promoting.The third is to be the tensio-active agent that major ingredient adds sub-fraction again with Mierocrystalline cellulose, thin up becomes the outward appearance denseness of common liquid detergent on similar market, outward appearance tradition after this product dilution, more in practical application, do not reach cleaning performance, and the quality guaranteed period of finished product is shorter apt to deteriorate.
Summary of the invention
The present invention proposes a kind of multifunctional detergent and preparation method thereof, the effect of this washing composition be on market more than 10 times, and there is the moulding of being watered and the good two-fold advantage of washing effect.
Technical scheme of the present invention is achieved in that
A multifunctional detergent, its formula comprises: fatty alcohol-ether sodium sulfate, fatty acid methyl ester sulfonate and trimethyl-glycine; Its weight ratio is 4-7:2-5:1-3.
As preferred technical scheme, in described formula, also comprise Witco 1298 Soft Acid, a-alkenyl sulphonate and pH adjusting agent.
As preferred technical scheme, the mass percent of described fatty alcohol-ether sodium sulfate, fatty acid methyl ester sulfonate, trimethyl-glycine, Witco 1298 Soft Acid, a-alkenyl sulphonate, auxiliary agent is
20-35%:10-25%:5-15%:10-25%:5-15%:31-50%。
As preferred technical scheme, in described formula, also comprise pH adjusting agent.Be used for regulating the pH value of formula, owing to being all neutral material in this formula, therefore, generally do not need to add pH adjusting agent.
As preferred technical scheme, described fatty alcohol-ether sodium sulfate is polyoxyethylenated alcohol sodium sulfate.
As preferred technical scheme, described trimethyl-glycine is cocamidopropyl betaine.
As preferred technical scheme, described auxiliary agent is sodium sulfate, or sodium sulfate and Na2EDTA.
As preferred technical scheme, described pH adjusting agent is citric acid.
It is the powdered detergent of the tensio-active agent of main interpolation sub-fraction that this product does not comprise by Mierocrystalline cellulose.
A preparation method for multifunctional detergent, comprising:
Step S1: poly alkyl alcohol ether sodium sulfate, Witco 1298 Soft Acid, α-sodium olefin sulfonate, fatty acid methyl ester sulfonate, trimethyl-glycine and auxiliary agent are uniformly mixed;
Step S2, in the temperature 80-150 ℃ moulding of dusting, obtains the mixed solution after above-mentioned adjusting pH.
As preferred technical scheme, described in dust time of moulding be 1-3min.
Beneficial effect:
(1) washing composition of the present invention has the moulding of being watered and the good two-fold advantage of washing effect;
(2) washing composition of the present invention is equivalent to the effect of 10 times of above liquid washing agents on market;
(3) product of the present invention can dissolve at any condition chance water, stimulates little, degradable, reduces environmental pollution and harm, is the product of environment-friendly type;
(4) preparation method is simple, and cost is low, is suitable for suitability for industrialized production.
Embodiment
Below the technical scheme in the embodiment of the present invention is clearly and completely described, obviously, described embodiment is only the present invention's part embodiment, rather than whole embodiment.Embodiment based in the present invention, those of ordinary skills, not making the every other embodiment obtaining under creative work prerequisite, belong to the scope of protection of the invention.
A kind of multifunctional detergent of the present invention, the material in its formula is the commercially available material being easy to get.The present invention is through rationally composite, and through the high temperature moulding of dusting by kinds of surface promoting agent and inorganic additive.According to specific needs, be watered by a certain percentage the conventional shape outward appearance that can form 5-15 times of effective concentration, have that stronger decontamination is deoiled, the comprehensive multifunctional washing composition of performance gentleness.The formula of 10 times of above liquid washing agents on the suitable market of this product, Xian Yi our company, now with the productivity of annual 20000 tons, is namely equivalent to 200,000 tons of above quantity on market.Greatly reduce and produce institute's some electric energy that produced and thing energy, and the waste gas of a large amount of discharges that produce at transport point, reducing social energy loss and also improved clean environment simultaneously, social benefit is huge, has very strong market competition advantage.Product of the present invention is met water in any condition and can be dissolved, and stimulates little, degradable, reduces environmental pollution and harm, is the product of environment-friendly type.Product key point be different from some powdered detergents on other market they can not be watered moulding and some can moulding but product that can not corresponding washing effect, this product has just made in conjunction with their two kinds of advantages the washing composition that has outward appearance and have identical function.It is the powdered detergent of the tensio-active agent of main interpolation sub-fraction that this product does not comprise by Mierocrystalline cellulose.
Embodiment 1
Multifunctional detergent 1, its formula comprises: fatty alcohol-ether sodium sulfate, fatty acid methyl ester sulfonate and trimethyl-glycine; Its weight ratio is 4:2:3.
Its preparation comprises:
Step S1: above-mentioned substance is uniformly mixed;
Step S2, delivers to tower top by the material being uniformly mixed by high-pressure pump, and in 80-150 ℃ of moulding of dusting of tower body temperature, time 1-3min, obtains.
Embodiment 2
Multifunctional detergent 2, its formula comprises: the mass percent of fatty alcohol-ether sodium sulfate, fatty acid methyl ester sulfonate, trimethyl-glycine, Witco 1298 Soft Acid, a-alkenyl sulphonate, sodium sulfate is 20:25:9:10:5:31.
Its preparation method, comprising:
Step S1: poly alkyl alcohol ether sodium sulfate, Witco 1298 Soft Acid, α-sodium olefin sulfonate, fatty acid methyl ester sulfonate and trimethyl-glycine are uniformly mixed, add afterwards sodium sulfate to obtain mixed solution;
Step S2, delivers to tower top by above-mentioned mixed solution by high-pressure pump, and in the temperature 80-150 ℃ moulding of dusting, the time is 3min and get final product.
Embodiment 3
Multifunctional detergent 3, its formula comprises: the mass percent of fatty alcohol-ether sodium sulfate, fatty acid methyl ester sulfonate, trimethyl-glycine, Witco 1298 Soft Acid, a-alkenyl sulphonate, sodium sulfate is 20:10:5:10:5:50.
Preparation is same with embodiment 2.
Embodiment 4
Multifunctional detergent 4, its formula comprises: the mass percent of fatty alcohol-ether sodium sulfate, fatty acid methyl ester sulfonate, trimethyl-glycine, Witco 1298 Soft Acid, a-alkenyl sulphonate, Na2EDTA and sodium sulfate is 25:15:6:12:8:1:33.
Its preparation method, comprising:
Step S1: fatty alcohol-ether sodium sulfate, fatty acid methyl ester sulfonate, trimethyl-glycine, Witco 1298 Soft Acid, a-alkenyl sulphonate, Na2EDTA and sodium sulfate are uniformly mixed, add afterwards as lemon acid for adjusting pH be 6.5-7.5;
Step S2, delivers to tower top by above-mentioned mixed solution by high-pressure pump, and in 80-150 ℃ of moulding of dusting of tower body temperature, the time is 1-3min and get final product.
Embodiment 5
Multifunctional detergent 5, its formula comprises: fatty alcohol-ether sodium sulfate, fatty acid methyl ester sulfonate and trimethyl-glycine; Its weight ratio is 7:3:2.
Product of the present invention, can add the water of 5 parts to 15 parts, while add, water stirs until added water adds, and just can convert into the washing composition of different mass.Product of the present invention has the moulding of being watered and the good two-fold advantage of washing effect.
The foregoing is only preferred embodiment of the present invention, in order to limit the present invention, within the spirit and principles in the present invention not all, any modification of doing, be equal to replacement, improvement etc., within all should being included in protection scope of the present invention.

Claims (5)

1. a multifunctional detergent, is characterized in that, its formula is comprised of following component: polyoxyethylenated alcohol sodium sulfate, fatty acid methyl ester sulfonate, cocamidopropyl betaine, Witco 1298 Soft Acid, a-alkenyl sulphonate and auxiliary agent; Its mass percent is
20-35%:10-25%:5-15%:10-25%:5-15%:31-50%;
Described auxiliary agent is sodium sulfate, or sodium sulfate and Na2EDTA.
2. a kind of multifunctional detergent according to claim 1, is characterized in that, also comprises pH adjusting agent in described formula.
3. a kind of multifunctional detergent according to claim 2, is characterized in that, described pH adjusting agent is citric acid.
4. according to the preparation method of a kind of multifunctional detergent described in the arbitrary claim of claim 1-3, comprising:
Step S1: polyoxyethylenated alcohol sodium sulfate, fatty acid methyl ester sulfonate, cocamidopropyl betaine, Witco 1298 Soft Acid, a-alkenyl sulphonate and auxiliary agent are uniformly mixed; Its mass percent is
20-35%:10-25%:5-15%:10-25%:5-15%:31-50%;
Described auxiliary agent is sodium sulfate, or sodium sulfate and Na2EDTA
Step S2: above-mentioned mixed solution is regulated after pH to the moulding of dusting at temperature 80-150 ℃, obtain.
5. the preparation method of a kind of multifunctional detergent according to claim 4, is characterized in that, described in dust time of moulding be 1-3min.
CN201210523511.2A 2012-12-04 2012-12-04 Multifunctional detergent and preparation method thereof Expired - Fee Related CN102978030B (en)

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Application Number Priority Date Filing Date Title
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CN102978030B true CN102978030B (en) 2014-04-16

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CN111793529A (en) * 2020-08-10 2020-10-20 訾孟州 Natural composite detergent of high-purity pineapple enzyme and preparation method thereof
CN112251299A (en) * 2020-10-21 2021-01-22 沈阳脱普生活用品服务有限公司上海分公司 High-concentration detergent and preparation method thereof

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CN102051278A (en) * 2011-01-24 2011-05-11 北京洛娃日化有限公司 All-purpose cleaning agent
CN102559406A (en) * 2011-08-06 2012-07-11 威莱(广州)日用品有限公司 Compound type cleaning solution

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PE01 Entry into force of the registration of the contract for pledge of patent right
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Denomination of invention: Multifunctional detergent and preparation method thereof

Effective date of registration: 20171227

Granted publication date: 20140416

Pledgee: Zhejiang Cangnan rural commercial bank Limited by Share Ltd.

Pledgor: ZHEJIANG YUANMIN SCIENCE & TECHNOLOGY Co.,Ltd.

Registration number: 2017330000332

PC01 Cancellation of the registration of the contract for pledge of patent right
PC01 Cancellation of the registration of the contract for pledge of patent right

Date of cancellation: 20210312

Granted publication date: 20140416

Pledgee: Zhejiang Cangnan rural commercial bank Limited by Share Ltd.

Pledgor: ZHEJIANG YUANMIN SCIENCE & TECHNOLOGY Co.,Ltd.

Registration number: 2017330000332

CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20140416

Termination date: 20211204