CN102907725A - Preparation method of blueberry oral liquid containing vitamin A and vitamin P - Google Patents

Preparation method of blueberry oral liquid containing vitamin A and vitamin P Download PDF

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Publication number
CN102907725A
CN102907725A CN2012102062592A CN201210206259A CN102907725A CN 102907725 A CN102907725 A CN 102907725A CN 2012102062592 A CN2012102062592 A CN 2012102062592A CN 201210206259 A CN201210206259 A CN 201210206259A CN 102907725 A CN102907725 A CN 102907725A
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China
Prior art keywords
blueberry
juice
preparation
vitamin
oral liquid
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CN2012102062592A
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Chinese (zh)
Inventor
徐静
张百灵
王林
王晓辉
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HEILONGJIANG YUEJU MANOR BIOTECHNOLOGY CO Ltd
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HEILONGJIANG YUEJU MANOR BIOTECHNOLOGY CO Ltd
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Priority to CN2012102062592A priority Critical patent/CN102907725A/en
Publication of CN102907725A publication Critical patent/CN102907725A/en
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Abstract

The invention provides a preparation method of blueberry oral liquid containing vitamin A(VA) and vitamin P (VP), relates to the preparation method of nutritional healthcare oral liquids, and aims to solve the problem that the nutritional ingredients in the existing blueberry product cannot be easily absorbed by a human body. The preparation method comprises the following steps: after cleaning fresh blueberries, carrying out crushing, enzymolysis and centrifugal separation, fermenting an obtained centrifugal liquid at a low temperature to obtain a fermented liquid and carrying out rough filtering and fine filtering to obtain a low-alcohol fermented liquid; after cleaning the fresh blueberries, crushing, extracting a self-flow blueberry juice and carrying out rough filtering and fine filtering to obtain a blueberry fresh juice; mixing the low-alcohol fermented liquid, the blueberry fresh juice, pure water and white granulated sugar; and after filtering an obtained mixed solution, carrying UHT (ultra high temperature) sterilization and then obtaining the blueberry oral liquid. The preparation method is scientific and avoids the use of any biological additive. With adoption of the low-alcohol fermented liquid obtained in the manner of ternary low-temperature fermentation, the nutritional ingredients such as VP and VA can fast enter the internal microcirculation system of the human body, so that the absorbing rate and the absorbing speed of the human body to the nutritional ingredients are improved. The preparation method is used for preparing the blueberry oral liquid containing VA and VP.

Description

The preparation method who contains the blueberry oral liquid of vitamin A and citrin
Technical field
The present invention relates to a kind of preparation method of Nutrious health-care oral tonic.
Background technology
Blueberry (Blueberry) means the meaning of blue berry.Low shrub, short pin is wild, and particle is little, and the content of anthocyanidin is very high.China mainly produces in Daxing'an Mountainrange and forest zone, the Xiaoxinanlin Mountains, and all is pure wild.Just successfully carried out in recent years domestication's cultivation.Contain abundant nutritional labeling in the Blueberry, it not only has good nutrition health-care functions, also has the functions such as the cranial nerve of preventing is aging, cardiac stimulant, anticancer softening blood vessel, enhancing human organism immunity.Wild blueberry, unique flavor, sour-sweet suitable, mouthfeel is good, can be used to eat, make the usefulness of beverage, spices, wine brewing, but the nutritional labeling in the existing blueberry product be difficult for being absorbed fast by human body, and absorption rate is lower.
Summary of the invention
The nutritional labeling that the present invention will solve in the existing blueberry product is difficult for being absorbed fast and the low problem of absorption rate by human body, and a kind of preparation method who contains the blueberry oral liquid of vitamin A and citrin is provided.
The preparation method that the present invention contains the blueberry oral liquid of vitamin A and citrin carries out according to the following steps:
One, prepare low alcohol fermented juice:
Get ripe blueberry fresh fruit, remove impurity, the water spray irrigation, after the blueberry fresh fruit fragmentation of cleaning, place sterile chamber, obtain blueberry juice pulp, add pectase in the blueberry juice pulp after, stir 45min with the speed of 40～47r/min after, enzymolysis 48～60h under 40～50 ℃ temperature, centrifugation, gained centrifugate stop fermentation when 16～20 ℃ temperature bottom fermentation to ethanol degree is 4～4.5 °, obtain the juice that ferments, to ferment juice with 0.45 μ m filter plate coarse filtration after, with the smart filter of 0.2 μ m filter plate, obtain low alcohol fermented juice again, refrigerate for subsequent use;
Two, extract blueberry fresh fruit juice:
Get ripe blueberry fresh fruit, remove impurity, the water spray irrigation, after the blueberry fresh fruit fragmentation of cleaning, place sterile chamber, obtain the blueberry juice pulp mixture, in the blueberry juice pulp mixture, add pectase, speed with 47～57r/min stirs, stir every day 1～2 time, stir 30～45min at every turn, process after 7～10 days, extract blueberry gravity flow fruit juice, reclaim the seed of lower floor; Blueberry is flow automatically fruit juice with 1.0 μ m filter plate coarse filtration, use again 0.2 μ m membrane filtration, get blueberry fresh fruit juice, refrigerate for subsequent use;
Three, by volume umber takes by weighing low alcohol fermented juice, 60～75 portions of blueberry fresh fruit juice, 10 parts of pure water and 10～15 portions of white granulated sugars that step 2 obtains that 10～20 parts of step 1 obtain, be mixed to get mixed liquor, with mixed liquor with 0.2 μ m membrane filtration after, carry out ultra high temperature short time sterilization, obtain containing the blueberry oral liquid of vitamin A and citrin.
The invention has the beneficial effects as follows:
1, on technology, adopted the biological assistant without any artificial interpolation to keep " three is former " (former fruit, Normal juice, former fructose) low temperature (16～20 ℃) zymotechnique, neither add any fermentation assistant, the unartificial yeast cold fermentation of utilizing former fructose and blueberries self to adhere to, greatly keep the nutritional labeling in the fruit, and produced new nutriment after the fermentation, such as multiple nutritional components such as amino acid, polysaccharide, phenolic compound and flavor and fragrance substances.
2, adopted the compatibility of the bright juice of blueberry fermented juice and blueberry, utilize the micro ethanol of fermented juice to do the importing medium, make the high nutrition of blueberry enter fast the microcirculation in human body system, because containing little alcohol in the blueberry fermented juice, played the unique effect of quick importing microcirculation in human body system.The science compatibility of the bright juice of blueberry fermented juice and blueberry is so that the prepared blueberry oral liquid of the present invention has faster absorption of human body speed and higher active ingredient absorptivity.Particularly contain rutin (VP) composition in the blueberry oral liquid of vitamin A and citrin under the effect of fermented juice, can enter fast microcirculqtory system in the human body, reached the function of best nutrition, at home and abroad initiated to have and absorb the blueberry oral liquid that contains VP+VA fast, the high new function of nutritional labeling.
3, effective efficiency nutritive index science safety: 1. without any additive, 2. scientific allocation technology blueberry VP+VA oral liquid is because of the innovation of scientific formula, so that the effective nutrition of blueberry oral liquid more comprehensively, more outstanding, be rich in the oral liquid anthocyanidin and several amino acids, high mallow element, heteroside 11.5mg/L, particularly rutin (VP) content up to 58mg/L, VA up to 81～100 international units.
4, after blueberry fresh fruit extracts free juice, leave-2～0 ℃ the interior refrigeration of cool room in, farthest kept the nutritional labeling of former fruit.
In sum: the ferment juice through " three is former " fermentation adds that the bright juice that keeps under the specific environment is through the science compatibility, accelerated the infiltration rate of nutritional labeling, improved the content of nutritional labeling, the technology that VP and VA enter the microcirculation in human body system has fast been proposed, filled up blank both domestic and external, belonged to international pioneering.
The main physical and chemical index of the blueberry oral liquid that contains vitamin A and citrin that the present invention is prepared is as follows: total acid 16-20g/L; Total reducing sugar 140-160g/L; Soluble solid 〉=15%; Volatile acid≤0.5g/L.Wine degree 0.3～0.5%Vol.
Instructions of taking and the nutritive effect of the blueberry oral liquid that contains vitamin A and citrin that the present invention is prepared: once drink 30～60ml, every day 1～2 time, can reach remove free radical, anti-oxidant, anti-inflammatory, detumescence, anti-aging, strengthen blood vessel elasticity and strengthen the health-care effect of eyesight.
The present invention is for the preparation of blueberry oral liquid, and is prepared as to contain the blueberry oral liquid of vitamin A and citrin for the nutrition and health care field.
The specific embodiment
Technical solution of the present invention is not limited to the following cited specific embodiment, also comprises any combination between each specific embodiment.
The specific embodiment one: the preparation method that present embodiment contains the blueberry oral liquid of vitamin A and citrin carries out according to the following steps:
One, the low pure ferment juice of preparation:
Get ripe blueberry fresh fruit, remove impurity, the water spray irrigation, after the blueberry fresh fruit fragmentation of cleaning, place sterile chamber, obtain blueberry juice pulp, add pectase in the blueberry juice pulp after, stir 45min with the speed of 40～47r/min after, enzymolysis 48～60h under 40～50 ℃ temperature, centrifugation, gained centrifugate are 4～4.5 to stop fermentation when spending at 16～20 ℃ temperature bottom fermentation to ethanol degree, obtain the juice that ferments, to ferment juice with 0.45 μ m filter plate coarse filtration after, with the smart filter of 0.2 μ m filter plate, obtain low pure ferment juice again, refrigerate for subsequent use;
Two, extract blueberry fresh fruit juice:
Get ripe blueberry fresh fruit, remove impurity, the water spray irrigation, after the blueberry fresh fruit fragmentation of cleaning, place sterile chamber, obtain the blueberry juice pulp mixture, in the blueberry juice pulp mixture, add pectase, speed with 47～57r/min stirs, stir every day 1～2 time, stir 30～45min at every turn, process after 7～10 days, extract blueberry gravity flow fruit juice, reclaim the seed of lower floor; Blueberry is flow automatically fruit juice with 1.0 μ m filter plate coarse filtration, use again 0.2 μ m membrane filtration, get blueberry fresh fruit juice, refrigerate for subsequent use;
Three, by volume umber takes by weighing low alcohol fermented juice, 60～75 portions of blueberry fresh fruit juice, 10 parts of pure water and 10～15 portions of white granulated sugars that step 2 obtains that 10～20 parts of step 1 obtain, be mixed to get mixed liquor, with mixed liquor with 0.2 μ m membrane filtration after, carry out ultra high temperature short time sterilization, obtain containing the blueberry oral liquid of vitamin A and citrin.
The beneficial effect of present embodiment is:
1, on technology, adopted the biological assistant without any artificial interpolation to keep " three is former " (former fruit, Normal juice, former fructose) low temperature (16～20 ℃) zymotechnique, neither add any fermentation assistant, the unartificial yeast cold fermentation of utilizing former fructose and blueberries self to adhere to, greatly keep the nutritional labeling in the fruit, and produced new nutriment after the fermentation, such as multiple nutritional components such as amino acid, polysaccharide, phenolic compound and flavor and fragrance substances.
2, adopted the compatibility of the bright juice of blueberry fermented juice and blueberry, utilize the micro ethanol of fermented juice to do the importing medium, make the high nutrition of blueberry enter fast the microcirculation in human body system, because containing little alcohol in the blueberry fermented juice, played the unique effect of quick importing microcirculation in human body system.The science compatibility of the bright juice of blueberry fermented juice and blueberry is so that the prepared blueberry oral liquid of the present invention has faster absorption of human body speed and higher active ingredient absorptivity.Particularly contain rutin (VP) composition in the blueberry oral liquid of vitamin A and citrin under the effect of fermented juice, can enter fast microcirculqtory system in the human body, reached the function of best nutrition, at home and abroad initiated to have and absorb the blueberry oral liquid that contains VP+VA fast, the high new function of nutritional labeling.
3, effective efficiency nutritive index science safety: 1. without any additive, 2. scientific allocation technology blueberry VP+VA oral liquid is because of the innovation of scientific formula, so that the effective nutrition of blueberry oral liquid more comprehensively, more outstanding, be rich in the oral liquid anthocyanidin and several amino acids, high mallow element, heteroside 11.5mg/L, particularly rutin (VP) content up to 58mg/L, VA up to 81～100 international units.
4, after blueberry fresh fruit extracts free juice, leave-2～0 ℃ the interior refrigeration of cool room in, farthest kept the nutritional labeling of former fruit.
In sum: the ferment juice through " three is former " fermentation adds that the bright juice that keeps under the specific environment is through the science compatibility, accelerated the infiltration rate of nutritional labeling, improved the content of nutritional labeling, the technology that VP and VA enter the microcirculation in human body system has fast been proposed, filled up blank both domestic and external, belonged to international pioneering.
The specific embodiment two: what present embodiment and the specific embodiment one were different is: the mass ratio of pectase and blueberry juice pulp is (1.5～2.5g): 100kg in the step 1.Other is identical with the specific embodiment one.
The specific embodiment three: what present embodiment was different from the specific embodiment one or two is: the mass ratio of pectase and blueberry juice pulp mixture is (1.5～2.5g): 100kg in the step 2.Other is identical with the specific embodiment one.
The specific embodiment four: what present embodiment was different from one of specific embodiment one to three is: the refrigerated storage temperature for subsequent use of the refrigeration described in step 1 and the step 2 is-2～0 ℃.Other is identical with one of specific embodiment one to three.
The specific embodiment five: what present embodiment was different from one of specific embodiment one to four is: ultra high temperature short time sterilization refers in temperature to be that 128～132 ℃, mixed liquor flow are to process 5～6s under the condition of 1200L/h in the step 3.Other is identical with one of specific embodiment one to four.
Adopt following examples and contrast experiment to verify beneficial effect of the present invention:
Embodiment one:
The preparation method that present embodiment contains the blueberry oral liquid of vitamin A and citrin carries out according to the following steps:
One, the low pure ferment juice of preparation:
Get ripe blueberry fresh fruit, remove impurity, the water spray irrigation, after the blueberry fresh fruit fragmentation of cleaning, place sterile chamber, obtain blueberry juice pulp, add pectase in the blueberry juice pulp after, stir 45min with the speed of 45r/min after, enzymolysis 48h under 40 ℃ temperature, centrifugation, gained centrifugate stop fermentation when 16～20 ℃ temperature bottom fermentation to ethanol degree is 4 °, obtain the juice that ferments, to ferment juice with 0.45 μ m filter plate coarse filtration after, with the smart filter of 0.2 μ m filter plate, obtain low pure ferment juice again ,-2～0 ℃ temperature under refrigeration for subsequent use;
Two, extract blueberry fresh fruit juice:
Get ripe blueberry fresh fruit, remove impurity, the water spray irrigation, after the blueberry fresh fruit fragmentation of cleaning, place sterile chamber, obtain the blueberry juice pulp mixture, in the blueberry juice pulp mixture, add pectase, speed with 50r/min stirs, stir every day 2 times, stir 30min at every turn, process after 7 days, extract blueberry gravity flow fruit juice, reclaim the seed of lower floor; Blueberry is flow automatically fruit juice with 1.0 μ m filter plate coarse filtration, use 0.2 μ m membrane filtration again, get blueberry fresh fruit juice, refrigeration is for subsequent use under-2～0 ℃ temperature;
Three, by volume umber takes by weighing low alcohol fermented juice, 75 portions of blueberry fresh fruit juice, 5 parts of pure water and 10 portions of white granulated sugars that step 2 obtains that 10 parts of step 1 obtain, be mixed to get mixed liquor, with mixed liquor with 0.2 μ m membrane filtration after, be that 130 ℃, mixed liquor flow are under the condition of 1200L/h with mixed liquor in temperature, process 6s, obtain containing the blueberry oral liquid of vitamin A and citrin.
In the step 1 during water spray irrigation blueberry fresh fruit, avoid that blueberry fresh fruit is broken, stream juice, guarantee that fruit is intact.
With stirring at low speed, be beneficial to the nutrient that is rich in stripping pericarp, the pulp in step 1 and the step 2, if mixing speed is too fast, seed is fragile, has grease and other materials are separated out, and is unfavorable for fermentation.
In the step 7, carry out ultra high temperature short time sterilization (UHT sterilization), make feed liquid be unlikely to long-time sterilization and change nutritional labeling and flavor characteristic.
Main physical and chemical index and the nutritive index of the blueberry oral liquid that contains vitamin A and citrin that present embodiment is prepared:
1, physical and chemical index:
Total acid 16～20g/L;
Total reducing sugar 140～160g/L;
Soluble solid 〉=15%;
Volatile acid≤0.5g/L;
Alcoholic strength 0.3～0.5%Vol.
2, nutritive index
1. VP:58mg/L VA:100IV (international unit)
2. vitamin total amount 800mg/L
3. micro-total amount 100mg/L
4. anthocyanidin 15mg/L
5. total phenol 800mg/L
6. chlorogenic acid 60mg/L
7. Quercetin 31mg/L
8. myricetin 13mg/L
9. heteroside 11mg/L
Instructions of taking and the nutritive effect of the blueberry oral liquid that contains vitamin A and citrin that present embodiment is prepared:
Once drink 30～60ml, every day 1～2 time, can reach remove free radical, anti-oxidant, anti-inflammatory, detumescence, anti-aging, strengthen blood vessel elasticity and strengthen the nutrition health-care functions of eyesight.

Claims (5)

1. the preparation method who contains the blueberry oral liquid of vitamin A and citrin, the preparation method who it is characterized in that containing the blueberry oral liquid of vitamin A and citrin carries out according to the following steps:
One, the low pure ferment juice of preparation:
Get ripe blueberry fresh fruit, remove impurity, the water spray irrigation, after the blueberry fresh fruit fragmentation of cleaning, place sterile chamber, obtain blueberry juice pulp, add pectase in the blueberry juice pulp after, stir 45min with the speed of 40～47r/min after, enzymolysis 48～60h under 40～50 ℃ temperature, centrifugation, gained centrifugate stop fermentation when 16～20 ℃ temperature bottom fermentation to ethanol degree is 4～4.5 °, obtain the juice that ferments, to ferment juice with 0.45 μ m filter plate coarse filtration after, with the smart filter of 0.2 μ m filter plate, obtain low alcohol fermented juice again, refrigerate for subsequent use;
Two, extract blueberry fresh fruit juice:
Get ripe blueberry fresh fruit, remove impurity, the water spray irrigation, after the blueberry fresh fruit fragmentation of cleaning, place sterile chamber, obtain the blueberry juice pulp mixture, in the blueberry juice pulp mixture, add pectase, speed with 47～57r/min stirs, stir every day 1～2 time, stir 30～45min at every turn, process after 7～10 days, extract blueberry gravity flow fruit juice, reclaim the seed of lower floor; Blueberry is flow automatically fruit juice with 1.0 μ m filter plate coarse filtration, use again 0.2 μ m membrane filtration, get blueberry fresh fruit juice, refrigerate for subsequent use;
Three, by volume umber takes by weighing low alcohol fermented juice, 60～75 portions of blueberry fresh fruit juice, 10 parts of pure water and 10～15 portions of white granulated sugars that step 2 obtains that 10～20 parts of step 1 obtain, be mixed to get mixed liquor, with mixed liquor with 0.2 μ m membrane filtration after, carry out ultra high temperature short time sterilization, obtain containing the blueberry oral liquid of vitamin A and citrin.
2. the preparation method who contains the blueberry oral liquid of vitamin A and citrin according to claim 1 is characterized in that the mass ratio of pectase and blueberry juice pulp is (1.5～2.5g): 100kg in the step 1.
3. the preparation method who contains the blueberry oral liquid of vitamin A and citrin according to claim 1 is characterized in that the mass ratio of pectase and blueberry juice pulp mixture is (1.5～2.5g): 100kg in the step 2.
4. the preparation method who contains the blueberry oral liquid of vitamin A and citrin according to claim 1 is characterized in that the refrigerated storage temperature for subsequent use of the refrigeration described in step 1 and the step 2 is-2～0 ℃.
5. the preparation method who contains the blueberry oral liquid of vitamin A and citrin according to claim 1 is characterized in that it is that 128～132 ℃, mixed liquor flow are to process 5～6s under the condition of 1200L/h that ultra high temperature short time sterilization in the step 3 refers in temperature.
CN2012102062592A 2012-06-21 2012-06-21 Preparation method of blueberry oral liquid containing vitamin A and vitamin P Pending CN102907725A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105558255A (en) * 2015-12-29 2016-05-11 陕西省植物蛋白食品工程技术研究中心有限公司 Blueberry-leaf peptide nutrient and preparation method thereof
CN108185257A (en) * 2017-12-28 2018-06-22 熙可食品(安徽)有限公司 A kind of mulberry solid beverage and preparation method thereof

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1915111A (en) * 2006-09-06 2007-02-21 大连轻工业学院 Fermented beverage of blueberries acetic acid and brewage method
CN101283824A (en) * 2008-05-21 2008-10-15 辽宁新大地食品饮料有限公司 Blueberry fruit vinegar beverage
CN101864353A (en) * 2010-06-25 2010-10-20 裴光泰 Starch liquid sugar blueberry wine and production method thereof
CN102181350A (en) * 2011-04-20 2011-09-14 白山市林源春生态科技有限公司 Method for preparing blueberry raw wine

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1915111A (en) * 2006-09-06 2007-02-21 大连轻工业学院 Fermented beverage of blueberries acetic acid and brewage method
CN101283824A (en) * 2008-05-21 2008-10-15 辽宁新大地食品饮料有限公司 Blueberry fruit vinegar beverage
CN101864353A (en) * 2010-06-25 2010-10-20 裴光泰 Starch liquid sugar blueberry wine and production method thereof
CN102181350A (en) * 2011-04-20 2011-09-14 白山市林源春生态科技有限公司 Method for preparing blueberry raw wine

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105558255A (en) * 2015-12-29 2016-05-11 陕西省植物蛋白食品工程技术研究中心有限公司 Blueberry-leaf peptide nutrient and preparation method thereof
CN105558255B (en) * 2015-12-29 2019-10-01 陕西省植物蛋白食品工程技术研究中心有限公司 Blueberry leaf peptide nutrient food and preparation method thereof
CN108185257A (en) * 2017-12-28 2018-06-22 熙可食品(安徽)有限公司 A kind of mulberry solid beverage and preparation method thereof

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Application publication date: 20130206