CN102852314A - Manufacturing method of rubber patterned coiled material floor - Google Patents
Manufacturing method of rubber patterned coiled material floor Download PDFInfo
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- CN102852314A CN102852314A CN2011101832637A CN201110183263A CN102852314A CN 102852314 A CN102852314 A CN 102852314A CN 2011101832637 A CN2011101832637 A CN 2011101832637A CN 201110183263 A CN201110183263 A CN 201110183263A CN 102852314 A CN102852314 A CN 102852314A
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Abstract
The invention relates to a manufacturing method of a rubber patterned coiled material floor. Raw materials comprise 15-25 parts of natural rubber, 75-85 parts of thiakol rubber, 35-50 parts of filling agent, 30-50 parts of rear earth; 4-6 parts of sulfur, 1-3 parts of zinc oxide, 0.5-2 parts of stearic acid, 0.3-0.8 part of accelerant, 0.6-0.9 part of anti-aging agent, 3-5 parts of antimonous oxide, 2-3 parts of phosphorus fire retardant, 1-3 parts of molybdates, and 15-30 parts of pigment. The product of the rubber patterned coiled material floor is obtained by mixing, carrying out open mixing, lacing, filtering, rolling, patterning, edging, vulcanizing, polishing and carrying out surface UV (Ultra Violet) treatment. Compared with the prior art, the manufacturing method provided by the invention organically combines a rubber rolling process with a continuous vulcanizing process, so that the manufactured product has the characteristics of stronger wearing resistance, uniform color, low smoke and toxic contents, low erosion, good anti-flaming property, high stretching intensity, anti-sliding and rebounding properties and the like, has a wider applicable range, and is environment-friendly in application.
Description
Technical field
The present invention relates to a kind of manufacture method of coiled material floor, especially relate to a kind of manufacture method of rubber scattered flower floor made of coiled material.
Background technology
Along with China's expanding economy, the improvement of people's life, communal facility constantly perfects and beautifies, and the pavement of application and airport, high ferro, subway, passenger steamer, hospital etc. public place is more and more pursued practicality, top grade.At present domestic rubber floor covering production line is also not bery ripe, and domestic rubber floor covering market is now almost captured by external floor merchant.Have Germany the Nola and (NORA), gondola Ya Digao (ARTIGO), Italian Pai Erpai (PRIALPAS).Wherein, by sales volume, the Nola is the first in the world.And the rubber floor covering product on the market mostly is block (800*800mm), and it is functional, all there is defective in various degree in usability.Being mainly manifested in mats formation seam, and aberration is serious, easy cleaning not, scent of etc.The present invention relates to an improved rubber coiled material floor, rubber rolling process, two kinds of techniques of continuous vulcanization are organically combined, this method is higher than other process products made thereby compactnesss, and abrasion resistance is stronger, and color is unified, and applicability is wider, uses more environmental protection.Be the top product of present pavement, the leftover pieces that produce and defective products be recoverable all, and the quality value of itself is not only arranged, and also has good social value.Along with the reinforcement of people's environmental consciousness, rubber floor covering itself has its irreplaceable advantage and characteristic in addition, and the rubber floor covering market prospects are good.
Summary of the invention
Purpose of the present invention be exactly provide in order to overcome the defective that above-mentioned prior art exists that a kind of abrasion resistance is stronger, color unified, the manufacture method of low cigarette, low toxicity, the low rubber scattered flower floor made of coiled material that the burn into fire resistance is good, hot strength is high.
Purpose of the present invention can be achieved through the following technical solutions:
A kind of manufacture method of rubber scattered flower floor made of coiled material is characterized in that, the method may further comprise the steps:
(1) prepare raw material according to following component and weight portion content:
Natural rubber 15～25, nitrile rubber 75～85, filler 35～50, rare earth 30～50, sulphur 4～6, zinc oxide 1～3, stearic acid 0.5～2, accelerator 0.3～0.8, age resistor 0.6～0.9, antimony oxide 3～5, phosphorus flame retardant 2～3, molybdenum compound 1～3, pigment 15～30;
(2) mixing: as by prescription material add to be mixed in the banbury, be heated to 60～70 ℃ of mixing 10～15min, obtain lump material after mixing;
(3) open refining: lump material is sent into flaking machine roll sheet, by conveyer belt sheet material is sent into again and beaten sheet in the tablet machine, cut apart the thick sheet of rubber that obtains the thick 3cm of the wide 50cm of long 100cm from tablet machine;
(4) lacing film: the thick sheet of rubber that tablet machine is partitioned into is delivered to and is carried out the nature cooling on the film hangers;
(5) filter: the thick sheet of rubber is cooled to lacing film behind the normal temperature sends into filter and filter, remove the impurity in the thick sheet of rubber;
(6) calendering: the thick sheet of the rubber after will filtering is delivered to calender, and rolling out film obtains rubber coiled material;
(7) spread flower: the rubber grain heating with pulverizing is sprinkling upon then pressing on the rubber coiled material uniformly by spreading colored machine;
(8) cutting edge: the workprint at the rubber coiled material two ends after the excision pressing cuts;
(9) sulfuration: the coiled material that step (8) is processed needs vulcanize by drum vulcanizer, and then after sending into vulcanizer top and 160 ℃ of roll shafts contact by belt, contacts cooling in the vulcanizer bottom with the roll shaft of built-in cooling water cycle water again;
(10) polishing: the rubber floor covering that carries out after the vulcanizing treatment is polished, form lines;
(11) surperficial UV processes: the rubber floor covering after polishing is coated with ties up one deck UV coating, and solidifies through ultraviolet equipment, by the thermal stress cancellation element, again cools off rolling, namely obtains rubber scattered flower floor made of coiled material.
The preferred following component of raw material described in the step (1) and weight portion content: natural rubber 20, nitrile rubber 80, filler 50, rare earth 40, sulphur 5, zinc oxide 2, stearic acid 1, accelerator 0.5, age resistor 0.7, antimony oxide 4, phosphorus flame retardant 5, molybdenum compound 2, pigment 20.
Described filler is titanium dioxide.
Described accelerator is PZ.
Described age resistor is ketoamine age resistor, secondary diarylamine age resistor or p-phenylenediamine (PPD) age resistor.
Described molybdenum compound is for being molybdenum potassium or molybdenum sodium.
Described pigment is for regulating the toner of background color, comprises that former orchid, heat-resisting purplish red, carbon black, You Ji perylene are red, permanent yellow, phthalein viridescent or phthalocyanine blue.
The nitrile rubber particle of the rubber grain of the pulverizing described in the step (7) for pulverizing.
Drum vulcanizer described in the step (9) is not except charging and discharging opening seal, and closed processing is all done at all the other positions, and the top of drum vulcanizer is provided with gas skirt.
UV coating described in the step (11) is polyurethane coating.
The shortcoming of existing product is mainly manifested in to mat formation seam, and aberration is serious, easy cleaning not, scent of etc.Compared with prior art, rubber coiled material of the present invention floor, rubber rolling process, two kinds of techniques of continuous vulcanization are organically combined, the characteristics such as unified, the low cigarette of, color stronger than other process products made thereby abrasion resistancies, low toxicity, low burn into fire resistance is good, hot strength is high, anti-skidding and rebound performance is good, applicability is wider, use more environmental protection, it is the top product of present pavement, intensity reaches the wear-resisting class requirement of European public place T level, be more suitable for hospital, the airport, subway, the public place that the visitors flowrate such as megastore are large uses.
Description of drawings
Fig. 1 is process chart of the present invention.
The specific embodiment
The present invention is described in detail below in conjunction with the drawings and specific embodiments.
Embodiment 1
A kind of manufacture method of rubber scattered flower floor made of coiled material is characterized in that, the method may further comprise the steps:
20kg natural rubber and 80kg nitrile rubber are added in the mixing banbury, be heated to 60～70 ℃, stirred 4～5 minutes, then add successively 5kg sulphur, 50kg titanium dioxide (filler increases the floor whiteness) and 40kg rare earth, 20kg toner (regulating the background color of rubber floor covering), zinc oxide 2, stearic acid 1, accelerator 0.5, age resistor 0.7, antimony oxide 4, phosphorus flame retardant 3, molybdenum potassium 2.Stirring about 60～70 ℃ about 15～17 minutes again, mixed lump material is sent into flaking machine roll sheet, by conveyer belt sheet material is sent into tablet machine again, the thick sheet of rubber about the thick 3cm of the wide 50cm of long 100cm that splits from tablet machine is delivered to and is carried out the nature cooling on the film hangers.Be cooled to lacing film behind the normal temperature and send into filter (130 ℃) and filter, mainly the contaminant filter in the thick sheet of rubber is fallen, it is rough and uneven in surface to guarantee that follow-up calendering and vulcanization process can not produce, products quality guarantee.Delivering to calender rolling out film temperature by the rubber after the filter processing is 130-135 ℃ again; Spread flower: the rubber grain heating with pulverizing, be sprinkling upon uniformly then pressing on the coiled material by spreading colored machine, then the two ends workprint is cut, workprint is delivered to mixer and is continued to feed intake.Coiled material vulcanizes by drum vulcanizer again, 165 ℃-168 ℃ of curing temperatures, the coiled material vulcanizer is not except charging and discharging opening seal, closed processing is all done at all the other positions, the vulcanizing equipment top carries gas skirt, sheet rubber behind the trimming contacts cooling in the vulcanizer bottom with the roll shaft of built-in cooling water cycle water after sending into vulcanizer top and 160 ℃ of roll shafts contact by belt again, finishes whole sulfuration, cooling procedure.Rubber floor covering after the sulfuration through polishing, forms corresponding lines again, and surperficial UV processes (be coated with and tie up one deck UV coating, and solidify through ultraviolet equipment), and the thermal stress cancellation element cools off rolling again.Packing is put in storage at last.
Embodiment 2
A kind of manufacture method of rubber scattered flower floor made of coiled material may further comprise the steps, its technique as shown in Figure 1:
(1) prepare raw material according to following component and content:
Natural rubber 15kg, nitrile rubber 75kg, filler 35kg, rare earth 30kg, sulphur 4kg, zinc oxide 1kg, stearic acid 0.5kg, accelerator 0.3kg, age resistor 0.6kg, antimony oxide 3kg, phosphorus flame retardant 2kg, molybdenum potassium 1kg, pigment 15kg, wherein, filler is titanium dioxide, accelerator is the rubber accelerator PZ, age resistor is the secondary diarylamine age resistor, pigment can adopt the Ji perylene red for regulating the toner of background color;
(2) mixing: as by prescription material add to be mixed in the banbury, be heated to 60 ℃ of mixing 15min, obtain lump material after mixing;
(3) open refining: lump material is sent into flaking machine roll sheet, by conveyer belt sheet material is sent into again and beaten sheet in the tablet machine, cut apart the thick sheet of rubber that obtains the thick 3cm of the wide 50cm of long 100cm from tablet machine;
(4) lacing film: the thick sheet of rubber that tablet machine is partitioned into is delivered to and is carried out the nature cooling on the film hangers;
(5) filter: the thick sheet of rubber is cooled to lacing film behind the normal temperature sends into filter and filter, remove the impurity in the thick sheet of rubber;
(6) calendering: the thick sheet of the rubber after will filtering is delivered to calender, and rolling out film obtains rubber coiled material;
(7) spread flower: the nitrile rubber particle heating with pulverizing is sprinkling upon then pressing on the rubber coiled material uniformly by spreading colored machine;
(8) cutting edge: the workprint at the rubber coiled material two ends after the excision pressing cuts;
(9) sulfuration: the coiled material that step (8) is processed needs to vulcanize by drum vulcanizer, drum vulcanizer is not except charging and discharging opening seal, closed processing is all done at all the other positions, the top of drum vulcanizer is provided with gas skirt, and then after sending into vulcanizer top and 160 ℃ of roll shafts contact by belt, contact cooling in the vulcanizer bottom with the roll shaft of built-in cooling water cycle water again;
(10) polishing: the rubber floor covering that carries out after the vulcanizing treatment is polished, form lines;
(11) surperficial UV processes: the rubber floor covering after polishing is coated with ties up one deck polyurethane coating as UV coating, and solidifies through ultraviolet equipment, by the thermal stress cancellation element, again cools off rolling, namely obtains rubber scattered flower floor made of coiled material.
Embodiment 3
A kind of manufacture method of rubber scattered flower floor made of coiled material is characterized in that, the method may further comprise the steps:
(1) prepare raw material according to following component and content:
Natural rubber 25kg, nitrile rubber 85kg, filler 50kg, rare earth 50kg, sulphur 6kg, zinc oxide 3kg, stearic acid 2kg, accelerator 0.8kg, age resistor 0.9kg, antimony oxide 5kg, phosphorus flame retardant 3kg, molybdenum sodium 3kg, pigment 30kg, wherein, filler is titanium dioxide, accelerator is the rubber accelerator PZ, age resistor is the secondary diarylamine age resistor, pigment can adopt phthalein dark green for regulating the toner of background color;
(2) mixing: as by prescription material add to be mixed in the banbury, be heated to 70 ℃ of mixing 10min, obtain lump material after mixing;
(3) open refining: lump material is sent into flaking machine roll sheet, by conveyer belt sheet material is sent into again and beaten sheet in the tablet machine, cut apart the thick sheet of rubber that obtains the thick 3cm of the wide 50cm of long 100cm from tablet machine;
(4) lacing film: the thick sheet of rubber that tablet machine is partitioned into is delivered to and is carried out the nature cooling on the film hangers;
(5) filter: the thick sheet of rubber is cooled to lacing film behind the normal temperature sends into filter and filter, remove the impurity in the thick sheet of rubber;
(6) calendering: the thick sheet of the rubber after will filtering is delivered to calender, and rolling out film obtains rubber coiled material;
(7) spread flower: the nitrile rubber particle heating with pulverizing is sprinkling upon then pressing on the rubber coiled material uniformly by spreading colored machine;
(8) cutting edge: the workprint at the rubber coiled material two ends after the excision pressing cuts;
(9) sulfuration: the coiled material that step (8) is processed needs vulcanize by drum vulcanizer, and then after sending into vulcanizer top and 160 ℃ of roll shafts contact by belt, contacts cooling in the vulcanizer bottom with the roll shaft of built-in cooling water cycle water again;
(10) polishing: the rubber floor covering that carries out after the vulcanizing treatment is polished, form lines;
(11) surperficial UV processes: the rubber floor covering after polishing is coated with ties up one deck polyurethane coating as UV coating, and solidifies through ultraviolet equipment, by the thermal stress cancellation element, again cools off rolling, namely obtains rubber scattered flower floor made of coiled material.
Claims (10)
1. the manufacture method of a rubber scattered flower floor made of coiled material is characterized in that, the method may further comprise the steps:
(1) prepare raw material according to following component and weight portion content:
Natural rubber 15～25, nitrile rubber 75～85, filler 35～50, rare earth 30～50, sulphur 4～6, zinc oxide 1～3, stearic acid 0.5～2, accelerator 0.3～0.8, age resistor 0.6～0.9, antimony oxide 3～5, phosphorus flame retardant 2～3, molybdenum compound 1～3, pigment 15～30;
(2) mixing: as by prescription material add to be mixed in the banbury, be heated to 60～70 ℃ of mixing 10～15min, obtain lump material after mixing;
(3) open refining: lump material is sent into flaking machine roll sheet, by conveyer belt sheet material is sent into again and beaten sheet in the tablet machine, cut apart the thick sheet of rubber that obtains the thick 3cm of the wide 50cm of long 100cm from tablet machine;
(4) lacing film: the thick sheet of rubber that tablet machine is partitioned into is delivered to and is carried out the nature cooling on the film hangers;
(5) filter: the thick sheet of rubber is cooled to lacing film behind the normal temperature sends into filter and filter, remove the impurity in the thick sheet of rubber;
(6) calendering: the thick sheet of the rubber after will filtering is delivered to calender, and rolling out film obtains rubber coiled material;
(7) spread flower: the rubber grain heating with pulverizing is sprinkling upon then pressing on the rubber coiled material uniformly by spreading colored machine;
(8) cutting edge: the workprint at the rubber coiled material two ends after the excision pressing cuts;
(9) sulfuration: the coiled material that step (8) is processed needs vulcanize by drum vulcanizer, and then after sending into vulcanizer top and 160 ℃ of roll shafts contact by belt, contacts cooling in the vulcanizer bottom with the roll shaft of built-in cooling water cycle water again;
(10) polishing: the rubber floor covering that carries out after the vulcanizing treatment is polished, form lines;
(11) surperficial UV processes: the rubber floor covering after polishing is coated with ties up one deck UV coating, and solidifies through ultraviolet equipment, by the thermal stress cancellation element, again cools off rolling, namely obtains rubber scattered flower floor made of coiled material.
2. the manufacture method of a kind of rubber scattered flower floor made of coiled material according to claim 1, it is characterized in that the preferred following component of the raw material described in the step (1) and weight portion content: natural rubber 20, nitrile rubber 80, filler 50, rare earth 40, sulphur 5, zinc oxide 2, stearic acid 1, accelerator 0.5, age resistor 0.7, antimony oxide 4, phosphorus flame retardant 5, molybdenum compound 2, pigment 20.
3. the manufacture method of a kind of rubber scattered flower floor made of coiled material according to claim 1 and 2 is characterized in that, described filler is titanium dioxide.
4. the manufacture method of a kind of rubber scattered flower floor made of coiled material according to claim 1 and 2 is characterized in that, described accelerator is PZ.
5. the manufacture method of a kind of rubber scattered flower floor made of coiled material according to claim 1 and 2 is characterized in that, described age resistor is ketoamine age resistor, secondary diarylamine age resistor or p-phenylenediamine (PPD) age resistor.
6. the manufacture method of a kind of rubber scattered flower floor made of coiled material according to claim 1 and 2 is characterized in that, described molybdenum compound is molybdenum potassium or molybdenum sodium.
7. the manufacture method of a kind of rubber scattered flower floor made of coiled material according to claim 1 and 2 is characterized in that, described pigment is for regulating the toner of background color, comprises that former orchid, heat-resisting purplish red, carbon black, You Ji perylene are red, permanent yellow, phthalein viridescent or phthalocyanine blue.
8. the manufacture method of a kind of rubber scattered flower floor made of coiled material according to claim 1 is characterized in that, the nitrile rubber particle of the rubber grain of the pulverizing described in the step (7) for pulverizing.
9. the manufacture method of a kind of rubber scattered flower floor made of coiled material according to claim 1, it is characterized in that, drum vulcanizer described in the step (9) is not except charging and discharging opening seal, and closed processing is all done at all the other positions, and the top of drum vulcanizer is provided with gas skirt.
10. the manufacture method of a kind of rubber scattered flower floor made of coiled material according to claim 1 is characterized in that, the UV coating described in the step (11) is polyurethane coating.
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| CN103982023A (en) * | 2014-05-22 | 2014-08-13 | 李萍 | Health protection music and dance room |
| CN104194096A (en) * | 2014-09-22 | 2014-12-10 | 安徽电气集团股份有限公司 | High-strength modified butadiene-acrylonitrile rubber and preparation method thereof |
| CN104403151A (en) * | 2014-12-22 | 2015-03-11 | 孙宝林 | Elastic rubber floorboard |
| CN104494032A (en) * | 2014-12-22 | 2015-04-08 | 孙宝林 | Preparation method of elastic rubber floor |
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| CN103982023A (en) * | 2014-05-22 | 2014-08-13 | 李萍 | Health protection music and dance room |
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