CN102851944A - Fire-retardant finishing method of terylene fabric - Google Patents
Fire-retardant finishing method of terylene fabric Download PDFInfo
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- CN102851944A CN102851944A CN2012103110930A CN201210311093A CN102851944A CN 102851944 A CN102851944 A CN 102851944A CN 2012103110930 A CN2012103110930 A CN 2012103110930A CN 201210311093 A CN201210311093 A CN 201210311093A CN 102851944 A CN102851944 A CN 102851944A
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- terylene fabric
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Abstract
The invention discloses a fire-retardant finishing method of a terylene fabric. The method comprises the following steps: dipping the terylene fabric in a dipping liquid containing a composite fire retardant at 80-95DEG C for 5-30min; and carrying out temperature maintenance of the terylene fabric at 115-130DEG C for 0.5-2h, wherein the composite fire retardant comprises 30-45 parts by weight of an organophosphorus compound, 50-70 parts by weight of zirconium oxide, and 2-5 parts by weight of an aluminum-zirconium coupling agent. The method has a substantial fire retardation effect to the terylene fabric, so the finished terylene fabric has a good fire retardation endurance, and the color, the appearance, the hand feel and other physical and mechanical performances of the fabric are not affected.
Description
Technical field
The present invention relates to a kind of flame-retardant finishing method of dacron.
Background technology
According to statistics, the Fire in China death toll reaches thousands of people every year, and the fire that is wherein caused by textiles accounts for half, 500,000,000 yuan of direct economic losses.Wherein bedding, furniture decoration are main causes on fire with cloth and drapery.Particularly build home fire, it is larger that textiles the shared ratio of fire spread.Textile garment directly contact with human, in case burn, gently then partial skin is burnt, and suffers misery, and is heavy then the skin large tracts of land is burnt burn, threat to life.In addition, the pernicious gas that textile combustion produces also endangers people's life, such as carbon monoxide, carbon dioxide, hydrogen cyanide, nitrogen oxide, Ammonia and gaseous aldehyde etc., all can cause suffocating or poisoning and death of people.Therefore, research weaving flame-retarded technology is developed the important topic that various flame retardant textiles have just become researcher research.
The present flame-retardant finishing method of dacron adopts brominated, antimonial as fire retardant usually, but above-mentioned fire retardant in European Union as the forbidding product.Therefore, exploitation low toxicity even nontoxic, and the lasting flame-resistant terylene fabric of flame retardant effect becomes the task of top priority.
Summary of the invention
The technical problem to be solved in the present invention provides a kind of flame-retardant finishing method of dacron, the defects that exists to overcome prior art.
For solving the problems of the technologies described above, the flame-retardant finishing method of dacron of the present invention comprises the steps: dacron was flooded 5～30 minutes in the maceration extract that is containing composite flame-retardant agent under 80～95 ℃; Then with dacron constant temperature 0.5～2 hour between 115～130 ℃.
Described composite flame-retardant agent is comprised of the component of following weight portion:
30～45 parts of organic phosphorus compounds;
50～70 parts of zirconias;
2～5 parts of Aluminum zirconium coupling agents.
Adding water after each component of composite flame-retardant agent is mixed is made into mass content and is not less than 15% maceration extract; Preferably be made into the maceration extract of mass content 35～50%.
As a kind of preferred version, described organic phosphorus compound is for being selected from tetra methylol phosphonium chloride, N-methylol-3-dimethoxyphosphoryl propionamide or cyclic phosphonate ester.
The TL series aluminum zirconium ester coupling agent product that Aluminum zirconium coupling agent can adopt Chongqing high credit Science and Technology Ltd. to produce.
The present invention adopts organic phosphorus compound, zirconia, the composite composite flame-retardant agent of Aluminum zirconium coupling agent, can with the dacron strong bonded, durability is strong, and has following beneficial effect: 1, dacron is had significant fire retardation; 2, have good durability of fire-retardant, comprise water-fastness, anti-dry-cleaning, weather fastness etc.; 3, do not affect color and luster, outward appearance, feel and other physical and mechanical propertiess of fabric.
The specific embodiment
Embodiment 1
The preparation of composite flame-retardant agent:
Cyclic phosphonate ester 35 gram, zirconia 60 grams, Aluminum zirconium coupling agent 5 grams are added to the water to be hybridly prepared into the quality solid content be 40% maceration extract.
The arrangement of flame-resistant terylene fabric:
Dacron was flooded 30 minutes in the maceration extract that is containing above-mentioned composite flame-retardant agent under 95 ℃, then with dacron 120 ℃ of lower constant temperature 1 hour.
Embodiment 2
The preparation of composite flame-retardant agent:
Tetra methylol phosphonium chloride 40 gram, zirconia 55 grams, Aluminum zirconium coupling agent 2 grams are added to the water to be hybridly prepared into the quality solid content be 20% maceration extract.
The arrangement of flame-resistant terylene fabric:
Dacron was flooded 20 minutes in the maceration extract that is containing above-mentioned composite flame-retardant agent under 80 ℃, then with dacron 115 ℃ of lower constant temperature 2 hours.
Application Example
1, durability
With containing the neutral detergent of 1 grams per liter with the ratio of 1: 50 fabric and detergent solution, washing is 30 minutes about 60 ℃ with dacron, and is dry about 60 ℃ behind the centrifuge dewatering.Wash respectively as stated above 5 times, 30 times.
2, anti-flammability
Method according to national standard GB/T 17591-2006 " flame-retardant textile " is measured fire resistance (product category is according to FURNISHING FABRIC), and the result is as follows:
Fire resistance behind the different washing times of table 1
A represents that b represents to wash 5 times without the dacron of washing in the table, and c represents to wash 30 times.
As seen, the present invention has good wash durability, through repeatedly still having good flame retardant effect after the washing.
Claims (4)
1. the flame-retardant finishing method of a dacron is characterized in that, comprises the steps: dacron was flooded 5～30 minutes in the maceration extract that is containing composite flame-retardant agent under 80～95 ℃; Then with dacron constant temperature 0.5～2 hour between 115～130 ℃;
Described composite flame-retardant agent is comprised of the component of following weight portion:
30～45 parts of organic phosphorus compounds;
50～70 parts of zirconias;
2～5 parts of Aluminum zirconium coupling agents.
2. method according to claim 1 is characterized in that, adds water after each component of composite flame-retardant agent is mixed and is made into mass content and is not less than 15% maceration extract.
3. method according to claim 1 is characterized in that, adds the maceration extract that water is made into mass content 35～50% after each component of composite flame-retardant agent is mixed.
4. method according to claim 1 is characterized in that, described organic phosphorus compound is selected from tetra methylol phosphonium chloride, N-methylol-3-dimethoxyphosphoryl propionamide or cyclic phosphonate ester.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012103110930A CN102851944A (en) | 2012-08-29 | 2012-08-29 | Fire-retardant finishing method of terylene fabric |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012103110930A CN102851944A (en) | 2012-08-29 | 2012-08-29 | Fire-retardant finishing method of terylene fabric |
Publications (1)
| Publication Number | Publication Date |
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| CN102851944A true CN102851944A (en) | 2013-01-02 |
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| CN2012103110930A Pending CN102851944A (en) | 2012-08-29 | 2012-08-29 | Fire-retardant finishing method of terylene fabric |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103284368A (en) * | 2013-05-13 | 2013-09-11 | 上海特安纶纤维有限公司 | Blended flame-retardant fabric and flame-retardant protecting clothes |
| CN103469556A (en) * | 2013-08-21 | 2013-12-25 | 昆山铁牛衬衫厂 | Ultraviolet-proof antibacterial finishing agent |
| CN103643500A (en) * | 2013-11-30 | 2014-03-19 | 江苏常朔针纺纱科技有限公司 | Finishing method of flame-retarding textile material |
| CN103789999A (en) * | 2013-11-30 | 2014-05-14 | 常熟市亚欧进出口贸易有限公司 | Flame-retardant finishing method for polyester fabric |
| CN104047091A (en) * | 2014-06-27 | 2014-09-17 | 江苏金宏针纺织有限公司 | Flame-retardant anticorrosion knitted polyester fabric |
| CN104060478A (en) * | 2014-06-27 | 2014-09-24 | 江苏金宏针纺织有限公司 | Anti-cutting corrosion-resistant fabric |
| CN105369628A (en) * | 2015-12-18 | 2016-03-02 | 江苏新凯奇纺织实业有限公司 | Finishing process of polyester fabric |
| CN105696342A (en) * | 2016-03-14 | 2016-06-22 | 湖州新创丝织品有限公司 | Polyester fabric flame-retardant finishing method |
| CN107881773A (en) * | 2017-12-05 | 2018-04-06 | 苏州兆海纺织科技有限公司 | A kind of arrangement application process of phosphor nitrogen combustion inhibitor on dacron |
| CN109293696A (en) * | 2018-11-20 | 2019-02-01 | 上海应用技术大学 | One-step synthesis method cotton N- methylol -3-(dimethoxyphosphoryl) propionamide fire retardant method |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20060218733A1 (en) * | 2003-11-08 | 2006-10-05 | Lally Thomas J | Fire-retardant, method for manufacturing fire-retardant cellulose-based |
| CN1849420A (en) * | 2003-06-27 | 2006-10-18 | 罗狄亚化学公司 | Yarns, fibres and filaments made of synthetic, flame-resistant material |
| CN101024920A (en) * | 2006-02-21 | 2007-08-29 | 罗门哈斯公司 | Treated articles and methods of making and using same |
-
2012
- 2012-08-29 CN CN2012103110930A patent/CN102851944A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1849420A (en) * | 2003-06-27 | 2006-10-18 | 罗狄亚化学公司 | Yarns, fibres and filaments made of synthetic, flame-resistant material |
| US20060218733A1 (en) * | 2003-11-08 | 2006-10-05 | Lally Thomas J | Fire-retardant, method for manufacturing fire-retardant cellulose-based |
| CN101024920A (en) * | 2006-02-21 | 2007-08-29 | 罗门哈斯公司 | Treated articles and methods of making and using same |
Non-Patent Citations (1)
| Title |
|---|
| 陆锦昌，方纫芝: "《丝绸染整手册》", 31 December 1995 * |
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103284368A (en) * | 2013-05-13 | 2013-09-11 | 上海特安纶纤维有限公司 | Blended flame-retardant fabric and flame-retardant protecting clothes |
| CN103469556A (en) * | 2013-08-21 | 2013-12-25 | 昆山铁牛衬衫厂 | Ultraviolet-proof antibacterial finishing agent |
| CN103643500A (en) * | 2013-11-30 | 2014-03-19 | 江苏常朔针纺纱科技有限公司 | Finishing method of flame-retarding textile material |
| CN103789999A (en) * | 2013-11-30 | 2014-05-14 | 常熟市亚欧进出口贸易有限公司 | Flame-retardant finishing method for polyester fabric |
| CN104047091A (en) * | 2014-06-27 | 2014-09-17 | 江苏金宏针纺织有限公司 | Flame-retardant anticorrosion knitted polyester fabric |
| CN104060478A (en) * | 2014-06-27 | 2014-09-24 | 江苏金宏针纺织有限公司 | Anti-cutting corrosion-resistant fabric |
| CN104047091B (en) * | 2014-06-27 | 2016-04-13 | 江苏金宏针纺织有限公司 | Fire retardant, anticorrosive polyester knitted fabric |
| CN105369628A (en) * | 2015-12-18 | 2016-03-02 | 江苏新凯奇纺织实业有限公司 | Finishing process of polyester fabric |
| CN105696342A (en) * | 2016-03-14 | 2016-06-22 | 湖州新创丝织品有限公司 | Polyester fabric flame-retardant finishing method |
| CN107881773A (en) * | 2017-12-05 | 2018-04-06 | 苏州兆海纺织科技有限公司 | A kind of arrangement application process of phosphor nitrogen combustion inhibitor on dacron |
| CN109293696A (en) * | 2018-11-20 | 2019-02-01 | 上海应用技术大学 | One-step synthesis method cotton N- methylol -3-(dimethoxyphosphoryl) propionamide fire retardant method |
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Application publication date: 20130102 |