CN102824889A - Phosphate solution producing reaction kettle - Google Patents
Phosphate solution producing reaction kettle Download PDFInfo
- Publication number
- CN102824889A CN102824889A CN2012103506637A CN201210350663A CN102824889A CN 102824889 A CN102824889 A CN 102824889A CN 2012103506637 A CN2012103506637 A CN 2012103506637A CN 201210350663 A CN201210350663 A CN 201210350663A CN 102824889 A CN102824889 A CN 102824889A
- Authority
- CN
- China
- Prior art keywords
- kettle
- reaction
- phosphatization liquid
- still
- agitated reactor
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000006243 chemical reaction Methods 0.000 title abstract description 17
- 229910019142 PO4 Inorganic materials 0.000 title abstract description 5
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 title abstract description 5
- 239000010452 phosphate Substances 0.000 title abstract description 5
- 239000002699 waste material Substances 0.000 claims abstract description 14
- 239000007788 liquid Substances 0.000 claims description 23
- 210000004916 vomit Anatomy 0.000 claims description 7
- 230000008673 vomiting Effects 0.000 claims description 7
- 239000000463 material Substances 0.000 claims description 6
- 239000002994 raw material Substances 0.000 abstract description 11
- 238000003756 stirring Methods 0.000 abstract description 9
- 238000004519 manufacturing process Methods 0.000 abstract description 7
- 239000002184 metal Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 2
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 2
- 239000012263 liquid product Substances 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 230000032050 esterification Effects 0.000 description 1
- 238000005886 esterification reaction Methods 0.000 description 1
- 238000006068 polycondensation reaction Methods 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000004381 surface treatment Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Images
Landscapes
- Mixers Of The Rotary Stirring Type (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The invention discloses a phosphate solution producing reaction kettle, comprising a kettle body, a kettle cover, a kettle bottom and a stirring device, wherein the kettle cover and the kettle bottom are respectively fixed at the two ends of the kettle body; the stirring device is arranged in the kettle body and is driven by a motor; the kettle cover is provided with a raw material inlet; the kettle bottom is connected with a phosphate solution discharge pipe and a waste residue emptying pipe; and the kettle bottom is flat. The reaction kettle disclosed by the invention has the advantages that the kettle bottom is flat, thus the phenomenon that unreacted raw materials and waste residue produced in a reaction process are deposited on the kettle bottom is reduced, and the effects of fully stirring and mixing can be achieved; and meanwhile, by virtue of multiple stirring paddles which are arranged on a stirring shaft, reaction raw materials can be fully mixed, and reaction is sped up. The reaction kettle disclosed by the invention is simple in structure, convenient for manufacturing and high in production efficiency.
Description
Technical field
The present invention relates to phosphatization liquid production technical field, be specifically related to a kind of phosphatization liquid and produce agitated reactor.
Background technology
It is a kind of effective ways that improve the metal etch resistant properties that phosphatization is handled.Phosphatization is that metal is put into phosphate is main solution, makes itself and solution generation chemical reaction, forms a kind of even, method of being insoluble in the phosphate coating of water on its surface.Phosphating coat combines more firm with the metal surface; Space in the phosphating coat has strengthened antioxygen G&W diffusivity; Have resistance to chemical attack, these excellent performances make phosphating coat be used for metal rust preventing in a large number and seal up for safekeeping, in the antirust many technologies such as (like steel rust preventions) of surface treatment.
In the prior art; The method that the production of phosphatization liquid is generally adopted is to obtain phosphide liquid product with stirring in the various raw material adding agitated reactors, mix, reacting, and the agitated reactor that is adopted is the popular response still, is that sphere and Polycondensation Reactor and Esterification Reactor are the concave shape at the bottom of the still; And in actual production process; The waste residue that produces in phosphatization liquid raw material and the raw material reaction process is deposited on least significant end at the bottom of the spherical still easily, causes mixing inhomogeneous, reaction not exclusively, is unfavorable for the production of phosphide liquid product.And the blade on the shaft in the common agitated reactor is two oval blades, and simple in structure, mixing intensity is too little, can't reach the well-beaten effect of material.
Summary of the invention
The technical problem that the present invention will solve provides a kind of phosphatization liquid and produces agitated reactor, produces in the agitated reactor raw material and reaction waste residue and is prone to be deposited at the bottom of the still least significant end and becomes and stir the dead angle and raw material mixes the problem uneven, that mixing intensity is not enough thereby solve in the prior art phosphatization liquid.
A kind of phosphatization liquid is produced agitated reactor; By at the bottom of kettle, the kettle cover that is separately fixed at the kettle two ends and the still and be arranged in the kettle and form by motor-driven agitating device; Described kettle cover is provided with material inlet; Being connected with phosphatization liquid discharge nozzle and waste residue vomit pipe at the bottom of the described still, is flat at the bottom of the described still.
Described agitating device comprise shaft and with vertically disposed several paddles of shaft, described paddle is provided with plate shaped blade.
Preferably, described kettle cover is provided with the outlet that links to each other with air-introduced machine.
Preferably, the junction is equipped with extension upward type discharge valve or bottom open type discharge valve at the bottom of described phosphatization liquid discharge nozzle, waste residue vomit pipe and the still, deposits in the pipeline to prevent in the course of reaction waste residue or material powder.
Be flat at the bottom of the agitated reactor still of the present invention, avoided having neither part nor lot in the existing agitated reactor phenomenon at the bottom of the waste residue that occurs in raw material and the course of reaction of reaction is deposited on still, can reach the effect of abundant stirring, mixing; Can fully mix the carrying out of accelerated reaction between reaction raw materials through being arranged on a plurality of paddles on the shaft, making; Agitated reactor of the present invention is simple in structure, easy to make, production efficiency is high.
Description of drawings
Fig. 1 is the structural representation that phosphatization liquid of the present invention is produced agitated reactor.
Fig. 2 be phosphatization liquid of the present invention produce agitated reactor A-A to view.
The specific embodiment
Following specific embodiments of the invention is done further to describe.
Like Fig. 1, shown in Figure 2; A kind of phosphatization liquid is produced agitated reactor, and by kettle 1, be separately fixed at the kettle cover 2 at kettle 1 two ends with at the bottom of the still 3 and be arranged on the agitating devices 5 that driven by motor 4 in the kettle 2 and form, kettle cover 1 is provided with material inlet 6; Kettle cover 1 links to each other with air-introduced machine 7; 3 is flat at the bottom of the still, is connected with phosphatization liquid discharge nozzle 8 and waste residue vomit pipe 9 at the bottom of the still on 3, and phosphatization liquid discharge nozzle 8, waste residue vomit pipe 9 are equipped with the bottom open type discharge valve with 3 contact positions at the bottom of the still; Agitating device 5 comprise shaft 10 and with shaft 10 vertically disposed two paddles 11, be equipped with 16 plate shaped blades 12 on each paddle 11.
During work; Each raw material is added in the agitated reactor by material inlet, use agitating device 5 to stir, mix, open air-introduced machine 7 immediately; Each stock yard fully reacts; After question response was accomplished, product phosphatization liquid was discharged, is collected by phosphatization liquid discharge nozzle 8, and the waste residue that reaction produces is discharged through waste residue vomit pipe 9.
Claims (4)
1. a phosphatization liquid is produced agitated reactor; By kettle (1), be separately fixed at kettle (1) two ends kettle cover (2) with (3) at the bottom of the still and be arranged on the agitating device (5) that drives by motor (4) in the kettle (1) and form; Described kettle cover (2) is provided with material inlet (6); (3) are connected with phosphatization liquid vomit pipe (8) and waste residue discharge nozzle (9) at the bottom of the described still, it is characterized in that, (3) are flat at the bottom of the described still.
2. phosphatization liquid as claimed in claim 1 is produced agitated reactor; It is characterized in that; Described agitating device (5) comprise shaft (10) and with vertically disposed several paddles of shaft (10) (11), described paddle (11) is provided with plate shaped blade (12).
3. phosphatization liquid as claimed in claim 1 is produced agitated reactor, it is characterized in that described kettle cover (2) is provided with the outlet that links to each other with air-introduced machine (7).
4. phosphatization liquid as claimed in claim 1 is produced agitated reactor, it is characterized in that, described phosphatization liquid vomit pipe (8), waste residue discharge nozzle (9) are equipped with extension upward type discharge valve or bottom open type discharge valve with (3) junction at the bottom of the still.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012103506637A CN102824889A (en) | 2012-09-19 | 2012-09-19 | Phosphate solution producing reaction kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012103506637A CN102824889A (en) | 2012-09-19 | 2012-09-19 | Phosphate solution producing reaction kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN102824889A true CN102824889A (en) | 2012-12-19 |
Family
ID=47328324
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2012103506637A Pending CN102824889A (en) | 2012-09-19 | 2012-09-19 | Phosphate solution producing reaction kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102824889A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103285617A (en) * | 2013-06-19 | 2013-09-11 | 宿迁科思化学有限公司 | Uniform stirrer |
| CN104941557A (en) * | 2015-06-17 | 2015-09-30 | 高金建 | Polymerization reactor |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0462875A1 (en) * | 1990-06-19 | 1991-12-27 | Société des Techniques en Milieu Ionisant (STMI) | Device for pressurising an emulsion having a solid phase, a liquid phase and a gas phase |
| CN201271577Y (en) * | 2008-07-23 | 2009-07-15 | 湖北犇星化工有限责任公司 | High-pressure reactor for methyltin chlorides |
| CN201935545U (en) * | 2010-12-31 | 2011-08-17 | 山东润科化工股份有限公司 | Rake type dryer for producing and drying fire retardant |
| CN202315892U (en) * | 2011-11-17 | 2012-07-11 | 成都诚诺新技术有限公司 | Reaction kettle with three wings for mixing |
| CN202762437U (en) * | 2012-09-19 | 2013-03-06 | 杨洋 | Linhua fluid production reaction kettle |
-
2012
- 2012-09-19 CN CN2012103506637A patent/CN102824889A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0462875A1 (en) * | 1990-06-19 | 1991-12-27 | Société des Techniques en Milieu Ionisant (STMI) | Device for pressurising an emulsion having a solid phase, a liquid phase and a gas phase |
| CN201271577Y (en) * | 2008-07-23 | 2009-07-15 | 湖北犇星化工有限责任公司 | High-pressure reactor for methyltin chlorides |
| CN201935545U (en) * | 2010-12-31 | 2011-08-17 | 山东润科化工股份有限公司 | Rake type dryer for producing and drying fire retardant |
| CN202315892U (en) * | 2011-11-17 | 2012-07-11 | 成都诚诺新技术有限公司 | Reaction kettle with three wings for mixing |
| CN202762437U (en) * | 2012-09-19 | 2013-03-06 | 杨洋 | Linhua fluid production reaction kettle |
Non-Patent Citations (1)
| Title |
|---|
| 董大勤等: "《压力容器与化工设备实用手册》", 31 March 2000, 化学工业出版社 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103285617A (en) * | 2013-06-19 | 2013-09-11 | 宿迁科思化学有限公司 | Uniform stirrer |
| CN104941557A (en) * | 2015-06-17 | 2015-09-30 | 高金建 | Polymerization reactor |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20121219 |