CN102757075A - 一种不同结构和形貌碳酸钙粉体的制备方法 - Google Patents
一种不同结构和形貌碳酸钙粉体的制备方法 Download PDFInfo
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- CN102757075A CN102757075A CN2012101613032A CN201210161303A CN102757075A CN 102757075 A CN102757075 A CN 102757075A CN 2012101613032 A CN2012101613032 A CN 2012101613032A CN 201210161303 A CN201210161303 A CN 201210161303A CN 102757075 A CN102757075 A CN 102757075A
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- calcium carbonate
- calcium
- additive
- carbonate powder
- aqueous solution
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- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 title claims abstract description 168
- 229910000019 calcium carbonate Inorganic materials 0.000 title claims abstract description 67
- 239000000843 powder Substances 0.000 title claims abstract description 46
- 238000000034 method Methods 0.000 title abstract description 32
- 239000000654 additive Substances 0.000 claims abstract description 27
- 230000000996 additive effect Effects 0.000 claims abstract description 27
- 238000006243 chemical reaction Methods 0.000 claims abstract description 25
- NKWPZUCBCARRDP-UHFFFAOYSA-L calcium bicarbonate Chemical compound [Ca+2].OC([O-])=O.OC([O-])=O NKWPZUCBCARRDP-UHFFFAOYSA-L 0.000 claims abstract description 24
- 229910000020 calcium bicarbonate Inorganic materials 0.000 claims abstract description 24
- 239000002245 particle Substances 0.000 claims abstract description 5
- 230000035484 reaction time Effects 0.000 claims abstract description 4
- 235000010216 calcium carbonate Nutrition 0.000 claims description 66
- 239000007864 aqueous solution Substances 0.000 claims description 21
- 238000002360 preparation method Methods 0.000 claims description 20
- ODINCKMPIJJUCX-UHFFFAOYSA-N Calcium oxide Chemical compound [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 claims description 18
- 239000007789 gas Substances 0.000 claims description 18
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 claims description 16
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 14
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims description 13
- 239000000920 calcium hydroxide Substances 0.000 claims description 13
- 229910001861 calcium hydroxide Inorganic materials 0.000 claims description 13
- 238000003756 stirring Methods 0.000 claims description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 10
- 239000000292 calcium oxide Substances 0.000 claims description 9
- 235000012255 calcium oxide Nutrition 0.000 claims description 9
- 239000005639 Lauric acid Substances 0.000 claims description 8
- 239000001569 carbon dioxide Substances 0.000 claims description 7
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 7
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims description 5
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 claims description 4
- 229910001424 calcium ion Inorganic materials 0.000 claims description 4
- 238000010907 mechanical stirring Methods 0.000 claims description 4
- MDSVGJAUFNXYRR-TUNPWDSISA-N (2s)-n-[(4-aminocyclohexyl)methyl]-1-[(2r)-2-(methylamino)-3-phenylpropanoyl]pyrrolidine-2-carboxamide Chemical compound C([C@@H](NC)C(=O)N1[C@@H](CCC1)C(=O)NCC1CCC(N)CC1)C1=CC=CC=C1 MDSVGJAUFNXYRR-TUNPWDSISA-N 0.000 claims description 2
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 claims description 2
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 claims description 2
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 claims description 2
- 239000005642 Oleic acid Substances 0.000 claims description 2
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 claims description 2
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 2
- 239000013256 coordination polymer Substances 0.000 claims description 2
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 claims description 2
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 2
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 claims description 2
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 claims description 2
- -1 polyoxyethylene Polymers 0.000 claims description 2
- 239000013078 crystal Substances 0.000 abstract description 40
- 238000010438 heat treatment Methods 0.000 abstract 1
- 238000005516 engineering process Methods 0.000 description 20
- 238000003763 carbonization Methods 0.000 description 19
- 229910021532 Calcite Inorganic materials 0.000 description 17
- 230000008569 process Effects 0.000 description 14
- 239000011575 calcium Substances 0.000 description 13
- 230000005587 bubbling Effects 0.000 description 12
- 238000010000 carbonizing Methods 0.000 description 12
- 235000012204 lemonade/lime carbonate Nutrition 0.000 description 11
- 235000003283 Pachira macrocarpa Nutrition 0.000 description 10
- 235000014364 Trapa natans Nutrition 0.000 description 10
- 235000009165 saligot Nutrition 0.000 description 10
- 239000000126 substance Substances 0.000 description 10
- 241001083492 Trapa Species 0.000 description 9
- 238000001914 filtration Methods 0.000 description 6
- 229960003511 macrogol Drugs 0.000 description 6
- 239000002002 slurry Substances 0.000 description 5
- 239000007921 spray Substances 0.000 description 5
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 4
- 238000002425 crystallisation Methods 0.000 description 4
- 230000008025 crystallization Effects 0.000 description 4
- 230000006872 improvement Effects 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 239000002202 Polyethylene glycol Substances 0.000 description 3
- 230000032683 aging Effects 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 3
- 238000011161 development Methods 0.000 description 3
- 230000018109 developmental process Effects 0.000 description 3
- 239000000839 emulsion Substances 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 229920001223 polyethylene glycol Polymers 0.000 description 3
- 229940093429 polyethylene glycol 6000 Drugs 0.000 description 3
- 238000001878 scanning electron micrograph Methods 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 238000012546 transfer Methods 0.000 description 3
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 2
- 241000276489 Merlangius merlangus Species 0.000 description 2
- 235000011941 Tilia x europaea Nutrition 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 229910052791 calcium Inorganic materials 0.000 description 2
- 238000000354 decomposition reaction Methods 0.000 description 2
- 238000005265 energy consumption Methods 0.000 description 2
- 239000010419 fine particle Substances 0.000 description 2
- 239000004571 lime Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000011164 primary particle Substances 0.000 description 2
- 230000004044 response Effects 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 238000001228 spectrum Methods 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 239000005997 Calcium carbide Substances 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 235000019738 Limestone Nutrition 0.000 description 1
- 240000001085 Trapa natans Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000004913 activation Effects 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000005255 carburizing Methods 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 238000001311 chemical methods and process Methods 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 238000013467 fragmentation Methods 0.000 description 1
- 238000006062 fragmentation reaction Methods 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 239000006028 limestone Substances 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 238000001465 metallisation Methods 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 238000000053 physical method Methods 0.000 description 1
- 238000004663 powder metallurgy Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 238000005057 refrigeration Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000012552 review Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 238000010008 shearing Methods 0.000 description 1
- 238000003980 solgel method Methods 0.000 description 1
- 238000003746 solid phase reaction Methods 0.000 description 1
- 238000010671 solid-state reaction Methods 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- CLZWAWBPWVRRGI-UHFFFAOYSA-N tert-butyl 2-[2-[2-[2-[bis[2-[(2-methylpropan-2-yl)oxy]-2-oxoethyl]amino]-5-bromophenoxy]ethoxy]-4-methyl-n-[2-[(2-methylpropan-2-yl)oxy]-2-oxoethyl]anilino]acetate Chemical compound CC1=CC=C(N(CC(=O)OC(C)(C)C)CC(=O)OC(C)(C)C)C(OCCOC=2C(=CC=C(Br)C=2)N(CC(=O)OC(C)(C)C)CC(=O)OC(C)(C)C)=C1 CLZWAWBPWVRRGI-UHFFFAOYSA-N 0.000 description 1
- 238000001132 ultrasonic dispersion Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Images
Landscapes
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Abstract
Description
图5 | 添加剂 | SEM图像 |
(a) | 0 | 菱方体的方解石晶体和少量的片状球霰石晶体 |
(b) | 2wt%月桂酸 | 菱方体方解石晶体、棒状文石晶体、极少量球霰石晶体 |
(c) | 4wt%月桂酸 | 菱方体的方解石晶体和球状的球霰石晶体 |
(d) | 6wt%硬脂酸 | 大量的片状球霰石晶体和少量的方解石和文石晶体 |
(e) | 2wt%聚乙二醇2000 | 纯净的方解石晶体 |
(f) | 6wt%聚乙二醇2000 | 大量的棒状文石晶体和少量的菱方体方解石 |
(g) | 2wt%聚乙二醇6000 | 大量棒状的文石晶体和少量的方解石晶体 |
(h) | 4wt%聚乙二醇6000 | 大量棒状的方解石晶体和少量的文石晶体。 |
Claims (5)
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Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103539187A (zh) * | 2013-10-22 | 2014-01-29 | 山东大学 | 一种基于介质强化制备轻质碳酸钙的间接工艺 |
CN104710378A (zh) * | 2015-03-06 | 2015-06-17 | 西安近代化学研究所 | 一种高品质单质炸药重结晶方法 |
CN106048709A (zh) * | 2016-02-16 | 2016-10-26 | 沈阳建筑大学 | 一种自石灰石中提取的碳酸钙晶须的制备方法 |
CN106365191A (zh) * | 2016-08-30 | 2017-02-01 | 宁波高智科技咨询服务有限公司 | 一种利用钟乳石制备高分散性纳米碳酸钙的方法 |
CN107986310A (zh) * | 2017-11-17 | 2018-05-04 | 宁波普莱斯帝金属制品有限公司 | 一种制备空心氧化钙粉体的方法 |
CN108163879A (zh) * | 2018-02-24 | 2018-06-15 | 陕西学前师范学院 | 一种不同形貌和物相结构的碳酸钙的制备方法 |
CN109627742A (zh) * | 2018-11-29 | 2019-04-16 | 荣德铵家新型材料(福州)有限公司 | 一种烧结烟气脱硫灰制备聚氨酯板材的方法 |
CN113264597A (zh) * | 2021-04-22 | 2021-08-17 | 四川绵阳岷山实业集团有限公司 | 一种利用碳酸钙文石晶种阻垢的方法 |
CN115072757A (zh) * | 2022-06-27 | 2022-09-20 | 山西石器时代新材料科技有限公司 | 一种微细棒状文石型碳酸钙及其制备方法 |
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KR20100103231A (ko) * | 2009-03-13 | 2010-09-27 | 한국과학기술원 | 미세구조의 패턴이 표면에 형성된 탄산칼슘 박막, 이의 제조방법 및 상기 미세구조의 패턴이 표면에 형성된 탄산칼슘 박막의 용도 |
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Cited By (13)
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CN103539187B (zh) * | 2013-10-22 | 2015-07-08 | 山东大学 | 一种基于介质强化制备轻质碳酸钙的间接工艺 |
CN103539187A (zh) * | 2013-10-22 | 2014-01-29 | 山东大学 | 一种基于介质强化制备轻质碳酸钙的间接工艺 |
CN104710378A (zh) * | 2015-03-06 | 2015-06-17 | 西安近代化学研究所 | 一种高品质单质炸药重结晶方法 |
CN106048709B (zh) * | 2016-02-16 | 2018-11-13 | 沈阳建筑大学 | 一种自石灰石中提取的碳酸钙晶须的制备方法 |
CN106048709A (zh) * | 2016-02-16 | 2016-10-26 | 沈阳建筑大学 | 一种自石灰石中提取的碳酸钙晶须的制备方法 |
CN106365191A (zh) * | 2016-08-30 | 2017-02-01 | 宁波高智科技咨询服务有限公司 | 一种利用钟乳石制备高分散性纳米碳酸钙的方法 |
CN107986310A (zh) * | 2017-11-17 | 2018-05-04 | 宁波普莱斯帝金属制品有限公司 | 一种制备空心氧化钙粉体的方法 |
CN108163879A (zh) * | 2018-02-24 | 2018-06-15 | 陕西学前师范学院 | 一种不同形貌和物相结构的碳酸钙的制备方法 |
CN109627742A (zh) * | 2018-11-29 | 2019-04-16 | 荣德铵家新型材料(福州)有限公司 | 一种烧结烟气脱硫灰制备聚氨酯板材的方法 |
CN109627742B (zh) * | 2018-11-29 | 2021-01-29 | 荣德铵家新型材料(福州)有限公司 | 一种烧结烟气脱硫灰制备聚氨酯板材的方法 |
CN113264597A (zh) * | 2021-04-22 | 2021-08-17 | 四川绵阳岷山实业集团有限公司 | 一种利用碳酸钙文石晶种阻垢的方法 |
CN115072757A (zh) * | 2022-06-27 | 2022-09-20 | 山西石器时代新材料科技有限公司 | 一种微细棒状文石型碳酸钙及其制备方法 |
CN115072757B (zh) * | 2022-06-27 | 2024-03-15 | 山西石器时代新材料科技有限公司 | 一种微细棒状文石型碳酸钙及其制备方法 |
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