CN102747278A - Manufacturing method of steel plate for pressure vessel - Google Patents
Manufacturing method of steel plate for pressure vessel Download PDFInfo
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- CN102747278A CN102747278A CN2012102236522A CN201210223652A CN102747278A CN 102747278 A CN102747278 A CN 102747278A CN 2012102236522 A CN2012102236522 A CN 2012102236522A CN 201210223652 A CN201210223652 A CN 201210223652A CN 102747278 A CN102747278 A CN 102747278A
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Abstract
The present invention relates to a manufacturing method of a steel plate for a pressure vessel. The method comprises the following successive steps: I. smelting molten iron, and conducting continuous casting to obtain a continuous casting billet with thickness of 200-220mm; II. billet heating: heating the billet to 1200-1250 DEG C in a heating furnace, and insulating for 3-4 hours;III. rolling: descaling the billet with high pressure water, rolling the billet on a 3000 mm roughing mill, and rolling the billet on a 3300 finishing mill, with a final rolling temperature controlled at 800-850 DEG C; IV. cooling: carrying out air cooling on the steel plate to 700-750 DEG C, starting water cooling and controlling a self-tempering temperature of the plate at 320-580 DEG C; V. straightening: carrying out hot straightening on the steel plate to realize no more than 6mm / 1000mm; VI. off-line tempering: heating the steel plate to 615-655 DEG C, insulating for 40-50 minutes, and taking out the steel plate for natural cooling; and VII. tensile test: conducting tensile test on the steel plate after tempering. The manufacturing method of the steel plate for pressure vessel has short production process and low cost.
Description
Technical field
The present invention relates to a kind of method of manufacture of steel heavy plate for pressure vessels.
Background technology
The applicant uses the quenching and tempering, high plate in order to develop a kind of pressurized vessel, and this steel plate is mainly used in the crucial metallic substance of Large Oil Tank.This steel plate tensile strength Rm behind off-line quenching+high tempering reaches 610~730Mpa, unit elongation A >=17% ,-20 ℃ of ballistic work AKv >=100J.In actual trial-manufacturing process, owing to behind the steel plate rolling, need off-line heating, quenching, tempering, the technological process of production is long, and cost is high.
Summary of the invention
In order to overcome the high above-mentioned deficiency of off-line quenching+tempering process long flow path, cost of the method for manufacture that has steels for pressure vessel use now, the present invention provides the method for manufacture of the steel heavy plate for pressure vessels that a kind of Production Flow Chart is short, cost is low, quality is high.
Design of the present invention is that steel heavy plate for pressure vessels is adopted controlled rolling+controlled chilling+off-line tempering process, obtains good comprehensive mechanical properties, good plate shape, reduces manufacturing cost simultaneously.
The method of manufacture of this steel heavy plate for pressure vessels comprises following sequential steps:
ISmelt
After hot metal pretreatment, 180 tons of converter top and bottom complex blowings, LF refining and RH outgased, continuous casting became the thick continuously cast bloom of 200~220mm;
IIThe steel billet heating
The steel billet that 200~220mm is thick is incubated 3~4 hours process furnace internal heating to 1200 ℃~1250 ℃.
IIIRolling
Through high-pressure water descaling, the steel billet behind the high-pressure water descaling is rolling on the 3000mm roughing mill, 1050-1080 ℃ of start rolling temperatures, the intermediate blank gauge control is at 45~65mm, and is rolling on 3300 finishing mills afterwards, and finishing temperature is controlled at 800~850 ℃.
IVCooling
Steel plate air cooling to 700~750 ℃, the beginning water-cooled, the water yield is 120~200m
3/ h, the water yield is than 2.0~2.5, roller speed 0.85~0.95m/s, steel plate returns red temperature and is controlled at 320~580 ℃.
VAligning
Steel plate is carried out hot straightening, reach≤6mm/1000mm.
VIThe off-line tempering
Steel plate after the side cut takes out steel billet and in air, naturally cools to room temperature normalizing furnace internal heating to 615 ℃~655 ℃ insulation 40~50 minutes.
VIITensile testing
Steel plate after the tempering carries out tensile testing.Ys Rel is 515~575MPa, and tensile strength is Rm 630~690MPa MPa, and unit elongation A is that 21~25% ,-20 ℃ of ballistic work KV2 are 190~250J, and steel plate width direction roughness is 5mm ± 1/1000mm.
Excellent its of the method for manufacture of this steel heavy plate for pressure vessels is applicable to following two steel grades:
The quality per distribution ratio of the composition of steel grade one is (%):
C:0.08~0.12,?Si:0.25~0.40, Mn:1.20~1.60, ?P:≤0.010,
S:≤0.005, Ni:0.15~0.40, V:0.02~0.06, Nb:0.02~0.04,
Ti:0.01~0.03, Al:0.01~0.03, O :≤20PPm, N:25~50PPm, all the other are Fe and unavoidable impurities.
The quality per distribution ratio of the composition of steel grade two is (%):
C:0.08~0.12,?Si:0.25~0.40, Mn:1.20~1.60, P:≤0.010,
S:≤0.005, Ni:0.15~0.40,?V:0.02~0.06, Ti:0.01~0.03,
Al:0.01~0.03,O:≤20PPm,N:25~50PPm,
All the other are Fe and unavoidable impurities.
This steels for pressure vessel use adopts controlled rolling and controlled cooling+off-line tempering method, and rolling intact back direct water-cooling has been cancelled reheat, two operations of quenching, and production cost reduces by 300~500 yuan/ton.After the steel billet heating; Adopt non-recrystallize controlled rolling, control lower finishing temperature, get into laminar flow cooling carrying out controlled rolling and controlled cooling fast; Control is the suitable water yield evenly; Steel plate returns 300~600 ℃ of red temperature, and off-line carries out 620~650 ℃ tempering, and the mechanical property of steel plate, plate shape are satisfied standard-required.
Embodiment
Specify embodiment of the present invention below in conjunction with embodiment, but embodiment of the present invention is not limited to following embodiment.
Embodiment 1
Steel heavy plate for pressure vessels is thick to be 32mm.The quality per distribution ratio of its chemical ingredients is (%):
C:0.08~0.12,?Si:0.25~0.40, Mn:1.20~1.60, ?P:≤0.010,
S:≤0.005, Ni:0.15~0.40, V:0.02~0.06, Nb:0.02~0.04,
Ti:0.01~0.03, Al:0.01~0.03, O :≤20PPm, N:25~50PPm, all the other are Fe and unavoidable impurities.
The embodiment one of this steels for pressure vessel use method of manufacture is a following sequential steps:
ISmelt
Adopt hot metal pretreatment, 180 tons of converter top and bottom complex blowings, 180 tons of LF refinings, 180 tons of RH to outgas, be cast into the thick continuously cast bloom of 220mm.The mass percent of the composition of continuously cast bloom is:
C:0.08, Si:0.25, Mn:1.25,?P:0.005, S:0.0020,
Ni:0.25, V:0.04, Nb:0.02, Ti:0.02, Al:0.02,
O:15PPm, N:30PPm, all the other are Fe and unavoidable impurities.
IIThe steel billet heating
The steel billet that 220mm is thick is incubated 4 hours at process furnace internal heating to 1220 ℃.
IIIRolling
Through high-pressure water descaling, the steel billet behind the high-pressure water descaling is rolling on the 3000mm roughing mill, 1060 ℃ of start rolling temperatures, the intermediate blank gauge control is at 65mm, and is rolling on 3300 finishing mills afterwards, and finishing temperature is controlled at 805 ℃.
IVCooling
Steel plate air cooling to 728 ℃, the beginning water-cooled, the water yield is 180 m
3/ h, the water yield is than 2.3, roller speed 0.85m/s, steel plate returns red temperature and is controlled at 550 ℃.
VAligning
With the steel plate hot straightening, aligning back 4mm/1000mm.
VIThe off-line tempering
Steel plate after the side cut takes out steel billet and in air, naturally cools to room temperature normalizing furnace internal heating to 625 ℃ insulation 45 minutes.
VIITensile testing
Steel plate after the tempering carries out tensile testing.Ys Rel is 525MPa, and tensile strength is Rm 640 MPa, and unit elongation A is that 23% ,-20 ℃ of ballistic work KV2 are 225J, and steel plate width direction roughness is 5mm/1000mm.Plate quality satisfies request for utilization.
Embodiment 2
Steel heavy plate for pressure vessels is thick to be 12mm.The quality per distribution ratio of its chemical ingredients is following:
C:0.08~0.12,?Si:0.25~0.40,?Mn:1.20~1.60, P:≤0.010,
S:≤0.005, Ni:0.15~0.40,V:0.02~0.06,Ti:0.01~0.03,
Al:0.01~0.03, O :≤20PPm, N:25~50PPm, all the other are Fe and unavoidable impurities.
The embodiment of this steels for pressure vessel use sends out two and is following sequential steps:
ISmelt
Adopt hot metal pretreatment, 180 tons of converter top and bottom complex blowings, 180 tons of LF refinings, 180 tons of RH to outgas, be cast into the thick continuously cast bloom of 220mm.
The mass percent of the composition of continuously cast bloom is:
C:0.10, Si:0.32, Mn:1.40,?P:0.008, S:0.0025,
Ni:0.27, V:0.04, Ti:0.02, Al:0.02, O:18 PPm, N:32 PPm, all the other are Fe and unavoidable impurities
IIThe steel billet heating
The steel billet that 220mm is thick is incubated 4 hours at process furnace internal heating to 1220 ℃.
IIIRolling
Steel billet behind the high-pressure water descaling is rolling on the 3000mm roughing mill, 1070 ℃ of start rolling temperatures, the intermediate blank gauge control is at 45mm, and is rolling on the 3300mm finishing mill afterwards, and finishing temperature is controlled at 815 ℃.
IVCooling
Steel plate air cooling to 729 ℃, the beginning water-cooled, the water yield is 160 m
3/ h, water be than 2.2, roller speed 0.95 m/s, and steel plate returns red temperature and is controlled at 350 ℃.
VAligning
With the steel plate aligning, aligning back steel plate roughness is 3mm/1000mm.
VIThe off-line tempering
Steel plate after the side cut takes out steel billet and in air, naturally cools to room temperature normalizing furnace internal heating to 635 ℃ insulation 45 minutes.
VIITensile testing
Steel plate after the tempering carries out tensile testing, and ys Rel is 545MPa, and tensile strength Rm is 655MPa, and unit elongation A is that 22% ,-20 ℃ of ballistic work KV2 are 200J, and steel plate width direction roughness is 5mm/1000mm.Plate property satisfies standard-required.
Claims (3)
1. the method for manufacture of a steel heavy plate for pressure vessels, it comprises following sequential steps:
ISmelt
After hot metal pretreatment, 180 tons of converter top and bottom complex blowings, LF refining and RH outgased, continuous casting became the thick continuously cast bloom of 200~220mm;
IIThe steel billet heating
The steel billet that 200~220mm is thick is incubated 3~4 hours process furnace internal heating to 1200 ℃~1250 ℃;
IIIRolling
Through high-pressure water descaling, the steel billet behind the high-pressure water descaling is rolling on the 3000mm roughing mill, 1050-1080 ℃ of start rolling temperatures, the intermediate blank gauge control is at 45~65mm, and is rolling on 3300 finishing mills afterwards, and finishing temperature is controlled at 800~850 ℃;
IVCooling
Steel plate air cooling to 700~750 ℃, the beginning water-cooled, the water yield is 120~200m
3/ h, the water yield is than 2.0~2.5, roller speed 0.85~0.95m/s, steel plate returns red temperature and is controlled at 320~580 ℃;
VAligning
Steel plate is carried out hot straightening, reach≤6mm/1000mm;
VIThe off-line tempering
Steel plate after the side cut takes out steel billet and in air, naturally cools to room temperature normalizing furnace internal heating to 615 ℃~655 ℃ insulation 40~50 minutes;
VIITensile testing
Steel plate after the tempering carries out tensile testing, and ys Rel is 515~575MPa, and tensile strength is Rm 630~690MPa MPa, and unit elongation A is that 21~25% ,-20 ℃ of ballistic work KV2 are 190~250J, and steel plate width direction roughness is 5mm ± 1/1000mm.
2. the method for manufacture of steel heavy plate for pressure vessels according to claim 1, it is characterized in that: the quality per distribution ratio of the composition of described steel plate is:
C:0.08~0.12,?Si:0.25~0.40, Mn:1.20~1.60, ?P:≤0.010,
S:≤0.005, Ni:0.15~0.40, V:0.02~0.06, Nb:0.02~0.04,
Ti:0.01~0.03, Al:0.01~0.03, O :≤20PPm, N:25~50PPm, all the other are Fe and unavoidable impurities.
3. the method for manufacture of steel heavy plate for pressure vessels according to claim 1, it is characterized in that: the quality per distribution ratio of the composition of described steel plate is:
C:0.08~0.12,?Si:0.25~0.40, Mn:1.20~1.60, P:≤0.010,
S:≤0.005, Ni:0.15~0.40,?V:0.02~0.06, Ti:0.01~0.03,
Al:0.01~0.03,O:≤20PPm,N:25~50PPm,
All the other are Fe and unavoidable impurities.
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Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103014282A (en) * | 2012-12-21 | 2013-04-03 | 首钢总公司 | Production method of high-strength and good-low-temperature-toughness wind power steel plate |
CN103343298A (en) * | 2013-07-12 | 2013-10-09 | 鞍钢股份有限公司 | Production method of 07MnNiMoDR steel for low-temperature container |
CN103468903A (en) * | 2013-08-23 | 2013-12-25 | 内蒙古包钢钢联股份有限公司 | Method for improving low-temperature impact toughness of high-strength steel |
CN103468902A (en) * | 2013-08-23 | 2013-12-25 | 内蒙古包钢钢联股份有限公司 | Method for improving through-thickness characteristics of thickness-specification high-strength steel |
CN105861924A (en) * | 2016-05-31 | 2016-08-17 | 舞阳钢铁有限责任公司 | Low-alloy 15CrMo steel plate and production method thereof |
CN106319372A (en) * | 2015-06-29 | 2017-01-11 | 鞍钢股份有限公司 | 345 MPa-grade welded bottle steel and manufacturing method thereof |
CN108655184A (en) * | 2018-05-11 | 2018-10-16 | 鞍钢股份有限公司 | Control method for shape of steel plate with width of 3500mm or more |
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CN102011047A (en) * | 2010-12-13 | 2011-04-13 | 首钢总公司 | Production method of steel plate for pressure vessel with low cost and high performance |
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Cited By (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103014282A (en) * | 2012-12-21 | 2013-04-03 | 首钢总公司 | Production method of high-strength and good-low-temperature-toughness wind power steel plate |
CN103014282B (en) * | 2012-12-21 | 2014-09-17 | 首钢总公司 | Production method of high-strength and good-low-temperature-toughness wind power steel plate |
CN103343298A (en) * | 2013-07-12 | 2013-10-09 | 鞍钢股份有限公司 | Production method of 07MnNiMoDR steel for low-temperature container |
CN103468903A (en) * | 2013-08-23 | 2013-12-25 | 内蒙古包钢钢联股份有限公司 | Method for improving low-temperature impact toughness of high-strength steel |
CN103468902A (en) * | 2013-08-23 | 2013-12-25 | 内蒙古包钢钢联股份有限公司 | Method for improving through-thickness characteristics of thickness-specification high-strength steel |
CN103468902B (en) * | 2013-08-23 | 2015-04-22 | 内蒙古包钢钢联股份有限公司 | Method for improving through-thickness characteristics of thickness-specification high-strength steel |
CN103468903B (en) * | 2013-08-23 | 2015-06-03 | 内蒙古包钢钢联股份有限公司 | Method for improving low-temperature impact toughness of high-strength steel |
CN106319372A (en) * | 2015-06-29 | 2017-01-11 | 鞍钢股份有限公司 | 345 MPa-grade welded bottle steel and manufacturing method thereof |
CN106319372B (en) * | 2015-06-29 | 2018-12-04 | 鞍钢股份有限公司 | 345 MPa-grade welded bottle steel and manufacturing method thereof |
CN105861924A (en) * | 2016-05-31 | 2016-08-17 | 舞阳钢铁有限责任公司 | Low-alloy 15CrMo steel plate and production method thereof |
CN108655184A (en) * | 2018-05-11 | 2018-10-16 | 鞍钢股份有限公司 | Control method for shape of steel plate with width of 3500mm or more |
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Application publication date: 20121024 |