CN102718471B - Green body of red soil ceramic and formula of transmutation glaze of red soil ceramic - Google Patents
Green body of red soil ceramic and formula of transmutation glaze of red soil ceramic Download PDFInfo
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- CN102718471B CN102718471B CN 201210174415 CN201210174415A CN102718471B CN 102718471 B CN102718471 B CN 102718471B CN 201210174415 CN201210174415 CN 201210174415 CN 201210174415 A CN201210174415 A CN 201210174415A CN 102718471 B CN102718471 B CN 102718471B
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- 239000002689 soil Substances 0.000 title claims abstract description 33
- 238000009377 nuclear transmutation Methods 0.000 title claims abstract description 18
- 239000000919 ceramic Substances 0.000 title abstract description 11
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium monoxide Chemical compound [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 claims abstract description 30
- 239000002994 raw material Substances 0.000 claims abstract description 30
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 25
- 238000010304 firing Methods 0.000 claims abstract description 17
- QVQLCTNNEUAWMS-UHFFFAOYSA-N Barium oxide Chemical compound [Ba]=O QVQLCTNNEUAWMS-UHFFFAOYSA-N 0.000 claims abstract description 16
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 16
- XLOMVQKBTHCTTD-UHFFFAOYSA-N zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000000292 calcium oxide Substances 0.000 claims abstract description 15
- 235000019832 sodium triphosphate Nutrition 0.000 claims abstract description 15
- 239000010453 quartz Substances 0.000 claims abstract description 10
- 229910052904 quartz Inorganic materials 0.000 claims abstract description 10
- 239000005995 Aluminium silicate Substances 0.000 claims abstract description 8
- PZZYQPZGQPZBDN-UHFFFAOYSA-N Aluminium silicate Chemical compound O=[Al]O[Si](=O)O[Al]=O PZZYQPZGQPZBDN-UHFFFAOYSA-N 0.000 claims abstract description 8
- OGIDPMRJRNCKJF-UHFFFAOYSA-N TiO Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims abstract description 8
- 235000012211 aluminium silicate Nutrition 0.000 claims abstract description 8
- HWGNBUXHKFFFIH-UHFFFAOYSA-I pentasodium;[oxido(phosphonatooxy)phosphoryl] phosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O HWGNBUXHKFFFIH-UHFFFAOYSA-I 0.000 claims abstract description 8
- 239000000843 powder Substances 0.000 claims abstract description 8
- 239000000454 talc Substances 0.000 claims abstract description 8
- 229910052623 talc Inorganic materials 0.000 claims abstract description 8
- 229910001929 titanium oxide Inorganic materials 0.000 claims abstract description 8
- 239000011787 zinc oxide Substances 0.000 claims abstract description 8
- 229910052656 albite Inorganic materials 0.000 claims abstract description 3
- 239000000758 substrate Substances 0.000 claims description 27
- 229910052700 potassium Inorganic materials 0.000 claims description 16
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims description 14
- 229910001710 laterite Inorganic materials 0.000 claims description 12
- 239000011504 laterite Substances 0.000 claims description 12
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 9
- 229910001845 yogo sapphire Inorganic materials 0.000 claims description 9
- 239000000463 material Substances 0.000 claims description 8
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 8
- 239000011591 potassium Substances 0.000 claims description 8
- 101700015827 FYPP3 Proteins 0.000 claims description 7
- 101700004450 phpP Proteins 0.000 claims description 7
- 239000000377 silicon dioxide Substances 0.000 claims description 7
- 235000012222 talc Nutrition 0.000 claims description 7
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 claims description 7
- 239000004576 sand Substances 0.000 claims description 3
- 239000000126 substance Substances 0.000 abstract description 5
- 229910052500 inorganic mineral Inorganic materials 0.000 abstract description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 239000011707 mineral Substances 0.000 abstract description 3
- 235000019738 Limestone Nutrition 0.000 abstract 1
- DLHONNLASJQAHX-UHFFFAOYSA-N aluminum;potassium;oxygen(2-);silicon(4+) Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[Al+3].[Si+4].[Si+4].[Si+4].[K+] DLHONNLASJQAHX-UHFFFAOYSA-N 0.000 abstract 1
- 239000003086 colorant Substances 0.000 abstract 1
- 239000010459 dolomite Substances 0.000 abstract 1
- 229910000514 dolomite Inorganic materials 0.000 abstract 1
- 239000000446 fuel Substances 0.000 abstract 1
- 239000006028 limestone Substances 0.000 abstract 1
- 230000036314 physical performance Effects 0.000 abstract 1
- -1 silicate compound Chemical class 0.000 description 11
- 238000005755 formation reaction Methods 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- YEXPOXQUZXUXJW-UHFFFAOYSA-N oxolead Chemical compound [Pb]=O YEXPOXQUZXUXJW-UHFFFAOYSA-N 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 210000003298 Dental Enamel Anatomy 0.000 description 1
- 235000008331 Pinus X rigitaeda Nutrition 0.000 description 1
- 235000011613 Pinus brutia Nutrition 0.000 description 1
- 241000018646 Pinus brutia Species 0.000 description 1
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 1
- 229910052796 boron Inorganic materials 0.000 description 1
- 229910052906 cristobalite Inorganic materials 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 230000036748 firing rate Effects 0.000 description 1
- 239000003317 industrial substance Substances 0.000 description 1
- 229910052863 mullite Inorganic materials 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000002915 spent fuel radioactive waste Substances 0.000 description 1
Abstract
The invention relates to a green body of red soil ceramic. The green body of the red soil ceramic is prepared from the following raw materials: red soil, quartz, talc, limestone and dolomite; the transmutation glaze of the red soil ceramic is prepared from the following raw materials: potassium feldspar, albite, calcium oxide, barium oxide, kaolin, quartz powder, sodium tripolyphosphate, titanium oxide, rutile, zinc oxide and a coloring agent. By addition of other mineral raw materials, chemical raw materials and the like, the physical performance and the chemical performance of the green body are changed and the technical problems that the green body glaze of the red soil product is difficult to combine and the product is loose and fragile are solved; the firing temperature of the glaze is reduced from 1,310 DEG C to 1,230 DEG C, so thatthe firing temperature is reduced by 80 DEG C, the using amount of the fuel and the discharge quantity of harmful gas are reduced, environmental protection is contributed and production cost is greatly saved; and by development of the lead-free transmutation glaze, the lead-free transmutation glaze is suitable for being combined with the green body of the red soil ceramic, so that the problem of pollution to the ceramic decorative environment is solved fundamentally.
Description
Technical field
The present invention relates to the formula of a kind of ceramic body and cover-coat enamel thereof, refer to especially a kind of base substrate of red soil pottery and the formula of furnace transmutation glaze thereof.
Background technology
The main raw material Red Earth Resource of laterite base substrate is abundant, the good and easy-formation of plasticity, and firing range is wide, can be from 1000 ℃ to 1250 ℃, but most of laterite is because of the directly glazing of reason of its coefficient of expansion, and the Chemical Composition of laterite is mainly 52.78% SiO
2, 33.57% Al
2O
3, 10.43% Fe
20
3, 3.16% K
2O, 0.06% Na
2O。Only take the raw material of laterite as the preparation base substrate, its SiO
2Content is on the low side, Al
2O
3, Fe
2O
3Content is higher, is unfavorable for the formation of silicate compound; K
2O, Na
2The biscuiting temperature of O content major effect base substrate, too high levels, the base substrate firing temperature is reduced and be unfavorable for the formation of cristobalite, can reduce the base substrate coefficient of expansion, affect the base glaze in conjunction with and produce glaze and split defective, quartz, potassium felspar sand, mullite are arranged, glassy phase and pore etc. in the mineral composition because of base substrate, wherein glassy phase is few, therefore the base substrate porous.
In addition, because the chemical constitution difference of the glaze of existing red soil pottery is larger, the coefficient of expansion of glaze is higher, and the firing temperature of glaze also reaches the height of 1310 ℃, very easily produces early stage glaze and splits, and spent fuel is also larger, and production cost is higher; For this reason, glaze is usually to contain lead solution as solvent, and apply the larger lead of elasticity one boron glaze on red soil greenwave body, this can offset the harmful effect that the thermal expansion of base glaze causes within the specific limits, but this also makes product have the excessive shortcoming of lead release, causes product not use on domestic ceramics.
Summary of the invention
The invention provides a kind of base substrate of red soil pottery and the formula of furnace transmutation glaze thereof, be not easy glazing, easily produce that glaze splits, the base substrate porous with what the base substrate that overcomes existing red soil pottery existed, and the firing temperature that red soil bristol glaze material exists is high, the problems such as early stage glaze splits, the product lead release large, can not use on domestic ceramics very easily occur.
The present invention adopts following technical scheme:
Red soil greenwave body, the preparation of this base substrate comprises following raw material: laterite, quartz, talcum, Wingdale, rhombspar; More specifically, the raw materials of this base substrate comprises following component: 49.3% SiO
2, 26.3% Al
2O
3, 2.1% Fe
20
3, 1.6% K
2O, 1.9% MgO, 18.8% CaO.
Red soil pottery furnace transmutation glaze, the preparation of this glaze comprises following raw material: potassium felspar sand 35-40 part, albite 22-25 part, calcium oxide 8-15 part, barium oxide 15-20 part, Longyan kaolin 8-15 part, silica powder 6-12 part, tripoly phosphate sodium STPP 0.2-0.4 part, titanium oxide 10-20 part, rutile 2-10 part, zinc oxide 3-10 part; The raw materials of this glaze also comprises the tinting material of 3-25 part.
The firing temperature of this glaze is 1210 ℃～1250 ℃; More specifically, the firing temperature of this glaze is 1230 ℃.
By the above-mentioned description of this invention as can be known, compared to the prior art, the present invention has following advantage: by adding other mineral raw material and industrial chemicals etc., changed the physical and chemical performance of base substrate, solved laterite product base glaze in conjunction with being difficult to and the frangible technical barrier of the uncommon pine of product quality; The firing temperature of glaze is down to 1230 ℃ by 1310 ℃, and firing temperature has reduced by 80 ℃, has reduced and has burnt till energy consumption, reduced the quantity discharged of firing rate and harmful body, both be conducive to environment protection, also saved a large amount of production costs, also improved class and the share of market of product; To traditional low temperature frit glaze formula reform, introduce novel material, replace plumbous oxide, develop unleaded furnace transmutation glaze, make it to be suitable for red soil greenwave body, fundamentally solve the ceramic decoration problem of environmental pollution.
Embodiment
Embodiment one
Present embodiment is preferred implementation.
Red soil greenwave body, the preparation of this base substrate comprises following raw material: laterite, quartz, talcum, Wingdale, rhombspar; More specifically, the raw materials of this base substrate comprises following component: 49.3% SiO
2, 26.3% Al
2O
3, 2.1% Fe
20
3, 1.6% K
2O, 1.9% MgO, 18.8% CaO.
Red soil pottery furnace transmutation glaze, the preparation of this glaze comprises following raw material: 37 parts of potassium felspar sands, 23 parts of albites, 12 parts, calcium oxide, 18 parts, barium oxide, 12 parts of Longyan kaolin, 9 parts of silica powders, 0.3 part of tripoly phosphate sodium STPP, 15 parts of titanium oxide, 6 parts of rutile, 8 parts, zinc oxide, 14 parts of tinting materials; The firing temperature of this glaze is 1230 ℃.
Embodiment two
Red soil greenwave body, the preparation of this base substrate comprises following raw material: laterite, quartz, talcum, Wingdale, rhombspar; More specifically, the raw materials of this base substrate comprises following component: 49.3% SiO
2, 26.3% Al
2O
3, 2.1% Fe
20
3, 1.6% K
2O, 1.9% MgO, 18.8% CaO.
Red soil pottery furnace transmutation glaze, the preparation of this glaze comprises following raw material: 35 parts of potassium felspar sands, 25 parts of albites, 8 parts, calcium oxide, 15 parts, barium oxide, 15 parts of Longyan kaolin, 6 parts of silica powders, 0.4 part of tripoly phosphate sodium STPP, 20 parts of titanium oxide, 2 parts of rutile, 10 parts, zinc oxide; The firing temperature of this glaze is 1210 ℃.
Embodiment three
Red soil greenwave body, the preparation of this base substrate comprises following raw material: laterite, quartz, talcum, Wingdale, rhombspar; More specifically, the raw materials of this base substrate comprises following component: 49.3% SiO
2, 26.3% Al
2O
3, 2.1% Fe
20
3, 1.6% K
2O, 1.9% MgO, 18.8% CaO.
Red soil pottery furnace transmutation glaze, the preparation of this glaze comprises following raw material: 40 parts of potassium felspar sands, 22 parts of albites, 15 parts, calcium oxide, 20 parts, barium oxide, 8 parts of Longyan kaolin, 12 parts of silica powders, 0.2 part of tripoly phosphate sodium STPP, 10 parts of titanium oxide, 10 parts of rutile, 3 parts, zinc oxide, 25 parts of tinting materials; The firing temperature of this glaze is 1250 ℃.
Embodiment four
Red soil greenwave body, the preparation of this base substrate comprises following raw material: laterite, quartz, talcum, Wingdale, rhombspar; More specifically, the raw materials of this base substrate comprises following component: 49.3% SiO
2, 26.3% Al
2O
3, 2.1% Fe
20
3, 1.6% K
2O, 1.9% MgO, 18.8% CaO.
Red soil pottery furnace transmutation glaze, the preparation of this glaze comprises following raw material: 38 parts of potassium felspar sands, 24 parts of albites, 10 parts, calcium oxide, 16 parts, barium oxide, 13 parts of Longyan kaolin, 8 parts of silica powders, 0.3 part of tripoly phosphate sodium STPP, 12 parts of titanium oxide, 4 parts of rutile, 5 parts, zinc oxide, 14 parts of tinting materials; The firing temperature of this glaze is 1230 ℃.
Embodiment five
Red soil greenwave body, the preparation of this base substrate comprises following raw material: laterite, quartz, talcum, Wingdale, rhombspar; More specifically, the raw materials of this base substrate comprises following component: 49.3% SiO
2, 26.3% Al
2O
3, 2.1% Fe
20
3, 1.6% K
2O, 1.9% MgO, 18.8% CaO.
Red soil pottery furnace transmutation glaze, the preparation of this glaze comprises following raw material: 36 parts of potassium felspar sands, 25 parts of albites, 13 parts, calcium oxide, 19 parts, barium oxide, 10 parts of Longyan kaolin, 10 parts of silica powders, 0.3 part of tripoly phosphate sodium STPP, 18 parts of titanium oxide, 8 parts of rutile, 9 parts, zinc oxide, 3 parts of tinting materials; The firing temperature of this glaze is 1230 ℃.
Above-mentioned is only the specific embodiment of the present invention, but design concept of the present invention is not limited to this, allly utilizes this design to carry out the change of unsubstantiality to the present invention, all should belong to the behavior of invading protection domain of the present invention.
Claims (5)
1. red soil greenwave body, is characterized in that, the preparation of this base substrate comprises following raw material: laterite, quartz, talcum, Wingdale, rhombspar; The raw materials of this base substrate comprises following component: 49.3% SiO
2, 26.3% Al
2O
3, 2.1% Fe
2O
3, 1.6% K
2O, 1.9% MgO, 18.8% CaO.
2. red soil pottery furnace transmutation glaze, it is characterized in that, the preparation of this glaze comprises following raw material: potassium felspar sand 35-40 part, albite 22-25 part, calcium oxide 8-15 part, barium oxide 15-20 part, kaolin 8-15 part, silica powder 6-12 part, tripoly phosphate sodium STPP 0.2-0.4 part, titanium oxide 10-20 part, rutile 2-10 part, zinc oxide 3-10 part.
3. red soil as claimed in claim 2 pottery furnace transmutation glaze, it is characterized in that: the raw materials of this glaze comprises the tinting material of 3-25 part.
4. red soil as claimed in claim 2 pottery furnace transmutation glaze, it is characterized in that: the firing temperature of this glaze is 1210 ℃～1250 ℃.
5. red soil as claimed in claim 4 pottery furnace transmutation glaze, it is characterized in that: the firing temperature of this glaze is 1230 ℃.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201210174415 CN102718471B (en) | 2012-05-31 | 2012-05-31 | Green body of red soil ceramic and formula of transmutation glaze of red soil ceramic |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201210174415 CN102718471B (en) | 2012-05-31 | 2012-05-31 | Green body of red soil ceramic and formula of transmutation glaze of red soil ceramic |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102718471A CN102718471A (en) | 2012-10-10 |
| CN102718471B true CN102718471B (en) | 2013-06-12 |
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| CN103396093B (en) * | 2013-08-07 | 2015-08-05 | 福建省德化永惠尔红壤土陶艺有限公司 | A kind of red soil pottery and preparation method thereof |
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| CN109053137B (en) * | 2018-09-17 | 2020-05-12 | 泉州市陶瓷科学技术研究所 | Laterite underglaze art porcelain and preparation method thereof |
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| DE3444627A1 (en) * | 1984-12-07 | 1986-06-19 | Hans Dipl.-Ing. 4030 Ratingen Liebermann | High-strength alumina porcelain body for high-tension insulators |
| CN101481261A (en) * | 2009-02-05 | 2009-07-15 | 苏志强 | Titanium, zinc and pyroxene crystal glaze and preparing method thereof |
| CN101921136B (en) * | 2010-04-13 | 2013-01-02 | 张垠 | Raw material matting glaze |
| KR101021620B1 (en) * | 2010-07-06 | 2011-03-17 | (주)에릭스 | Glaze compositon for heat resistant ceramic ware and ceramic ware manufactured thereof |
| CN102093034B (en) * | 2010-12-10 | 2012-09-26 | 望城县铜官泥人刘艺术陶瓷厂 | Ceramic and preparation method thereof |
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Effective date of registration: 20201222 Address after: 362500 Guandong Ring Road, Dehua County, Quanzhou City, Fujian Province Patentee after: FUJIAN JIAMEI Group Corp. Patentee after: FUJIAN DEHUA COUNTY JINFU CERAMICS Co.,Ltd. Address before: 362500 Po Mei Development Zone, Longxun Town, Dehua County, Quanzhou, Fujian Patentee before: FUJIAN DEHUA COUNTY JINFU CERAMICS Co.,Ltd. |