CN102557732A - Method for preparing glaze from sludge of water source and ceramic product prepared from glaze - Google Patents
Method for preparing glaze from sludge of water source and ceramic product prepared from glaze Download PDFInfo
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- CN102557732A CN102557732A CN201110291568XA CN201110291568A CN102557732A CN 102557732 A CN102557732 A CN 102557732A CN 201110291568X A CN201110291568X A CN 201110291568XA CN 201110291568 A CN201110291568 A CN 201110291568A CN 102557732 A CN102557732 A CN 102557732A
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- glaze
- mud
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- water source
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- 238000000034 method Methods 0.000 title claims abstract description 19
- 239000000919 ceramic Substances 0.000 title abstract description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title abstract description 6
- 239000010802 sludge Substances 0.000 title description 6
- 239000000203 mixture Substances 0.000 claims abstract description 19
- 239000002994 raw material Substances 0.000 claims abstract description 15
- 239000002689 soil Substances 0.000 claims abstract description 11
- 239000000843 powder Substances 0.000 claims abstract description 5
- 238000004458 analytical method Methods 0.000 claims abstract description 4
- 239000012535 impurity Substances 0.000 claims abstract description 4
- 238000012216 screening Methods 0.000 claims abstract description 4
- 239000000463 material Substances 0.000 claims description 21
- 229910052500 inorganic mineral Inorganic materials 0.000 claims description 9
- 239000011707 mineral Substances 0.000 claims description 9
- 230000008569 process Effects 0.000 claims description 5
- 238000001354 calcination Methods 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims description 2
- 239000010419 fine particle Substances 0.000 claims description 2
- 230000000295 complement effect Effects 0.000 abstract 1
- 239000004503 fine granule Substances 0.000 abstract 1
- 238000005242 forging Methods 0.000 abstract 1
- 238000009472 formulation Methods 0.000 abstract 1
- 239000004615 ingredient Substances 0.000 abstract 1
- 230000000087 stabilizing effect Effects 0.000 abstract 1
- 235000010755 mineral Nutrition 0.000 description 6
- 239000000047 product Substances 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 4
- 239000003086 colorant Substances 0.000 description 3
- 210000003298 dental enamel Anatomy 0.000 description 3
- 239000003317 industrial substance Substances 0.000 description 3
- 239000013049 sediment Substances 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 2
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 2
- 239000004927 clay Substances 0.000 description 2
- 238000010276 construction Methods 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- YOBAEOGBNPPUQV-UHFFFAOYSA-N iron;trihydrate Chemical compound O.O.O.[Fe].[Fe] YOBAEOGBNPPUQV-UHFFFAOYSA-N 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 239000010453 quartz Substances 0.000 description 2
- 239000004576 sand Substances 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 239000011573 trace mineral Substances 0.000 description 2
- 235000013619 trace mineral Nutrition 0.000 description 2
- 239000005995 Aluminium silicate Substances 0.000 description 1
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 235000012211 aluminium silicate Nutrition 0.000 description 1
- 230000003466 anti-cipated effect Effects 0.000 description 1
- AYJRCSIUFZENHW-DEQYMQKBSA-L barium(2+);oxomethanediolate Chemical compound [Ba+2].[O-][14C]([O-])=O AYJRCSIUFZENHW-DEQYMQKBSA-L 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000004035 construction material Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000010433 feldspar Substances 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000010881 fly ash Substances 0.000 description 1
- BDAGIHXWWSANSR-NJFSPNSNSA-N hydroxyformaldehyde Chemical compound O[14CH]=O BDAGIHXWWSANSR-NJFSPNSNSA-N 0.000 description 1
- 230000008676 import Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000008595 infiltration Effects 0.000 description 1
- 238000001764 infiltration Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 1
- 235000012204 lemonade/lime carbonate Nutrition 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000001095 magnesium carbonate Substances 0.000 description 1
- 229910000021 magnesium carbonate Inorganic materials 0.000 description 1
- ZLNQQNXFFQJAID-UHFFFAOYSA-L magnesium carbonate Chemical compound [Mg+2].[O-]C([O-])=O ZLNQQNXFFQJAID-UHFFFAOYSA-L 0.000 description 1
- 229960001708 magnesium carbonate Drugs 0.000 description 1
- 235000014380 magnesium carbonate Nutrition 0.000 description 1
- 230000035800 maturation Effects 0.000 description 1
- 238000005065 mining Methods 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 229910000018 strontium carbonate Inorganic materials 0.000 description 1
- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 239000011787 zinc oxide Substances 0.000 description 1
- GFQYVLUOOAAOGM-UHFFFAOYSA-N zirconium(iv) silicate Chemical compound [Zr+4].[O-][Si]([O-])([O-])[O-] GFQYVLUOOAAOGM-UHFFFAOYSA-N 0.000 description 1
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Abstract
The invention relates to a method for preparing glaze with the silt of the water source and ceramic products prepared from this glaze, it is to dig silt from water source, after removing the unnecessary impurity by screening, dry and pulverize to the fine powder (or fine granule), after removing excessive stickness in the mud by high-temperature forging and burning finally, get the raw materials soil, then carry on the composition analysis to this raw materials soil, and complement the ingredient lacking, after stabilizing the formulation, get the stable glaze; the glaze is coated on the surface of the ceramic adobe and then is sintered to obtain the ceramic product with the pre-glaze color.
Description
Technical field
The present invention relates to a kind of method of glaze and pottery that is prepared by this glaze of preparing, the silt soil that particularly relates to a kind of digging waterhead area natural accretion prepares the method for glaze, and by its made pottery.
Background technology
Recycling to the mud of different qualities has carried out a large amount of research all over the world.And at present domestic and international rivers and lakes all have alluvial in various degree to pollute; Various places government all need drop into substantial contribution and manpower and handle these alluvial pollution problems; Existing for many years many development that the mud resource utilization is utilized again, existing multinomial product proposes on the construction engineering material especially.Wherein have with these mud and flyash as main raw material, be aided with additives such as grouan and quartz, burning the person that the ceramic tile, but the employed mud content of this product is lower, needs to add the material of assisting a ruler in governing a country of higher proportion relatively, and production cost is higher relatively.Other utilizes bottom sludge such as lake and reservoir, and infiltration grinds to form construction material person after stirring, add properties-correcting agent, removal moisture content.
Cause the many geographic faces of land seriously exposed because the demand of human development industry is improper for the control of face of land exploitation nearly recent decades; Add the landform of TaiWan, China for example etc. type; The upper reaches, the rivers and creeks gradient is very steep, and annual rainfall is also abundant, cause rainwash to wash away loss very violent; According to statistics, single Taiwan, the silt siltation volume of annual reservoir is approximately up near 1,500 ten thousand steres, with all over the world reservoir or total amount of sludge in lake at present, is difficult to especially estimate.And the severe siltation in these reservoirs or lake not only reduces whole water storage, more day by day loses the function of taking precautions against natural calamities, and therefore, various places government all will clear up the mud work in dredging reservoir and lake, be set at one of the most important problem of being in power.
Mud in reservoir or the lake again, its material is very careful, but if its material may be made in above-mentioned material of construction greater than No. 200 standard sifters (diameter is greater than 0.71mm) after separating in the past, but less than this diameter person, on the contrary by as the mud waste; Yet; Mud in the reservoir is to float for a long time through the upper reaches to take, and is deposited into above-mentioned water reserve person again, its course just like ceramics for comparatively complicated " water elutration method " consuming time in the clay treatment; The sediment grain size of gained is mostly below 20 μ m; If it is applied to the ceramic glaze industry, obviously can omit above-mentioned clay handling procedure, a part of unwanted grains of sand of removal that only need sieve get final product.
Glaze is a kind of ceramic ware idiosome that is used for being covered, and burns till thing to form the permanent vitreous, and it must have general liquid or gas are had no the characteristic that absorbs or permeate, and therefore, it is very careful that the quality of glaze also needs; Existing industrial community is for the manufacturing of glaze; Be to use the powder (like quartz, feldspar, lime carbonate, barium carbonate, zinc oxide, magnesiumcarbonate, Strontium carbonate powder, kaolin, titanium oxide, White tin oxide, zirconium silicate etc.) of raw mineral materials or industrial chemicals; After suitable ratio mediation; Be coated on the ceramic ware idiosome, go into that klining becomes; This method not only causes the consume of natural resources and the destruction of ecotope, and the providing from external import of most raw materials, and production cost can't fall at the end.
And the mud in reservoir or lake, except that as above-mentionedly have the superfine quality that causes, and its composition is very complicated, the raw mineral materials of instead thumping majority or industrial chemicals make and can add under the less material condition, reach the purpose of enamel frit makeing; And, in the mud in reservoir or lake, contain many trace elements, be that general raw mineral materials or industrial chemicals lack, just can form finer and smoother changeable glaze appearance tactile impression; Therefore; If can use reservoir or mud that the lake generated to process glaze, not only can be serious day by day reservoir sedimentation in various places and sludge treatment problem, seek the pipeline of going; And utilize these to need depleted resource material originally; Also can reduce the mining requirement of above-mentioned raw mineral materials relatively, the natural, ecological that is brought consume, the relative cost that also can significantly reduce the former material of enamel frit makeing.
Summary of the invention
Main purpose of the present invention is promptly in that waterhead area mud such as a kind of direct employing reservoir or lake are provided, to be prepared into the method for glaze, to solve the above-mentioned problem that exists.
A purpose more of the present invention promptly utilizes the glaze of above-mentioned generation to come the Low fire ceramic article, makes this pottery because the polynary composition of above-mentioned glaze forms more careful and changeable appearance tactile impression.
For reaching above-mentioned purpose; The present invention mainly is after digging goes out the mud in reservoir or lake in advance; Pulverizes after removing impurity through screening, calcination becomes raw material soil, analyzes the composition of this raw material soil again, and replenish add its insufficient composition raw material after stable components of each part glaze.
According to the above glaze that burns till, be covered in the surface of forming process of ceramics idiosome, or mix in the idiosome material and burn till, can achieve the ceramic body product that has enamel surfaces.
Description of drawings
Fig. 1 is glaze preparation flow figure of the present invention.
Embodiment
Do more detailed explanation to the present invention is above-mentioned with other technical characterictic and advantage below in conjunction with embodiment.
The preparation method of glaze of the present invention; As shown in Figure 1, mainly be to go out mud by waterhead area diggings such as reservoir or lakes earlier, again this mud is removed unnecessary impurity or composition (like sand grains or non-local product matter) through screening; Then with facility this sludge material is given being ground into fine particle or powder after the drying again; Below the diameter 124 μ m, carry out high temperature (600-850 ℃) calcination again and remove over-drastic stickiness in the sludge material, be raw material soil; Then again this raw material soil is carried out composition analysis; With analyze wherein lack insufficient mineral or material composition (mud in each place of production all has different shortage compositions) after; Be added into insufficient mineral or material composition again, and the step that repeats repeatedly this analysis and supply material composition, until the composition or the prescription of the native each several part of this raw material; After evenly reaching the glaze composition content of anticipated demand, the available glaze.
According to the glaze that said process burnt till, ratio on demand is in harmonious proportion or adds after the colorant, is coated on the surface of ceramic ware idiosome, reenters klining, can achieve the ceramic body product with glaze outward appearance.
After giving actually operating according to aforesaid method; What (please join annex one) fired at present success has oil-spot glaze, iron-red glaze, iron red crystal glaze, mirror black glaze, Zijin glaze, brown glaze, yellow glaze, cream-coloured glaze, a celadon glaze etc., and restores the iron rust flower decorative technique in Song dynasty Cizhouyao.In the glaze of Success in Experiment, the usage quantity of Shimen Dam mud is different because of glaze colours.The usage quantity of celadon and yellowish glaze is minimum, and about 10～20%; Other are then many more than 50% like iron oxide red, oil droplet, black glaze, Zijin glaze etc., part glaze side even can reach 80,90%.Because fine sediment of reservoir comprises a greater variety of trace elements, finer and smoother variation effect is arranged for glaze colours and texture performance.With regard to artistic expression, be that existing glaze is incomparable; Seeing from experimental data, is that the glaze of main raw material has bigger maturation TR (40～50 ℃) with the fine sediment of reservoir, and the failure of burning till that causes because the interior temperature of kiln is unequal is seldom arranged.
Above-described embodiment describes preferred implementation of the present invention; Be not that scope of the present invention is limited; Design under the prerequisite of spirit not breaking away from the present invention; Various distortion and improvement that those of ordinary skills make technical scheme of the present invention all should fall in the definite protection domain of claims of the present invention.
Claims (3)
1. the mud with waterhead area prepares the method for glaze, and key step is:
(1) goes out mud by the waterhead area digging, with after this mud process screening and removing unnecessary composition or impurity, give drying and be ground into fine particle or powder again, impose calcination again and form raw material soil;
(2) this raw material soil is analyzed, to draw mineral or the material composition that lacks in this raw material soil, add again supply the mineral or material composition of this shortage after, glaze.
2. the mud with waterhead area as claimed in claim 1 prepares the method for glaze, it is characterized in that: the analysis of said (2) step and supply mineral or the process of material composition, recirculation is implemented repeatedly, the stable components of analyzing until raw material soil each several part.
3. pottery, behind the formed glaze of surface-coated method according to claim 1 or claim 2, the pottery that burns till again.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| TW099133930 | 2010-10-05 | ||
| TW99133930A TW201215586A (en) | 2010-10-05 | 2010-10-05 | Method of preparing glaze using sludge of head-water point and ceramic product made of the glaze |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN102557732A true CN102557732A (en) | 2012-07-11 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201110291568XA Pending CN102557732A (en) | 2010-10-05 | 2011-09-30 | Method for preparing glaze from sludge of water source and ceramic product prepared from glaze |
Country Status (2)
| Country | Link |
|---|---|
| CN (1) | CN102557732A (en) |
| TW (1) | TW201215586A (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103224413A (en) * | 2013-04-06 | 2013-07-31 | 湖南益嘉瓷业有限公司 | Producing method of violet gold glaze |
| CN103693989A (en) * | 2013-11-27 | 2014-04-02 | 刘新安 | Pottery inner wall glaze and inner glaze prepared from the same |
| CN104987045A (en) * | 2015-06-24 | 2015-10-21 | 史江伟 | Preparation process of greyness temmoku oil-spot glaze porcelain |
| CN107162567A (en) * | 2016-03-07 | 2017-09-15 | 上海铭成永美环保科技有限公司 | The Fujian system modelled after an antique common brick and its production method of a kind of utilization Taihu Lake mud production |
| CN111423120A (en) * | 2020-04-27 | 2020-07-17 | 许昌学院 | Preparation method of pine and cypress green ceramic glaze |
| CN111533577A (en) * | 2020-05-20 | 2020-08-14 | 许昌学院 | Dredged sediment resource utilization method and application |
| CN111574054A (en) * | 2019-03-04 | 2020-08-25 | 长沙市坐北朝南陶艺有限公司 | Glaze containing moisture soil and method for preparing ceramic product by using glaze |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0829313B2 (en) * | 1991-09-10 | 1996-03-27 | 有限会社美濃資源開発 | Manufacturing method of ceramic raw materials and manufacturing method of fired products using incinerated ash of municipal waste |
| CN101121612A (en) * | 2007-07-17 | 2008-02-13 | 桂林工学院 | Method for preparing glaze self-releasing ceramic material by red mud and red sandstone |
| CN101125756A (en) * | 2007-09-05 | 2008-02-20 | 孙建兴 | Method for manufacturing black glaze tea bowl with rabbit hair design and color |
-
2010
- 2010-10-05 TW TW99133930A patent/TW201215586A/en not_active IP Right Cessation
-
2011
- 2011-09-30 CN CN201110291568XA patent/CN102557732A/en active Pending
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103224413A (en) * | 2013-04-06 | 2013-07-31 | 湖南益嘉瓷业有限公司 | Producing method of violet gold glaze |
| CN103224413B (en) * | 2013-04-06 | 2016-03-16 | 湖南益嘉瓷业有限公司 | The making method of Zijin glaze |
| CN103693989A (en) * | 2013-11-27 | 2014-04-02 | 刘新安 | Pottery inner wall glaze and inner glaze prepared from the same |
| CN104987045A (en) * | 2015-06-24 | 2015-10-21 | 史江伟 | Preparation process of greyness temmoku oil-spot glaze porcelain |
| CN107162567A (en) * | 2016-03-07 | 2017-09-15 | 上海铭成永美环保科技有限公司 | The Fujian system modelled after an antique common brick and its production method of a kind of utilization Taihu Lake mud production |
| CN111574054A (en) * | 2019-03-04 | 2020-08-25 | 长沙市坐北朝南陶艺有限公司 | Glaze containing moisture soil and method for preparing ceramic product by using glaze |
| CN111423120A (en) * | 2020-04-27 | 2020-07-17 | 许昌学院 | Preparation method of pine and cypress green ceramic glaze |
| CN111533577A (en) * | 2020-05-20 | 2020-08-14 | 许昌学院 | Dredged sediment resource utilization method and application |
| CN111533577B (en) * | 2020-05-20 | 2022-06-07 | 许昌学院 | Dredged sediment resource utilization method and application |
Also Published As
| Publication number | Publication date |
|---|---|
| TWI426061B (en) | 2014-02-11 |
| TW201215586A (en) | 2012-04-16 |
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Application publication date: 20120711 |