CN102511921B - Preparation method of film-shaped tobacco capable of being kept in mouth - Google Patents

Preparation method of film-shaped tobacco capable of being kept in mouth Download PDF

Info

Publication number
CN102511921B
CN102511921B CN201110456202.3A CN201110456202A CN102511921B CN 102511921 B CN102511921 B CN 102511921B CN 201110456202 A CN201110456202 A CN 201110456202A CN 102511921 B CN102511921 B CN 102511921B
Authority
CN
China
Prior art keywords
film
kept
tobacco
preparation method
capable
Prior art date
Application number
CN201110456202.3A
Other languages
Chinese (zh)
Other versions
CN102511921A (en
Inventor
吕翠翠
施栩翎
Original Assignee
华宝食用香精香料(上海)有限公司
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 华宝食用香精香料(上海)有限公司 filed Critical 华宝食用香精香料(上海)有限公司
Priority to CN201110456202.3A priority Critical patent/CN102511921B/en
Publication of CN102511921A publication Critical patent/CN102511921A/en
Application granted granted Critical
Publication of CN102511921B publication Critical patent/CN102511921B/en

Links

Abstract

The invention relates to a preparation method of film-shaped tobacco capable of being kept in mouth. The preparation method comprises the following steps of: extracting and obtaining extractum for tobacco by ethanol; making film-forming material solution formed by selecting pullulan, sodium alginate, sodium carboxy methyl cellulose, Arabic gum and the like; mixing the extractum for the tobacco with the film-forming material solution; and coating the mixed solution on glass, and then obtaining the film-shaped tobacco capable of being kept in mouth after drying. According to the film-shaped tobacco capable of being kept in mouth disclosed by the invention, tobacco flavor exists in the film-shaped tobacco capable of being kept in mouth as the extractum for the tobacco is used, the physiological requirement of a smoker can be met at a certain extent, the environment cannot be influenced, and harm of passive smoking is effectively eliminated. The preparation method disclosed by the invention is simple and convenient to operate, and is beneficial to being promoted.

Description

A kind of preparation method of film-shaped tobacco capable of being kept in mouth

[technical field]

The invention belongs to technical field of tobacco.More specifically, the present invention relates to a kind of preparation method of film-shaped tobacco capable of being kept in mouth.

[background technology]

Cigarette smoke is a kind of extremely complicated mixture.No matter toxic action about cigarette smoke to human body, be initiatively smoking and passive smoking, and report is a lot.2002, Rodgman and Green summed up the harmful components of having reported in flue gas, thought and in cigarette smoke, co-existed in 149 kinds of harmful components.International cancer research institution (IARC) is thought in 46 kinds of harmful components to the carcinogenicity evaluation result of harmful components in Canada's detection list according to the result of the test of pure chemicals, 11 kinds of compositions are human body carcinogen, 5 kinds of compositions are the carcinogenic composition of questionable person's body, and 9 kinds of compositions are the indefinite compound of carcinogenicity.

Although the work of Chinese tobacco reducing tar and reducing harm has also been made significant headway after the general orientation of State Tobacco Monopoly Bureau's proposition reducing tar and reducing harm in 2003, part cigarette product tar content has dropped to below 10 milligrams, but as long as cigarette combustion will produce harmful substance, environment and human body are damaged.This patent is from the viewpoint of non-burning type cigarette, and having prepared can be containing a kind of film-shaped tobacco capable of being kept in mouth of changing.This invention can solve cigarette smoke effectively also can meet numerous smokers' psychological need to the harm of environment and human body, reaches satisfaction.

[summary of the invention]

[technical problem that will solve]

The preparation method who the object of this invention is to provide a kind of film-shaped tobacco capable of being kept in mouth.

[technical scheme]

The present invention is achieved through the following technical solutions.

The preparation method of film-shaped tobacco capable of being kept in mouth, comprises the following steps:

(1) prepare tobacco extract

In there-necked flask, add the tobacco leaf through pulverizing, then adding mass fraction is the ethanol water of 50-95%, and gained mixture stirs 1-4h, and the filtrate decompression of filtering gained is concentrated into density 0.92-1.12kg/m 3, more standing 6-48h, the upper strata grease obtaining is cigarette ointment, lower floor's solution is tobacco extract;

(2) be prepared into membrane material

In 100 parts of total weight parts, get pulullan polysaccharide: sodium alginate: sodium carboxymethylcellulose: Arabic gum: agar: polyvinyl alcohol 1788: dispersant=10-15: 2-5: 3-5: 0.5-5: 0-1: 0-1: 0.1-1.5, surplus is deionized water, be dissolved in deionized water, obtain filmogen solution;

(3) mix film forming

In weight portion, getting 10-20 part step (1) gained tobacco extract joins in the long-pending absolute ethyl alcohol of triploid, obtain uniform tobacco extract ethanolic solution, described tobacco extract ethanolic solution is joined in the filmogen solution that 100 parts of steps (2) obtain and mixed, regulate pH to 6.2-7.2, after standing and defoaming, coat on sheet glass, at 40-60 ℃, dry and obtain film-shaped tobacco capable of being kept in mouth.

According to preferred embodiment a kind of, in 100 parts of gross weights, the tobacco leaf of pulverizing in step (1): ethanol water=5-15: 85-95.

Preferably, in step (1), stir and with 250-350rpm, carry out at 60-80 ℃.

Preferably, reduced pressure concentration carries out under 50-60 ℃, 0.07-0.1Mpa in step (1).

Particularly preferably, pulullan polysaccharide in step (2): sodium alginate: sodium carboxymethylcellulose: Arabic gum=12: 3: 4: 1.

In the present invention, described in step (2), dispersant is selected from ethanol, glycerine, propane diols or their mixture.

Preferably, in step (2), solution temperature is 50-90 ℃.

According to preferred embodiment a kind of, in step (3), use citric acid-sodium citrate buffer solution to regulate pH, the citric acid that described citric acid-sodium citrate buffer solution is 0.1moL/L, the natrium citricum of 0.1moL/L.

Particularly preferably, in step (3), pH is adjusted to 6.8.

Preferably, described in step (3), the coating thickness on sheet glass is 1-4mm.

Below by more detailed description technical scheme of the present invention.

Prepare a kind of film-shaped tobacco capable of being kept in mouth, comprise the following steps:

(1) in there-necked flask, add the tobacco leaf through pulverizing.Described tobacco leaf is can generally buy the product of acquisition on market, for example the tobacco leaf product of Yunnan Yuxi's group sale.The process of pulverizing is not crucial for this step, conventionally tobacco leaf powder is broken to particle diameter and is less than 2mm.Then adding mass fraction is the ethanol water of 50-95%, and after gained mixture fully stirs, the filtrate decompression of filtering gained is concentrated into density 0.92-1.12kg/m 3, then sufficient standing, the upper strata grease obtaining is cigarette ointment, lower floor's solution is tobacco extract, separated stand-by.

In this step, the ratio of tobacco leaf and ethanol water is also non-key, as long as finally can obtain ointment and the medicinal extract that density is suitable, for example, in 100 parts of gross weights, gets tobacco leaf 5-15 part, and ethanol water is supplied.

Stirring can adopt the mode of backflow, or adopts mechanical stirring equipment.As adopted compared with the whipping temp higher than room temperature, will be conducive to operating efficiency, but whipping temp, mixing time and time of repose are also also non-key in this step.For example at 60-80 ℃, with 250-350rpm, stir.The reduced pressure concentration of filtrate is the common means that those skilled in the art can grasp, for example, under 50-60 ℃, 0.07-0.1Mpa, carry out, and can obtain good concentrated effect.

(2) in 100 parts of total weight parts, get pulullan polysaccharide 10-15 part, sodium alginate 2-5 part, sodium carboxymethylcellulose 3-5 part, Arabic gum 0.5-5 part, agar 0-1 part, polyvinyl alcohol 1788 0-1 parts and dispersant 0.1-1.5 part, with deionized water, supply 100 parts and then mix, obtain filmogen solution for standby.

In this step, if the Arabic gum component more (for example 3-5 part) using, can be without adding agar or polyvinyl alcohol 1788, otherwise should correspondingly add agar or polyvinyl alcohol 1788 to be held in the viscosity of membrane material.

In the present invention, pulullan polysaccharide is commercially available prod, for example the pulullan polysaccharide product of Zhengzhou Shunda food additives Co., Ltd production and sales.

In this step, sodium alginate, sodium carboxymethylcellulose, Arabic gum, agar and polyvinyl alcohol 1788 are the product that can buy acquisition on market, for example go up sodium alginate, sodium carboxymethylcellulose, Arabic gum and agar product that ingression Ke biochemical reagents Co., Ltd sells, polyvinyl alcohol 1788 products that fond dream good Chemical Industry Science Co., Ltd in Shanghai sells.

Dispersant can be selected ethanol, glycerine, propane diols or their mixture.

Can heat ionized water better more promptly to dissolve various materials, for example, at 50-90 ℃, mix, but this is also non-essential.

(3) in weight portion, getting 10-20 part step (1) gained tobacco extract joins in the long-pending absolute ethyl alcohol of triploid, obtain uniform tobacco extract ethanolic solution, described tobacco extract ethanolic solution is joined in the filmogen solution that 100 parts of steps (2) obtain and mixed, regulate pH to 6.2-7.2, after standing and defoaming, coat on sheet glass, at 40-60 ℃, dry and obtain film-shaped tobacco capable of being kept in mouth.

While regulating pH, can adopt for example 0.1moL/L citric acid-0.1moL/L sodium citrate buffer solution, the pH of this buffer solution approximately 3.5.Particularly preferably pH is adjusted to 6.8.Coating thickness on sheet glass is generally 1-4mm, and the variation of thickness can affect the baking needed time, and the smear of generally drying 1-4mm at 40-60 ℃ needs 2-10h.

[beneficial effect]

The feature of filmogen of the present invention obtains a kind ofly take water-soluble eatable material and prepares buccal film as raw material, belong to without smoke product, this is sucked cigarette and contains tobacco extract and have tobacco breath, can to a certain degree meet smoker's physiological requirements, and environment is not polluted, effectively stop second-hand-cigarette harm.The method is simple, is conducive to promote.

[accompanying drawing explanation]

Accompanying drawing 1 is the process chart of the inventive method.

[specific embodiment]

embodiment 1

In there-necked flask, add and pulverize tobacco leaf 50g and 50wt% ethanol water 950g, after 60 ℃ of 250rpm stir 4h, filter, filtrate is evaporated to density 0.92kg/m3 at 0.07Mpa, 60 ℃, more standing 48h, brown tobacco extract 13g obtained.

Get pulullan polysaccharide 5g, sodium alginate 1g, sodium carboxymethylcellulose 1.5g, Arabic gum 0.25g, agar 0.5g, polyvinyl alcohol 1788 0.5g, glycerine 0.05g, deionized water 41.2g, at 50 ℃, mix, obtain filmogen solution 50g.

Taking tobacco extract 10g adds in the long-pending absolute ethyl alcohol of triploid, join again in filmogen solution and mix, with 0.1moL/L citric acid-0.1moL/L sodium citrate buffer solution, regulate pH to 6.2, on standing and defoaming back glass sheet, be coated with 1mm thin slice, at 40 ℃, dry and within 5 hours, obtain film-shaped tobacco capable of being kept in mouth.

embodiment 2

In there-necked flask, add and pulverize tobacco leaf 150g and 95wt% ethanol water 850g, after 80 ℃ of 350rpm stir 1h, filter, filtrate is evaporated to density 1.12kg/m at 0.1Mpa, 50 ℃ 3, more standing 6h, obtain brown tobacco extract 35g.

Get pulullan polysaccharide 30g, sodium alginate 10g, sodium carboxymethylcellulose 10g, Arabic gum 10g, propane diols 3g, deionized water 137g, at 50 ℃, mix, obtain filmogen solution 200g.

Taking tobacco extract 20g adds in the long-pending absolute ethyl alcohol of triploid, join again in filmogen solution and mix, with 0.1moL/L citric acid-0.1moL/L sodium citrate buffer solution, regulate pH to 7.2, on standing and defoaming back glass sheet, be coated with 4mm thin slice, at 60 ℃, dry and within 10 hours, obtain film-shaped tobacco capable of being kept in mouth.

embodiment 3

In there-necked flask, add and pulverize tobacco leaf 100g and 75wt% ethanol water 900g, after 60 ℃ of 300rpm stir 2h, filter, filtrate is evaporated to density 1.08kg/m at 0.08Mpa, 60 ℃ 3, more standing 10h, obtain brown tobacco extract 26g.

Get pulullan polysaccharide 12g, sodium alginate 3g, sodium carboxymethylcellulose 4g, Arabic gum 1g, agar 0.5g, polyvinyl alcohol 17880.5g, glycerine and each 0.1g of ethanol, deionized water 78.8g, at 60 ℃, mix, obtain filmogen solution 100g.

Taking tobacco extract 15g adds in the long-pending absolute ethyl alcohol of triploid, join again in filmogen solution and mix, with 0.1moL/L citric acid-0.1moL/L sodium citrate buffer solution, regulate pH to 6.8, on standing and defoaming back glass sheet, be coated with 2mm thin slice, at 60 ℃, dry and within 2 hours, obtain film-shaped tobacco capable of being kept in mouth.

By the film of sucking preparing, to take blade cuts rectangular as 2 * 5cm, is placed in maxilla containing changing.This sucks smoking set soft tobacco breath, can to a certain degree meet smoker's physiological requirements.

Claims (10)

1. a preparation method for film-shaped tobacco capable of being kept in mouth, is characterized in that said method comprising the steps of:
(1) prepare tobacco extract
In there-necked flask, add the tobacco leaf through pulverizing, then adding mass fraction is the ethanol water of 50-95%, and gained mixture stirs 1-4h, and the filtrate decompression of filtering gained is concentrated into density 0.92-1.12kg/m 3, more standing 6-48h, the upper strata grease obtaining is cigarette ointment, lower floor's solution is tobacco extract;
(2) be prepared into membrane material
In 100 parts of total weight parts, get pulullan polysaccharide: sodium alginate: sodium carboxymethylcellulose: Arabic gum: agar: polyvinyl alcohol 1788: dispersant=10-15:2-5:3-5:0.5-5:0-1:0-1:0.1-1.5, surplus is deionized water, be dissolved in deionized water, obtain filmogen solution;
(3) mix film forming
In weight portion, getting 10-20 part step (1) gained tobacco extract joins in the long-pending absolute ethyl alcohol of triploid, obtain uniform tobacco extract ethanolic solution, described tobacco extract ethanolic solution is joined in the filmogen solution that 100 parts of steps (2) obtain and mixed, regulate pH to 6.2-7.2, after standing and defoaming, coat on sheet glass, at 40-60 ℃, dry and obtain film-shaped tobacco capable of being kept in mouth.
2. the preparation method of film-shaped tobacco capable of being kept in mouth according to claim 1, is characterized in that in 100 parts of gross weights, the tobacco leaf of pulverizing in step (1): ethanol water=5-15:85-95.
3. the preparation method of film-shaped tobacco capable of being kept in mouth according to claim 1, is characterized in that stirring and with 250-350rpm, carrying out at 60-80 ℃ in step (1).
4. the preparation method of film-shaped tobacco capable of being kept in mouth according to claim 1, is characterized in that in step (1) that reduced pressure concentration carries out under 50-60 ℃, 0.07-0.1Mpa.
5. the preparation method of film-shaped tobacco capable of being kept in mouth according to claim 1, is characterized in that pulullan polysaccharide in step (2): sodium alginate: sodium carboxymethylcellulose: Arabic gum=12:3:4:1.
6. the preparation method of film-shaped tobacco capable of being kept in mouth according to claim 1, is characterized in that described in step (2), dispersant is selected from ethanol, glycerine, propane diols or their mixture.
7. the preparation method of film-shaped tobacco capable of being kept in mouth according to claim 1, is characterized in that described in step (2), solution temperature is 50-90 ℃.
8. the preparation method of film-shaped tobacco capable of being kept in mouth according to claim 1, is characterized in that with citric acid-sodium citrate buffer solution, regulating pH, the citric acid that described citric acid-sodium citrate buffer solution is 0.1moL/L, the natrium citricum of 0.1moL/L in step (3).
9. the preparation method of film-shaped tobacco capable of being kept in mouth according to claim 1, is characterized in that, in step (3), pH is adjusted to 6.8.
10. the preparation method of film-shaped tobacco capable of being kept in mouth according to claim 1, is characterized in that described in step (3), the coating thickness on sheet glass is 1-4mm.
CN201110456202.3A 2011-12-30 2011-12-30 Preparation method of film-shaped tobacco capable of being kept in mouth CN102511921B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201110456202.3A CN102511921B (en) 2011-12-30 2011-12-30 Preparation method of film-shaped tobacco capable of being kept in mouth

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201110456202.3A CN102511921B (en) 2011-12-30 2011-12-30 Preparation method of film-shaped tobacco capable of being kept in mouth

Publications (2)

Publication Number Publication Date
CN102511921A CN102511921A (en) 2012-06-27
CN102511921B true CN102511921B (en) 2014-02-26

Family

ID=46283227

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201110456202.3A CN102511921B (en) 2011-12-30 2011-12-30 Preparation method of film-shaped tobacco capable of being kept in mouth

Country Status (1)

Country Link
CN (1) CN102511921B (en)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103015175B (en) * 2012-12-06 2016-05-25 张家口卷烟厂有限责任公司 Pulullan polysaccharide modification polypropylene fibre for cigarettes and preparation method thereof
CN103478890B (en) * 2013-09-09 2016-08-24 湖南中烟工业有限责任公司 A kind of smokeless tobacco containing durian flavor
CN103484245B (en) * 2013-09-18 2015-10-14 浙江中烟工业有限责任公司 The one directed composite extracting method growing tobacco this Studies of The Aromatic Substances of endogenous
CN103462206B (en) * 2013-09-18 2015-10-28 浙江中烟工业有限责任公司 A kind of reconstituted tobacco of this Studies of The Aromatic Substances of tobacco endogenous containing directed compound collecting and cigarette prepared therefrom
CN103462210B (en) * 2013-09-29 2015-08-19 中国烟草总公司郑州烟草研究院 A kind of tobacco membrane preparation method being applicable to heating non-combustion-type tobacco goods
CN103960783A (en) * 2014-05-15 2014-08-06 湖北中烟工业有限责任公司 Gel type solid-liquid electronic cigarette cartridge and manufacturing method thereof
CN105768195B (en) * 2016-05-13 2018-10-12 广东中烟工业有限责任公司 Using the buccal cigarette and preparation method thereof of large scale tobacco-containing material

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010079793A1 (en) * 2009-01-08 2010-07-15 日本たばこ産業株式会社 Filter for cigarette
CN101862024A (en) * 2010-06-07 2010-10-20 中国烟草总公司郑州烟草研究院 Refreshing tablets containing tobacco components

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AU2005280249B2 (en) * 2004-08-25 2009-03-05 Intercontinental Great Brands Llc Liquid-filled chewing gum composition
US20080286340A1 (en) * 2007-05-16 2008-11-20 Sven-Borje Andersson Buffered nicotine containing products

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010079793A1 (en) * 2009-01-08 2010-07-15 日本たばこ産業株式会社 Filter for cigarette
CN101862024A (en) * 2010-06-07 2010-10-20 中国烟草总公司郑州烟草研究院 Refreshing tablets containing tobacco components

Also Published As

Publication number Publication date
CN102511921A (en) 2012-06-27

Similar Documents

Publication Publication Date Title
CN104068467B (en) A kind of tobacco juice for electronic smoke being rich in plant flavone
CN1161043C (en) Smokable filler material for smoking articles and smoking articles
CN102813278B (en) A kind of mixed type electronic cigarette tobacco liquid
EP2543265B1 (en) Preparation method of E-cigarette liquid
CN1064221C (en) Nutritive health cigarette and its preparing process
CN102960852A (en) Light-fragrance electronic cigarette atomized smoke solution and preparation method thereof
US9538781B2 (en) Oral nicotine-substituted cytisine atomized liquid and its preparation method
CN101548797B (en) One kind Tobacco and its production method
WO2016034100A1 (en) E-liquid for water-atomizing electronic cigarette and water-atomizing electronic cigarette comprising the e-liquid
CN102697168B (en) Additive for boosting maillard reaction of recombined tobacco leaves and method for preparing tobacco leaves by using additive
CN101570716B (en) Method for extracting natural Chinese medicinal herb fragrance component and application of extract thereof
CN103989244A (en) Chinese style flue-cured tobacco odor type electronic cigarette tobacco juice capable of improving smoking satisfaction sense
CN106235375A (en) A kind of method of the suncured tabacco reconstituted tobacco manufacturing applicable flue-cured tobacco local flavor
CN101536737B (en) Preparation method of chewing tobacco
CN102742861B (en) The processing method of special type wild boar bacon
CN103989245A (en) Chinese flue-cured tobacco type electronic cigarette liquid capable of effectively reducing oral cavity sweet greasy feeling
CN104026730B (en) A kind of burnt fragrant and sweet type tobacco juice for electronic smoke
CN1813601B (en) Cigarette filter tip additive capable of reducing smoke harmful effect to respiratory system
CN104839883B (en) A kind of tobacco juice for electronic smoke with pipe tobacco style and features
CN104489905A (en) Liquor-fragrance E-cigarette nicotine liquid
CN1135860A (en) Atomized cigarette
CN1818210A (en) Formed paper coating for lowering harm and decreasing coking smoke
CN104041935A (en) Method for extracting Chinese-style flue-cured tobacco fragrance cigarette juice for electronic cigarette
CN104403794A (en) Preparation method and application of Pu'er tea extract to cigarettes
CN102986391A (en) Method for improving content and aromas of tobacco secondary metabolite products

Legal Events

Date Code Title Description
PB01 Publication
C06 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
C56 Change in the name or address of the patentee
CP01 Change in the name or title of a patent holder

Address after: 850000 Lhasa economic and Technological Development Zone, Tibet autonomous region, road, investment building,

Patentee after: Huabao flavor Limited by Share Ltd

Address before: 850000 Lhasa economic and Technological Development Zone, Tibet autonomous region, road, investment building,

Patentee before: Huabao flavor Limited

CP03 Change of name, title or address

Address after: 850000 Lhasa economic and Technological Development Zone, Tibet autonomous region, road, investment building,

Patentee after: Huabao flavor Limited

Address before: 201821 Yecheng Road, Shanghai, No. 1299, No.

Patentee before: Huabao Edible Essence And Spice (Shanghai) Co., Ltd.

C41 Transfer of patent application or patent right or utility model
TR01 Transfer of patent right

Effective date of registration: 20170123

Address after: 650503 Yunnan city of Kunming province high tech Zone Jinpu rural Metro high-tech industrial base A6-2

Patentee after: YUNNAN XINYUN TECHNOLOGY DEVELOPMENT CO., LTD.

Address before: 850000 Lhasa economic and Technological Development Zone, Tibet autonomous region, road, investment building,

Patentee before: Huabao flavor Limited by Share Ltd

TR01 Transfer of patent right

Effective date of registration: 20180808

Address after: 335000 Longgang Industrial Park, Yingtan Hi-tech Industrial Development Zone, Jiangxi Province

Patentee after: Yingtan Huayu Biotechnology Co., Ltd.

Address before: 650503 new town high tech industrial base A6-2, Ma Jin Pu Township, Kunming high tech Zone, Yunnan

Patentee before: YUNNAN XINYUN TECHNOLOGY DEVELOPMENT CO., LTD.

TR01 Transfer of patent right