CN102318650B - Mosquito-repellent incense with residue obtained after volatile oil extraction from typus physiologions cinnanloni leaf as base material and production method thereof - Google Patents
Mosquito-repellent incense with residue obtained after volatile oil extraction from typus physiologions cinnanloni leaf as base material and production method thereof Download PDFInfo
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- CN102318650B CN102318650B CN2011102551471A CN201110255147A CN102318650B CN 102318650 B CN102318650 B CN 102318650B CN 2011102551471 A CN2011102551471 A CN 2011102551471A CN 201110255147 A CN201110255147 A CN 201110255147A CN 102318650 B CN102318650 B CN 102318650B
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- 239000000077 insect repellent Substances 0.000 title claims abstract description 64
- 239000000341 volatile oil Substances 0.000 title claims abstract description 27
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 19
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- 238000000605 extraction Methods 0.000 title claims abstract description 10
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- VXSIXFKKSNGRRO-MXOVTSAMSA-N [(1s)-2-methyl-4-oxo-3-[(2z)-penta-2,4-dienyl]cyclopent-2-en-1-yl] (1r,3r)-2,2-dimethyl-3-(2-methylprop-1-enyl)cyclopropane-1-carboxylate;[(1s)-2-methyl-4-oxo-3-[(2z)-penta-2,4-dienyl]cyclopent-2-en-1-yl] (1r,3r)-3-[(e)-3-methoxy-2-methyl-3-oxoprop-1-enyl Chemical class CC1(C)[C@H](C=C(C)C)[C@H]1C(=O)O[C@@H]1C(C)=C(C\C=C/C=C)C(=O)C1.CC1(C)[C@H](/C=C(\C)C(=O)OC)[C@H]1C(=O)O[C@@H]1C(C)=C(C\C=C/C=C)C(=O)C1 VXSIXFKKSNGRRO-MXOVTSAMSA-N 0.000 description 4
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- HYJYGLGUBUDSLJ-UHFFFAOYSA-N pyrethrin Natural products CCC(=O)OC1CC(=C)C2CC3OC3(C)C2C2OC(=O)C(=C)C12 HYJYGLGUBUDSLJ-UHFFFAOYSA-N 0.000 description 4
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- 239000002728 pyrethroid Substances 0.000 description 4
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- DTGKSKDOIYIVQL-NQMVMOMDSA-N (+)-Borneol Natural products C1C[C@]2(C)[C@H](O)C[C@@H]1C2(C)C DTGKSKDOIYIVQL-NQMVMOMDSA-N 0.000 description 1
- DTGKSKDOIYIVQL-WEDXCCLWSA-N (+)-borneol Chemical compound C1C[C@@]2(C)[C@@H](O)C[C@@H]1C2(C)C DTGKSKDOIYIVQL-WEDXCCLWSA-N 0.000 description 1
- ZCVAOQKBXKSDMS-PVAVHDDUSA-N (+)-trans-(S)-allethrin Chemical compound CC1(C)[C@H](C=C(C)C)[C@H]1C(=O)O[C@@H]1C(C)=C(CC=C)C(=O)C1 ZCVAOQKBXKSDMS-PVAVHDDUSA-N 0.000 description 1
- ZCVAOQKBXKSDMS-AQYZNVCMSA-N (+)-trans-allethrin Chemical compound CC1(C)[C@H](C=C(C)C)[C@H]1C(=O)OC1C(C)=C(CC=C)C(=O)C1 ZCVAOQKBXKSDMS-AQYZNVCMSA-N 0.000 description 1
- FMTFEIJHMMQUJI-NJAFHUGGSA-N 102130-98-3 Natural products CC=CCC1=C(C)[C@H](CC1=O)OC(=O)[C@@H]1[C@@H](C=C(C)C)C1(C)C FMTFEIJHMMQUJI-NJAFHUGGSA-N 0.000 description 1
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- 206010011224 Cough Diseases 0.000 description 1
- 241000256113 Culicidae Species 0.000 description 1
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- 206010059866 Drug resistance Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
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- 238000011109 contamination Methods 0.000 description 1
- KAATUXNTWXVJKI-UHFFFAOYSA-N cypermethrin Chemical compound CC1(C)C(C=C(Cl)Cl)C1C(=O)OC(C#N)C1=CC=CC(OC=2C=CC=CC=2)=C1 KAATUXNTWXVJKI-UHFFFAOYSA-N 0.000 description 1
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- 150000002148 esters Chemical class 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N ferric oxide Chemical compound O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 239000011152 fibreglass Substances 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 238000003958 fumigation Methods 0.000 description 1
- 230000008676 import Effects 0.000 description 1
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- 231100000037 inhalation toxicity test Toxicity 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 239000003350 kerosene Substances 0.000 description 1
- 231100000225 lethality Toxicity 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 235000010603 pastilles Nutrition 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- SMKRKQBMYOFFMU-UHFFFAOYSA-N prallethrin Chemical compound CC1(C)C(C=C(C)C)C1C(=O)OC1C(C)=C(CC#C)C(=O)C1 SMKRKQBMYOFFMU-UHFFFAOYSA-N 0.000 description 1
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Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a mosquito-repellent incense with residues obtained after volatile oil extraction from typus physiologions cinnanloni leaves as a base material for the mosquito-repellent incense and a production method thereof. The mosquito-repellent incense comprises the following raw materials by weight: 40-70 parts of typus physiologions cinnanloni leaf residue powder, 30-40 parts of starch, and 5-10 parts of perfume. The production method comprises the following steps: drying and crushing typus physiologions cinnanloni leaf residues, sieving through 100-120 meshes to remove impurities, adding pure typus physiologions cinnanloni leaf residue powder into starch and perfume, uniformly stirring with water to obtain a pasty mixture, performing extrusion moulding in an incense-making machine, drying and packaging the finished product. The mosquito-repellent incense with residues obtained after volatile oil extraction from typus physiologions cinnanloni leaves as a base material of the invention has fewer but better raw material composition, and because of the addition of typus physiologions cinnanloni leaf residue powder, the product has obvious mosquito-repelling effect. The invention makes full use of typus physiologions cinnanloni leaf residue powder as a main raw material, changes waste into valuables; the product has faint scent after ignited, has the function of mosquito, fly, and insect repellence, and is an environment-friendly product. The production method has the characteristics of simple preparation process flow, and low raw material cost.
Description
Technical field
The present invention relates to a kind of production method of mosquito-repellent incense, specifically, is a kind ofly to extract behind the volatile oil residue as mosquito-repellent incense and the production method thereof of base-material take the Borneolum leaf.
Background technology
Mosquito-repellent incense is a kind of daily living article, is mainly used in autumn in summer mosquito repellent, and this has had very long history in China.Just period occurs the culicifuge incense rod that Chinese medicine makes as far back as the Southern Song Dynasty, the mosquito-repellent incense industry development has been crossed over century more than one so far, in numerous mosquito protective articles market still in occupation of leading position.Mosquito-repellent incense can be divided into chemical pesticide mosquito repellent mosquito-repellent incense and biopesticide mosquito repellent mosquito-repellent incense by the mosquito repellent active ingredient of adding.It is the active ingredient mosquito repellent that the getting up early mosquito-repellent incense mainly adopts chemical pesticide.This class mosquito-repellent incense causes the uncomfortable of people in the use procedure meeting, and cough and the infection of the upper respiratory tract etc. also can cause simultaneously environmental pollution, thereby its production are banned by country.
In recent years, the mosquito-repellent incense production industry mainly adopts the active ingredient of adding from plant extract to prepare mosquito-repellent incense, to reach mosquito repellent and safe effect, as adding the pyrethrins such as cypermethrin, Prallethrin, allethrin, ES Esbiothrin.At present, the safety mosquito-repellent of market sale mainly adopts active ingredients such as adding chrysanthemum ester insecticide, and the content in mosquito-repellent incense is about 0.2% ~ 0.4%.Pyrethrins is the main component in the liposoluble substance that extracts from the Dalmatian chrysanthemum plant, is a kind of middle low toxic pesticide, is to be added on active ingredient the most frequently used in the mosquito-repellent incense, and the nerve that can benumb mosquito causes its death.People are referred to as botanical pesticide to plant and the preparation thereof that these are used for disinfection and deinsectization, substantially belong to the natural agricultural chemicals of nontoxic residue-free.But the market pyrethrins is in short supply, and import price is expensive, does not satisfy the Production and consumption demand.In addition, pyrethrins is insoluble in water, can be dissolved in the organic solvents such as benzene, dimethylbenzene, apply at present in the mosquito-repellent incense technique, solvent mainly is kerosene and alcohol, the medicament that is dissolved in these organic solvents being applied on the dish mosquito-repellent incense of not pastille of air-dry moulding is a kind of comparatively common method, i.e. coating technique.In the method products obtained therefrom, active ingredient only concentrates on the mosquito-repellent incense surface, and limited, the combustion-supporting auxiliary material of content is more, and organic solvent wherein and a large amount of combustion-supporting auxiliary materials have spread effect to the human respiratory tract in combustion process, certain toxic and side effect is arranged.
Thereby, need exploitation that a kind of cheap, raw material is natural and repelling effect is good product is provided.
Summary of the invention
The present invention is intended to address the above problem, overcome the deficiencies in the prior art, provide a kind of and extract behind the volatile oil residue as green mosquito-repellent incense and the production method thereof of base-material take the Borneolum leaf, effective mosquito repellent, not only can not cause the excitant injury to human body, and calm the nerves in addition the effect that helps for sleep.A kind ofly extract take the Borneolum leaf that residue is characterized in that including following weight portion raw material as the green mosquito-repellent incense of base-material behind the volatile oil: the Borneolum leaf extracts residue powder 40-70 part behind the volatile oil, starch 30-40 part, spices 5-10 part.Wherein the preferred weight umber is respectively: 55 parts in residue powder, 35 parts of starch, 10 parts of spices behind the Borneolum leaf extraction volatile oil.Remove in addition, also include following weight portion raw material: charcoal powder 30-40 part, wood powder 30-40 part and tree root glue powder 20-40 part.Wherein the weight portion of preferred charcoal powder, wood powder and the sticking powder of tree root is respectively 35 parts, 35 parts and 30 parts.
Preparation method of the present invention is: first that spices etc. is soluble in water, be mixed with the aqueous solution.Then a small amount of aqueous solution is added in the starch, dispersed with stirring evenly after, add again excess water solution, mix and be uniformly dispersed, heating is also constantly stirred, until the whole gelatinizations of starch.Residue powder, charcoal powder, wood powder and the sticking powder of tree root behind the Borneolum leaf extraction volatile oil are mixed in the adding binder, after fully stirring, namely get sticky body of paste.With press molding in the above sticky body of paste injection model that makes, or after the type frame of pouring into makes plates, dry, make formed body through cutting again, at last packing.
It is primary raw material that the present invention selects the residue powder behind the Borneolum leaf extraction volatile oil, and that mixes glues powder in starch, spices, charcoal powder, wood powder and tree root, does not contain any chemical insecticide, organic solvent, and not only repelling effect is good, plays the restraining and sterilizing bacteria effect; Can also purify the air of a room, and harmless, free from environmental pollution, the smell fragrance.
For existing market demand and people's needs of life, the present invention courageously improves existing market mosquito-repellent incense production technology, and the residue powder that employing Borneolum leaf extracts behind the volatile oil is that primary raw material is developed into a kind of bacteriostatic green mosquito-repellent incense.Mosquito-repellent incense raw materials of the present invention is the residue powder after the Borneolum leaf extracts volatile oil, is a kind of of waste resource fully effectively utilized, and with low cost, meet the requirement of energy-saving and environmental protecting.In China, the Borneolum tree mainly is distributed in Yunnan and East of Guangdong Province area.The characteristics of Borneolum leaf are that its leaf contains abundant d-Bomeol, and d-Bomeol has the camphoraceous special spine smell of class, thereby have mosquito repellent function.And natural d-borneol is nontoxic to human body.Usually, the Borneolum leaf has extracted residue behind the volatile oil often as waste material and abandoned, but still has dense and special spine smell in view of it, therefore, from the angle of comprehensive utilization, will make mosquito-repellent incense take Borneolum leaf residue as base-material in the hope of reaching the purpose of mosquito repellent.
Embodiment
Embodiment 1
Residue is as base-material mosquito-repellent incense and production method thereof after extracting volatile oil take the Borneolum leaf
Spices 4g is soluble in water, and the mass volume ratio of spices and water is 1:6, is mixed with spice solution.Pour 1/3 spice solution into pour again remainder in the 15g corn starch behind the stirring 30min into spice solution, stir, while stirring in 70 ℃ of heating until starch gelatinization.The sticking powder 10g of residue powder 20g, charcoal powder 15g, wood powder 15g and tree root behind the Borneolum leaf extraction volatile oil is fully mixed with gelatinized starch, namely get the thickness body of paste.The above thickness body of paste that makes is put into the joss sticks manufacturing machine moulding, and then baking oven is 60 ℃ of lower oven dry, and mosquito-repellent incense gets product.
Embodiment 2
Residue is as base-material mosquito-repellent incense and production method thereof after extracting volatile oil take the Borneolum leaf
Spices 4.5g is soluble in water, and the mass volume ratio of spices and water is 1:8, is mixed with spice solution.Pour 1/3 spice solution into pour again remainder in the 18g corn starch behind the stirring 35min into spice solution, stir, while stirring in 80 ℃ of heating until starch gelatinization.The sticking powder 15g of residue powder 22g, charcoal powder 18g, wood powder 18g and tree root behind the Borneolum leaf extraction volatile oil is fully mixed with gelatinized starch, namely get the thickness body of paste.The above thickness body of paste that makes is put into the joss sticks manufacturing machine moulding, and then baking oven is 70 ℃ of lower oven dry, and mosquito-repellent incense gets product.
Embodiment 3
Residue is as base-material mosquito-repellent incense and production method thereof after extracting volatile oil take the Borneolum leaf
Spices 5g is soluble in water, and the mass volume ratio of spices and water is 1:10, is mixed with spice solution.Pour 1/3 spice solution into pour again remainder in the 20g corn starch behind the stirring 40min into spice solution, stir, while stirring in 85 ℃ of heating until starch gelatinization.The sticking powder 20g of residue powder 25g, charcoal powder 20g, wood powder 20g and tree root behind the Borneolum leaf extraction volatile oil is fully mixed with gelatinized starch, namely get the thickness body of paste.The above thickness body of paste that makes is put into the joss sticks manufacturing machine moulding, and then baking oven is 80 ℃ of lower oven dry, and mosquito-repellent incense gets product.
Check the method for combustion mosquito coil incense of above-mentioned technique preparation as follows:
(1) smell inspection: sense organ, nonirritant peculiar smell.
(2) drug effect inspection: press the GB/T13917 test.Under the room temperature condition, adopt cylinder unit, draw 30 of examination mosquitos, put into the jam-pack plug from the central circular hole place of cylinder below plectane.After trying worm recovery normal activity, get at random one section of mosquito-repellent incense to be measured, horizontal on mosquito coil frame; after lighting 5min in advance elsewhere, move to fumigation 1min in the cylinder, immediately mosquito-repellent incense is removed; plug, and timing beyond the Great Wall records down and out examination borer population at set intervals.Be limited to 20min during observation.Simultaneously, must carry out skip test, the rate of knockdown of skip test and lethality are as greater than 20%, and test need re-start.In repeated test, select at random the different mosquito-repellent incense for preparing among the embodiment to detect.And after each off-test, the washing test device.Testing result KT
50(under rated condition, 50% the examination worm required time of going down.) expression.
(3) smoke discharge amount inspection: press HJ/T 310 tests.
According to national environmental protection industry standard HJ/T 310 test, after the individual pen coiled mosquito-repellent incense lighted, collect whole flue dust of discharging with filter membrane (paper), until light completely, the flue dust weight of collecting represents with the g/ individual pen.Ultra-fine fibre glass filter paper is accurately weighed with analytical balance, filter paper is fixed on the sampling folder, pick and place filter paper with antimagnetic type tweezer during operation.Regulate the flow to 20 liter/min of sampler, sampler is placed on apart from tested mosquito-repellent incense 10cm place, making sampling folder aligning mosquito-repellent incense.Igniting mosquito-repellent incense sampling 0.5 ~ 2h.Filter paper is taken off, put into drier, behind the 1h, accurately weigh with analytical balance.It is complete to sample, and namely extinguishes mosquito-repellent incense, weighs up quality before and after the burning mosquito incense with pharmacist balance, perhaps goes out length.Simultaneously, with the indoor blank of another filter paper work, as room air flue dust background.Testing result represents with smoke discharge amount (mg/ individual pen).
Comparing result shows: the drug effect 6-7min of the mosquito-repellent incense among the comparative example 4, and the combustion mosquito coil incense drug effect has reached 4min among the embodiment 1-3, smoke discharge amount is all less than the 20mg/ individual pen.As seen, compare with the mosquito-repellent incense of comparative example's preparation, the mosquito-repellent incense mosquito rate of knockdown that provides among the embodiment of the invention 1-3 has improved about about 30-50%.Concrete comparing result is as shown in table 1.
Table one mosquito-repellent incense proterties comparative test result
Table 1
(4) mosquito-repellent incense safety inspection
1. rat acute Oral toxicity
First above-mentioned three kinds of example mosquito-repellent incense samples are pulverized, weighed after sieving, the solution that is made into doses carries out gavage to three rats respectively.All visible 3 mouse are movable normal behind gavage 20 ~ 30 min, the situations such as external reaction is blunt, rat is suffered from diarrhoea, dull do not occur, and viewing duration is without animal dead.Male and female rat oral LD
50All greater than 5 000 mg/kg.According to agricultural chemicals acute oral grade scale, the toxicity of the Ministry of Agriculture's 1.2,1.8 G products and classer's description judgement all belong to nontoxic level.
2. rat acute toxicity on inhalation test
Take by weighing a certain amount of above-mentioned three kinds of example mosquito-repellent incenses, place 3 exposure in static total enclosure chamber cabinets to light, it is slowly volatilized, in small fan is housed ceaselessly stirs and make it even.Then put into respectively 3 rats.Undertaken by relevant rat acute drug resistance test in the GB15670-1995 agriculture chemical registration toxicology test method.Experimental result is as follows: the symptoms such as deeply slow, that activity reduces, external reaction is blunt all appear perspiring, breathing in 3 mouse during the contamination, and viewing duration is without animal dead.Female male rat sucks LC
50All greater than 5 000 mg/m
3According to agricultural chemicals acute inhalation toxicity grade scale, the toxicity of the Ministry of Agriculture's 1.2,1.8 G products and classer's description are judged, all belong to nontoxic level.
Claims (5)
1. one kind is extracted take the Borneolum leaf that residue is characterized in that including following weight portion raw material as the mosquito-repellent incense of base-material behind the volatile oil: the Borneolum leaf extracts residue powder 40-70 part behind the volatile oil, starch 30-40 part, spices 5-10 part.
2. by mosquito-repellent incense claimed in claim 1, it is characterized in that the parts by weight of raw material are: 55 parts in residue powder, 35 parts of starch, 10 parts of spices behind the Borneolum leaf extraction volatile oil.
3. extract take the Borneolum leaf by claimed in claim 1 that residue is as the mosquito-repellent incense of base-material behind the volatile oil, characterized by further comprising following weight portion raw material: charcoal powder 30-40 part, wood powder 30-40 part and tree root glue powder 20-40 part.
4. extract take the Borneolum leaf by claimed in claim 3 that residue is characterized in that as the mosquito-repellent incense of base-material the weight of the sticking powder of charcoal powder, wood powder and tree root is respectively 35 parts, 35 parts and 30 parts behind the volatile oil.
5. production claim 3 is described extracts take the Borneolum leaf that residue is characterized in that as the method for the mosquito-repellent incense of base-material behind the volatile oil: first that spices is soluble in water, be mixed with the aqueous solution; Then a small amount of aqueous solution is added in the starch, dispersed with stirring evenly after, add again excess water solution, mix and be uniformly dispersed, heating is also constantly stirred, until the whole gelatinizations of starch; The Borneolum leaf is extracted residue powder behind the volatile oil, charcoal powder, wood powder and the sticking powder of tree root mix in the starch that adds after the gelatinization, after fully stirring, namely get sticky body of paste; With press molding in the sticky body of paste injection model that makes, or after the type frame of pouring into makes plates, dry, make formed body through cutting again.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011102551471A CN102318650B (en) | 2011-08-31 | 2011-08-31 | Mosquito-repellent incense with residue obtained after volatile oil extraction from typus physiologions cinnanloni leaf as base material and production method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011102551471A CN102318650B (en) | 2011-08-31 | 2011-08-31 | Mosquito-repellent incense with residue obtained after volatile oil extraction from typus physiologions cinnanloni leaf as base material and production method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102318650A CN102318650A (en) | 2012-01-18 |
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| CN104207975B (en) * | 2014-08-14 | 2016-10-05 | 华南理工大学 | A kind of perfume with anophelifuge bacteriostasis efficacy and preparation method thereof |
| CN107412830A (en) * | 2017-06-19 | 2017-12-01 | 吉安市高盛生物科技发展有限公司 | A kind of kapur and preparation method thereof |
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| CN1823949A (en) * | 2005-12-12 | 2006-08-30 | 林蔼煌 | Disinfecting pain relieving heat dispersing spirit raising medicinal liquid |
| CN101879134A (en) * | 2009-05-06 | 2010-11-10 | 许淑珠 | Multipurpose mosquito repellant water |
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