CN102258970A - Microwave reaction kettle - Google Patents

Microwave reaction kettle Download PDF

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Publication number
CN102258970A
CN102258970A CN201010181014XA CN201010181014A CN102258970A CN 102258970 A CN102258970 A CN 102258970A CN 201010181014X A CN201010181014X A CN 201010181014XA CN 201010181014 A CN201010181014 A CN 201010181014A CN 102258970 A CN102258970 A CN 102258970A
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microwave
working chamber
waveguide
sealing assembly
stainless steel
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CN201010181014XA
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CN102258970B (en
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罗代洪
罗凯
赵晓琴
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Abstract

The invention relates to a microwave reaction kettle. The microwave reaction kettle provided by the invention is characterized in that the structure comprises a microwave generator, a circulator, a water load, a tuner, a waveguide, a waveguide connector, a microwave work cavity, a wave transparent seal assembly, an interface of a reaction kettle rectangular flange and a stainless steel reaction kettle, wherein the microwave generator, the circulator, the water load, the tuner and the waveguide form microwave generation and transmission systems; the waveguide connector, the microwave work cavity and the wave transparent seal assembly form a microwave workroom with a wave transparent sealing function; the microwave workroom is connected with the side of the stainless steel reaction kettle through the interface of the reaction kettle rectangular flange; microwaves are transmitted into the microwave workroom through the transmission system to radiate wave absorption substances in the reaction kettle, thereby carrying out a heating or excitation chemical reaction; and a mode stirrer is installed in the microwave workroom, thereby improving microwave utilization.

Description

A kind of microwave reaction kettle
Technical field
The present invention relates to the new device that the microwave energy transmission technology combines with Sealing Technology, can select this device for use, belong to the chemical industry equipment field for heating and the chemical reaction of inhaling the ripple material.
Background technology
Microwave has heat for the fuel factor of inhaling the ripple material and produces internally, does not need the heat conduction, heats unique heating properties such as fast, that the temperature field is even; Research finds that also microwave has non-thermal effect to some chemical reaction, and this microwave chemical reaction has significant facilitation with respect to thermal chemical reaction, not only can improve reaction speed, shorten the reaction time, also can improve reaction conversion ratio.To these chemical reactions, have characteristics such as quick, efficient, energy-conservation.The present invention has designed a kind of microwave reaction kettle, and it is significant that microwave technology is applied to chemical field.
The present existing reactor that utilizes microwave, structure mostly are reactor and place built-in in the microwave studio, and its shortcoming is a complex structure, inconvenient operation, cost height.As Societe Prolabo " a large amount of materials are carried out the device of microwave chemical reaction " (<publication number〉CN1228910A,<application number〉97197512.4).
Summary of the invention
The objective of the invention is in order to solve: (1) microwave side imports the technology of reactor; (2) Sealing Technology between waveguide and the reactor; (3) improve the technology that microwave utilizes.
The present invention's design is to utilize the microwave energy transmission technology to combine with saturating Bomi encapsulation technique, and additional microwave working cavity with Bomi envelope function makes its suitable microwave transmission and utilization in the reactor side; Import microwave by this microwave working cavity, inhale the ripple material in the radioreaction still and heat or excite chemical reaction.
A kind of microwave reaction kettle that the present invention proposes, structure comprises microwave generator [1], circulator [2], water load [3], tuner [4], waveguide [5], waveguide connector [20], microwave working chamber [13], saturating Bomi sealing assembly [6], the interface [7] of reactor rectangular flange, stainless steel cauldron [8], and described microwave generator [1] is connected with circulator [2]; Described water load [3] is connected the lateral port of circulator [2]; Described circulator [2] is characterized in that, the side connects water load [3] and is installed between microwave generator [1] and the tuner [4]; Described tuner [4] is installed between circulator [2] and the waveguide [5]; Described waveguide [5] is installed between tuner [4] and the waveguide connector [20]; Described waveguide connector [20] is installed between waveguide [5] and the microwave working chamber [13]; Described microwave working chamber [13] is installed between waveguide connector [20] and the saturating Bomi sealing assembly [6]; Described Bomi sealing assembly [6] is characterized in that, connects microwave working chamber [13] back and is connected with stainless steel cauldron [8] by reactor rectangular flange interface [7]; Described reactor rectangular flange interface [7] is a stainless steel material, is welded on the rectangular opening place outer wall of stainless steel cauldron [8] middle and lower part, side; Described stainless steel cauldron [8] is characterised in that rectangular opening is opened in the middle and lower part of kettle side, the interface [7] of outer wall welding rectangular flange, and reactor is connected with saturating Bomi sealing assembly [6] by rectangular flange interface [7].
A kind of microwave reaction kettle that the present invention proposes, be further characterized in that, described Bomi sealing assembly [6], form by black box base [9], saturating ripple division board [11], black box cover plate [10], gasket seal [12], described black box base [9], be stainless steel, aluminium or copper product, it is characterized in that it is shaped as the shaped as frame of band groove; Described black box cover plate [10] is stainless steel, aluminium or copper product, it is characterized in that, it is shaped as the shaped as frame of band projection; Described ripple division board [11] is glass, microwave ceramics or tetrafluoroethene material, it is characterized in that, both sides add gasket seal [12] respectively and are installed between black box base [9] and the black box cover plate [10]; Described gasket seal [12] is glue, tetrafluoroethene or polyamine fat material; Described microwave working chamber [13] is a stainless steel, aluminium or copper product, cavity size is relevant with the wavelength that microwave generator [1] produces microwave, it is characterized in that, be divided into by shape bucket shape is arranged, rectangle, compound three kinds, by being divided into two kinds of solder type and flange-types with saturating Bomi sealing assembly [6] connected mode, described rectangle microwave working chamber, it is characterized in that, cavity is a rectangle, cavity top is connected with a breather pipe [16], the bottom connects the pipe [15] that leaks hunting, and the end that microwave working chamber [13] connects waveguide connector [20] has mode stirrer [14] axis hole [17], is installed between waveguide connector [20] and the saturating Bomi sealing assembly [6]; Described bucket shape microwave working chamber is characterized in that cavity is a bucket shape, and its cross section can be circle, rectangle or polygon, and cavity top is connected with a breather pipe [16], and the bottom connects the pipe [15] that leaks hunting, and is installed in and waveguide [5] and thoroughly between the Bomi sealing assembly [6]; Described compound microwave working chamber, it is characterized in that, cavity is made of for two sections bucket shape section and rectangle, cavity and waveguide [5] link is a bucket shape, with saturating Bomi sealing assembly [6] link be rectangle, bucket shape section cross section can be circle, rectangle or polygon, the rectangular section size is greater than the bucket shape section, be connected with a breather pipe [16], bottom on rectangular section cavity top and connect the pipe [15] that leaks hunting, rectangular section cavity platform has mode stirrer [14] axis hole [17] and bracing strut [18] is installed, be installed in and waveguide [5] and saturating Bomi sealing assembly [6] between; Described solder type microwave working chamber is characterized in that, working chamber and saturating Bomi sealing assembly [6] are by being welded to connect; Described flange-type microwave working chamber is characterized in that, working chamber is connected by the flange mode with saturating Bomi sealing assembly [6]; Described waveguide connector [20], it is characterized in that, its with rectangle adpting flange [19] that microwave working chamber [13] is connected on have mode stirrer [14] axis hole [17] and bracing strut [18] be housed, be installed between waveguide [5] and the rectangle microwave working chamber [13], be used for Installation Modes agitator [14]; Described mode stirrer [14] is stainless steel, aluminium or copper product, it is characterized in that, 3-6 reflecting surface arranged, and is installed in the microwave working chamber [13]; Described breather pipe [15] is characterized in that, is stainless steel, aluminium or copper product, is installed in microwave working chamber [13] cavity top; The described pipe [16] that leaks hunting is characterized in that, be stainless steel, aluminium or copper product be installed in microwave working chamber [13] cavity bottom; Described mode stirrer [14] bracing strut [18] is stainless steel, aluminium or copper product.
Description of drawings
Further specify details of the present invention below in conjunction with accompanying drawing
The present invention has 13 accompanying drawings:
Fig. 1 is the cross-sectional view of a kind of waveguide connector in apparatus of the present invention
Fig. 2 is the cross-sectional view of saturating Bomi sealing assembly cover plate in apparatus of the present invention
Fig. 3 is a saturating Bomi sealing assembly base cross-sectional view in apparatus of the present invention
Fig. 4 is the cross-sectional view of a kind of flange-type rectangle microwave working chamber in apparatus of the present invention
Fig. 5 is the cross-sectional view of a kind of solder type rectangle microwave working chamber in apparatus of the present invention
Fig. 6 is the cross-sectional view of a kind of flange-type bucket shape microwave working chamber in apparatus of the present invention
Fig. 7 is the cross-sectional view of a kind of solder type bucket shape microwave working chamber in apparatus of the present invention
Fig. 8 is the cross-sectional view of a kind of flange-type composite microwave working chamber in apparatus of the present invention
Fig. 9 is the cross-sectional view of a kind of solder type composite microwave working chamber in apparatus of the present invention
Figure 10 is the arrangement relation cross-sectional view of waveguide connector in apparatus of the present invention, solder type rectangle microwave working chamber, mode stirrer, saturating Bomi sealing assembly parts
Figure 11 is the integral planar arrangement relation structural representation that installs among first kind of embodiment of the present invention
Figure 12 is the part section structural representation that installs among first kind of embodiment of the present invention
Figure 13 is the part section structural representation that installs among second kind of embodiment of the present invention
Fig. 1 is the cross-sectional view of a kind of waveguide connector in apparatus of the present invention, described waveguide connector [20], it is characterized in that, have mode stirrer [14] axis hole [17] and bracing strut [18] is housed on the rectangle adpting flange [19] of itself and microwave working chamber [13] link
Fig. 2 is the cross-sectional view of saturating Bomi sealing assembly cover plate in apparatus of the present invention, and described black box base [9] is characterised in that, it is shaped as the shaped as frame of band groove.
Fig. 3 is a saturating Bomi sealing assembly base cross-sectional view in apparatus of the present invention, and described black box cover plate [10] is characterised in that, it is shaped as the shaped as frame of band projection.
Fig. 4 is the cross-sectional view of a kind of flange-type rectangle microwave working chamber in apparatus of the present invention, flange-type rectangle microwave working chamber of the present invention, it is characterized in that, cavity is a rectangle, cavity top is connected with a breather pipe [16], the bottom connects the pipe [15] that leaks hunting, the end that microwave working chamber [13] connects waveguide connector [20] has mode stirrer [14] axis hole [17], inner horizontal Installation Modes agitator [14], be installed between waveguide connector [20] and the saturating Bomi sealing assembly [6], be connected by rectangle adpting flange [19] with saturating Bomi sealing assembly base [9].
Fig. 5 is the cross-sectional view of a kind of solder type rectangle microwave working chamber in apparatus of the present invention, and solder type rectangle microwave working chamber of the present invention is characterized in that, with saturating Bomi sealing assembly base [9] by being welded to connect.
Fig. 6 is the cross-sectional view of a kind of flange-type bucket shape microwave working chamber in apparatus of the present invention, flange-type bucket shape microwave working chamber of the present invention, it is characterized in that, cavity is a bucket shape, its cross section can be circle, rectangle or polygon, and cavity top is connected with a breather pipe [16], and the bottom connects the pipe [15] that leaks hunting, be installed in and waveguide [5] and saturating Bomi sealing assembly [6] between, be connected by rectangle adpting flange [19] with saturating Bomi sealing assembly base [9].
Fig. 7 is a kind of solder type bucket shape microwave working chamber in apparatus of the present invention, and solder type bucket shape microwave working chamber of the present invention is characterized in that, with saturating Bomi sealing assembly base [9] by being welded to connect.
Fig. 8 is the cross-sectional view of a kind of flange-type composite microwave working chamber in apparatus of the present invention, the compound microwave working chamber of described flange-type, it is characterized in that, cavity is made of bucket shape section and rectangular section two parts, cavity and waveguide [5] link is a bucket shape, with saturating Bomi sealing assembly [6] link be rectangle, bucket shape section cross section can be circle, rectangle or polygon, the rectangular section size is greater than the bucket shape section, be connected with a breather pipe [16] on rectangular section cavity top, the bottom connects the pipe [15] that leaks hunting, rectangular section cavity platform has mode stirrer [14] axis hole [17] and bracing strut [18] is installed, be installed in and waveguide [5] and saturating Bomi sealing assembly [6] between, rectangular end is connected by rectangle adpting flange [19] with base [9].
Fig. 9 is the cross-sectional view of a kind of solder type composite microwave working chamber in apparatus of the present invention, and solder type composite microwave working chamber of the present invention is characterized in that, with saturating Bomi sealing assembly base [9] by being welded to connect.
Figure 10 is the waveguide connector, solder type rectangle microwave working chamber, mode stirrer in apparatus of the present invention, the arrangement relation cross-sectional view of saturating Bomi sealing assembly parts, it is characterized in that, rectangle microwave working chamber [13] is welded on the base [9] of Bomi sealing assembly [6] and goes up composition one solder type rectangle microwave working chamber, is installed between waveguide connector [20] and the saturating Bomi sealing assembly cover plate [10]; Described ripple division board [11], both sides add respectively gasket seal [12] be installed in Bomi sealing assembly base [9] groove and cover plate [10] convex surface between; Described mode stirrer [14] is installed in the microwave working chamber [13] by the bracing strut [18] on the waveguide connector [20].
Embodiment 1
Figure 11 is the integral planar arrangement relation structural representation that installs among first kind of embodiment of the present invention
The microwave that microwave generator [1] produces successively circulator [2], tuner [4], waveguide [5], microwave working chamber [13], the saturating Bomi sealing assembly [6] by water load [3] are installed, be transmitted to stainless steel cauldron [8], inhale the ripple material in the radioreaction still and heat or excite chemical reaction.
Microwave generator [1] is connected with circulator [2]; Water load [3] is connected the side of circulator [2]; Circulator [2] side connects water load [3], is installed between microwave generator [1] and the tuner [4]; Tuner [4] is installed between circulator [2] and the waveguide [5]; Described waveguide [5] is installed between tuner [4] and the waveguide connector [20]; Described waveguide connector [20] is installed between waveguide [5] and the microwave working chamber [13]; Described microwave working chamber [13] is installed between waveguide connector [20] and the saturating Bomi sealing assembly [6]; Described Bomi sealing assembly [6] is installed in the opening part inboard, middle and lower part of stainless steel cauldron [8] kettle side by the interface [7] of the outer rectangular flange of reactor.Figure 12 is the part section structural representation that installs among first kind of embodiment of the present invention
Described stainless steel cauldron [8] is characterised in that, the interface [7] of the middle and lower part opening part outer wall welding reactor rectangular flange of kettle side; Described Bomi sealing assembly [6] is characterized in that, is installed in the opening part inboard, middle and lower part of stainless steel cauldron [8] kettle side by the interface [7] of reactor rectangular flange; Described microwave working chamber [13], it is characterized in that, cavity is a rectangle, cavity top is connected with a breather pipe [16], the bottom connects the pipe [15] that leaks hunting, and is installed between waveguide connector [20] and the saturating Bomi sealing assembly [6], and it is further characterized in that, the horizontal Installation Modes agitator [14] of microwave working chamber [13] and waveguide [5] link inside is welded to connect formation one solder type rectangle microwave working chamber with black box base [9]; Described waveguide connector [20] is characterized in that, its with rectangle adpting flange [19] that microwave working chamber [13] is connected on mode stirrer [14] bracing strut [18] is installed.Described mode stirrer [14] is characterized in that, goes up bracing strut [18] by waveguide connector [20] and is installed in the solder type rectangle microwave working chamber.
Embodiment 2
Figure 13 is the part section structural representation that installs among second kind of embodiment of the present invention
Described stainless steel cauldron [8] is characterised in that, the interface [7] of the middle and lower part opening part outer wall welding one band rectangular flange of kettle side, and stainless steel cauldron [8] links to each other with saturating Bomi sealing assembly [6] by the interface [7] of rectangular flange; Described Bomi sealing assembly [6] is characterized in that, is installed between the interface [7] and microwave working chamber [13] of stainless steel cauldron [8] rectangular flange; Described microwave working chamber [13], it is characterized in that, cavity is a rectangle, cavity top is connected with a breather pipe [16], the bottom connects the pipe [15] that leaks hunting, and is installed between waveguide connector [20] and the saturating Bomi sealing assembly [6], and it is further characterized in that, the horizontal Installation Modes agitator [14] of microwave working chamber [13] and waveguide [5] link inside, microwave working chamber [13] are welded to connect with black box base [9] and constitute a solder type rectangle microwave working chamber; Described waveguide connector [20] is characterized in that, its with rectangle adpting flange [19] that microwave working chamber [13] is connected on mode stirrer [14] bracing strut [18] is installed.Described mode stirrer [14] is characterized in that, goes up bracing strut [18] by waveguide connector [20] and is installed in the solder type rectangle microwave working chamber.

Claims (4)

1. microwave reaction kettle, structure comprises microwave generator [1], circulator [2], water load [3], tuner [4], waveguide [5], waveguide connector [20], microwave working chamber [13], saturating Bomi sealing assembly [6], the interface [7] of reactor rectangular flange, stainless steel cauldron [8], and described microwave generator [1] is connected with circulator [2]; Described water load [3] is connected the lateral port of circulator [2]; Described circulator [2] is characterized in that, the side connects water load [3] and is installed between microwave generator [1] and the tuner [4]; Described tuner [4] is installed between circulator [2] and the waveguide [5]; Described waveguide [5] is installed between tuner [4] and the waveguide connector [20]; Described waveguide connector [20] is installed between waveguide [5] and the microwave working chamber [13]; Described microwave working chamber [13] is installed between waveguide connector [20] and the saturating Bomi sealing assembly [6]; Described Bomi sealing assembly [6] is characterized in that, connects microwave working chamber [13] back and is connected with stainless steel cauldron [8] by reactor rectangular flange interface [7]; Described reactor rectangular flange interface [7] is a stainless steel material, is welded on the rectangular opening place outer wall of stainless steel cauldron [8] middle and lower part, side; Described stainless steel cauldron [8] is characterised in that rectangular opening is opened in the middle and lower part of kettle side, the interface [7] of outer wall welding rectangular flange, and reactor is connected with saturating Bomi sealing assembly [6] by rectangular flange interface [7].
2. according to the described microwave reaction kettle of claim 1, it is characterized in that, described Bomi sealing assembly [6], form by black box base [9], saturating ripple division board [11], black box cover plate [10], gasket seal [12], described black box base [9], be stainless steel, aluminium or copper product, it is characterized in that it is shaped as the shaped as frame of band groove; Described black box cover plate [10] is stainless steel, aluminium or copper product, it is characterized in that, it is shaped as the shaped as frame of band projection; Described ripple division board [11] is glass, microwave ceramics or tetrafluoroethene material, it is characterized in that, both sides add gasket seal [12] respectively and are installed between black box base [9] and the black box cover plate [10]; Described gasket seal [12] is glue, tetrafluoroethene or polyamine fat material.
3. according to claim 1 or 2 described microwave reaction kettles, it is characterized in that, described microwave working chamber [13] is a stainless steel, aluminium or copper product, cavity size is relevant with the wavelength that microwave generator [1] produces microwave, it is characterized in that, be divided into by shape bucket shape is arranged, rectangle, compound three kinds, by being divided into two kinds of solder type and flange-types with saturating Bomi sealing assembly [6] connected mode, described rectangle microwave working chamber, it is characterized in that, cavity is a rectangle, cavity top is connected with a breather pipe [16], the bottom connects the pipe [15] that leaks hunting, and the end that microwave working chamber [13] connects waveguide connector [20] has mode stirrer [14] axis hole [17], is installed between waveguide connector [20] and the saturating Bomi sealing assembly [6]; Described bucket shape microwave working chamber is characterized in that cavity is a bucket shape, and its cross section can be circle, rectangle or polygon, and cavity top is connected with a breather pipe [16], and the bottom connects the pipe [15] that leaks hunting, and is installed in and waveguide [5] and thoroughly between the Bomi sealing assembly [6]; Described compound microwave working chamber, it is characterized in that, cavity is made of for two sections bucket shape section and rectangle, cavity and waveguide [5] link is a bucket shape, with saturating Bomi sealing assembly [6] link be rectangle, bucket shape section cross section can be circle, rectangle or polygon, the rectangular section size is greater than the bucket shape section, rectangular section cavity top is connected with a breather pipe [16], the bottom connects the pipe [15] that leaks hunting, rectangular section cavity platform has mode stirrer [14] axis hole [17] and bracing strut [18] is installed, be installed in and waveguide [5] and saturating Bomi sealing assembly [6] between; Described solder type microwave working chamber is characterized in that, working chamber and saturating Bomi sealing assembly [6] are by being welded to connect; Described flange-type microwave working chamber is characterized in that, working chamber is connected by the flange mode with saturating Bomi sealing assembly [6].
4. according to claim 1 or 3 described microwave reaction kettles, it is characterized in that, described waveguide connector [20], it is characterized in that, its with rectangle adpting flange [19] that microwave working chamber [13] is connected on have mode stirrer [14] axis hole [17] and bracing strut [18] be housed, be installed between waveguide [5] and the rectangle microwave working chamber [13], be used for Installation Modes agitator [14]; Described mode stirrer [14] is stainless steel, aluminium or copper product, it is characterized in that, 3-6 reflecting surface arranged, and is installed in the microwave working chamber [13]; Described breather pipe [15] is characterized in that, is stainless steel, aluminium or copper product, is installed in microwave working chamber [13] cavity top; The described pipe [16] that leaks hunting is characterized in that, be stainless steel, aluminium or copper product be installed in microwave working chamber [13] cavity bottom; Described mode stirrer [14] bracing strut [18] is stainless steel, aluminium or copper product.
CN201010181014.XA 2010-05-25 2010-05-25 Microwave reaction kettle Expired - Fee Related CN102258970B (en)

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Cited By (7)

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Publication number Priority date Publication date Assignee Title
CN103623755A (en) * 2013-11-18 2014-03-12 陕西科技大学 Industrial continuous type microwave reactor
CN103623756A (en) * 2013-11-18 2014-03-12 陕西科技大学 Industrial batch-type microwave reaction kettle
CN106215801A (en) * 2016-08-29 2016-12-14 贵州苗仁堂制药有限责任公司 Chinese medicine blender
CN106658803A (en) * 2016-10-20 2017-05-10 上海海洋大学 Heating device capable of adjusting microwave energy distribution
CN109250885A (en) * 2018-10-23 2019-01-22 新疆中科天沐生态环保股份有限公司 A kind of processing method of oil gas field oily sludge
CN110449099A (en) * 2019-09-16 2019-11-15 四川大学 A kind of chemical reactor based on microwave separation field reconfiguration technique
CN115742438A (en) * 2022-10-21 2023-03-07 华为数字能源技术有限公司 Die-casting forming method, die and compression molding device

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Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103623755A (en) * 2013-11-18 2014-03-12 陕西科技大学 Industrial continuous type microwave reactor
CN103623756A (en) * 2013-11-18 2014-03-12 陕西科技大学 Industrial batch-type microwave reaction kettle
CN103623755B (en) * 2013-11-18 2016-02-10 陕西科技大学 Industrialization continuous type microwave reactor
CN106215801A (en) * 2016-08-29 2016-12-14 贵州苗仁堂制药有限责任公司 Chinese medicine blender
CN106658803A (en) * 2016-10-20 2017-05-10 上海海洋大学 Heating device capable of adjusting microwave energy distribution
CN106658803B (en) * 2016-10-20 2023-06-20 上海海洋大学 Heating device capable of adjusting microwave energy distribution
CN109250885A (en) * 2018-10-23 2019-01-22 新疆中科天沐生态环保股份有限公司 A kind of processing method of oil gas field oily sludge
CN110449099A (en) * 2019-09-16 2019-11-15 四川大学 A kind of chemical reactor based on microwave separation field reconfiguration technique
CN115742438A (en) * 2022-10-21 2023-03-07 华为数字能源技术有限公司 Die-casting forming method, die and compression molding device

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