CN102243156A - Cup-shaped water sample online filtering device - Google Patents

Cup-shaped water sample online filtering device Download PDF

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Publication number
CN102243156A
CN102243156A CN2011100995393A CN201110099539A CN102243156A CN 102243156 A CN102243156 A CN 102243156A CN 2011100995393 A CN2011100995393 A CN 2011100995393A CN 201110099539 A CN201110099539 A CN 201110099539A CN 102243156 A CN102243156 A CN 102243156A
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cup
water sample
cup body
gland
water
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CN2011100995393A
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周小平
周紫光
周国平
万众欢
奚森斌
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Shanghai Mtw Automatic Control Equipment & Engineering Co ltd
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Shanghai Mtw Automatic Control Equipment & Engineering Co ltd
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Abstract

The invention discloses a cup-shaped water sample online filtering device, belonging to the technical field of water quality online analysis. The cup-shaped water sample online filtering device is characterized in that a water sample inlet and a cleaning water inlet are arranged at the top of a gland liner, a liquid level switch is fixedly connected with the top of the gland liner, a clapboard of which the periphery is fixedly connected with an internal side face of a cup body is arranged in the central section of the cup body, a part above the clapboard is an upper cup body while a part below the clapboard is a lower cup body, a water permeable hole is axially arranged on the clapboard so as to communicate the upper cup body with the lower cup body, and filter leaves are arranged between the part above the clapboard and an edge of a lower end of the gland liner. The cup-shaped water sample online filtering device has the advantages of simple structure and convenience in operation. Sample introduction quantity and filtering are controlled by upper limit and lower limit of the liquid level switch, procedures of sample introduction, sampling, cleaning, discharging and the like all can be automatically controlled by opening and closing a valve connected with the water sample inlet and a water sample outlet, and the filter leaves can be replaced very simply and conveniently, so that the cup-shaped water sample online filtering device is suitable for water sample online automatic filtering, particularly for occasions where effective decontamination is needed for measuring the water sample of a soluble object to be measured by using a photometry analyzer.

Description

一种杯式水样在线过滤装置A cup-type water sample on-line filtration device

技术领域 technical field

本发明属水质在线分析技术领域,涉及一种地表水水质分析测试领域的水样预处理过滤装置,可应用于可溶性待测物光度法分析测试的水样预处理。 The invention belongs to the technical field of online water quality analysis, and relates to a water sample pretreatment filter device in the field of surface water quality analysis and testing, which can be applied to water sample pretreatment for photometric analysis and testing of soluble analytes.

背景技术 Background technique

污水排放必须达到环境保护排放标准,水污染各项指标的在线自动监测是环境保护工作中重要一环。在水质分析测试行业内,分光光度法是常用的仪器分析方法之一,但较高浊度(浊度高于50NTU)的存在会严重影响光度法分析仪器的正确测量。化学实验室用于水样过滤的市售商品有锥形漏斗和抽滤漏斗,但锥形漏斗和抽滤漏斗等产品都无法应用于水质在线自动监测系统的水样在线自动过滤。特别是需要使用光度法分析仪测量可溶性待测物水样场合,能应用于水质自动监测系统中并能有效地去除浊度的水样在线自动过滤装置尚属空白。 Sewage discharge must meet environmental protection discharge standards, and online automatic monitoring of various indicators of water pollution is an important part of environmental protection work. In the water quality analysis and testing industry, spectrophotometry is one of the commonly used instrumental analysis methods, but the existence of high turbidity (turbidity higher than 50NTU) will seriously affect the correct measurement of photometric analysis instruments. Commercially available products for water sample filtration in chemical laboratories include conical funnels and suction funnels, but products such as conical funnels and suction funnels cannot be applied to the online automatic filtration of water samples in the online automatic monitoring system for water quality. Especially when photometric analyzers are required to measure water samples of soluble analytes, an online automatic filter device for water samples that can be applied to an automatic water quality monitoring system and can effectively remove turbidity is still blank.

发明内容 Contents of the invention

本发明的目的在于,提供一种能应用于水质在线自动监测系统的,且能有效去除水样浊度的杯式水样在线过滤装置。 The object of the present invention is to provide a cup-type water sample on-line filter device that can be applied to an online automatic water quality monitoring system and can effectively remove the turbidity of the water sample.

为达到上述目的,采用的技术方案是:一种杯式水样在线过滤装置,包括压盖衬筒、杯体和滤片,其特征在于:所述压盖衬筒的顶端置有水样进口和清洗水进口,液位开关与压盖衬筒顶端固定连接,压盖衬筒上端一侧置有溢流口、下端一侧置有压盖衬筒排放口;杯体中部置有四周与所述杯体内侧面固定连接的隔板,所述隔板以上为上杯体,隔板以下为下杯体,隔板上轴向置有的透水孔连通上杯体和下杯体,所述上杯体下端一侧置有上杯体排放口,所述上杯体的内径与所述压盖衬筒的外径吻合匹配,所述上杯体排放口与所述压盖衬筒排放口的位置口径对应一致,下杯体上端侧面置有清洗水进口、下端侧面置有取样口、正中下端为下杯体排放口;隔板上方与压盖衬筒的下端边沿之间置有滤片。 In order to achieve the above purpose, the technical solution adopted is: a cup-type water sample on-line filter device, including a gland liner, a cup body and a filter piece, characterized in that: the top of the gland liner is equipped with a water sample inlet and the cleaning water inlet, the liquid level switch is fixedly connected with the top of the gland liner, the upper side of the gland liner is equipped with an overflow port, and the lower end of the gland liner is equipped with a discharge port of the gland liner; Above the partition is the upper cup, below the partition is the lower cup, and the water permeable holes arranged in the axial direction on the partition are connected to the upper cup and the lower cup. There is an upper cup discharge port on the lower end of the cup body, the inner diameter of the upper cup body matches the outer diameter of the gland liner, and the upper cup discharge port matches the gland liner discharge port. The position and caliber correspond to each other. There is a cleaning water inlet on the upper side of the lower cup, a sampling port on the lower side, and a discharge port on the lower center of the lower cup. A filter is placed between the top of the partition and the lower edge of the gland liner.

所述滤片可以是任何片状的过滤材料,如滤纸、滤膜、滤网等。 The filter sheet can be any sheet-shaped filter material, such as filter paper, filter membrane, filter screen and the like.

所述滤片与所述压盖衬筒的下端边沿之间置有密封垫。 A gasket is placed between the filter piece and the lower edge of the gland liner.

所述压盖衬筒与所述上杯体端部边沿螺纹连接。 The gland liner is threadedly connected to the end edge of the upper cup body.

本发明的有益效果是:结构简单、操作方便。进样总量和过滤完成由液位开关的上下限自动控制,进样、采样、清洗、排放等程序均可通过与水样进出口相连的阀门的开启和关闭实现自动控制,所述滤片可以根据过滤的水样中颗粒物和悬浮物含量的多少选择,更换滤片操作相当简便,只要松开压盖上的手拧螺丝或活扣将压盖衬筒抽出即可。本发明适用于水样在线自动过滤,特别适用于使用光度法分析仪测量可溶性待测物水样需要有效地去除浊度的场合。 The invention has the beneficial effects of simple structure and convenient operation. The total amount of sample injection and the completion of filtration are automatically controlled by the upper and lower limits of the liquid level switch. The procedures of sample injection, sampling, cleaning, and discharge can all be automatically controlled by opening and closing the valve connected to the inlet and outlet of the water sample. It can be selected according to the content of particles and suspended solids in the filtered water sample. It is very simple to replace the filter, just loosen the thumb screw or snap button on the gland to pull out the gland liner. The invention is suitable for on-line automatic filtration of water samples, and is especially suitable for occasions where turbidity needs to be effectively removed when using a photometric analyzer to measure water samples of soluble analytes.

附图说明 Description of drawings

以下通过附图说明和实施例对本发明作进一步说明。 The present invention will be further described below by means of drawings and examples.

图1为本发明结构示意图(剖视); Fig. 1 is a structural representation (section) of the present invention;

图2为本发明分解结构示意图(剖视)。 Fig. 2 is a schematic diagram (sectional view) of an exploded structure of the present invention.

图中,1-压盖衬筒;2-滤片;3-杯体;4-隔板;5-密封垫;6-液位开关;7-水样进口;8-清洗水进口;9-螺钉;10-溢流口;11-压盖衬筒排放口;12-上杯体排放口;13-下杯体清洗水进口;14-下杯体排放口;15-取样口。 In the figure, 1-gland liner; 2-filter; 3-cup body; 4-partition; 5-sealing gasket; 6-liquid level switch; 7-water sample inlet; 8-cleaning water inlet; 9- Screw; 10-overflow port; 11-gland liner discharge port; 12-upper cup discharge port; 13-lower cup cleaning water inlet; 14-lower cup discharge port; 15-sampling port.

具体实施方式 Detailed ways

图1为本发明结构示意图,图2为本发明分解结构示意图。由图可见一种杯式水样在线自动过滤装置,包括压盖衬筒1、杯体3和滤片2,其特征在于:所述压盖衬筒1的顶端置有水样进口7和清洗水进口8,液位开关6与压盖衬筒1顶端固定连接,压盖衬筒1上端一侧有溢流口10、下端一侧有压盖衬筒排放口11;杯体3中部置有四周与所述杯体3内侧面固定连接的隔板4,所述隔板4以上为上杯体,隔板4以下为下杯体,隔板4上轴向置有的透水孔连通上杯体和下杯体,所述上杯体下端一侧有上杯体排放口12,所述上杯体的内径与所述压盖衬筒1的外径吻合匹配,所述上杯体排放口12与所述压盖衬筒排放口11的位置口径对应一致,下杯体上端侧面有下杯体清洗水进口13和透气口、下端侧面有取样口15、正中下端为下杯体排放口14;隔板4上方与压盖衬筒1的下端边沿之间置有滤片2。 Fig. 1 is a schematic diagram of the structure of the present invention, and Fig. 2 is a schematic diagram of the decomposition structure of the present invention. It can be seen from the figure that a cup-type water sample online automatic filtration device includes a gland liner 1, a cup body 3 and a filter piece 2. It is characterized in that: the top of the gland liner 1 is provided with a water sample inlet 7 and a cleaning The water inlet 8, the liquid level switch 6 are fixedly connected to the top of the gland liner 1, the gland liner 1 has an overflow port 10 on the upper side, and a gland liner discharge port 11 on the lower side; the cup body 3 has a A partition 4 that is fixedly connected to the inner surface of the cup body 3 around, the upper cup body is above the partition board 4, and the lower cup body is below the partition board 4, and the permeable hole provided on the upper axis of the partition board 4 is connected to the upper cup body. body and the lower cup body, the lower end side of the upper cup body has an upper cup body discharge port 12, the inner diameter of the upper cup body matches the outer diameter of the gland liner 1, and the upper cup body discharge port 12 corresponds to the position and diameter of the gland liner discharge port 11, the upper side of the lower cup body has a lower cup body cleaning water inlet 13 and an air vent, the lower side has a sampling port 15, and the middle and lower end is the lower cup body discharge port 14 ; There is a filter 2 between the top of the separator 4 and the lower edge of the gland liner 1 .

所述滤片2可以是任何片状的过滤材料,如滤纸、滤膜、滤网等。 The filter sheet 2 can be any sheet-shaped filter material, such as filter paper, filter membrane, filter screen and the like.

所述滤片2与压盖衬筒1的下端边沿之间置有密封垫5。 A gasket 5 is placed between the filter piece 2 and the lower edge of the gland liner 1 .

所述压盖衬筒1与所述上杯体端部边沿螺纹9连接。 The gland liner 1 is connected with the edge thread 9 at the end of the upper cup body.

以下以应用于水质在线自动监测系统的本发明为例,作进一步描述。本发明主要由压盖衬筒1、液位开关6、滤片2和杯体3构成,整体呈圆柱形。杯体3和压盖衬筒1由优质高强度耐酸碱有机玻璃成型制成,杯体3内径为130mm,压盖衬筒1的外径为125mm,所有管件接头均采用6mm市售优质塑料接头,采用一层直径为125mm的中速定量滤纸作为滤片2,滤纸和压盖衬筒1的末端之间用环片状橡胶密封垫5密封,压盖衬筒1和杯体3之间用四个6mm手拧螺钉螺纹连接紧固时,隔板4、滤纸2、密封垫5与压盖衬筒1末端之间就形成很好的密封效果。所有水样进口或清洗水进口、各排放口均分别连接相应阀门,如下杯体排放口14与下杯体排放阀连接,水样排放与否受所述排放阀控制。 The following takes the present invention applied to the online automatic monitoring system of water quality as an example for further description. The present invention is mainly composed of a gland liner 1, a liquid level switch 6, a filter piece 2 and a cup body 3, and the whole is cylindrical. The cup body 3 and the gland liner 1 are made of high-quality high-strength acid and alkali resistant plexiglass. The inner diameter of the cup body 3 is 130mm, and the outer diameter of the gland liner 1 is 125mm. All pipe joints are made of 6mm commercially available high-quality plastic The joint adopts a layer of medium-speed quantitative filter paper with a diameter of 125mm as the filter piece 2. The end of the filter paper and the end of the gland liner 1 is sealed with a ring-shaped rubber gasket 5, and the space between the gland liner 1 and the cup body 3 is sealed. When fastened with four 6mm thumb screws, a good sealing effect is formed between the separator 4, the filter paper 2, the sealing gasket 5 and the end of the gland liner 1. All water sample inlets or cleaning water inlets, and each discharge port are respectively connected to corresponding valves. The lower cup body discharge port 14 is connected to the lower cup body discharge valve, and whether the water sample is discharged is controlled by the discharge valve.

装置工作时,水样从水样进口7进入压盖衬筒1内部,当压盖衬筒1内部的液位上升,推动液位开关6的浮子到达开关高限时,停止进样。液位开关6的高低限位可根据需要预先进行人工调节固定,以控制进样总量,确保水量满足分析测试需要又不至于冗余过多。压盖衬筒1内的水及水溶性物质,在自身重力的作用下渗透滤片2,通过隔板4的透水孔流入并储存于下杯体中,而水样中泥沙等不溶性颗粒物和悬浮物则被滤片2截留,从而达到过滤的目的。当液位开关6的浮子随着压盖衬筒1内水位的下降到达开关下限时,过滤完成。过滤后的水样通过杯体3下方的取样口15可直接供分析测试使用。采样完毕后,下杯体排放阀打开,将剩余的水样从下杯体排放口14排出,同时,清洗水阀、上杯体排放阀打开,清洗水从清洗水进口8进入压盖衬筒1内部,并从压盖衬筒排放口11和上杯体排放口12流出,从而形成对压盖衬筒1内部和滤片2的清洗。清洗水从下杯体清洗水进口13进入下杯体,并从下杯体排放口14流出,从而形成对下杯体的清洗,清洗完毕,清洗水阀、上杯体排放阀和下杯体排放阀依次关闭,整个周期过程完毕。 When the device is working, the water sample enters the gland liner 1 from the water sample inlet 7. When the liquid level inside the gland liner 1 rises and the float of the liquid level switch 6 reaches the upper limit of the switch, the sample injection is stopped. The high and low limits of the liquid level switch 6 can be manually adjusted and fixed in advance as required to control the total amount of sample injection and ensure that the water volume meets the needs of analysis and testing without excessive redundancy. The water and water-soluble substances in the gland liner 1 permeate the filter piece 2 under the action of its own gravity, flow into and store in the lower cup through the permeable holes of the partition plate 4, and the insoluble particles such as sediment in the water sample and Suspended matter is intercepted by the filter sheet 2, so as to achieve the purpose of filtration. When the float of the liquid level switch 6 reaches the lower limit of the switch along with the drop of the water level in the gland liner 1, the filtration is completed. The filtered water sample can be directly used for analysis and testing through the sampling port 15 below the cup body 3 . After the sampling is completed, the discharge valve of the lower cup is opened, and the remaining water samples are discharged from the discharge port 14 of the lower cup. At the same time, the cleaning water valve and the discharge valve of the upper cup are opened, and the cleaning water enters the gland liner from the cleaning water inlet 8 1, and flow out from the discharge port 11 of the gland liner and the discharge port 12 of the upper cup body, thereby forming the cleaning of the interior of the gland liner 1 and the filter disc 2. The cleaning water enters the lower cup body from the cleaning water inlet 13 of the lower cup body, and flows out from the discharge port 14 of the lower cup body, thereby forming the cleaning of the lower cup body. After cleaning, the cleaning water valve, the upper cup body discharge valve and the lower cup body The discharge valves are closed one by one, and the whole cycle process is completed.

滤片2使用一段时间后需要更换,由人工操作,松开压盖衬筒1上的螺钉9或活扣将压盖衬筒1抽出,即可对滤片2进行更换,操作相当简便。滤片2的更换频率,受所过滤的水样中颗粒物和悬浮物含量的多少、过滤水样的总量以及滤片材质结构的影响,视实际应用情况而定。 The filter disc 2 needs to be replaced after being used for a period of time. By manual operation, loosen the screw 9 or the snap button on the gland liner 1 to extract the gland liner 1, and then the filter disc 2 can be replaced. The operation is quite simple. The replacement frequency of the filter sheet 2 is affected by the amount of particles and suspended solids in the filtered water sample, the total amount of the filtered water sample, and the material structure of the filter sheet, depending on the actual application situation.

Claims (4)

1. cup type water sample on-line filtration device, comprise gland lining, cup and filter disc, it is characterized in that: the top of described gland lining is equipped with water sample import and rinse water import, level switch is fixedlyed connected with gland lining top, and gland lining upper end one side has overflow vent, lower end one side that gland lining floss hole is arranged; The dividing plate of fixedlying connected with described cup medial surface around the cup middle part is equipped with, described dividing plate is above to be last cup, dividing plate is following to be lower cup body, the permeable hole that axially is equipped with on the dividing plate is communicated with goes up cup and lower cup body, described cup lower end one side of going up has last cup floss hole, the described identical coupling of external diameter that goes up the internal diameter and the described gland lining of cup, described upward the cup floss hole is corresponding consistent with the position bore of described gland lining floss hole, and the lower cup body upper side is equipped with the rinse water import, lower end side is equipped with sample tap, hits exactly the lower end is the lower cup body floss hole; Be equipped with filter disc between the edge, lower end of dividing plate top and gland lining.
2. according to the described a kind of cup type water sample on-line filtration device of claim 1, it is characterized in that: described filter disc is the filtering material of sheet.
3. according to the described a kind of cup type water sample on-line filtration device of claim 1, it is characterized in that: be equipped with sealing gasket between the edge, lower end of described filter disc and described gland lining.
4. according to the described a kind of cup type water sample on-line filtration device of claim 1, it is characterized in that: described gland lining is threaded with the edge, upper end of described cup.
CN2011100995393A 2011-04-20 2011-04-20 Cup-shaped water sample online filtering device Pending CN102243156A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103698194A (en) * 2013-11-04 2014-04-02 浙江省海洋水产研究所 A water sample filtration device
CN106644580A (en) * 2016-11-21 2017-05-10 成都格瑞思文化传播有限公司 Water sampler
CN107727435A (en) * 2017-09-13 2018-02-23 新疆电力建设调试所有限责任公司 Total organic carbon on-line checking sampler
CN109238909A (en) * 2018-11-21 2019-01-18 扬州大学 A kind of device and method of portable measurement sewage solid suspension content

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103698194A (en) * 2013-11-04 2014-04-02 浙江省海洋水产研究所 A water sample filtration device
CN103698194B (en) * 2013-11-04 2015-12-30 浙江省海洋水产研究所 A kind of water sample suction filtration device
CN106644580A (en) * 2016-11-21 2017-05-10 成都格瑞思文化传播有限公司 Water sampler
CN107727435A (en) * 2017-09-13 2018-02-23 新疆电力建设调试所有限责任公司 Total organic carbon on-line checking sampler
CN109238909A (en) * 2018-11-21 2019-01-18 扬州大学 A kind of device and method of portable measurement sewage solid suspension content

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Application publication date: 20111116