CN102198067B - Salt-containing pharmaceutical bath liquid and preparation method thereof - Google Patents
Salt-containing pharmaceutical bath liquid and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a salt-containing pharmaceutical bath liquid and a preparation method thereof. The salt-containing pharmaceutical bath liquid contains the raw materials as follows: 8-25 parts of anionic surface active agent, 5-15 parts of non-ionic surface active agent, 3-12 parts of zwitterionic surface active agent, 3-8 parts of univalent mineral salt, 1- 5 parts of bivalent mineral salt, 0.5-5 parts of alcohol extract of traditional Chinese medicine, 0.2-5 parts of stearinic acid, -20 parts of polyol, 0.2-5 parts of humectant, 0.1-3 parts of vitamin E, 1-10 parts of lanolin, 1-5 parts of pearl concentrate, 25-60 parts of deionized water, 0.05-0.5 parts of citric acid and 0.01-0.3 parts of essence. In the invention, pure natural Chinese medicine extracts and mineral salts are selectively added on the basis of the traditional bath liquid product, so that the effects of bacteriostasis, toxic elimination and anti-oxidization to skin are achieved. The product has excellent moisture retention, moderate foam height, no irritation to skin and a favorable market prospect.
Description
Technical field
The invention belongs to the bath article technical field, be specifically related to a kind ofly contain inorganic salt and medicinal herb components, have the preferably bath foam of moisture-keeping bacterium-restraining toxin-expulsion oxidation-resistance effect.The present invention also relates to the preparation method of this bath foam simultaneously.
Background technology
The modern is because of contact external environment condition variation, the factor affecting such as diet is unbalanced, bad life habits, so that skin metabolism speed is slowed down, abnormal metabolism so that horn cell can't naturally come off, thereby be deposited in skin surface, cause pachylosis, obscure, even can't absorb skin care products.Bath foam is to rise in recent years, the clean skin product of a kind of Novel bath that liked by consumer.Its major function is the decontamination skin moistening.Present bath foam mainly is comprised of kinds of surface activating agent, emollient, dispersant, disinfectant, antiseptic and essence etc., can not well satisfy the demand of people's real life.
Shower product and clean, the product of washing one's hands are different, owing to be that whole body uses, and except decontamination will be arranged, also should be gentle, non-stimulated, the effect such as moisturizing.The inventor is at patent applied for (application number: further research discovery on the basis 200910094564.5,200810058121.6), with inorganic mineral salt, the Chinese medicine ethanol extract with antibacterial, moisturizing and antioxidation through screening is main component, through composite with basis shower system, preparation medicine bathing salt emulsion, give full play to the bacteriostasis and sterilization of salt and toxin expelling effect, the moisturizing of Chinese medicine ethanol extract, antibacterial and antioxidation, make product have bacteriostasis and sterilization, moisturizing, toxin expelling, antioxidative effect, the crowd who is fit to various skin quality uses.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, on the basis of existing bath foam product, by optionally adding natural Chinese medicines extract and mineral salt, obtain a kind of salt-containing pharmaceutical bath liquid with degerming, moisturizing, exfoliation effect.
Another object of the present invention is to provide a kind of method for preparing described salt-containing pharmaceutical bath liquid.
Purpose of the present invention is achieved by the following technical programs.
Except as otherwise noted, percent of the present invention is percetage by weight.
A kind of salt-containing pharmaceutical bath liquid, the weight portion proportioning that its raw material forms is as follows: 8～25 parts of anion surfactants, 5～15 parts of non-ionic surface active agents, 3～12 parts of zwitterionic surfactants, 3～8 parts of monovalence mineral salts, 1～5 part of bivalence mineral salt, 0.5～5 part of Chinese medicine ethanol extract, 0.2～5 part of stearic acid, 5～20 parts of polyhydric alcohol, 0.2～5 part of wetting agent, 0.1～3 part of vitamin E, 1～10 part of lanoline, 1～5 part of Pearl Concentrate, 25～60 parts of deionized waters, 0.01～0.3 part in 0.05～0.5 part of citric acid and essence; Wherein, described monovalence mineral salt is one or both in sodium chloride, potassium chloride, sodium sulfate and the potassium sulfate; Described bivalence mineral salt is one or both in magnesium chloride, magnesium sulfate, zinc chloride, zinc sulfate, Nickel dichloride., nickel sulfate, the chlorination copper and copper sulfate; Described Chinese medicine ethanol extract is made behind alcohol steep by the raw material of Chinese medicine of following weight parts: 5～20 parts of the Radixs Angelicae Dahuricae, 5～12 parts of Flos Eriocaulis, 2～8 parts of Rhizoma Typhoniis, 1～10 part of Rhizoma Chuanxiong, 2～10 parts of Herba Artemisiae Scopariaes, 4～8 parts of Semen Cassiaes, 5～15 parts of Ramulus Moris, 5～15 parts of Flos Chrysanthemis, 7～15 parts of Fructus Chaenomeliss, 5～20 parts on Folium Mori, 5～20 parts in 2～10 parts on Pericarpium Citri Reticulatae Viride and Radix Glycyrrhizae.
Described anion surfactant is selected from one or more in sodium lauroyl sarcosine, polyoxyethylenated alcohol sodium sulfate, sodium lauryl sulphate, ammonium lauryl sulfate and the dodecylbenzene sodium sulfonate;
Described non-ionic surface active agent is selected from one or more in coconut oil fatty acid monoethanolamide, cocoanut fatty acid diethanolamide, APG, lauroyl diglycollic amide, lauroyl isopropanol amide, glyceryl monostearate and the fatty acid alkyl alcohol amide;
Described zwitterionic surfactant is selected from one or more in cocamido propyl betaine, dodecyldimethylammonium hydroxide inner salt and the alkyl dimethyl amine-oxides;
Described polyhydric alcohol is selected from a kind of in propylene glycol, glycerol, sorbitol, 1,3 butylene glycol and the Polyethylene Glycol;
Described wetting agent is selected from least a in squalane, sodium alginate, Jojoba oil, ocean wetting agent, pyrrolidone sodium carboxylate, lactic acid and sodium lactate, collagen protein, aminoacid and the hyaluronic acid.
The method for preparing described salt-containing pharmaceutical bath liquid comprises the step of following order:
(1) with polyhydric alcohol dissolving lanoline, wetting agent and stearic acid, 60～95 ℃ of heated and stirred are even;
(2) in deionized water, add respectively anion surfactant, non-ionic surface active agent, zwitterionic surfactant, and stir;
(3) step (1) and (2) gains are placed the homogenous disperse mulser, the setting shearing force is 500～1500rpm, is warming up to 60～80 ℃, and constant temperature stirs 20～60min;
(4) add monovalence mineral salt and bivalence mineral salt, be cooled to 60～40 ℃, the setting shearing force is 500～1500rpm, and mixing time 20～60min makes mineral salt fully dissolving under strong shear action, and reaches emulsifying and homogenizing;
(5) add Chinese medicine ethanol extract and Pearl Concentrate, temperature, shearing force are constant, mixing time 10～40min;
(6) add vitamin E, essence, the reduction shearing force is 500～1000rpm, is cooled to room temperature;
(7) add citric acid, regulating pH value is 6.5～7.5;
(8) with still aging 20～28 hours of step (7) gains, namely get product.
Wherein, described Chinese medicine ethanol extract is made as follows: raw material of Chinese medicine is clean, dried and crushed to 20～40 orders, add 5～20 times heavy, the soak with ethanol 0.5～5h of concentration 60～95%, 40～75 ℃ of reflux, extract, 1～3h filter behind ebuillition of heated 10～40min, and filtering residue repeats to extract three times, merging filtrate, concentrating filter liquor after the spray drying, gets the Chinese medicine ethanol extract.
With respect to prior art, the present invention has the following advantages:
1, not only realized the dirt-removing functions of bath foam, moistening effect is good, and gentleness is non-stimulated, and foam is abundant fine and smooth, and has significant exfoliation, antifungal efficacy.
2, the used inorganic salt of the present invention and Chinese medicine extract and shower system are composite, and synergy is good, have antibiotic, moisturizing, the antioxidant effect of highly significant, and owing to be natural additive, no dependence have no side effect.In addition, because compound system is taken into account other effect, its foam is abundant, antipruritic effect is arranged, easy cleaning.
The specific embodiment
By specific embodiment given below and typical Application Example, can further be well understood to the present invention, but they not limitation of the invention.
Embodiment 1
(1) with 95g glycerol dissolving 15g lanoline, and add 10g squalane and 5g stearic acid, 70 ℃ of heated and stirred are even;
(2) in the 300g deionized water, add respectively sodium lauroyl sarcosine 55g, coconut oil fatty acid monoethanolamide 35g, cocamido propyl betaine 30g, and stir;
(3) step (1) and (2) gains are placed the homogenous disperse mulser, the setting shearing force is 900rpm, is warming up to 70 ℃, and constant temperature stirs 35min;
(4) add sodium chloride 40g, potassium chloride 10g, magnesium sulfate 5g, zinc sulfate 10g is cooled to 45 ℃, and the setting shearing force is 1000rpm, and mixing time 30min makes mineral salt fully dissolving under strong shear action, and reaches emulsifying and homogenizing;
(5) add Chinese medicine ethanol extract 10g and Pearl Concentrate 7g, temperature, shearing force are constant, mixing time 25min;
(6) add vitamin E 5g, essence 1g, the reduction shearing force is 800rpm, is cooled to room temperature;
(7) add citric acid, regulating pH value is 6.5;
(8) with still aging 20～28 hours of step (7) gains, namely get product.
Wherein said Chinese medicine ethanol extract is made by following methods: take by weighing Radix Angelicae Dahuricae 30g, Flos Eriocauli 10g, Rhizoma Typhonii 10g, Rhizoma Chuanxiong 10g, Herba Artemisiae Scopariae 10g, Semen Cassiae 10g, Ramulus Mori 20g, Flos Chrysanthemi 26g, Fructus Chaenomelis 20g, Folium Mori 14g, Pericarpium Citri Reticulatae Viride 10g, Radix Glycyrrhizae 10g are for subsequent use.Said herbal medicine is cleaned, dried and be crushed to 20 orders, add 10 times of weight portions of concentration percetage by weight 80% ethanol and soak 2h, 50 ℃ of reflux, extract, 2h, filter behind the ebuillition of heated 30min, filtering residue repeats to extract three times, and merging filtrate is concentrated with filtrate, namely get the Chinese medicine alcohol extract, the spray-dried Chinese medicine dry powder that makes of Chinese medicine alcohol extract is required Chinese medicine ethanol extract.
Embodiment 2
Repeat embodiment 1, following difference is arranged: in the step (1), with 85g propylene glycol dissolving 16g lanoline, 5g hyaluronic acid and 10g stearic acid; In the 270g deionized water, add respectively 50g polyoxyethylenated alcohol sodium sulfate, 35g lauroyl diglycollic amide, 22g dodecyldimethylammonium hydroxide inner salt in the step (2), and stir; In the step (3), temperature is 55 ℃, and constant temperature stirs 20min; In the step (4), the sodium chloride of adding is 35g, zinc sulfate 4g, nickel sulfate 5g, and temperature is 50 ℃, the setting shearing force is 1200rpm, mixing time 30min.
Wherein said Chinese medicine ethanol extract is made by following methods: take by weighing Radix Angelicae Dahuricae 25g, Flos Eriocauli 20g, Rhizoma Typhonii 15g, Rhizoma Chuanxiong 15g, Herba Artemisiae Scopariae 5g, Semen Cassiae 10g, Ramulus Mori 25g, Flos Chrysanthemi 20g, Fructus Chaenomelis 25g, Folium Mori 10g, Pericarpium Citri Reticulatae Viride 5g, Radix Glycyrrhizae 15g are for subsequent use.All the other operations are with embodiment 1
Embodiment 3
Repeat embodiment 1, following difference is arranged: in the step (1), with 100g sorbitol dissolving 30g lanoline, 15g sodium alginate and 20g stearic acid; In the 230g deionized water, add respectively 70g polyoxyethylenated alcohol sodium sulfate, 45g glyceryl monostearate, 25g cocamido propyl betaine in the step (2), and stir; In the step (3), temperature is 60 ℃, and constant temperature stirs 25min; In the step (4), the sodium chloride of adding is 30g, copper chloride 7g, zinc sulfate 8g, and temperature is 45 ℃, the setting shearing force is 1500rpm, mixing time 20min.
Wherein said Chinese medicine ethanol extract is made by following methods: take by weighing Radix Angelicae Dahuricae 20g, Flos Eriocauli 13g, Rhizoma Typhonii 10g, Rhizoma Chuanxiong 15g, Herba Artemisiae Scopariae 5g, Semen Cassiae 8g, Ramulus Mori 25g, Flos Chrysanthemi 18g, Fructus Chaenomelis 22g, Folium Mori 15g, Pericarpium Citri Reticulatae Viride 12g, Radix Glycyrrhizae 20g are for subsequent use.All the other operations are with embodiment 1.
Embodiment 4
Repeat embodiment 1, following difference is arranged: in the step (1), with 90g glycerol dissolving 10g lanoline, 4g sun caul-fat, 6g ocean wetting agent and 13g stearic acid; In the 300g deionized water, add respectively 55g sodium lauroyl sarcosine, 35g lauroyl isopropanol amide, 20g alkyl dimethyl amine-oxides in the step (2), and stir; In the step (3), temperature is 70 ℃, and constant temperature stirs 40min; In the step (4), the sodium chloride of adding is 30g, potassium chloride 4g, nickel sulfate 10g, and temperature is 55 ℃, and the setting shearing force is 1000rpm, mixing time 30min.
Wherein said Chinese medicine ethanol extract is made by following methods: take by weighing Radix Angelicae Dahuricae 20g, Flos Eriocauli 10g, Rhizoma Typhonii 7g, Rhizoma Chuanxiong 8g, Herba Artemisiae Scopariae 12g, Semen Cassiae 10g, Ramulus Mori 18g, Flos Chrysanthemi 15g, Fructus Chaenomelis 18g, Folium Mori 22g, Pericarpium Citri Reticulatae Viride 18g, Radix Glycyrrhizae 32g are for subsequent use.All the other operations are with embodiment 1.
Embodiment 5
Repeat embodiment 1, following difference is arranged: in the step (1), with 100g sorbitol dissolving 12g lanoline, 5g Jojoba oil, 5g collagen protein and 15g stearic acid; In the 260g deionized water, add respectively 50g polyoxyethylenated alcohol sodium sulfate, 40g fatty acid alkyl alcohol amide, 25g cocamido propyl betaine in the step (2), and stir; In the step (3), temperature is 75 ℃, and constant temperature stirs 30min; In the step (4), the sodium chloride of adding is 40g, sodium sulfate 7g, copper chloride 12g, zinc sulfate 6g, and temperature is 60 ℃, and the setting shearing force is 800rpm, mixing time 45min.
Wherein said Chinese medicine ethanol extract is made by following methods: take by weighing Radix Angelicae Dahuricae 18g, Flos Eriocauli 20g, Rhizoma Typhonii 5g, Rhizoma Chuanxiong 12g, Herba Artemisiae Scopariae 15g, Semen Cassiae 10g, Ramulus Mori 20g, Flos Chrysanthemi 20g, Fructus Chaenomelis 20g, Folium Mori 15g, Pericarpium Citri Reticulatae Viride 10g, Radix Glycyrrhizae 20g are for subsequent use.All the other operations are with embodiment 1.
Embodiment 6
Repeat embodiment 1, following difference is arranged: in the step (1), with 85g glycerol dissolving 20g lanoline, 4g sodium alginate, 5g hyaluronic acid and 12g stearic acid; In the 300g deionized water, add respectively 85g sodium lauroyl sarcosine, 40g coconut oil fatty acid monoethanolamide, 28g dodecyldimethylammonium hydroxide inner salt in the step (2), and stir; In the step (3), temperature is 65 ℃, and constant temperature stirs 25min; In the step (4), the potassium chloride of adding is 30g, sodium sulfate 7g, magnesium chloride 7g, nickel sulfate 4g, and temperature is 55 ℃, and the setting shearing force is 900rpm, mixing time 40min.
Wherein said Chinese medicine ethanol extract is made by following methods: take by weighing Radix Angelicae Dahuricae 18g, Flos Eriocauli 15g, Rhizoma Typhonii 10g, Rhizoma Chuanxiong 10g, Herba Artemisiae Scopariae 10g, Semen Cassiae 10g, Ramulus Mori 25g, Flos Chrysanthemi 22g, Fructus Chaenomelis 15g, Folium Mori 20g, Pericarpium Citri Reticulatae Viride 12g, Radix Glycyrrhizae 25g are for subsequent use.All the other operations are with embodiment 1.
Detect this embodiment total plate count according to GBT 7918.1-87 Cosmetics microorganism standard test method general provisions, it is as follows to obtain the result:
Table 1 colony counting result
* CFU: colony-forming units.
According to QB1994-2004 bath shampoo operative norm, adult type bath shampoo total plate count is necessary≤1000 CFU/g.As shown in table 2.
The microbiological indicator of table 2 bath shampoo
Therefore, as shown in Table 1, product of the present invention meets state health standards, and has stronger fungistatic effect.
Use the DPPH method that product of the present invention is carried out the antioxidant activity evaluation.The result is as follows:
Owing to contain a large amount of flavonoid materials in the alcohol extract of Chinese medicine, so non-oxidizability is strong than vitamin C and vitamin E.
Claims (6)
1. salt-containing pharmaceutical bath liquid, the weight portion proportioning that its raw material forms is as follows: 8～25 parts of anion surfactants, 5～15 parts of non-ionic surface active agents, 3～12 parts of zwitterionic surfactants, 3～8 parts of monovalence mineral salts, 1～5 part of bivalence mineral salt, 0.5～5 part in Chinese medicine ethanol extract dry powder, 0.2～5 part of stearic acid, 5～20 parts of polyhydric alcohol, 0.2～5 part of wetting agent, 0.1～3 part of vitamin E, 1～10 part of lanoline, 1～5 part of Pearl Concentrate, 25～60 parts of deionized waters, 0.01～0.3 part in 0.05～0.5 part of citric acid and essence; Wherein, described monovalence mineral salt is one or both in sodium chloride, potassium chloride, sodium sulfate and the potassium sulfate; Described bivalence mineral salt is one or both in magnesium chloride, magnesium sulfate, zinc chloride, zinc sulfate, Nickel dichloride., nickel sulfate, the chlorination copper and copper sulfate; Described Chinese medicine ethanol extract is made behind alcohol steep by the raw material of Chinese medicine of following weight parts: 5～20 parts of the Radixs Angelicae Dahuricae, 5～12 parts of Flos Eriocaulis, 2～8 parts of Rhizoma Typhoniis, 1～10 part of Rhizoma Chuanxiong, 2～10 parts of Herba Artemisiae Scopariaes, 4～8 parts of Semen Cassiaes, 5～15 parts of Ramulus Moris, 5～15 parts of Flos Chrysanthemis, 7～15 parts of Fructus Chaenomeliss, 5～20 parts on Folium Mori, 5～20 parts in 2～10 parts on Pericarpium Citri Reticulatae Viride and Radix Glycyrrhizae; Described polyhydric alcohol is selected from a kind of in propylene glycol, glycerol, sorbitol, 1,3 butylene glycol and the Polyethylene Glycol; Described wetting agent is selected from least a in squalane, sodium alginate, Jojoba oil, ocean wetting agent, pyrrolidone sodium carboxylate, lactic acid and sodium lactate, collagen protein, aminoacid and the hyaluronic acid.
2. salt-containing pharmaceutical bath liquid according to claim 1, it is characterized in that: described anion surfactant is selected from one or more in sodium lauroyl sarcosine, polyoxyethylenated alcohol sodium sulfate, sodium lauryl sulphate, ammonium lauryl sulfate and the dodecylbenzene sodium sulfonate.
3. salt-containing pharmaceutical bath liquid according to claim 1, it is characterized in that: described non-ionic surface active agent is selected from one or more in coconut oil fatty acid monoethanolamide, cocoanut fatty acid diethanolamide, APG, lauroyl diglycollic amide, lauroyl isopropanol amide, glyceryl monostearate and the fatty acid alkyl alcohol amide.
4. salt-containing pharmaceutical bath liquid according to claim 1, it is characterized in that: described zwitterionic surfactant is selected from one or more in cocamido propyl betaine, dodecyldimethylammonium hydroxide inner salt and the alkyl dimethyl amine-oxides.
5. the method for preparing the described salt-containing pharmaceutical bath liquid of claim 1 comprises the step of following order:
(1) with polyhydric alcohol dissolving lanoline, wetting agent and stearic acid, 60～95 ℃ of heated and stirred are even;
(2) in deionized water, add respectively anion surfactant, non-ionic surface active agent, zwitterionic surfactant, and stir;
(3) step (1) and (2) gains are placed the homogenous disperse mulser, the setting shearing force is 500～1500rpm, is warming up to 60～80 ℃, and constant temperature stirs 20～60min;
(4) add monovalence mineral salt and bivalence mineral salt, be cooled to 60～40 ℃, the setting shearing force is 500～1500rpm, and mixing time 20～60min makes mineral salt fully dissolving under strong shear action, and reaches emulsifying and homogenizing;
(5) add Chinese medicine ethanol extract and Pearl Concentrate, temperature, shearing force are constant, mixing time 10～40min;
(6) add vitamin E, essence, the reduction shearing force is 500～1000rpm, is cooled to room temperature;
(7) add citric acid, regulating pH value is 6.5～7.5;
(8) with still aging 20～28 hours of step (7) gains, namely get product.
6. salt-containing pharmaceutical bath liquid preparation method according to claim 5, it is characterized in that: wherein, described Chinese medicine ethanol extract is made as follows: take by weighing 5～20 parts of the Radixs Angelicae Dahuricae, 5～12 parts of Flos Eriocaulis, 2～8 parts of Rhizoma Typhoniis, 1～10 part of Rhizoma Chuanxiong, 2～10 parts of Herba Artemisiae Scopariaes, 4～8 parts of Semen Cassiaes, 5～15 parts of Ramulus Moris, 5～15 parts of Flos Chrysanthemis, 7～15 parts of Fructus Chaenomeliss, 5～20 parts on Folium Mori, 5～20 parts in 2～10 parts on Pericarpium Citri Reticulatae Viride and Radix Glycyrrhizae; Raw material of Chinese medicine is clean, dried and crushed to 20～40 orders, add 5～20 times heavy, the soak with ethanol 0.5～5h of concentration 60～95%, 40～75 ℃ of reflux, extract, 1～3h, filter behind ebuillition of heated 10～40min, filtering residue repeats to extract three times, merging filtrate, concentrating filter liquor, after the spray drying, get Chinese medicine ethanol extract dry powder.
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Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102579306B (en) * | 2012-03-29 | 2014-06-04 | 安徽两面针·芳草日化有限公司 | Toothpaste containing chrysanthemum extraction solution compound mineral salt |
| CN103655314A (en) * | 2013-12-05 | 2014-03-26 | 青岛海芬海洋生物科技有限公司 | Moisturizing bath liquid containing sea biologically-active substances |
| CN103860427B (en) * | 2014-03-07 | 2016-04-06 | 澳宝化妆品（惠州）有限公司 | A kind of moisturizing shower glue |
| WO2018184250A1 (en) * | 2017-04-08 | 2018-10-11 | 格兰比圣（深圳）科技有限公司 | Body wash and preparation method therefor |
| CN107184437A (en) * | 2017-05-31 | 2017-09-22 | 云南省盐业有限公司 | A kind of preoperative saliferous disinfection bath liquid and preparation method thereof |
| CN107854363A (en) * | 2017-12-15 | 2018-03-30 | 福建省为民生物科技有限公司 | A kind of skin protection bath cream containing mulberry leaf |
| CN107890443A (en) * | 2017-12-15 | 2018-04-10 | 福建省为民生物科技有限公司 | A kind of skin protection bath cream |
| CN107982081A (en) * | 2017-12-26 | 2018-05-04 | 洛阳神佳窑业有限公司 | A kind of shampoo used also as bath lotion |
| CN111012728A (en) * | 2020-01-10 | 2020-04-17 | 云南省能源研究院有限公司 | Sterilizing bath foam and preparation method thereof |
| GB202001208D0 (en) * | 2020-01-29 | 2020-03-11 | Nutrition Res Ltd | Nutrient bath salt |
| EP4108229A4 (en) * | 2020-02-19 | 2023-11-22 | Yaokun Huang | Mild cleansing composition containing nearly saturated, saturated or supersaturated active ingredients and preparation method therefor |
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