CN102190802B - 交联聚合物蜡微粉的制备方法 - Google Patents
交联聚合物蜡微粉的制备方法 Download PDFInfo
- Publication number
- CN102190802B CN102190802B CN 201110069688 CN201110069688A CN102190802B CN 102190802 B CN102190802 B CN 102190802B CN 201110069688 CN201110069688 CN 201110069688 CN 201110069688 A CN201110069688 A CN 201110069688A CN 102190802 B CN102190802 B CN 102190802B
- Authority
- CN
- China
- Prior art keywords
- wax
- polymer
- preparation
- water
- silane
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 229920006037 cross link polymer Polymers 0.000 title claims abstract description 7
- 238000000034 method Methods 0.000 claims abstract description 19
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229910000077 silane Inorganic materials 0.000 claims abstract description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229920000642 polymer Polymers 0.000 claims abstract description 11
- 238000004132 cross linking Methods 0.000 claims abstract description 8
- 238000002844 melting Methods 0.000 claims abstract description 3
- 230000008018 melting Effects 0.000 claims abstract description 3
- 239000003595 mist Substances 0.000 claims description 21
- 238000000576 coating method Methods 0.000 claims description 13
- 238000007639 printing Methods 0.000 claims description 11
- 150000004756 silanes Chemical class 0.000 claims description 8
- 239000003999 initiator Substances 0.000 claims description 7
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims description 4
- 239000003795 chemical substances by application Substances 0.000 claims description 4
- 230000000694 effects Effects 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 239000002002 slurry Substances 0.000 claims description 4
- 239000011248 coating agent Substances 0.000 claims description 3
- FWDBOZPQNFPOLF-UHFFFAOYSA-N ethenyl(triethoxy)silane Chemical compound CCO[Si](OCC)(OCC)C=C FWDBOZPQNFPOLF-UHFFFAOYSA-N 0.000 claims description 3
- 238000000227 grinding Methods 0.000 claims description 3
- AZOWAZWIDBFJDK-UHFFFAOYSA-N C(CCC)[Sn].C(CCCCCCCCCCC)(=O)O Chemical compound C(CCC)[Sn].C(CCCCCCCCCCC)(=O)O AZOWAZWIDBFJDK-UHFFFAOYSA-N 0.000 claims description 2
- ZZHNUBIHHLQNHX-UHFFFAOYSA-N butoxysilane Chemical class CCCCO[SiH3] ZZHNUBIHHLQNHX-UHFFFAOYSA-N 0.000 claims description 2
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 claims description 2
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 claims description 2
- 239000000292 calcium oxide Substances 0.000 claims description 2
- NKSJNEHGWDZZQF-UHFFFAOYSA-N ethenyl(trimethoxy)silane Chemical group CO[Si](OC)(OC)C=C NKSJNEHGWDZZQF-UHFFFAOYSA-N 0.000 claims description 2
- 230000008014 freezing Effects 0.000 claims description 2
- 238000007710 freezing Methods 0.000 claims description 2
- 238000003801 milling Methods 0.000 claims description 2
- 230000035515 penetration Effects 0.000 claims description 2
- 150000002976 peresters Chemical class 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- UMFJXASDGBJDEB-UHFFFAOYSA-N triethoxy(prop-2-enyl)silane Chemical compound CCO[Si](CC=C)(OCC)OCC UMFJXASDGBJDEB-UHFFFAOYSA-N 0.000 claims description 2
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims description 2
- 229920002554 vinyl polymer Polymers 0.000 claims description 2
- 238000001238 wet grinding Methods 0.000 claims description 2
- 230000032683 aging Effects 0.000 abstract description 2
- 239000002245 particle Substances 0.000 abstract description 2
- 230000007613 environmental effect Effects 0.000 abstract 1
- 239000012847 fine chemical Substances 0.000 abstract 1
- 229920000578 graft copolymer Polymers 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 235000013873 oxidized polyethylene wax Nutrition 0.000 abstract 1
- 239000004209 oxidized polyethylene wax Substances 0.000 abstract 1
- 239000003973 paint Substances 0.000 abstract 1
- 239000001993 wax Substances 0.000 description 51
- 229920000573 polyethylene Polymers 0.000 description 17
- -1 Polyethylene Polymers 0.000 description 15
- 239000004698 Polyethylene Substances 0.000 description 15
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 6
- 238000005336 cracking Methods 0.000 description 4
- 239000000839 emulsion Substances 0.000 description 3
- 239000011347 resin Substances 0.000 description 3
- 229920005989 resin Polymers 0.000 description 3
- OUUQCZGPVNCOIJ-UHFFFAOYSA-M Superoxide Chemical compound [O-][O] OUUQCZGPVNCOIJ-UHFFFAOYSA-M 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- XMNIXWIUMCBBBL-UHFFFAOYSA-N 2-(2-phenylpropan-2-ylperoxy)propan-2-ylbenzene Chemical compound C=1C=CC=CC=1C(C)(C)OOC(C)(C)C1=CC=CC=C1 XMNIXWIUMCBBBL-UHFFFAOYSA-N 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- LUZSPGQEISANPO-UHFFFAOYSA-N butyltin Chemical compound CCCC[Sn] LUZSPGQEISANPO-UHFFFAOYSA-N 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 239000004200 microcrystalline wax Substances 0.000 description 1
- 235000019808 microcrystalline wax Nutrition 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 125000000962 organic group Chemical group 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000012188 paraffin wax Substances 0.000 description 1
- 239000002861 polymer material Substances 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 229930195735 unsaturated hydrocarbon Natural products 0.000 description 1
Abstract
Description
Claims (9)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 201110069688 CN102190802B (zh) | 2011-03-23 | 2011-03-23 | 交联聚合物蜡微粉的制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 201110069688 CN102190802B (zh) | 2011-03-23 | 2011-03-23 | 交联聚合物蜡微粉的制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN102190802A CN102190802A (zh) | 2011-09-21 |
CN102190802B true CN102190802B (zh) | 2013-06-26 |
Family
ID=44599739
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN 201110069688 Active CN102190802B (zh) | 2011-03-23 | 2011-03-23 | 交联聚合物蜡微粉的制备方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN102190802B (zh) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105778331B (zh) * | 2016-03-14 | 2018-05-25 | 江苏华源医疗科技股份有限公司 | 一种抗静电环保竹炭聚氯乙烯手套及其成型工艺 |
CN107189020B (zh) * | 2017-07-14 | 2019-07-30 | 山西省化工研究所(有限公司) | 一种费托蜡离聚物的合成方法 |
CN110128683B (zh) * | 2019-04-30 | 2022-05-27 | 南京天诗新材料科技有限公司 | 一种采用辐照交联技术制备的改性蜡微粉及制备方法 |
CN113845671B (zh) * | 2021-09-30 | 2023-06-20 | 江苏天问新材料科技有限公司 | 一种球形聚乙烯蜡的制备方法 |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0813244A2 (en) * | 1996-06-14 | 1997-12-17 | The Bergquist Company | Semisolid thermal interface with low flow resistance |
CN101531727A (zh) * | 2008-03-11 | 2009-09-16 | 赢创德固赛有限责任公司 | 后交联的蜡及其制备方法 |
-
2011
- 2011-03-23 CN CN 201110069688 patent/CN102190802B/zh active Active
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0813244A2 (en) * | 1996-06-14 | 1997-12-17 | The Bergquist Company | Semisolid thermal interface with low flow resistance |
CN101531727A (zh) * | 2008-03-11 | 2009-09-16 | 赢创德固赛有限责任公司 | 后交联的蜡及其制备方法 |
Non-Patent Citations (1)
Title |
---|
李青山等.聚乙烯微粉蜡研究.《中国粉体技术》.2000,第6卷(第5期),23-24. * |
Also Published As
Publication number | Publication date |
---|---|
CN102190802A (zh) | 2011-09-21 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN104098972B (zh) | 一种水性金属防锈防腐漆及其制备方法 | |
CN103788328B (zh) | 氧化自交联型水性丙烯酸聚氨酯分散体及其制备方法 | |
CN101974277B (zh) | 密度板封边水性木器白底漆及其制备工艺 | |
CN101885943B (zh) | 纳米玻璃隔热涂料及其制备方法 | |
CN102190802B (zh) | 交联聚合物蜡微粉的制备方法 | |
US9969874B2 (en) | Polymer particle, polymer dispersion, method for producing said polymer dispersion, coating material produced from said polymer dispersion, and coated article | |
CN101932612B (zh) | 用于耐擦洗性以及湿粘附性的水性乳液聚合物 | |
CN103709885A (zh) | 一种水性环境友好型改性醇酸木器漆 | |
CN102134434A (zh) | 高性能水性白色封闭底漆 | |
CN103666174A (zh) | 热反射涂料及其制备方法和应用 | |
CN102603991B (zh) | 船舶内舱用环保型水性防护装饰涂料 | |
CN102993864B (zh) | 水性路标漆及其制备方法 | |
CN103012805B (zh) | 一种自交联水性木器涂料用乳液的制备方法 | |
CN106010046A (zh) | 一种水性铝粉漆及其制备方法 | |
CN112300703A (zh) | 水性生物基爬架涂料及其制备方法 | |
CN103819987A (zh) | 一种水性有机/无机杂合塑胶涂料及其制备方法 | |
CN103756396B (zh) | 一种增强涂料爽滑性能的混合蜡的制备方法 | |
CN110105856A (zh) | 水性羟基丙烯酸树脂和3c涂料的制备方法及其应用 | |
CN105153841A (zh) | 一种耐污耐化学品水性汽车内饰漆及其制备方法 | |
CN104356321A (zh) | 水性聚硅氧烷改性环氧树脂及其制备方法 | |
CN103834037A (zh) | 一种水溶性壳聚糖改性丙烯酸树脂皮革涂饰剂的制备方法 | |
CN103890125B (zh) | 一种新型和稳定的水性杂化粘结剂 | |
CN106478861A (zh) | 一种改性水性丙烯酸树脂及利用其制备人工彩砂的方法 | |
CN101517016B (zh) | 聚合物分散体在涂料组合物中的应用 | |
CN112662247B (zh) | 一种高韧性水性丙烯酸涂料及其制备方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
ASS | Succession or assignment of patent right |
Owner name: NANJING TIANSHI NEW MATERIAL TECHNOLOGIES CO., LTD Free format text: FORMER OWNER: NANJING TIANSHI EXPERIMENTAL MICRO POWDER LTD. Effective date: 20120919 |
|
C41 | Transfer of patent application or patent right or utility model | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20120919 Address after: 210047, Liuhe, Nanjing, Jiangsu province Mayor Lu Zhen Changfeng Road, Nanjing poetry, new Mstar Technology Ltd Applicant after: Nanjing Tianshi New Material Technology Co., Ltd. Address before: 210047 Changfeng Road, governor District, Nanjing, Jiangsu, Liuhe Applicant before: Nanjing Tianshi Micro Powder Co., Ltd. |
|
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Preparation method of cross-linked polymer wax micropowder Effective date of registration: 20150624 Granted publication date: 20130626 Pledgee: Bank of Beijing, Limited by Share Ltd, Nanjing branch Pledgor: Nanjing Tianshi New Material Technology Co., Ltd. Registration number: 2015320000006 |
|
PLDC | Enforcement, change and cancellation of contracts on pledge of patent right or utility model | ||
PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20191206 Granted publication date: 20130626 Pledgee: Bank of Beijing, Limited by Share Ltd, Nanjing branch Pledgor: Nanjing Tianshi New Material Technology Co., Ltd. Registration number: 2015320000006 |