CN102178149A - Health-care fragrant rice or rice paste and preparation method thereof - Google Patents
Health-care fragrant rice or rice paste and preparation method thereof Download PDFInfo
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- CN102178149A CN102178149A CN2011100944777A CN201110094477A CN102178149A CN 102178149 A CN102178149 A CN 102178149A CN 2011100944777 A CN2011100944777 A CN 2011100944777A CN 201110094477 A CN201110094477 A CN 201110094477A CN 102178149 A CN102178149 A CN 102178149A
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Abstract
The invention relates to health-care fragrant rice or rice paste and a preparation method thereof. The health-care fragrant rice or rice paste is a daily food product which is prepared from Chinese wolfberry, rice, Tibet lyonia leaves and fragrans oil and developed by screening according to a clinic formula in modern traditional Chinese medicine and combining modern Chinese medicine pharmacology and a preparation method thereof. In the invention, Wesennan fragrant rice, which has obvious effects of regulating immunity in human body and resisting fatigue, is made and processed by combining the development of modern health-care food science and a modern process according to the traditional health-care cooking method of Chinese; and the health-care fragrant rice or rice paste is suitable for people with low immunity and getting fatigue easily and is particularly suitable to be taken for a long time by old and weak people and sub-health people.
Description
Technical field
The present invention relates to the health food technology field, particularly relate to a kind of health-care fragrent rice or rice paste and preparation method thereof.
Background technology
Along with the fast development of modernization construction, people's rhythm of life is also more and more faster, and the cuisines of enjoying health-nutrition also become modern's a extravagant hope.
Summary of the invention
Purpose of the present invention just is to provide the life of a kind of adaptation modern fast pace, and is convenient, fast, nutritional supplementation is balanced, is easy to long-term edible health-care fragrent rice or rice and sticks with paste;
Another object of the present invention provides the preparation method of above-mentioned health-care fragrent rice or rice paste.
For realizing that the technical scheme that the object of the invention is taked is:
A kind of health-care fragrent rice or rice are stuck with paste, and it is characterized in that raw material is formed to count with weight proportion:
Matrimony vine 1-4 kilogram, rice 25-87 kilogram, oriental blueberry leaf 1-5 kilogram, bay-oil 1-6 milliliter;
Above-mentioned raw materials is formed optimum ratio: matrimony vine 1-2.2 kilogram, rice 25-50 kilogram, oriental blueberry leaf 3-5 kilogram, bay-oil 3-6 milliliter;
The preparation technology of above-mentioned health-care fragrent rice, its processing step is:
Become meal with wolfberry fruit powder is pure, add that purified water Microwave Extraction or boiling are extracted or in water bath with thermostatic control water carry, leave standstill then, filter, it is that 1.012～1.196 liquid extracts are standby that filtrate is concentrated into relative density;
Oriental blueberry leaf is ground into meal, with supersonic oscillations extract or with water boiling and extraction or in water bath with thermostatic control water carry, leave standstill then, filter, it is that 1.012～1.196 liquid extract is standby that filtrate is concentrated into relative density;
Above-mentioned matrimony vine concentrated extract and oriental blueberry leaf concentrated extract are joined in the rice, the spray rice is 10～30 minutes after adding that suitable quantity of water was soaked 10 minutes-12 hours or above-mentioned matrimony vine concentrated extract and oriental blueberry leaf concentrated extract being heated to 48 ℃～55 ℃, filter, dry, the spray bay-oil, be dried to water content 14%-20% once more, sieve, packing gets final product;
Above-mentionedly add the purified water Microwave Extraction three times, at every turn with 6～8 times of amount purified water microwaves 1～2.5 hour;
Above-mentioned boiling is extracted three times, measures the purifying water boiling and extraction 1～2.5 hour with 6～8 times at every turn;
Above-mentioned in water bath with thermostatic control water carry and be meant under 80 ℃ of water bath condition and extracted 3.5～4.5 hours, extract twice, solid-to-liquid ratio 1:30;
Above-mentioned supersonic oscillations are extracted and are meant adding 60% ethanol in oriental blueberry leaf, then at room temperature, shake extraction 20～30 minutes, 2 times repeatedly with the frequency of 59kHz in ultrasonic oscillator;
It is an amount of to add 95% ethanol in the matrimony vine liquid extract of said extracted or oriental blueberry leaf liquid extract, and precipitation filters, and it is 1.106 medicinal extract that filtrate is concentrated into relative density, and then joins in the rice;
The preparation technology that above-mentioned health care rice is stuck with paste, its processing step is: with the pure one-tenth of wolfberry fruit powder meal, add 5～6 times of water, under 80 ℃ of water bath condition, extract, then with its under 4000r/min～4500r/min rotating speed centrifugal 18～35 minutes, get supernatant, be concentrated into relative density and be 1.106 medicinal extract, 95% ethanol that adds 5 times of volumes again, after shaking up, under 4 ℃～6 ℃ conditions, left standstill 12～24 hours, under 4000r/min～4500r/min rotating speed centrifugal 18～35 minutes once more, promptly get thick polysaccharide after the drying precipitate;
Oriental blueberry leaf is ground into meal, adds the ethanol supersonic oscillations and extract, it is 1.012～1.196 that extract is concentrated into relative density, adds an amount of 95% precipitation with alcohol, filters, and it is standby that filtrate is concentrated into the liquid extract of relative density 1.012～1.196 once more;
In thick polysaccharide of above-mentioned matrimony vine and oriental blueberry leaf concentrated extract, add suitable quantity of water, be heated to 48 ℃～55 ℃ after spray rice 5～20 minutes, the back filters, drying, the spray bay-oil to water content 10%～16% o'clock powder essence, sieves and promptly get a rice paste;
It is to add 60% ethanol in oriental blueberry leaf that above-mentioned supersonic oscillations are extracted, and then at room temperature, shakes extraction 20～30 minutes, 2 times repeatedly with the frequency of 59kHz in ultrasonic oscillator;
In the above-mentioned oriental blueberry leaf liquid extract that is concentrated into relative density 1.012～1.196, add CHC1
3, shake up, filter, collect filter residue, filter residue continues to add acetic acid ethyl ester, and jolting is filtered, and collects filter residue, is the oriental blueberry leaf extract.
The present invention is the custom of eating black rice according to tradition, designs by aesthetic feeling and the healthy theory that interpolation coarse food grain or dry fruit, matrimony vine in rice increase meal in conjunction with modern nutriology and modern.
Black rice is with a long history, comes across the Tang Dynasty, is " blue or green smart meal " at that time, is that Taoist school asks the health food of living forever and never die, and is the bait food of Taoist school's feast day.Tu Fu's " giving li po " poem is said: " do not have blue or green smart meal, make my color good.Bitter weary big medicine money, the mountain forest mark is as sweeping.", Pi Rixiu " the wide literary composition in Nanyang desire assist choose a dwelling-place thereby give in chaste tree ": " the ripe cloud of blue or green smart meal is invaded kitchen range, and white " Yi misfortune " Qiu Chengxue spatters window.", Testudo elongata is covered and to say in " chamber, road book thing " poem: " a black meal meal perfume (or spice) of newly cooking a meal, Taoist school's feast day is thought often.”。
Since the Song dynasty, the Buddhist begins the smart meal of green grass or young crops is eaten as vegetarian.Especially at insolation Buddhist joint in April eight, the Buddhist makes black rice for Buddhist more, because of this reason also is the A Mi meal." the black meal of Mongolian pay on April 8 " poem of Song dynasty Ge Sheng second month in a season has been described to bathe at that time Buddhist and gone on a diet with the sight of blue or green smart meal: " April eight is just tasted on hot border, and musk is irritated Buddhist Xiao Quan and trembled with fear.Wooden meal as assistant officer's public affairs cause suddenly, children are frightened to see joyful ball.", another first cloud: " select the lacquer meal and cover peace and quiet confession, turn over spoon that to dare to join sheep cold.Only glad method flavor is full of the vegetarian alms bowl, and bullet seen in the Shang Yushi diction.", the Song dynasty model causes brightly to be said in " Yueyang natural conditions and social customs of a place note ": " it is meal that April 8 was got sheep paulownia leaf wash rice rice in Yuezhou, with ancestral temple god and ancestors.", in addition, put down in writing the blue or green meal that last the sixth of the twelve Earthly Branches, joint was eaten according to Song dynasty beam gram man " pure prosperous three mountain will " and say: " summer in southern candelilla winter is evergreen, gets its leaf, smashs to pieces, and stain rice is meal, dyes dark purple look, and day advances to close, and can prolong life ... ".
The present invention is with matrimony vine, rice, oriental blueberry leaf and health-care fragrent rice is made in the bay-oil combination or rice is stuck with paste, and is to inherit and developed national health food, has novelty.
Its Central-South candle (vaccinium bracteatum thunb) is an Ericaceae evergreen shrubs plant, and oriental blueberry leaf has another name called blueberry leaf.The The Chemical Constituents of oriental blueberry leaf is found the plant polyphenol kind that it is rich in polyphenoils such as anthocyanidin, Quercetin contains a spot of vitamin, sugar, pectin, organic acid, protein and other one-tenth composition that grades in addition.Bibliographical information is arranged, and oriental blueberry leaf alcohol extract (VEE) has that alleviating physical fatigue, strong muscle, beneficial gas, controlling nocturnal emission with astringent drugs, benefit marrow, neuralgia, anaemia are weak, hypopsia, deficiency of blood wandering arthritis, waist pin are unablely ached, graying of hair, the suitable edible health-care effect of illness patient such as drowsiness of sleeping more.Wei state China, Liu Zhongdong etc. " food and fermentation industries " magazine report, the oxidation resistance of oriental blueberry leaf extract is inquired into a literary composition, and conclusion is for when concentration is all 1m g/mL, the oriental blueberry leaf extract is approaching with inhibition lipid peroxidation ability and vitamin C (Vc) at reducing power, is about 9.96 of Vc; And aspect the ability of removing the DPPH free radical, the oriental blueberry leaf extract is 1.4 times of Vc.
The fruit of Chinese wolfberry, record has hard muscles and bones, mends vital essence various symptims and signs of deficiency, the effects such as calming the nerves, make us longevity that makes eye bright in the Compendium of Material Medica, is the medicine-food two-purpose fruit, is the dry mature fruit of plant of Solanaceae lycium barbarum.Its flavor is sweet, property is put down has the effect of liver-kidney tonifying.Modern pharmacology studies confirm that the fruit of Chinese wolfberry can regulate body's immunity, can effectively suppress tumor growth and cell mutation, have delay senility, the effect of AFL, adjusting blood fat and aspects such as blood sugar, promotion hematopoiesis function.It is very high that the fruit of Chinese wolfberry contains abundant LBP-X, fat, protein, free amino acid, taurine, betaine, vitamin B1, B2, E, C, particularly carotenoid content.In addition, also contain a large amount of mineral elements, as nutritional labelings such as potassium, sodium, calcium, magnesium, iron, copper, manganese, zinc, selenium.Sallow to liver-kidney Yin deficiency, the deficiency of blood,, consumptive disease smartly loses, soreness and weakness of waist and knees, disease such as have a dizzy spell have remarkable result.Be used for the liver damage of suffering from a deficiency of the kidney, asthenia of essence and blood, soreness and weakness of waist and knees, dizzy tinnitus, seminal emission, infertile; Deficiency of kidney essence, the dry of quenching one's thirst, the frequent micturition tongue is red; Essence and blood can not on help in order, eyes is dim-sighted, hypopsia.Fruit of Chinese wolfberry taking convenience can be used as medicine, chews clothes, steep in wine.But most this traditional eating methods are difficult to adhere to for a long time, are to adhere to that the long period edible and the performance of the above-mentioned effect of the fruit of Chinese wolfberry needs, can obtain satisfied fruit; Adopt modern processing method to make her and grow precious scented rice, it is edible to make rice, can reach and adhere to that for a long time edible purpose, usage and consumption according to the design of human body requirement, satisfy needed by human body, balanced in nutrition, play good health-care effect, in addition in the life, that a lot of people like is soaked with the fruit of Chinese wolfberry, Baoshang or cook congee, but in fact, owing to be subjected to the influence of factors such as water temperature, soak time, have only the useful component in the part fruit of Chinese wolfberry can be discharged in water or the soup.And LBP-X is a kind of proteoglycan, if extract with poach heating, can make its sex change and causes drug effect to reduce.Therefore, utilize modern extracting method more abundant, more help bringing into play health-care effect the utilization of nutritional labeling.
That bay-oil has is relieving cough and reducing sputum, the effect of health moistening lung, removes mouth parched and tongue scorched, flatulence, digestive discomfort; Often drink, for halitosis, vision is failed to understand the ， hives, and duodenal ulcer, the stomach cold prophylactic treatment effect that had a stomach-ache can be relieving cough and reducing sputum, but supports sound moistening lung, the digestive discomfort of releiving, removing abnormal flavor in oral cavity, and skin care.Food extensive uses such as sweet osmanthus oil tea, sweet osmanthus ointment can be removed mouth parched and tongue scorched, relax bowel, and alleviate the flatulence digestive discomfort.All right skin whitening is removed vivotoxin; Fragrance is pure and fresh, and charming to make us refreshing essence happy, and the Ning Shen ﹗ that feels at ease particularly can drive away moisture in the body, happy spirit, and Yin nourishing and lung moistening can purify body and mind, Rosemary Essence Oil.Tourette production of aromatic, deodorizing detoxifcation.Be used for halitosis, acute toothache, stomach energy toothache and dirty teeth pain etc.
The present invention uses above-mentioned matrimony vine, rice, oriental blueberry leaf and bay-oil compatibility, plays useful additional mutually, coordinative role, human body is played the effect of nutrition complement.Particularly utilize the clinical prescription of modern Chinese medicine to screen and in conjunction with after the development of modern Chinese herbal medicine pharmacology and formulation method thereof, it is low to be specially adapted to body's immunity; Can effectively suppress tumor growth and cell mutation, have delay senility, effect that antifatigue, controlling nocturnal emission with astringent drugs are mended marrow, AFL, adjusting blood fat and aspects such as blood sugar, promotion hematopoiesis function.It is very high to have abundant former blue and white element, polysaccharide, fat, protein, free amino acid, taurine, betaine, vitamin B1, B2, B6, E, C, particularly carotenoid content.In addition, also contain a large amount of mineral elements, as nutritional labelings such as potassium, sodium, calcium, magnesium, iron, copper, manganese, zinc, selenium., consumptive disease sallow to liver-kidney Yin deficiency, the deficiency of blood be smart loses, soreness and weakness of waist and knees, disease such as have a dizzy spell have remarkable result.Be used for the liver damage of suffering from a deficiency of the kidney, asthenia of essence and blood, soreness and weakness of waist and knees, dizzy tinnitus, seminal emission, infertile; Deficiency of kidney essence, the dry of quenching one's thirst, the frequent micturition tongue is red; Essence and blood can not on help in order, eyes is dim-sighted, hypopsia.Fruit of Chinese wolfberry taking convenience can be used as medicine, chews clothes, steep in wine; But most this traditional eating methods are difficult to adhere to for a long time, are to adhere to that the long period edible and the performance of the above-mentioned effect of the fruit of Chinese wolfberry needs, can obtain satisfied effect; Adopt modern processing method to make health-care fragrent rice, it is edible to make rice, can reach and adhere to that for a long time edible purpose, usage and consumption according to the design of human body requirement, satisfy needed by human body, balanced in nutrition, play good health-care effect, in addition in the life, that a lot of people like is soaked with the fruit of Chinese wolfberry, Baoshang or cook congee, but in fact, owing to be subjected to the influence of factors such as water temperature, soak time, have only the useful component in the part fruit of Chinese wolfberry can be discharged in water or the soup.And LBP-X is a kind of proteoglycan, if extract with poach heating, can make its sex change and causes drug effect to reduce.Therefore, utilize modern extracting method more abundant, more help bringing into play its health-care effect the utilization of nutritional labeling.
The present invention is particularly useful for all groups, does not find any toxic and side effect, and the raw material source is wide, cheap and easy to get.
The specific embodiment
95% ethanol of the following stated, 60% ethanol all refer to the volumetric concentration of ethanol.
Embodiment 1
Scented rice, raw material is formed: matrimony vine 1.00kg, rice 30.00kg, oriental blueberry leaf 3.00kg, bay-oil 3.00ml.
Get matrimony vine 1.00kg, clean up, drying, powder becomes meal, with purified water Microwave Extraction three times, at every turn with 6 times of amount purified water microwaves 1 hour, leave standstill, filtration, merging filtrate, concentrate, add an amount of 95% precipitation with alcohol, filter, filtrate is concentrated into relative density 1.116 medicinal extract, and is standby.
Other gets oriental blueberry leaf 3.00kg, cleans up, and drying, powder becomes meal, with purifying water boiling and extraction three times, decocted 1.5 hours with 8 times of amount purified water at every turn, leave standstill, filtration, merging filtrate, concentrate, add an amount of 95% precipitation with alcohol, filter, be concentrated into relative density 1.116 medicinal extract, standby.
Other gets rice 30.00kg, adds the fructus lycii extracted solution liquid extract, and oriental blueberry leaf extract liquid extract adds an amount of purified water and soaked 12 hours, leaches moisture, microwave drying, and the spray bay-oil, drying is sieved, packing.
Quality control: outward appearance complete bright and clean, color and luster is even, hardness is suitable.
Weight differential: less than ± 5%.
Usage and dosage: every day three times, each 100.00g-150.00g, the conventional method boiling becomes rice edible.
Embodiment 2
Scented rice, raw material is formed: matrimony vine 0.50kg, rice 12.50kg, oriental blueberry leaf 1.50kg, bay-oil 3.00ml.
Get matrimony vine 500.00g, clean up, drying, powder becomes meal, with purified water Microwave Extraction three times, at every turn with 8 times of amount purified water microwaves 1 hour, leaves standstill, filtration, merging filtrate, concentrates, and adds precipitation with alcohol, and filtration is concentrated into relative density 1.106 medicinal extract, and is standby.
Other gets oriental blueberry leaf 1.50kg, cleans up, and drying, powder becomes meal, with purifying water boiling and extraction three times, decocted 1.5 hours with 8 times of amount purified water at every turn, leave standstill, filtration, merging filtrate, concentrate, add an amount of 95% precipitation with alcohol, filter, be concentrated into relative density 1.016 medicinal extract, standby.
Other gets rice 12.50kg, adds fructus lycii extracted solution liquid extract, oriental blueberry leaf medicinal extract, adds an amount of purified water and soaks 12 hours, leaches moisture, fluidized drying, and the spray bay-oil, drying is sieved, packing.
Embodiment 3
Scented rice, raw material is formed: matrimony vine 200.00g, rice 5.00kg, oriental blueberry leaf 500.00g, sweet osmanthus 0.5ml.
Get matrimony vine 200.00g, clean up, dry, pulverize, established the water bath with thermostatic control extraction, its optimum process condition that extracts fruit of Chinese wolfberry polysaccharide is for extracting 80 ℃ of temperature, solid-to-liquid ratio 1: 30, extraction times 3.5～4.5 h, extract 2 times, when polysaccharide concentration reached 229.5 μ g/ml, clearance rate reached 48.1%, and ascorbic clearance rate is 41.2%.Clearance rate to ultra-oxygen anion free radical is lower than vitamin C, and when polysaccharide concentration reached 229.5 μ g/ml, clearance rate reached 13.5%, and ascorbic clearance rate is 48.6%.Extract, be concentrated into the matrimony vine medicinal extract of relative density 1.016, standby.
Other takes by weighing 500.00g oriental blueberry leaf powder in the plug conical flask, add people's 7500.00 ml volume fractions 60% ethanol, at room temperature, in ultrasonic oscillator, shake extraction 20～30min with the frequency of 59kHz, repeat 2 times, merge extract, (bath temperature must not surpass 70 to be concentrated into about 2000 mL with vacuum rotary evaporator
0C), after solution to be concentrated is cooled to room temperature, join in the 2000.00 mL absolute ethyl alcohols, jolting, the filtering precipitation, filtrate is concentrated into relative density 1.116 medicinal extract with vacuum rotary evaporator, and is standby.
Other gets rice 5.00kg, adds matrimony vine medicinal extract and oriental blueberry leaf medicinal extract, and the spray bay-oil filters, and drying is sieved, packing.
Embodiment 4
Scented rice, raw material is formed: matrimony vine 200.00g, rice 5.00kg, oriental blueberry leaf 500.00g, bay-oil 0.5ml.
Get matrimony vine 200.00g, oriental blueberry leaf 500.0g and pulverize, add the water of 8 times of amounts, with purifying water boiling and extraction three times, decocted 1 hour with an amount of purified water at every turn, leave standstill, filtration, merging filtrate, concentrate, filtration is concentrated into relative density 1.016 medicinal extract, and is standby.
Other gets rice 5.00kg, vacuumizes, and pressurization sprays into matrimony vine, oriental blueberry leaf crude extract, leaches moisture, microwave drying, and the spray bay-oil, drying is sieved, packing.
Quality control: outward appearance complete bright and clean, color and luster is even, hardness is suitable, meets the rice food hygienic requirements.
Weight differential: less than ± 5%.
Usage and dosage: every day three times, every day three times, each 150.0g-200.0g, the conventional method boiling becomes rice edible.
Embodiment 5
Scented rice: matrimony vine 200.00g, rice 5.00kg, oriental blueberry leaf 500.00g, bay-oil 0.3ml.
Replenish this embodiment, require to provide matrimony vine to be any one extracting method wherein, oriental blueberry leaf adopts water bath with thermostatic control to extract.
Get matrimony vine 5.00kg, clean up, drying, powder becomes meal, with purified water Microwave Extraction three times, at every turn with 8 times of amount purified water microwaves 1 hour, leaves standstill, filtration, merging filtrate, concentrates, and adds precipitation with alcohol, and filtration is concentrated into relative density 1.196 medicinal extract, and is standby.
Other gets oriental blueberry leaf 500.00g and adopts water bath with thermostatic control to extract, and optimum process condition is 55 ℃ of extraction temperature, solid-to-liquid ratio 1: 30, and extraction times 2.5～3.5 h extracts 2 times, then extract is concentrated into relative density 1.196 medicinal extract, and is standby.
Other gets rice 5.00kg, said extracted liquid is sprayed in the rice, and mixing, drying, the spray bay-oil, drying is pulverized, and sieves packing.
Embodiment 6
Rice is stuck with paste: matrimony vine 0.22 kg, rice 5.00 kg, oriental blueberry leaf 0.50 kg, bay-oil 0.5ml.
Take by weighing in 70 ℃ of oven dry and the sub-2.0kg of crushed medlars, adds 5～6 times of water gagings, the water bath with thermostatic control extraction, its optimum process condition that extracts fruit of Chinese wolfberry polysaccharide is for extracting 80 ℃ of temperature, solid-to-liquid ratio 1: 30, extraction times 3.5～4.5 h, extract 2 times, then with extract with 4000r/min～centrifugal 18min of 4500 r/min, supernatant, through concentrating, 95% ethanol that adds 5 times of volumes again, after shaking up, in 4 ℃～6 ℃ refrigerators, place and spend the night, with 4000r/min～centrifugal 20min of 4500 r/min.Precipitation obtains the thick polysaccharide of 2.0g after drying.
Other takes by weighing 5.00g oriental blueberry leaf powder in 100.00ml tool plug conical flask, add people's 75.00 ml volume fractions 60% ethanol, at room temperature, in ultrasonic oscillator, shake extraction 20min with the frequency of 59kHz, repeat 2 times, merge extract, be concentrated into relative density 1.012 ~ 1.196 with vacuum rotary evaporator, after solution to be concentrated is cooled to room temperature, add the people in 20.00 mL absolute ethyl alcohols, jolting, filtering precipitation, filtrate concentrates until obtaining medicinal extract with vacuum rotary evaporator, and this is the oriental blueberry leaf crude extract.
Other gets rice 5.0g, will add suitable quantity of water in thick polysaccharide of above-mentioned matrimony vine and the oriental blueberry leaf concentrated extract, be heated to 48 ℃～55 ℃ after spray rice 5～20 minutes, leach moisture, fluidized drying is waited to dry in the air, the spray bay-oil, drying is pulverized, and sieves packing.
Embodiment 7
Rice is stuck with paste: matrimony vine 2.00kg, rice 50.00kg, oriental blueberry leaf 5.00kg, sweet osmanthus 3.00ml.
Take by weighing in 70 ℃ of oven dry and the sub-2.00kg of crushed medlars, add 5～6 times of water gagings, water bath with thermostatic control is extracted, its optimum process condition that extracts fruit of Chinese wolfberry polysaccharide is for extracting 80 ℃ of temperature, solid-to-liquid ratio 1: 30, extraction times 3.5～4.5 h, extract 2 times, then with extract with 4000r/min～centrifugal 18min of 4500 r/min, supernatant, through concentrating, 95% ethanol that adds 5 times of volumes again, after shaking up, in 4 ℃～6 ℃ refrigerators, place and spend the night, with 4000r/min～centrifugal 20min of 4500 r/min n.Precipitation obtains the thick polysaccharide of 2.00g after drying.
Other takes by weighing 5.00kg oriental blueberry leaf powder in container, adds people's 7500.00 ml volume fractions 60% ethanol, at room temperature, in ultrasonic oscillator, shake extraction 20min with the frequency of 59kHz, repeat 2 times, merge extract, be concentrated into relative density 1.012 ~ 1.196 with vacuum rotary evaporator, after solution to be concentrated is cooled to room temperature, add the people in 200.00 mL absolute ethyl alcohols, jolting, filtering precipitation, filtrate concentrates until obtaining medicinal extract with vacuum rotary evaporator, and this is the oriental blueberry leaf crude extract.
Get 200.00 ml oriental blueberry leaf crude extract medicinal extract in the 1000.00ml conical flask, in bottle, add people 200.00mlCHC1 then
3, jolting is filtered, and collects filter residue, and filter residue continues to add people 200.00ml acetic acid ethyl ester, and jolting is filtered, and collects filter residue, and this is the oriental blueberry leaf extract.With the refrigeration of oriental blueberry leaf extract, standby.
Get rice 50.00kg, will add suitable quantity of water in thick polysaccharide of above-mentioned matrimony vine and the oriental blueberry leaf extract, spray in rice after being heated to 48 ℃～55 ℃, spray time 5～20 minutes leaches moisture, and fluidized drying is waited to dry in the air, the spray bay-oil, and drying is pulverized, and sieves packing.
Claims (11)
1. health-care fragrent rice or rice are stuck with paste, and it is characterized in that raw material is formed to count with weight proportion:
Matrimony vine 1-4 kilogram, rice 25-87 kilogram, oriental blueberry leaf 1-5 kilogram, bay-oil 1-6 milliliter.
2. stick with paste according to described health-care fragrent rice of claim 1 or rice, it is characterized in that raw material is formed to count: matrimony vine 1-2.2 kilogram, rice 25-50 kilogram, oriental blueberry leaf 3-5 kilogram, bay-oil 3-6 milliliter with weight proportion.
3. according to the preparation technology of claim 1 or 2 described health-care fragrent rices, its processing step is:
Become meal with wolfberry fruit powder is pure, add that purified water Microwave Extraction or boiling are extracted or in water bath with thermostatic control water carry, leave standstill then, filter, it is that 1.012～1.196 liquid extracts are standby that filtrate is concentrated into relative density;
Oriental blueberry leaf is ground into meal, with supersonic oscillations extract or with water boiling and extraction or in water bath with thermostatic control water carry, leave standstill then, filter, it is that 1.012～1.196 liquid extract is standby that filtrate is concentrated into relative density;
Above-mentioned matrimony vine concentrated extract and oriental blueberry leaf concentrated extract are joined in the rice, the spray rice is 10～30 minutes after adding that suitable quantity of water was soaked 10 minutes-12 hours or above-mentioned matrimony vine concentrated extract and oriental blueberry leaf concentrated extract being heated to 48 ℃～55 ℃, filter, dry, the spray bay-oil, be dried to water content 14%-20% once more, sieve, packing gets final product.
4. according to the preparation technology of the described health-care fragrent rice of claim 3, it is characterized in that: above-mentionedly add the purified water Microwave Extraction three times, at every turn with 6～8 times of amount purified water microwaves 1～2.5 hour.
5. according to the preparation technology of the described health-care fragrent rice of claim 3, it is characterized in that: above-mentioned boiling is extracted three times, measures the purifying water boiling and extraction 1～2.5 hour with 6～8 times at every turn.
6. according to the preparation technology of the described health-care fragrent rice of claim 3, it is characterized in that: above-mentioned in water bath with thermostatic control water carry and be meant under 80 ℃ of water bath condition and extracted 3.5～4.5 hours, extract twice, solid-to-liquid ratio 1:30.
7. according to the preparation technology of the described health-care fragrent rice of claim 3, it is characterized in that: above-mentioned supersonic oscillations are extracted and are meant adding 60% ethanol in oriental blueberry leaf, then at room temperature, in ultrasonic oscillator, shake extraction 20～30 minutes, 2 times repeatedly with the frequency of 59kHz.
8. according to the preparation technology of the described health-care fragrent rice of claim 3, it is characterized in that: it is an amount of to add 95% ethanol in the matrimony vine liquid extract of said extracted or oriental blueberry leaf liquid extract, and precipitation filters, it is 1.106 medicinal extract that filtrate is concentrated into relative density, and then joins in the rice.
9. according to claim 1 or the 2 described health care meter preparation technologies that stick with paste, its processing step is: with the pure one-tenth of wolfberry fruit powder meal, add 5～6 times of water, under 80 ℃ of water bath condition, extract, then with its under 4000r/min～4500r/min rotating speed centrifugal 18～35 minutes, get supernatant, be concentrated into relative density and be 1.106 medicinal extract, 95% ethanol that adds 5 times of volumes again, after shaking up, under 4 ℃～6 ℃ conditions, left standstill 12～24 hours, under 4000r/min～4500r/min rotating speed centrifugal 18～35 minutes once more, promptly get thick polysaccharide after the drying precipitate;
Oriental blueberry leaf is ground into meal, adds the ethanol supersonic oscillations and extract, it is 1.012～1.196 that extract is concentrated into relative density, adds an amount of 95% precipitation with alcohol, filters, and it is standby that filtrate is concentrated into the liquid extract of relative density 1.012～1.196 once more;
In thick polysaccharide of above-mentioned matrimony vine and oriental blueberry leaf concentrated extract, add suitable quantity of water, be heated to 48 ℃～55 ℃ after spray rice 5～20 minutes, the back filters, drying, the spray bay-oil to water content 10%～16% o'clock powder essence, sieves and promptly get a rice paste.
10. according to the preparation technology of the described health-care fragrent rice of claim 9, it is characterized in that: it is to add 60% ethanol in oriental blueberry leaf that above-mentioned supersonic oscillations are extracted, then at room temperature, in ultrasonic oscillator, shake extraction 20～30 minutes, 2 times repeatedly with the frequency of 59kHz.
11. the preparation technology according to the described health-care fragrent rice of claim 9 is characterized in that: in the above-mentioned oriental blueberry leaf liquid extract that is concentrated into relative density 1.012～1.196, add CHC1
3, shake up, filter, collect filter residue, filter residue continues to add acetic acid ethyl ester, and jolting is filtered, and collects filter residue, is the oriental blueberry leaf extract.
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