CN102080333A - Process for dyeing cotton cheese by using natural dye - Google Patents
Process for dyeing cotton cheese by using natural dye Download PDFInfo
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- CN102080333A CN102080333A CN2010105755512A CN201010575551A CN102080333A CN 102080333 A CN102080333 A CN 102080333A CN 2010105755512 A CN2010105755512 A CN 2010105755512A CN 201010575551 A CN201010575551 A CN 201010575551A CN 102080333 A CN102080333 A CN 102080333A
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Abstract
The invention relates to a process for dyeing cotton cheese by using natural dye, belonging to the technical field of textile printing and dyeing. A two-step method is adopted to complete dyeing on the cotton cheese by using the natural dye, namely firstly modifying the cotton cheese by virtue of high pressure spray and then dyeing, thus the natural dye can have good dyeing depth and leveling property on one hand, on the other hand, the leveling property problem in dyeing by using the natural dye can be effectively solved.
Description
Technical field
A kind of natural dye belongs to technical field of textile printing to the dyeing of cotton cheese.
Technical background
Along with the continuous enhancing of people's environmental protection consciousness and the continuous decrease of petroleum resources, seek a kind of environmental protection, health, nontoxic, harmless, pollution-free, the graceful grace of tone, the natural dye that has the pharmacology health care again has been subjected to people's favor.Particularly in recent years along with the needs of market comsupton variation and back to nature, natural dye has had tremendous development in textile printing and dyeing industry.
In China, multidigit experts such as extra large billows group and Donghua University launch research to aspects such as the extracting method of natural dye and dyeing under the subsidy of national 863 new and high technology projects.The multidigit expert of Shanghai Communications University carries out data collection, puts in order and sets up database to the plant that has the dyeing function both at home and abroad, up to the present, has put out the plant that kind more than 300 has the dyeing function in order.The relevant expert of China Textile Academy has successfully extracted natural Huang and natural green, and it is used for the dyeing of cotton and silk.Abroad as countries such as Japan, Korea S, India, Britain, the U.S., as a kind of fashion, extremely the consumer favors with the natural fabric that uses natural dye dying.
In order to obtain the good dyeing fabric of color characteristics, the scientific worker has carried out number of research projects to natural dye extraction and application both at home and abroad.The dyeing object is primarily aimed at lining, wool yarn etc., and for improving natural dye to the coloration of textile materials effect, they, and mordant and the cation modifier of adopting carries out preliminary treatment to fabric earlier.Though preliminary treatment has improved natural dye to the coloration of textile materials degree of depth and dyeing rate, the level-dyeing property of DYED FABRICS be difficult to solve, and it is insufficient that reason is that dye liquor contacts with fabric.In order to overcome this defective, the applicant is used for cotton cheese dyeing with natural dye, under the effect of high-pressure spray, dye liquor is fully contacted with yarn, efficiently solves the problem of yarn level dyeing.
Summary of the invention
The purpose of this invention is to provide the dyeing of a kind of natural dye to cotton cheese.Promptly cotton cheese is carried out mordant dyeing and cation modifying earlier by high-pressure spray, and then dyeing, can give good dye level of natural dye and level-dyeing property so on the one hand, efficiently solve the problem of level-dyeing property in the natural dye dying on the other hand.
Technical scheme of the present invention: adopt two-step method to finish the dyeing of natural dye to cotton cheese; (1) cotton cheese modification, modification liquid is made up of modifier, surfactant, mordant, and the prescription of modification liquid is as follows:
Modifier (o.w.f): 0.1～2%
Mordant (o.w.f): 0.5～10%
Surfactant (g/L): 0.1～10
Bath raio: 1: 5～1: 20
In yarn package dyeing machine, dye cotton cheese, adopt outside and inside spraying cycle mode to dye, be warming up to 60～90 ℃ of insulations 10～60 minutes, washing.
(2) cotton cheese dyeing, dye bath is made up of natural dye, surfactant and pH regulator agent, and the prescription of dye bath is as follows: natural dye (o.w.f): 0.5～10%
Surfactant (g/L): 0.1～8
Bath raio: 1: 5～1: 20
According to the dyeing requirement, regulate the pH of dye bath, in yarn package dyeing machine, dye cheese, adopt outside and inside spraying cycle mode to dye, be warming up to 60～90 ℃ of insulations 10～120 minutes, then washing.
Here the selected modifier of modification liquid is epoxypropyl trimethylammonium chloride ammonium, glycidyl triethyl ammonium chloride, polyamide epoxy polyamine chloropropane, glytidyl methacrylate-quaternary ammonium salt monomer copolymer, chloro triazine type quarternary ammonium salt compound, 2, and one or more in 4-two chloro-6-(2-pyrido ethylamine)-s-triazine polyamide polymer mix use.
Here selected mordant is one or more in bichromate, aluminium salt, molysite, mantoquita and the cobalt salt.
Here selected surfactant is the polyoxyethylene alkyl ether class in modification liquid or the dye bath: polysorbate60, polysorbate65, Tween 80, triton x-100, Qu Latong X-10; Polyoxyethylene ester class: this dish 20, this dish 40, this dish 60, span 80; Or in the peregal os-15, paregal O P-10, peregal AS-20, peregal AEO-10 one or both.
Here selected natural dye is commercially available natural dye.
Here selected pH regulator agent, acid adjusting can be selected one or both in hydrochloric acid, sulfuric acid, phosphoric acid, hydrobromic acid, the acetic acid for use; The alkalescence adjusting can be selected one or both in NaOH, triethanolamine, sodium carbonate, ammoniacal liquor, the sodium bicarbonate for use, regulates according to the pH value of dyeing needs.
Beneficial effect of the present invention: by high-pressure spray cotton cheese is dyeed, it is simple to have a dyeing installation, and technological process is short, and water saving economizes advantages such as energy, efficiently solves the level-dyeing property problem in the natural dye dying.
The specific embodiment
Below by examples of implementation, further set forth outstanding advantage of the present invention and distinguishing feature, but the present invention never is confined to examples of implementation.
Embodiment 1
Cotton cheese 500g; Modification liquid 2.5kg, modifier: 0.5g wherein, copper sulphate: 2.5g, peregal: 2.5g.In yarn package dyeing machine, finish the modification of cotton cheese.With modification bathe place yarn package dyeing machine after, be 2 ℃/minute speed with programming rate, be warming up to 60 ℃ after, more cotton cheese is dipped in the dye bath, outwards adopt and sprayed 3 minutes, the endless form of inwardly spraying 2 minutes is to cotton cheese modification.Be incubated 30 minutes, wash 2 times.
Dye liquor 2.5kg, wherein purple potato is red: 25g, peregal: 2.5g, ammoniacal liquor: 12.5g.In yarn package dyeing machine, finish the dyeing of cotton cheese.Dye bath is placed yarn package dyeing machine, is 2 ℃/minute speed with programming rate, be warming up to 90 ℃ after, the more cotton cheese after the modification is dipped in the dye bath, outwards adopt and sprayed 3 minutes, the endless form of inwardly spraying 2 minutes dyes to cotton cheese.Dyeing time 60 minutes is washed 2 times.Obtain dyeing product 1, the color fastness of test fabric and K/S value the results are shown in Table 1.
Embodiment 2
Cotton cheese 200g; Modification liquid 4kg, modifier: 4g wherein, ferrous sulfate: 10g, Tween 80:4g.In yarn package dyeing machine, finish the modification of cotton cheese.With modification bathe place yarn package dyeing machine after, be 2 ℃/minute speed with programming rate, be warming up to 60 ℃ after, more cotton cheese is dipped in the dye bath, outwards adopt and sprayed 4 minutes, the endless form of inwardly spraying 6 minutes is to cotton cheese modification.Modification time 10 minutes is washed 2 times.
Dye liquor 4kg, tea dyestuff: 20g wherein, Tween 80:32g, triethanolamine: 12g.In yarn package dyeing machine, finish the dyeing of cotton cheese.Dye bath is placed yarn package dyeing machine, is 2 ℃/minute speed with programming rate, be warming up to 60 ℃ after, the more cotton cheese after the modification is dipped in the dye bath, outwards adopt and sprayed 3 minutes, the endless form of inwardly spraying 2 minutes dyes to cotton cheese.Dyeing time 120 minutes is washed 2 times.Obtain dyeing product 2, the color fastness of test fabric and K/S value the results are shown in Table 1.
Embodiment 3
Cotton cheese 400g; Modification liquid 4kg, modifier: 4g wherein, aluminum sulfate: 4g, Span 20:20g.In yarn package dyeing machine, finish the modification of cotton cheese.With modification bathe place yarn package dyeing machine after, be 2 ℃/minute speed with programming rate, be warming up to 80 ℃ after, more cotton cheese is dipped in the dye bath, outwards adopt and sprayed 4 minutes, the endless form of inwardly spraying 6 minutes is to cotton cheese modification.Modification time 30 minutes is washed 2 times.
Dye liquor 4kg, chrysanthemum dyestuff: 20g wherein, Span 20:16g, hydrochloric acid: 8g.In yarn package dyeing machine, finish the dyeing of cotton cheese.Dye bath is placed yarn package dyeing machine, is 2 ℃/minute speed with programming rate, be warming up to 70 ℃ after, the more cotton cheese after the modification is dipped in the dye bath, outwards adopt and sprayed 3 minutes, the endless form of inwardly spraying 2 minutes dyes to cotton cheese.Dyeing time 30 minutes is washed 2 times.Obtain dyeing product 3, the color fastness of test fabric and K/S value the results are shown in Table 1.
Embodiment 4
Cotton cheese 100g; Modification liquid 1.5kg, modifier: 1.5g wherein, aluminum sulfate: 0.5g, OP-10:4.5g.In yarn package dyeing machine, finish the modification of cotton cheese.With modification bathe place yarn package dyeing machine after, be 2 ℃/minute speed with programming rate, be warming up to 60 ℃ after, more cotton cheese is dipped in the dye bath, outwards adopt and sprayed 4 minutes, the endless form of inwardly spraying 6 minutes is to cotton cheese modification.Modification time 60 minutes is washed 2 times.
Dye liquor 1.5kg, wherein Gardenia Yellow: 3g, OP-10:3g, sodium carbonate: 1.5g.In yarn package dyeing machine, finish the dyeing of cotton cheese.Dye bath is placed yarn package dyeing machine, is 2 ℃/minute speed with programming rate, be warming up to 90 ℃ after, the more cotton cheese after the modification is dipped in the dye bath, outwards adopt and sprayed 3 minutes, the endless form of inwardly spraying 2 minutes dyes to cotton cheese.Dyeing time 60 minutes is washed 2 times.Obtain dyeing product 4, the color fastness of test fabric and K/S value the results are shown in Table 1.
Embodiment 5
Cotton cheese 300g; Modification liquid 2.4kg, modifier: 6g wherein, aluminum sulfate: 1.5g, OP-10:4.5g.In yarn package dyeing machine, finish the modification of cotton cheese.With modification bathe place yarn package dyeing machine after, be 2 ℃/minute speed with programming rate, be warming up to 60 ℃ after, more cotton cheese is dipped in the dye bath, outwards adopt and sprayed 4 minutes, the endless form of inwardly spraying 6 minutes is to cotton cheese modification.Modification time 60 minutes is washed 2 times.
Dye liquor 2.4kg, wherein Gardenia Yellow: 10g, OP-10:2g, sodium carbonate: 0.5g.In yarn package dyeing machine, finish the dyeing of cotton cheese.Dye bath is placed yarn package dyeing machine, is 2 ℃/minute speed with programming rate, be warming up to 90 ℃ after, the more cotton cheese after the modification is dipped in the dye bath, outwards adopt and sprayed 3 minutes, the endless form of inwardly spraying 2 minutes dyes to cotton cheese.Dyeing time 60 minutes is washed 2 times.Obtain dyeing product 5, the color fastness of test fabric and K/S value the results are shown in Table 1.
Table 1 natural dye dyes the K/S value and the color fastness of cheese
Claims (5)
1. a natural dye is characterized in that to the dyeing of cotton cheese natural dye adopts two-step method to the dyeing of cotton cheese; (1) cotton cheese modification, modification liquid is made up of modifier, surfactant, mordant, and the prescription of modification liquid is as follows:
Modifier (o.w.f): 0.1～2%
Mordant (o.w.f): 0.5～10%
Surfactant (g/L): 0.1～10
Bath raio: 1: 5～1: 20
In yarn package dyeing machine, dye cotton cheese, adopt outside and inside spraying cycle mode to dye, be warming up to 60～90 ℃ of insulations 10～60 minutes, washing;
(2) cotton cheese dyeing, dye bath is made up of natural dye, surfactant and pH regulator agent, and the prescription of dye bath is as follows:
Natural dye (o.w.f): 0.5～10%
Surfactant (g/L): 0.1～8
Bath raio: 1: 5～1: 20
pH：6～8
In yarn package dyeing machine, dye cheese, adopt outside and inside spraying cycle mode to dye, be warming up to 60～90 ℃ of insulations 10～120 minutes, washing then, oven dry.
2. dyeing according to claim 1, it is characterized in that used cation modifier is epoxypropyl trimethylammonium chloride ammonium, glycidyl triethyl ammonium chloride, polyamide epoxy polyamine chloropropane, glytidyl methacrylate-quaternary ammonium salt monomer copolymer, chloro triazine type quarternary ammonium salt compound, 2, one or more in 4-two chloro-6-(2-pyrido ethylamine)-s-triazine polyamide polymer mix use.
3. dyeing according to claim 1 is characterized in that used surfactant is the polyoxyethylene alkyl ether class: polysorbate60, polysorbate65, Tween 80, triton x-100, Qu Latong X-10; Polyoxyethylene ester class: this dish 20, this dish 40, this dish 60, span 80; Or in the peregal os-15, paregal O P-10, peregal AS-20, peregal AEO-10 one or both.
4. dyeing according to claim 1 is characterized in that used natural dye is commercially available various natural dyes.
5. dyeing method according to claim 1 is characterized in that the acid adjusting of used pH regulator agent can select one or both in hydrochloric acid, sulfuric acid, phosphoric acid, citric acid, the acetic acid for use; The alkalescence adjusting can be selected one or both in NaOH, triethanolamine, sodium carbonate, ammoniacal liquor, the sodium bicarbonate for use, regulates according to the dyeing demand.
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| CN2010105755512A CN102080333A (en) | 2010-12-07 | 2010-12-07 | Process for dyeing cotton cheese by using natural dye |
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Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102634993A (en) * | 2012-02-01 | 2012-08-15 | 常州美胜生物材料有限公司 | Method for dyeing cotton fibers by using natural dye |
| CN102767098A (en) * | 2011-12-30 | 2012-11-07 | 上海水星家用纺织品股份有限公司 | Preparation method of isatis root tie-dyed fabrics |
| CN103694731A (en) * | 2013-12-05 | 2014-04-02 | 安徽三喜针织有限公司 | Modified dye and preparation method thereof |
| CN103821014A (en) * | 2014-03-20 | 2014-05-28 | 海安县福兴漂染有限公司 | Cotton fiber based non-reactive type modified natural dye staining method |
| CN104088169A (en) * | 2014-07-10 | 2014-10-08 | 广东溢达纺织有限公司 | Natural dye dyeing method for fiber fabric containing celluloses |
| CN104389197A (en) * | 2014-12-15 | 2015-03-04 | 常熟市启弘纺织实业有限公司 | Fabric printing and dyeing method |
| CN104389200A (en) * | 2014-12-15 | 2015-03-04 | 常熟市启弘纺织实业有限公司 | Dyeing method of textile |
| CN105350329A (en) * | 2015-11-24 | 2016-02-24 | 武汉纺织大学 | Polymer cationic modifier for ramie fabric, and preparation method and application method thereof |
| CN106223004A (en) * | 2016-08-19 | 2016-12-14 | 长兴金发纺织有限公司 | A kind of preparation method of soft Washcloth material |
| CN106350994A (en) * | 2016-08-19 | 2017-01-25 | 长兴金发纺织有限公司 | Preparation method of soft and warm-keeping type bath towel fabric |
| CN108625197A (en) * | 2018-06-06 | 2018-10-09 | 常州纺织服装职业技术学院 | A method of improving cotton alkermes dye level |
| CN110344264A (en) * | 2019-07-31 | 2019-10-18 | 盐城工学院 | A kind of super-hydrophobic uvioresistant cotton fabric dyeing process method |
| CN111005171A (en) * | 2019-10-16 | 2020-04-14 | 鲁泰纺织股份有限公司 | Preparation device and method for cellulose fiber cheese online dyeing color point yarn |
| CN111996815A (en) * | 2020-08-26 | 2020-11-27 | 盐城工学院 | Preparation and dyeing of boron/silicon-containing hybrid functional protein fiber |
| CN113512893A (en) * | 2021-03-25 | 2021-10-19 | 一木生态纺织品(江苏)有限公司 | Cheese dyeing method based on plant dye |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102767098A (en) * | 2011-12-30 | 2012-11-07 | 上海水星家用纺织品股份有限公司 | Preparation method of isatis root tie-dyed fabrics |
| CN102767098B (en) * | 2011-12-30 | 2014-12-31 | 上海水星家用纺织品股份有限公司 | Preparation method of isatis root tie-dyed fabrics |
| CN102634993B (en) * | 2012-02-01 | 2015-07-08 | 常州美胜生物材料有限公司 | Method for dyeing cotton fibers by using natural dye |
| CN102634993A (en) * | 2012-02-01 | 2012-08-15 | 常州美胜生物材料有限公司 | Method for dyeing cotton fibers by using natural dye |
| CN103694731B (en) * | 2013-12-05 | 2016-05-11 | 安徽三喜针织有限公司 | A kind of modification dye well its preparation method |
| CN103694731A (en) * | 2013-12-05 | 2014-04-02 | 安徽三喜针织有限公司 | Modified dye and preparation method thereof |
| CN103821014A (en) * | 2014-03-20 | 2014-05-28 | 海安县福兴漂染有限公司 | Cotton fiber based non-reactive type modified natural dye staining method |
| CN104088169A (en) * | 2014-07-10 | 2014-10-08 | 广东溢达纺织有限公司 | Natural dye dyeing method for fiber fabric containing celluloses |
| CN104088169B (en) * | 2014-07-10 | 2016-02-17 | 广东溢达纺织有限公司 | A kind of natural dye dying method of containing cellulose fiber fabric |
| CN104389197A (en) * | 2014-12-15 | 2015-03-04 | 常熟市启弘纺织实业有限公司 | Fabric printing and dyeing method |
| CN104389200A (en) * | 2014-12-15 | 2015-03-04 | 常熟市启弘纺织实业有限公司 | Dyeing method of textile |
| CN105350329A (en) * | 2015-11-24 | 2016-02-24 | 武汉纺织大学 | Polymer cationic modifier for ramie fabric, and preparation method and application method thereof |
| CN106223004A (en) * | 2016-08-19 | 2016-12-14 | 长兴金发纺织有限公司 | A kind of preparation method of soft Washcloth material |
| CN106350994A (en) * | 2016-08-19 | 2017-01-25 | 长兴金发纺织有限公司 | Preparation method of soft and warm-keeping type bath towel fabric |
| CN108625197A (en) * | 2018-06-06 | 2018-10-09 | 常州纺织服装职业技术学院 | A method of improving cotton alkermes dye level |
| CN110344264A (en) * | 2019-07-31 | 2019-10-18 | 盐城工学院 | A kind of super-hydrophobic uvioresistant cotton fabric dyeing process method |
| CN111005171A (en) * | 2019-10-16 | 2020-04-14 | 鲁泰纺织股份有限公司 | Preparation device and method for cellulose fiber cheese online dyeing color point yarn |
| CN111996815A (en) * | 2020-08-26 | 2020-11-27 | 盐城工学院 | Preparation and dyeing of boron/silicon-containing hybrid functional protein fiber |
| CN111996815B (en) * | 2020-08-26 | 2021-08-17 | 盐城工学院 | Preparation and dyeing of boron/silicon-containing hybrid functional protein fiber |
| CN113512893A (en) * | 2021-03-25 | 2021-10-19 | 一木生态纺织品(江苏)有限公司 | Cheese dyeing method based on plant dye |
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Application publication date: 20110601 |