CN102068034A - Method for reducing tar and harm of papermaking reconstituted tobacco - Google Patents

Method for reducing tar and harm of papermaking reconstituted tobacco Download PDF

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Publication number
CN102068034A
CN102068034A CN201010614542XA CN201010614542A CN102068034A CN 102068034 A CN102068034 A CN 102068034A CN 201010614542X A CN201010614542X A CN 201010614542XA CN 201010614542 A CN201010614542 A CN 201010614542A CN 102068034 A CN102068034 A CN 102068034A
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China
Prior art keywords
reconstituted tobacco
method
extraction
temperature
harm
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CN201010614542XA
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Chinese (zh)
Inventor
石志发
熊伟
曾池
郭涛
孙畅
施鸣
熊灿普
杨林潇
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贵州中烟工业有限责任公司
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Priority to CN201010614542XA priority Critical patent/CN102068034A/en
Publication of CN102068034A publication Critical patent/CN102068034A/en

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Abstract

The invention discloses a method for reducing tar and harm of papermaking reconstituted tobacco, which comprises the following steps of: crushing lucid ganoderma into fine particles of 10 to 100 meshes, heating and performing reflux extraction by using water in an amount which is 4 to 10 times the weight of the fine particles or 40 to 80 percent alcohol and controlling the extraction temperature to be between 50 and 95 DEG C and the extraction time to be between 30 and 120 minutes; cooling the obtained product to 25 DEG C after the extraction, and filtering to obtain a filtrate A; extracting residue once again according to the requirement to obtain a filtrate B; mixing the two filtrates, standing for sedimentation, and evaporating and concentrating a supernatant to the density d2020 (equal to 1.180) to obtain lucid ganoderma cream; and adding the prepared lucid ganoderma cream in an amount which is 0.1 to 1.0 percent of the weight of a coating fluid into the coating fluid for reconstituted tobacco, uniformly mixing the obtained solution, heating to 60 DEG C, spreading the obtained solution on a film base, controlling the spreading rate to be 55+/-1 percent, and drying the film base at the temperature of between 100 and 150 DEG C to obtain the reconstituted tobacco. The method can improve the efficacy of the reconstituted tobacco in reduction of tar and harm.

Description

A kind of method of papermaking-method reconstituted tobaccos reducing tar and reducing harm

Technical field

The invention belongs to technical field of cigarettes, be specifically related to a kind of method of papermaking-method reconstituted tobaccos reducing tar and reducing harm.

Background technology

Papermaking-method reconstituted tobaccos is as a kind of effective auxiliary material of reducing cigarette tar and reducing harm reduction, and the application in cigarette is very extensive, and its consumption in cigarette composition reaches about 15% at present.But along with State Bureau proposes higher requirement to reducing tar and reducing harm, and consumer health's consideration is set out, existing reconstituted tobacco product can't satisfy the requirement of reducing tar and reducing harm.Press for the method for developing a kind of more effectively reducing tar and reducing harm at present.

Glossy ganoderma contains abundant active component as the medicinal bacterium of a kind of preciousness, and GL-B especially wherein has the regulating action of exempting from service, antitumor action, anti-ageing, antioxidation, antithrombotic, anticoagulant effect, antivirus action, anti-radical action, hypoglycemic, effect for reducing blood fat.Domestic patent publication No. CN 101236811A discloses a kind of application of non-tobacco raw-material lotus leaf in the paper process thin slice that utilize, and only widens the raw material scope of application of reconstituted tobacoo, does not relate to the effect in reducing tar and reducing harm.

Summary of the invention

The object of the present invention is to provide a kind of method that can promote the papermaking-method reconstituted tobaccos reducing tar and reducing harm of reconstituted tobacco reducing tar and reducing harm effect.

The method of papermaking-method reconstituted tobaccos reducing tar and reducing harm of the present invention may further comprise the steps:

(1) glossy ganoderma powder is broken into 10~100 order fine particles, adopts the alcohol heating and refluxing extraction of the water or 40~80% (weight concentration) of 4~10 times (by weight), extract temperature and be controlled at 50~95 ℃, 30~120 minutes extraction times; Be cooled to 25 ℃ after the extraction, filter, get filtrate A; Residue extracts once by above-mentioned requirements again, gets liquor B; Merge filtrate twice, standing sedimentation is got the supernatant liquor evaporation and concentration to density d 20 20=1.180, obtain glossy ganoderma ointment;

(2) the above-mentioned glossy ganoderma ointment for preparing is joined reconstituted tobacco with in the coating fluid by 0.1~1.0% of coating fluid weight, fully stirring and evenly mixing is heated to 60 ℃, and it is coated on the sheet base, the control spreading rate is 55 ± 1%, and oven dry promptly gets reconstituted tobacco under 100~150 ℃ of temperature.

The method of above-mentioned papermaking-method reconstituted tobaccos reducing tar and reducing harm, wherein: reconstituted tobacco is placed 22 ± 1 ℃ of temperature, and chopping rolled into the sample cigarette to balance to moisture about 12% in 48 hours under the environmental condition of relative humidity 60 ± 2%.

The present invention compared with prior art, has tangible beneficial effect, as can be known from the above technical solutions, the sample cigarette that this method is made is 22 ± 1 ℃ of temperature, balance 48 hours is to moisture about 12% under the environmental condition of relative humidity 60 ± 2%, tissue the relevant personnel that smoke panel test estimate, the fragrance of high spot review sample cigarette, flue gas, inhale three aspects of flavor, and compare with blank sample, through assess sample at fragrance, flue gas and suction flavor aspect obviously are better than blank sample, and the more common papermaking-method reconstituted tobaccos of its suction quality of papermaking-method reconstituted tobaccos that adds Ganodenna Lucidum P.E has obvious lifting; With the above-mentioned sample cigarette for preparing, pick out weight through weighing and be 0.890~0.910 gram/, each sample amounts to 100, divide two groups of methods to carry out flue gas analysis according to tobacco business standard YC/T156~157-2001 regulation, from analysis result, the range of decrease of the carbon monoxide in the sample flue gas is that 4.5~31.3% tar content ranges of decrease have been low 17.5~47.2%.Its reducing tar and reducing harm effect of papermaking-method reconstituted tobaccos of adding Ganodenna Lucidum P.E obviously is better than common papermaking-method reconstituted tobaccos.

The specific embodiment

Embodiment 1

(1) gets mistake 10~100 purpose glossy ganoderma powder that 50 grams crush, add 500 gram water heating and refluxing extraction in 2000 milliliters round-bottomed flask, extract temperature and be controlled at 95 ℃, 120 minutes extraction times were cooled to 25 ℃ after the extraction, filter, obtain filtrate A, residue extracts once by above-mentioned requirements again, is cooled to 25 ℃ after the extraction, filters, obtain liquor B, merge filtrate twice, standing sedimentation is got the supernatant liquor evaporation and concentration to density d 20 20=1.180, obtain glossy ganoderma ointment, yield is 56.7%;

(2) with the above-mentioned glossy ganoderma ointment for preparing by coating fluid weight 0.1% join reconstituted tobacco with coating fluid (coating fluid of cigarette elder brother ship RISESUN company in taking from), abundant stirring and evenly mixing, be heated to 60 ℃, it is coated on the sheet base (taking from the sheet base of company of cigarette elder brother ship RISESUN in the Yunnan), the control spreading rate promptly obtains reconstituted tobacco 55 ± 1% through 150 ℃ of temperature oven dry;

(3) with reconstituted tobacco in 22 ± 1 ℃ of temperature, chopping rolled into the sample cigarette to balance to moisture about 12% in 48 hours under the environmental condition of relative humidity 60 ± 2%.The coating fluid and the sheet base of company of cigarette elder brother ship RISESUN during the preparation material therefor of blank sample is all taken from addition, all the other methods are identical;

Evaluation method one: with 22 ± 1 ℃ of the above-mentioned sample cigarette temperature for preparing, balance 48 hours is to moisture about 12% under the environmental condition of relative humidity 60 ± 2%, tissue the relevant personnel that smoke panel test estimate, the fragrance of high spot review sample cigarette, flue gas, three aspects of suction flavor, and compare with blank sample, the results are shown in Table 1;

Evaluation method two: with the above-mentioned sample cigarette for preparing, pick out weight through weighing and be 0.890~0.910 gram/, each sample amounts to 100, divides two groups of methods according to tobacco business standard YC/T156~157-2001 regulation to carry out flue gas analysis, and it the results are shown in Table 2.

Embodiment 2

(1) gets 50 mistake 10~100 purpose glossy ganoderma powder that crush of gram, add 200 gram weight concentration and be 80% alcohol in 2000 milliliters round-bottomed flask, heating and refluxing extraction, extract temperature and be controlled at 65 ℃, extracted 60 minutes, be cooled to 25 ℃ after the extraction, filter, get filtrate A; Residue extracts once by above-mentioned requirements again, gets liquor B; Merge filtrate twice, standing sedimentation is got the supernatant liquor evaporation and concentration to density d 20 20=1.180, obtain glossy ganoderma ointment, yield is 49.4%;

(2) the above-mentioned glossy ganoderma ointment for preparing is joined reconstituted tobacco with in the coating fluid (coating fluid of company of cigarette elder brother ship RISESUN in taking from) by 0.3% of coating fluid weight, abundant stirring and evenly mixing, be heated to 60 ℃, it is coated on the sheet base (taking from the sheet base of company of cigarette elder brother ship RISESUN in the Yunnan), the control spreading rate is 55 ± 1%, and oven dry promptly gets reconstituted tobacco under 150 ℃ of temperature;

(3) reconstituted tobacco is placed 22 ± 1 ℃ of temperature, chopping rolled into the sample cigarette to balance to moisture about 12% in 48 hours under the environmental condition of relative humidity 60 ± 2%.

Evaluation method is with embodiment 1, and it the results are shown in Table 1,2.

Embodiment 3

(1) get 500 gram glossy ganoderma powder, add 4000 gram weight concentration and be alcohol heating and refluxing extraction in 5000 milliliters round-bottomed flask of 40%, it is 50 ℃ that temperature is extracted in control, stirs and extracts 30 minutes, extracts after be cooled to 25 ℃, filter, filtrate A; Residue extracts once by above-mentioned requirements again, gets liquor B; Merge filtrate twice, standing sedimentation is got the supernatant liquor evaporation and concentration to density d 20 20=1.180, obtain glossy ganoderma ointment, yield is 54.4%;

(2) the above-mentioned glossy ganoderma ointment for preparing is joined reconstituted tobacco with in the coating fluid (coating fluid of company of cigarette elder brother ship RISESUN in taking from) by 1.0% of coating fluid weight, abundant stirring and evenly mixing, be heated to 60 ℃, it is coated on the sheet base (taking from the sheet base of company of cigarette elder brother ship RISESUN in the Yunnan), the control spreading rate is 55 ± 1%, and oven dry promptly gets reconstituted tobacco under 100 ℃ of temperature;

(3) reconstituted tobacco is placed 22 ± 1 ℃ of temperature, chopping rolled into the sample cigarette to balance to moisture about 12% in 48 hours under the environmental condition of relative humidity 60 ± 2%.

Evaluation method is with embodiment 1, and it the results are shown in Table 1,2.

Table 1 glossy ganoderma reconstituted tobacco smoking result

Annotate: more than smoke panel test and smoke panel test by tobacco product sensory evaluation method (YC/T138-1998).Evaluation class wherein is described as follows:

Style and features: little shortage that has is significantly arranged;

Fine and smooth degree: fine and smooth still exquisiteness is coarse slightly than exquisiteness;

Coherency: more weak than persistent erection etc. by force;

Excitant: little lessly have more greatly;

Aftertaste: stay long short-and-medium of short duration few;

Level of comfort: comfortablely still comfortablely owe comfortable uncomfortable;

Plentiful degree: plentifully still plentifully owe plentiful thin;

Intensity: strong strong moderate more weak;

Assorted gas: few greatly rarer:

Dry sensation: weak have a little less than obviously;

Strength: big-and-middle slighter.

The flue gas analysis of table 2 glossy ganoderma reconstituted tobacco

From analysis result, the tar content in the sample flue gas has reduced by 17.5~47.2%.

The above, it only is preferred embodiment of the present invention, be not that the present invention is done any pro forma restriction, any technical solution of the present invention content that do not break away from,, all still belong in the scope of technical solution of the present invention any simple modification, equivalent variations and modification that above embodiment did according to technical spirit of the present invention.

Claims (2)

1. the method for a papermaking-method reconstituted tobaccos reducing tar and reducing harm may further comprise the steps:
(1) glossy ganoderma powder is broken into 10~100 order fine particles, adopting by weight 4~10 times water or weight concentration is 40~80% alcohol heating and refluxing extraction, extracts temperature and is controlled at 50~95 ℃, 30~120 minutes extraction times; Be cooled to 25 ℃ after the extraction, filter, get filtrate A; Residue extracts once by above-mentioned requirements again, gets liquor B; Merge filtrate twice, standing sedimentation is got the supernatant liquor evaporation and concentration to density d 20 20=1.180, obtain glossy ganoderma ointment;
(2) the above-mentioned glossy ganoderma ointment for preparing is joined reconstituted tobacco with in the coating fluid by 0.1~1.0% of coating fluid weight, fully stirring and evenly mixing is heated to 60 ℃, and it is coated on the sheet base, the control spreading rate is 55 ± 1%, and oven dry promptly gets reconstituted tobacco under 100~150 ℃ of temperature.
2. the method for papermaking-method reconstituted tobaccos reducing tar and reducing harm as claimed in claim 1, wherein: reconstituted tobacco is placed 22 ± 1 ℃ of temperature, and chopping rolled into the sample cigarette to balance to moisture about 12% in 48 hours under the environmental condition of relative humidity 60 ± 2%.
CN201010614542XA 2010-12-30 2010-12-30 Method for reducing tar and harm of papermaking reconstituted tobacco CN102068034A (en)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1144637A (en) * 1996-07-17 1997-03-12 邹剑钢 Anti-cancer traditional Chinese medicine health-care cigeratte
CN1931039A (en) * 2006-09-21 2007-03-21 广西卷烟总厂 Chinese herbal medicine additive for cigarette
CN101103839A (en) * 2006-07-13 2008-01-16 河南省轻工业科学研究所 Paper-making method producing recombination tobacco leaf method
CN101693745A (en) * 2009-09-01 2010-04-14 广东神农烟科技术有限公司 Lucid ganoderma polysaccharide and extraction method thereof as well as cigarette containing lucid ganoderma polysaccharide and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1144637A (en) * 1996-07-17 1997-03-12 邹剑钢 Anti-cancer traditional Chinese medicine health-care cigeratte
CN101103839A (en) * 2006-07-13 2008-01-16 河南省轻工业科学研究所 Paper-making method producing recombination tobacco leaf method
CN1931039A (en) * 2006-09-21 2007-03-21 广西卷烟总厂 Chinese herbal medicine additive for cigarette
CN101693745A (en) * 2009-09-01 2010-04-14 广东神农烟科技术有限公司 Lucid ganoderma polysaccharide and extraction method thereof as well as cigarette containing lucid ganoderma polysaccharide and preparation method thereof

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