CN102065965B - Submerged evaporator - Google Patents

Submerged evaporator Download PDF

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Publication number
CN102065965B
CN102065965B CN2009801226712A CN200980122671A CN102065965B CN 102065965 B CN102065965 B CN 102065965B CN 2009801226712 A CN2009801226712 A CN 2009801226712A CN 200980122671 A CN200980122671 A CN 200980122671A CN 102065965 B CN102065965 B CN 102065965B
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CN
China
Prior art keywords
liquid
submerged evaporator
circulating line
vertical plate
evaporator
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN2009801226712A
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Chinese (zh)
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CN102065965A (en
Inventor
L·利亚
S·库尔基
T·里塔萨洛
J·霍尔科拉
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Metso Outotec Oyj
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Outokumpu Technology Oyj
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Publication of CN102065965A publication Critical patent/CN102065965A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/14Evaporating with heated gases or vapours or liquids in contact with the liquid
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/0011Heating features
    • B01D1/0058Use of waste energy from other processes or sources, e.g. combustion gas
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/0094Evaporating with forced circulation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/06Evaporators with vertical tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/30Accessories for evaporators ; Constructional details thereof

Abstract

The invention relates to a submerged evaporator, which can attenuate the surface fluctuation of the liquid in the evaporator by means of the structures positioned inside it and thus control the vibration that is generated and prevent the formation of splashes.

Description

Submerged evaporator
Technical field
The present invention relates to a kind of submerged evaporator, this submerged evaporator can weaken by the structure that is arranged in its inside the surface wave of the liquid in the evaporimeter and the therefore vibration that produces of control and prevent from forming and splash.
Background technology
The term submerged evaporator represents a kind of device, in this device, at the lower face guiding hot flue gases of the liquid that will be evaporated, therefore realizes the evaporation of liquid and the product of wishing from liquid crystalization simultaneously.
Directly immersing in the evaporation, allowing to pass the liquid bubbling from the hot gas that immerses discharge of pipes.By this way, can produce the efficient transmission from gas to the liquid that is evaporated of material and heat.Owing to do not need heat exchanger, so problem of materials not being problem.For this reason, directly immerse evaporimeter and be used in particular for chemistry and metallurgical technology, in chemistry and metallurgical technology, etching condition causes the problem relevant with material.Typically, such problem appears in heating, evaporation and the crystallization of strongly acidic solution (such as solution of metal sulfates).
In submerged evaporator, immerse pipeline and usually be assemblied in the vertical position in order to minimize amount with the building material of wanting processed liquid directly to contact.
United States Patent (USP) 4278494 has been described a kind of submerged evaporator, wherein has a large pipeline that is used for supplying with hot gas.This causes the vibration of evaporimeter and splashing of liquid, and owing to this reason, and evaporimeter is equipped with the horizontal firing chamber and with the connector of bellows.Because the penetrability of known gas jet increases and increases along with speed, because gas can not be supplied to very high speed, therefore the amount along with gas increases, and the size of the bubble of generation also increases.When the speed of gas was relatively low, it was not absorbed well it and is fed in wherein the liquid, and this is buoyancy causes strong expansion effect in gas reason.
United States Patent (USP) 2867972 has been described a kind of submerged evaporator, and this submerged evaporator is by making gas discharging conduit engrail make every effort to minimized vibrations with saw-toothed profile.
In the scheme according to Deutsche Bundespatent 3447337, submerged evaporator operates by suction, thus, for discharge tube, only can use very little immersion depth.In this equipment, use the pipe of the separation of installing obliquely.Its shortcoming is that owing to moving away from guard system during safeguarding, therefore lid must be provided with the opening of correspondingly-sized.
In the scheme according to Finnish patent 85337, gas is fed in the liquid that will be evaporated by a plurality of quite little VERTICAL TUBE.Advantage is, can be with relatively high speed supply gas, but that penetrability is still kept is little, because jet size is little.In fact, even now, weakening of fluctuation is also insufficient generally.
Summary of the invention
Purpose according to submerged evaporator structure of the present invention is the shortcoming that reduces to have occurred in the submerged evaporator, and such as the fluctuation in the surface level, this fluctuation brings and causes splashing and causing further the vibration of the whole evaporimeter of fluctuation of corrosion.
It is obvious that essential feature of the present invention will become in claims.
The present invention relates to a kind of submerged evaporator, this submerged evaporator comprises: cylindrical liquid container and the immersion pipeline that is connected to it, immerse pipeline by this, hot gas passes the outlet of a plurality of separation and is fed into the below on the surface of liquid via the nozzle that is connected to outlet; With surround to immerse circulating line pipeline, that be equipped with opening so that at least three radially vertical plate be fixed to the inwall of circulating line.
The quantity that is fixed to the vertical plate of circulation plates is at least 3, is preferably 4-6.The typical structure of submerged evaporator is to leave the gap between vertical plate and immersion pipeline, in order to remove the immersion pipeline when circulating line is in place.
According to one embodiment of present invention, level board is connected to vertical plate, this level board be located substantially on liquid near surface but in the horizontal level of the lower face of liquid.The width of level board is preferably the 2-8% of the girth of circulating line.
According to another embodiment of the present invention, fluid box is equipped with grid, and this grid comprises two plates being arranged to be perpendicular to one another.Grid is arranged in the 2-7% of the height of the below on surface of liquid and its cylindrical part that highly is case.
Description of drawings
Fig. 1 is the schematic diagram of a scheme of prior art;
Fig. 2 is the schematic diagram of another program of prior art;
Fig. 3 is the schematic diagram that is equipped with the submerged evaporator of reducer according to of the present invention; And
Fig. 4 is the cross-sectional view of the submerged evaporator of Fig. 3.
The specific embodiment
Fig. 1 is the schematic diagram of submerged evaporator described in the prior, and this submerged evaporator comprises case 1, and this case comprises liquid 2 and a large immersion pipeline 3 that will be evaporated, and the lower face of the liquid in case immerses pipeline by this supplies with hot gas.Liquid is fed in the case and by connector 5 by pipe jointer 4 and removes gas.The salt of crystallization is removed by the bottom of connector 6 from case.Known being used for of gas jet obtains negative pressure region around it, so the solution in the peripheral region of exhaust openings is especially good with jet mixing.Effluxvelocity is larger, mixes stronger.
When using large submerged evaporator, must reduce the flowing velocity of gas in order to reduce the penetrability of gas especially.As a result, gas is as the surface of large air bubble expansion to liquid.Shown in schematic diagram and known from practical experience, large bubble causes significant surface wave and causes the vibration of whole submerged evaporator.
Fig. 2 is the diagram of another submerged evaporator device, and this submerged evaporator is comprised of case 7 and immersion pipeline 8.The bottom of immersing pipeline comprises several pipes 9 of downward sensing, and all gas is by in the liquid 10 of these tube drainages in the case.Liquid is fed in the case by pipe jointer 11, and gas is removed by connector 12, and the salt of crystallization is removed by bottom connector 13.Surrounded by circulating line 14 by the submerged pipe system that the gas vent that separates forms, wherein aperture arrangement supplies to gas in the liquid or the mixture permission of gas and liquid and is discharged into the liquid from this circulating line in this circulating line.
In the device of Fig. 2, at first form the jet of little separation, but they tend to be combined into large jet, be formed on the bubble that upwards rises in the circulation pipe.Compare with the method for showing among Fig. 1, the advantage of this method is can use than gas flow rates high in the scheme shown in Fig. 1, and gas penetration still to be kept rationally.As a result, buoyancy is significantly less, and as other result, has the surface wave more medium and small than the situation of Fig. 1.Aspect flowing, the scheme of Fig. 2 is well, but in fact, but, the pipe of separation is not durable.
Fig. 3 and 4 describes according to submerged evaporator 15 of the present invention, and this submerged evaporator comprises cylindrical liquid case 16 and immerses pipeline 17.The liquid that is heated and evaporates is fed into by supplying with connector 18, and gas is removed by gas connector 19 and the solid of crystallization is removed by discharge tube 20, and this discharge tube is connected to the conical bottom of case.A plurality of outlets 21 are formed in the bottom that enters pipeline during manufacture or by machined afterwards.By this way, be formed on the wearing and tearing of the ducted outlet of immersion less than the wearing and tearing of the pipe that separates.Circulating line 22 is arranged in the immersion pipeline, and is equipped with opening, and being introduced into gas in the liquid or the mixture of gas and liquid can be discharged into the liquid from described opening.
For the fluctuation on the surface of weakening liquid 23 with therefore weaken the vibration of submerged evaporator, at least three, preferably 4-6 vertical plate 24 is arranged in the circulating line.The quantity of vertical plate depends on the size that immerses pipeline.When this quantity is minimum of a value three, can be along both direction, namely vertical direction and horizontal direction prevent surface wave.Vertical plate preferably radially is fixed to the inwall of circulating line and the length that they typically are circulating line.At vertical plate with immerse between the wall of pipeline and leave the gap, realize its uncrossed removing so that maintenance purpose, even circulating line is in place.Vertical plate can help in essence to prevent from corroding splashing of immersion pipeline and upwards rise from the surface of liquid, and prevents surface wave.
In order to make surface wave smooth, the circulating line that belongs to according to submerged evaporator of the present invention can also be equipped with the level board 25 that is fixed to vertical plate 24, and this level board is horizontal-extending on the both sides of vertical plate preferably.Level board be positioned at liquid near surface but below the surface of liquid.Typically the development length with vertical plate is identical for development length from the circulating line wall towards the level board that immerses pipeline.The width of level board is not so that it hinders the rise of bubble in essence, and typically, the width of a level board is the 2-8% of the girth of circulating line.
The other method that weakens surface wave is outside and at the arranged beneath grid 26 on the surface of liquid 23, this grid further makes having an even surface of liquid in whole case at circulating line in submerged evaporator case 16.These grid comprise two plates being arranged to be perpendicular to one another.These grid typically are arranged in the horizontal level, extend to the edge of case always and have the height of about 2-7% of height of the cylindrical part of case.Grid is advantageous particularly in less evaporimeter.
It should be noted that, although Fig. 3 and 4 gives three kinds of diverse ways that have an even surface of the liquid in the submerged evaporator of sening as an envoy to, vertical plate especially can be according to the present invention in the situation that do not have level board or screen to use or with only a kind of being used in combination of described structure.

Claims (7)

1. a submerged evaporator (15), the circulating line (22) that described submerged evaporator comprises columniform case (16) and is connected to the immersion pipeline (17) of this columniform case and is equipped with opening, by described immersion pipeline, gas vent (21) via a plurality of separation in the bottom that is formed at described immersion pipeline (17) is supplied to hot gas in the below on the surface of liquid (23), described circulating line surrounds described immersion pipeline, it is characterized in that, at least three radially vertical plate (24) be fixed to the inwall of described circulating line; Between described vertical plate (24) and described immersion pipeline (17), leave the gap, remove described immersion pipeline when in place with the described circulating line of box lunch (22); Described vertical plate has the length of described circulating line.
2. according to claim 1 submerged evaporator is characterized in that, the quantity of vertical plate is 3.
3. according to claim 1 submerged evaporator is characterized in that, level board (25) is basically near the surface of described liquid (23) but be fixed to described vertical plate (24) in the horizontal level in the lower face of described liquid.
4. according to claim 3 submerged evaporator is characterized in that, the width of described level board (25) is the 2-8% of the girth of described circulating line (22).
5. according to claim 1 submerged evaporator is characterized in that, the case (16) that is used for the described submerged evaporator of liquid is equipped with grid (26), and described grid comprises two grizzly bars being arranged to be perpendicular to one another.
6. according to claim 5 submerged evaporator, it is characterized in that, described grid (26) is located substantially on the below on the surface of described liquid (23) basically at horizontal level, and the height of described grid is the 2-7% of height of the cylindrical part of described case (16).
7. according to claim 1 submerged evaporator is characterized in that, the quantity of vertical plate is 4-6.
CN2009801226712A 2008-06-19 2009-06-17 Submerged evaporator Expired - Fee Related CN102065965B (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FI20080410 2008-06-19
FI20080410A FI121163B (en) 2008-06-19 2008-06-19 A submerged evaporator
PCT/FI2009/050531 WO2009153403A1 (en) 2008-06-19 2009-06-17 Submerged evaporator

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CN102065965A CN102065965A (en) 2011-05-18
CN102065965B true CN102065965B (en) 2013-10-23

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CN (1) CN102065965B (en)
EA (1) EA018126B1 (en)
FI (1) FI121163B (en)
WO (1) WO2009153403A1 (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104307193A (en) * 2014-11-10 2015-01-28 华玉叶 Immersed evaporation method
US10974161B2 (en) 2017-09-20 2021-04-13 Purestream Services, Llc Fluid treatment systems

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3782300A (en) * 1971-09-30 1974-01-01 Mobile Systems Int Inc Human waste incinerator
CN1410359A (en) * 2002-11-28 2003-04-16 清华大学 Side stand immersion combustion evaporator for concentrating filtrate
CN1583205A (en) * 2004-05-28 2005-02-23 清华大学 Unitary immersed burning evaporator of concentrated percolate

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU912183A1 (en) * 1979-10-12 1982-03-15 Предприятие П/Я Р-6273 Evaporation apparatus
SU1243756A1 (en) * 1984-09-15 1986-07-15 Всесоюзный Научно-Исследовательский И Проектный Институт По Очистке Технологических Газов,Сточных Вод И Использованию Вторичных Энергоресурсов Предприятий Черной Металлургии Evaporator with immersion combustion
FI85337C (en) * 1990-04-04 1992-04-10 Outokumpu Oy DOPPROERSYSTEM.
US7416172B2 (en) * 2005-07-21 2008-08-26 Liquid Solutions Llc Submerged gas evaporators and reactors

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3782300A (en) * 1971-09-30 1974-01-01 Mobile Systems Int Inc Human waste incinerator
CN1410359A (en) * 2002-11-28 2003-04-16 清华大学 Side stand immersion combustion evaporator for concentrating filtrate
CN1583205A (en) * 2004-05-28 2005-02-23 清华大学 Unitary immersed burning evaporator of concentrated percolate

Also Published As

Publication number Publication date
EA018126B1 (en) 2013-05-30
FI20080410A0 (en) 2008-06-19
EA201001723A1 (en) 2011-08-30
FI20080410A (en) 2009-12-20
CN102065965A (en) 2011-05-18
FI121163B (en) 2010-08-13
WO2009153403A1 (en) 2009-12-23

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Granted publication date: 20131023

Termination date: 20160617