CN102020301A - Aluminium hydroxide drying system - Google Patents

Aluminium hydroxide drying system Download PDF

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CN102020301A
CN102020301A CN2009101174673A CN200910117467A CN102020301A CN 102020301 A CN102020301 A CN 102020301A CN 2009101174673 A CN2009101174673 A CN 2009101174673A CN 200910117467 A CN200910117467 A CN 200910117467A CN 102020301 A CN102020301 A CN 102020301A
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aluminium hydroxide
dryer
flash dryer
drying
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CN102020301B (en
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李锦�
杨晓波
田年益
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Ningxia Surplus Fluorine Gold And Technology Co Ltd
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Baiyin Zhongtian Chemical Co Ltd
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
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Abstract

The invention discloses an aluminium hydroxide drying system in order to solve the problems that aluminium hydroxide air drying requires long process route, has low production efficiency and consumes considerable energy, and that water in dried aluminium hydroxide cannot meet the requirements of aluminium hydroxide production with a dry method. The aluminium hydroxide drying system comprises a blower, a hot blast heater, a flash dryer, a double-swirl dryer, a cyclone separator, a material bin, a cloth bag dust remover and a draft fan, wherein the blower is connected with the hot blast heater, the hot blast heater is connected with the flash dryer, the flash dryer is connected with the double-swirl dryer, the double-swirl dryer is connected with the cyclone separator, the cyclone separator is connected with the cloth bag dust remover, and the cloth bag dust remover is connected with the draft fan. The invention has the advantages of short process flow, fully closed drying process, no impurity intrusion, high finished product quality, excellent operation environment, high thermal efficiency, short drying time and excellent energy saving effect.

Description

氢氧化铝干燥系统 Aluminum hydroxide drying system

技术领域technical field

本发明涉及一种氢氧化铝干燥系统。The invention relates to an aluminum hydroxide drying system.

背景技术Background technique

氢氧化铝是干法氟化铝生产主要原材料之一,其水分含量在5~10%,而干法氟化铝生产其工艺要求原材料氢氧化铝必须经干燥后使水分含量小于0.1%方可用于生产。Aluminum hydroxide is one of the main raw materials for dry-process aluminum fluoride production, and its moisture content is 5-10%. The dry-process aluminum fluoride production process requires that raw material aluminum hydroxide must be dried to make the moisture content less than 0.1%. in production.

氢氧化铝的干燥通常的方法是气流干燥,被加热的热气流在管道内高速流动,湿物料进入管道后被高速气流带走向管道出口运行;这个过程中由于对流传热传质的作用同时水蒸汽被蒸发。由于物料进入管道后被高速气流冲散二者充分混合,在管道出口用旋风分离器进行气固二相得分离,废气经排风机排出。无论物料初始含水量如何,一般物料水分降至为0.3%~0.5%,不易得到含水量更低的干燥产品。显然不能满足干法氟化铝生产,氢氧化铝干燥后水分含量小于0.1%的要求。另外,气流干燥,必须有高效能的粉尘收集装置,否则尾气携带的粉尘将造成很大的浪费,也会对形成对环境的污染;对结块、不易分散的物料,需要性能好的加料装置,有时还需附加粉碎过程;气流干燥系统的流动阻力降较大,一般为3000--4000Pa,必须选用高压或中压通风机,动力消耗较大。The usual method of drying aluminum hydroxide is air drying. The heated hot air flows in the pipeline at high speed, and the wet material enters the pipeline and is taken to the outlet of the pipeline by the high-speed airflow; in this process, due to the convective heat and mass transfer, water Steam is evaporated. Since the material is dispersed by the high-speed airflow after entering the pipeline, the two are fully mixed, and the gas-solid phase is separated by a cyclone separator at the pipeline outlet, and the exhaust gas is discharged through the exhaust fan. Regardless of the initial moisture content of the material, the moisture content of the general material is reduced to 0.3% to 0.5%, and it is not easy to obtain a dry product with a lower moisture content. Apparently it cannot meet the requirement of dry process aluminum fluoride production, the moisture content of aluminum hydroxide being less than 0.1% after drying. In addition, air drying requires a high-efficiency dust collection device, otherwise the dust carried by the exhaust gas will cause a lot of waste and pollute the environment; for materials that are agglomerated and difficult to disperse, a feeding device with good performance is required , Sometimes an additional crushing process is required; the flow resistance drop of the airflow drying system is relatively large, generally 3000--4000Pa, and a high-pressure or medium-pressure fan must be selected, and the power consumption is relatively large.

发明内容Contents of the invention

本发明的目的在于提供一种氢氧化铝干燥系统,以解决气流干燥氢氧化铝存在工艺路线长、生产效率低、能耗量大,氢氧化铝干燥后水分难以满足干法氟化铝生产要求的问题。The purpose of the present invention is to provide an aluminum hydroxide drying system to solve the problems of long process route, low production efficiency, and large energy consumption in air-drying aluminum hydroxide, and the moisture content of aluminum hydroxide after drying is difficult to meet the production requirements of dry-process aluminum fluoride. The problem.

本发明包括鼓风机、热风炉、闪蒸干燥机、双旋流干燥机、旋风分离器、料仓、布袋除尘器、引风机,鼓风机与热风炉相连,热风炉与闪蒸干燥机相连,闪蒸干燥机与双旋流干燥机相连,双旋流干燥机与旋风分离器相连,旋风分离器与布袋除尘器相连,布袋除尘器与引风机相连。The invention includes a blower, a hot blast stove, a flash dryer, a double swirl dryer, a cyclone separator, a silo, a bag filter, and an induced draft fan. The blower is connected to the hot blast stove, and the hot blast stove is connected to the flash dryer. The dryer is connected to the double-swirl dryer, the double-swirl dryer is connected to the cyclone separator, the cyclone separator is connected to the bag filter, and the bag filter is connected to the induced draft fan.

本发明具有工艺流程短、干燥过程全封闭、无杂质混入、成品质量高、操作环境好;热效率高,干燥时间短,节能效果好的优点。集物料的破碎、分散、沸腾干燥、气流干燥、分级过程为一体,连续操作;设备体积小,干燥强度大,结构简单、可靠,操作、维护方便。尤其氢氧化铝干燥后的水分小于0.1%,经生产实践氢氧化铝干燥后组分满足生产要求。The invention has the advantages of short technological process, fully closed drying process, no impurities, high product quality, good operating environment, high thermal efficiency, short drying time and good energy-saving effect. It integrates the crushing, dispersing, boiling drying, air drying and grading process of materials, and operates continuously; the equipment is small in size, strong in drying strength, simple and reliable in structure, and easy to operate and maintain. In particular, the moisture after drying the aluminum hydroxide is less than 0.1%, and the components after drying the aluminum hydroxide meet the production requirements through production practice.

本发明物料时间短,10秒钟内即可完成物料干燥的过程。闪蒸干燥比气流干燥节能。闪蒸干燥,干燥1吨氢氧化铝需煤气90m3,折标准煤16.07kg;气流干燥,干燥1吨氢氧化铝需煤气115m3,折标准煤20.54kg。干燥1吨氢氧化铝,闪蒸干燥比气流干燥节约标准煤21.76%。煤气折标系数均以0.1786kg/m3计。The material drying time of the invention is short, and the material drying process can be completed within 10 seconds. Flash drying is more energy efficient than airflow drying. Flash drying, drying 1 ton of aluminum hydroxide requires 90m 3 of gas, equivalent to 16.07kg of standard coal; airflow drying, drying of 1 ton of aluminum hydroxide requires 115m 3 of gas, equivalent to 20.54kg of standard coal. To dry 1 ton of aluminum hydroxide, flash drying saves 21.76% of standard coal compared with airflow drying. The conversion coefficient of gas is calculated at 0.1786kg/m 3 .

下面结合附图对本发明作进一步详细的说明。The present invention will be described in further detail below in conjunction with the accompanying drawings.

附图说明Description of drawings

图1是本发明的结构示意图;Fig. 1 is a structural representation of the present invention;

图2是本发明中闪蒸干燥机的结构示意图。Fig. 2 is a schematic structural view of the flash dryer in the present invention.

具体实施方式Detailed ways

下面的实施方式可以使本专业技术人员更全面地理解本发明,但不以任何方式限制本发明。The following embodiments can enable those skilled in the art to understand the present invention more comprehensively, but do not limit the present invention in any way.

如图1所示,本发明包括鼓风机1、热风炉2、闪蒸干燥机3、双旋流干燥机4、旋风分离器5、料仓6、布袋除尘器7、引风机8,鼓风机1与热风炉2相连,热风炉2与闪蒸干燥机3相连,闪蒸干燥机3与双旋流干燥机4相连,双旋流干燥机4与旋风分离器5相连,旋风分离器5与布袋除尘器7相连,布袋除尘器7与引风机8相连。As shown in Figure 1, the present invention comprises blower 1, hot blast furnace 2, flash dryer 3, double-swirl dryer 4, cyclone separator 5, silo 6, bag filter 7, induced draft fan 8, blower 1 and The hot blast stove 2 is connected, the hot blast stove 2 is connected with the flash dryer 3, the flash dryer 3 is connected with the double swirl dryer 4, the double swirl dryer 4 is connected with the cyclone separator 5, and the cyclone separator 5 is connected with the bag dust removal The device 7 is connected, and the bag filter 7 is connected with the induced draft fan 8.

图2示出了本发明中闪蒸干燥机的结构,闪蒸干燥机3内底部轴31上设有物料打散机34,闪蒸干燥机3内部设有中心筒35。中心筒35的中上部以120°与均匀分布三个固定点,与之相对应的闪蒸干燥机3内壁上设有三个固定点配合,以公母套的形式固定。中心筒35物料打散机34的叶片之间留有200mm的环隙。闪蒸干燥机3底部设有气流分配室33,气流分配室33的底面为锥形。气流分配室33锥形底面热风进口顶点32距干燥机筒体底平面37的高度为100mm。闪蒸干燥机3的气流分配室33热风进口环隙高度由60mm增至100mm。闪蒸干燥机3内的中心筒35的上面设有圆环状挡板分级器36。Fig. 2 shows the structure of the flash dryer in the present invention, the bottom shaft 31 of the flash dryer 3 is provided with a material breaker 34, and the flash dryer 3 is provided with a central cylinder 35 inside. The middle and upper part of the central cylinder 35 are evenly distributed with three fixed points at 120°, and the inner wall of the flash dryer 3 corresponding to it is provided with three fixed points for cooperation, and is fixed in the form of male and female sleeves. There is an annular gap of 200 mm between the blades of the central cylinder 35 material breaker 34 . An airflow distribution chamber 33 is provided at the bottom of the flash dryer 3, and the bottom surface of the airflow distribution chamber 33 is conical. The height of the hot air inlet apex 32 on the conical bottom surface of the air distribution chamber 33 from the bottom plane 37 of the dryer cylinder is 100 mm. The airflow distribution chamber 33 of the flash dryer 3 has an annular gap height of the hot air inlet increased from 60mm to 100mm. An annular baffle classifier 36 is arranged on the upper surface of the central cylinder 35 in the flash dryer 3 .

本发明工作过程如下:The working process of the present invention is as follows:

A、煤气由煤气站加压机经管道输送至热风炉2,煤气压力为7~10KPa,低于6KPa会自动报警,空气自鼓风机1进入,助燃风压力为6Kpa,低于3KPa自动报警。A. The gas is transported from the pressurizer of the gas station to the hot blast stove 2 through the pipeline. The gas pressure is 7-10KPa. If it is lower than 6KPa, it will automatically alarm. The air enters from the blower 1. The pressure of the combustion air is 6KPa.

B、煤气在热风炉2燃烧后,产生高温气体,热风炉的出气温度控制在350~400℃。B. After the coal gas is burned in the hot blast stove 2, high-temperature gas is produced, and the outlet gas temperature of the hot blast stove is controlled at 350-400°C.

C、被干燥的氢氧化铝经加料装置送入闪蒸干燥机干燥机筒体3内,在物料打散机34旋转带动下形成强有力的旋转风场,高温气体从干燥机底部沿切线方向进入气流分配室33内,物料与热风充分接触、受热、干燥、并在强烈的离心作用下互相碰撞、磨擦而被微粒化,处于流化状态。干燥后的微粒被热风带入上部的干燥段,在旋风场中继续干燥。闪蒸干燥机3上部有一圆环状挡板分级器36,对于那些处于较大颗粒的或含水量较大的物料,由于离心力作用被甩向干燥器筒壁时,被挡板分级器36挡回干燥段,重新干燥,而达到干燥程度和粒度较小的氢氧化铝随热风从干燥机上部带出。闪蒸干燥机3内设的中心筒35,使干燥机内被打散后物料迅速提升不积料。闪蒸干燥机内风速为5-6m/s,出口压力控制在-1.8~-2.5Kpa。干燥机电机功率为30KW。C. The dried aluminum hydroxide is sent into the cylinder body 3 of the flash dryer through the feeding device, and a strong rotating wind field is formed under the rotation of the material breaker 34, and the high-temperature gas flows from the bottom of the dryer along the tangential direction Entering the air distribution chamber 33, the materials are in full contact with the hot air, heated, dried, and collided with each other under strong centrifugal action, rubbed to be micronized, and are in a fluidized state. The dried particles are brought into the upper drying section by the hot air, and continue drying in the cyclone field. There is an annular baffle classifier 36 on the upper part of the flash dryer 3. For those materials with large particles or high water content, when they are thrown to the wall of the dryer due to centrifugal force, they are blocked by the baffle classifier 36. Go back to the drying section and re-dry, and the aluminum hydroxide that has reached the dryness and smaller particle size is taken out from the upper part of the dryer with the hot air. The central cylinder 35 provided in the flash dryer 3 enables the materials to be broken up in the dryer to be rapidly lifted without accumulating. The wind speed in the flash dryer is 5-6m/s, and the outlet pressure is controlled at -1.8~-2.5Kpa. The motor power of the dryer is 30KW.

D、为确保氢氧化铝干燥后水分小于0.1%,从闪蒸干燥机3出来氢氧化铝再经双旋流干燥机4进行干燥并由顶部排出,进入旋风分离器5,旋风分离器5的排气压力为-4~-7Kpa;温度为90~130℃,旋风分离器5排出的气体进入脉冲布袋除尘器7,布袋除尘器7的出气压力为-5~-8Kpa,经引风机8排空。D. In order to ensure that the moisture after the aluminum hydroxide is dried is less than 0.1%, the aluminum hydroxide comes out from the flash dryer 3 and is then dried by the double swirl dryer 4 and discharged from the top, and enters the cyclone separator 5, and the cyclone separator 5 The exhaust pressure is -4~-7Kpa; the temperature is 90~130℃, the gas discharged from the cyclone separator 5 enters the pulse bag filter 7, and the outlet pressure of the bag filter 7 is -5~-8Kpa, and is discharged by 8 induced draft fans. null.

系统内管道直径由DN300增至DN500,风速10~20m/s,引风机电机功率75KW。The pipe diameter in the system is increased from DN300 to DN500, the wind speed is 10-20m/s, and the power of the induced draft fan motor is 75KW.

E、由旋风分离器5和布袋除尘器7收集的干后氢氧化铝汇集到料仓6,再经气力输送泵9送至下一工序。E. The dried aluminum hydroxide collected by the cyclone separator 5 and the bag filter 7 is collected into the silo 6, and then sent to the next process through the pneumatic conveying pump 9.

Claims (5)

1. aluminium hydroxide dehumidification system, it is characterized in that: it comprises gas blower (1), hotblast stove (2), flash dryer (3), bispin fluidized drying machine (4), cyclonic separator (5), feed bin (6), sack cleaner (7), induced draft fan (8), gas blower (1) links to each other with hotblast stove (2), hotblast stove (2) links to each other with flash dryer (3), flash dryer (3) links to each other with bispin fluidized drying machine (4), bispin fluidized drying machine (4) links to each other with cyclonic separator (5), cyclonic separator (5) links to each other with sack cleaner (7), and sack cleaner (7) links to each other with induced draft fan (8).
2. aluminium hydroxide dehumidification system according to claim 1 is characterized in that: described flash dryer (3) inner bottom part axle (31) is provided with material beater (34), and flash dryer (3) inside is provided with central tube (35).
3. aluminium hydroxide dehumidification system according to claim 2 is characterized in that: described flash dryer (3) bottom is provided with gas distribution chamber (33), and the bottom surface of gas distribution chamber (33) is taper.
4. according to claim 2 or 3 described aluminium hydroxide dehumidification systems, it is characterized in that: described gas distribution chamber (33) hot blast import summit, taper bottom surface (32) is 100mm apart from the height of drying machine cylindrical shell baseplane (37).
5. aluminium hydroxide dehumidification system according to claim 4 is characterized in that: be provided with circular baffle plate classifier (36) above the central tube (35) in the described flash dryer (3).
CN200910117467.3A 2009-09-16 2009-09-16 Aluminium hydroxide drying system Active CN102020301B (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103877916A (en) * 2014-03-15 2014-06-25 宜章弘源化工有限责任公司 Fluidized bed tail gas utilization method and equipment in dry-method aluminum fluoride production
CN106082293A (en) * 2016-06-08 2016-11-09 白银中天化工有限责任公司 A kind of aluminium fluoride raw materials for production drying system of improvement
CN106082294A (en) * 2016-08-01 2016-11-09 刘冠华 Aluminium hydroxide is dried conveyer device and the method for conveying aluminium hydroxide
CN112880341A (en) * 2021-01-13 2021-06-01 中建材蚌埠玻璃工业设计研究院有限公司 Dry-method automatic sorting, drying and impurity removing system for waste glass
CN113493217A (en) * 2020-04-07 2021-10-12 蔡建程 Treatment method for recycling aluminum slag ash

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1149177C (en) * 2000-11-09 2004-05-12 中国铝业股份有限公司 Production method of aluminum hydroxide
CN201512420U (en) * 2009-09-16 2010-06-23 白银中天化工有限责任公司 Aluminum hydroxide drying system

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103877916A (en) * 2014-03-15 2014-06-25 宜章弘源化工有限责任公司 Fluidized bed tail gas utilization method and equipment in dry-method aluminum fluoride production
CN106082293A (en) * 2016-06-08 2016-11-09 白银中天化工有限责任公司 A kind of aluminium fluoride raw materials for production drying system of improvement
CN106082294A (en) * 2016-08-01 2016-11-09 刘冠华 Aluminium hydroxide is dried conveyer device and the method for conveying aluminium hydroxide
CN113493217A (en) * 2020-04-07 2021-10-12 蔡建程 Treatment method for recycling aluminum slag ash
CN113493217B (en) * 2020-04-07 2023-07-18 蔡建程 Treatment method of aluminum slag ash reuse
CN112880341A (en) * 2021-01-13 2021-06-01 中建材蚌埠玻璃工业设计研究院有限公司 Dry-method automatic sorting, drying and impurity removing system for waste glass

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