CN101941821A - 活性炭水泥复合材料及其制备方法 - Google Patents
活性炭水泥复合材料及其制备方法 Download PDFInfo
- Publication number
- CN101941821A CN101941821A CN2010102667238A CN201010266723A CN101941821A CN 101941821 A CN101941821 A CN 101941821A CN 2010102667238 A CN2010102667238 A CN 2010102667238A CN 201010266723 A CN201010266723 A CN 201010266723A CN 101941821 A CN101941821 A CN 101941821A
- Authority
- CN
- China
- Prior art keywords
- cement
- gac
- active carbon
- moulding
- cement composite
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 239000004568 cement Substances 0.000 title claims abstract description 43
- 239000002131 composite material Substances 0.000 title claims abstract description 18
- OKTJSMMVPCPJKN-UHFFFAOYSA-N carbon Chemical compound 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[C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 15
- 229910052799 carbon Inorganic materials 0.000 title claims abstract description 14
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicium dioxide Chemical compound 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- 238000000746 purification Methods 0.000 abstract 1
- UHOVQNZJYSORNB-UHFFFAOYSA-N benzene Chemical compound 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Abstract
本发明提供一种活性炭水泥复合材料及其制备方法，所述材料的原料配比为：活性炭10～80％；水泥10～70％；硅砂0～40%，经过混料、成型、养护、干燥等步骤进行制备。本发明原料易得、方法简单、成本低廉、用途广泛，性能优异。本发明均以市售的活性炭、水泥与硅砂为原料，采用现行的水泥制品的成型方法，制成固定的形状与适当强度的制品。解决了活性炭强度低、使用寿命短、回收困难等缺点，广泛适用于装饰装修，催化剂、催化剂载体及水与空气的净化处理等诸多领域，很适合大规模工业化生产。对保护环境、构筑循环经济与和谐社会，具有十分重大的意义。
Description
活性炭水泥复合材料及其制备方法
技术领域
[0001] 本发明属于一种新型功能材料与复合材料领域，具体涉及一种活性炭水泥复合材 料及其制备方法。
背景技术
[0002] 活性炭是一种重要的多孔功能材料，具有独特的孔隙结构和表面活性官能团，化 学性质稳定，耐酸、碱、热，不溶于水和有机溶剂，广泛地应用于液相和气相的吸附、脱色、精 制、分离、催化领域，在食品、医药、化工、环保等方面有重要意义。但是随着人们对活性炭的 需求，质量要求的不断提高，活性炭也显现出诸多的缺点，例如强度低，大多产品为粉状、粒 状，易造成粉尘污染，使用寿命短，回收再生使用费用高等，严重制约了活性炭的发展，成为 业界的焦点。
发明内容
[0003] 本发明的目的是提供一种活性炭水泥复合材料及其制备方法，利用水泥做结合 剂，将原本松散的活性炭材料，制成具有固定形状与较高强度的活性炭水泥制品。除了具有 各种观赏与装饰装修功能外，更重要的是还可发挥活性炭吸附与再生特性，可以广泛的应 用于工业、农业、环境治理、空气净化、水处理、日常生活的诸多领域，拓展了活性炭和水泥 材料的应用领域，对保护环境、构筑循环经济与和谐社会，具有十分重大的意义。
[0004] 一种活性炭水泥复合材料的原料组成按质量百分比表示为：活性炭10〜80%;水 泥10〜70%;砂0〜40% ；7jc 2(Γ40% ；所述的活性炭为市售的各种活性炭粉末；所述的水泥 为市售的各种水泥；所述的砂为细度小于20目筛的普通建筑硅砂。制备的基本过程为：采 用活性炭粉末、水泥和硅砂为原料，经过混料、成型、养护、干燥步骤制备一种活性炭水泥复 合材料。
[0005] 本发明的效益和优越性在于：本发明原料易得、方法简单、成本低廉、用途广泛，性 能优异。本发明均以市售的活性炭、水泥与硅砂为原料，可采用现行的各种水泥制品的成型 方法，可以制成固定的形状。易于再生使用，解决了活性炭强度低、使用寿命短、回收困难等 缺点，广泛适用于装饰装修，催化剂、催化剂载体及水与空气的净化处理。很适合大规模工 业化生产。
[0006] 具体实施方式
按照质量份数：活性炭10〜80% ；水泥10〜80% ；砂0〜40% ；水20〜40%。
[0007] 所述的活性炭为市售的活性炭粉末。
[0008] 所述的水泥为市售的水泥 所述的砂为普通建筑硅砂。
[0009] 具体制备步骤为：
(1)混料：将原料按一定的配比称量，投入混料机中，搅拌混勻；
(2)加水：根据成型工艺的要求加入适量的水，继续混合搅拌均勻，得到不同的粉料或浆料；
(3)成型：将粉料置于钢模中，用压制成型的方式制成各种形状的坯体；或用浇注成 型的方式将浆料倒入各种模具中捣实，凝固后制成坯体；
(4)养护：将上述成型并凝固好的坯体放在水中养护28天；
(5)干燥：将养护好后的制品取出晾干或烘干，即可得到本专利产品。 [0010]
下面结合具体实施例对本发明内容进行具体说明，但是本发明不仅限于此： 实施例1 ：
利用市售32. 5R硅酸盐水泥、市售椰子壳活性炭粉末、建筑硅砂为原料制备活性炭水 泥复合材料。其原料配方如下：椰壳活性炭47%，水泥40%，硅砂13% ；外加水20% 制备步骤：
a) 混料：先将建筑硅砂通过20目筛备用。再按上述的配比称各种原料，投入混料 机中，混勻。
[0011] b)加水造粒：将混勻后的粉体加入自来水继续混合、过30目筛，得到一定大小的 团粒粉料。
[0012] c)成型：将经过造粒后的粉料置于钢模中，用压力机压制成坯体，放置一天。
[0013] d)养护：将上述初步凝固后的坯体品放在水中养护28天。
[0014] e)干燥：将养护后的样品放在110°C的烘箱中烘干。
[0015] 性能测试：
(1)碘吸附值：402· 88mg/g
(2)甲醛吸附率：13. 30%
(3)苯吸附率：20. 14%
(4)抗压强度：13.89Mpa 实施例2 ：
利用市售42. 5R硅酸盐水泥、市售活性炭粉末、建筑硅砂为原料制备活性炭水泥复合 材料。其原料配方如下：活性炭粉末25%，水泥50%，硅砂25% ；外加水40%。
[0016] 制备步骤：
(a)混料：先将建筑硅砂通过20目筛备用。再按上述的配比称各种原料，投入混料机 中，混勻
(b)加水：将混勻后的粉体加入适量自来水后继续混合、得到粘稠的浆料。
[0017] (c)成型：把浆料倒入塑料模具中，振实后放置一天。
[0018] (d)养护：将初凝后的坯体出塑料模具中取出，放在水中养护28天。
[0019] (e)干燥：将养护后的样品放在110°C的烘箱中烘干。
[0020] 性能测试：
(1)碘吸附值：170.95mg/g
(2)甲醛吸附率：9·57%
(3)苯吸附率：13. 22%
(4)抗压强度：42· 71Mpa 实施例3 ：利用市售硫酸盐水泥、市售煤质活性炭粉末、建筑硅砂为原料制备活性炭水泥复合材 料，其原料配方如下：活性炭58%，水泥17%，砂25% ；外加水25%。
[0021] 制备步骤：
(a)混料：先将建筑硅砂通过20目筛备用。再按上述的配比称各种原料，投入混料机 中，混勻。
[0022] (b)加水造粒：将混勻后的粉体加入适量自来水继续混合、过30目筛，得到一定 大小的团粒粉料。
[0023] (c)成型：将经过造粒后的粉料置于钢模中，用压力机压制成坯体，放置一天。
[0024] (d)养护：将上述初步凝固后的坯体品放在水中养护28天。
[0025] (e)干燥：将养护后的样品放在110°C的烘箱中烘干。
[0026] 性能测试：
(1)碘吸附值：441· 73mg/g
(2)甲醛吸附率：15. 56%
(3)苯吸附率：19.15%
(4)抗压强度-J. 12Mpa 实施例4 ：
利用市售普通硅酸盐水泥、市售椰子壳活性炭、市建筑硅砂为原料制备活性炭水泥复 合材料，其原料配方如下：椰壳活性炭47%，水泥40%，砂13% ； 制备步骤：
(1)混料：先将建筑硅砂通过30目筛备用。再按上述的配比称各种原料，投入混料机 中，混勻。
[0027] (2)加水造粒：将混勻后的粉体加入适量自来水继续混合、过30目筛，得到一定大 小的团粒粉料。
[0028] (3)成型：将经过造粒后的粉料置于钢模中，用压力机压制成坯体，放置一天 (4)养护：将制备好的样品放在水中养护28天。
[0029] (5)干燥：将养护后的样品放在100°C的烘箱中烘干。
[0030] 性能测试：
(1)碘吸附值：385· 81mg/g
(2)甲醛吸附率：17. 58%
(3)苯吸附率：13. 78%
(4)抗压强度：16.48Mpa
Claims (6)
- 一种活性炭水泥复合材料，其特征在于：所述的原料按照质量百分比表示为：活性炭10～80％；水泥10～70％；砂0～40%；水20~40%。
- 2.根据权利要求1所述的活性炭水泥复合材料，其特征在于：所述的活性炭为市售的 各种活性炭粉末。
- 3.根据权利要求1所述的活性炭水泥复合材料，其特征在于：所述的水泥为市售的各 种水泥。
- 4.根据权利要求1所述的活性炭水泥复合材料，其特征在于：所述的砂为细度小于20 目筛的普通建筑硅砂。
- 5. 一种活性炭水泥复合材料的制备方法，其特征在于：采用活性炭粉末、水泥和硅砂 为原料，经过混料、成型、养护、干燥步骤制备一种活性炭水泥复合材料。
- 6.如权利要求5所述的活性炭水泥新材料的制备方法，具体制备步骤为：(1)混料：将原料按一定的配比称量，投入混料机中，搅拌混勻；(2)加水：根据成型工艺的不同要求加入适量的水，继续混合搅拌均勻，得到粉料或浆料；(3)成型：将粉料置于钢模中，用压制成型的方式制成各种形状的坯体；或用浇注成型 的方式将浆料倒入各种模具中捣实，凝固后制成坯体；(4)养护：将上述成型并凝固好的坯体放在水中养护7-28天；(5)干燥：将养护好后的制品取出晾干或烘干，即可得到本专利产品。
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| CN102417329A (zh) * | 2011-08-20 | 2012-04-18 | 福州大学 | 一种无机胶凝炭材料及其制备方法 |
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Non-Patent Citations (1)
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| CN102417329A (zh) * | 2011-08-20 | 2012-04-18 | 福州大学 | 一种无机胶凝炭材料及其制备方法 |
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| CN108863115A (zh) * | 2018-07-31 | 2018-11-23 | 四川忆昔生物科技有限公司 | 一种水泥及其制备方法 |
| CN110922114A (zh) * | 2019-11-26 | 2020-03-27 | 济南大学 | 一种利用活性炭材料制备多孔水泥基材料的方法 |
| CN110922114B (zh) * | 2019-11-26 | 2022-03-08 | 济南大学 | 一种利用活性炭材料制备多孔水泥基材料的方法 |
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