CN101463452A - 铁基高温自润滑复合材料及其制备方法 - Google Patents
铁基高温自润滑复合材料及其制备方法 Download PDFInfo
- Publication number
- CN101463452A CN101463452A CN 200710307295 CN200710307295A CN101463452A CN 101463452 A CN101463452 A CN 101463452A CN 200710307295 CN200710307295 CN 200710307295 CN 200710307295 A CN200710307295 A CN 200710307295A CN 101463452 A CN101463452 A CN 101463452A
- Authority
- CN
- China
- Prior art keywords
- iron
- powder
- metal fluoride
- molybdenum
- iron powder
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Chemical compound data:image/svg+xml;base64,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 data:image/svg+xml;base64,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 [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 title claims abstract description 54
- 229910052742 iron Inorganic materials 0.000 title claims abstract description 26
- 239000002131 composite material Substances 0.000 title claims abstract description 14
- 238000002360 preparation method Methods 0.000 title claims description 15
- 239000000463 material Substances 0.000 claims abstract description 34
- PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Chemical compound data:image/svg+xml;base64,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 data:image/svg+xml;base64,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 [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims abstract description 19
- YEXPOXQUZXUXJW-UHFFFAOYSA-N oxolead Chemical compound 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[Pb]=O YEXPOXQUZXUXJW-UHFFFAOYSA-N 0.000 claims abstract description 17
- 229910001512 metal fluoride Inorganic materials 0.000 claims abstract description 9
- ITRNXVSDJBHYNJ-UHFFFAOYSA-N Tungsten(IV) sulfide Chemical compound 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- ZOKXTWBITQBERF-UHFFFAOYSA-N molybdenum Chemical compound data:image/svg+xml;base64,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 data:image/svg+xml;base64,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 [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229910052750 molybdenum Inorganic materials 0.000 claims abstract description 8
- 239000011733 molybdenum Substances 0.000 claims abstract description 8
- 229910052759 nickel Inorganic materials 0.000 claims abstract description 8
- 238000010438 heat treatment Methods 0.000 claims abstract description 7
- 230000001939 inductive effect Effects 0.000 claims abstract description 6
- 238000007731 hot pressing Methods 0.000 claims abstract description 5
- 239000000843 powder Substances 0.000 claims description 19
- CWQXQMHSOZUFJS-UHFFFAOYSA-N Molybdenum disulfide Chemical compound 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S=[Mo]=S CWQXQMHSOZUFJS-UHFFFAOYSA-N 0.000 claims description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N carbon Chemical compound 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[C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 4
- 238000001816 cooling Methods 0.000 claims description 4
- 229910002804 graphite Inorganic materials 0.000 claims description 4
- 239000010439 graphite Substances 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- 238000005245 sintering Methods 0.000 claims description 4
- 238000005303 weighing Methods 0.000 claims description 4
- OYLGJCQECKOTOL-UHFFFAOYSA-L Barium fluoride Chemical compound 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[F-].[F-].[Ba+2] OYLGJCQECKOTOL-UHFFFAOYSA-L 0.000 claims description 3
- WUKWITHWXAAZEY-UHFFFAOYSA-L Calcium fluoride Chemical compound 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[F-].[F-].[Ca+2] WUKWITHWXAAZEY-UHFFFAOYSA-L 0.000 claims description 3
- 229910001632 barium fluoride Inorganic materials 0.000 claims description 3
- 229910001634 calcium fluoride Inorganic materials 0.000 claims description 3
- 238000009413 insulation Methods 0.000 claims description 2
- 238000000034 method Methods 0.000 abstract description 4
- 238000005299 abrasion Methods 0.000 abstract description 3
- 230000001050 lubricating Effects 0.000 abstract description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 2
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Abstract
本发明公开了一种铁基高温自润滑复合材料及其制备方法。材料由钼2％～13％、镍1％～9％、氧化铅1％～7％、二硫化钼0.5％～4％、二硫化钨1.5％～7％、金属氟化物0.4％～6％以及余量的铁组成。材料通过中频感应加热热压工艺制备而成。材料在500℃～700℃下有优良的抗磨性能并且可实现自润滑，适应于高温设备滑动部件，实现了结构材料与润滑材料设计的一体化。
Description
铁基高温自润滑复合材料及其制备方法
技术领域
本发明涉及一种金属基自润滑复合材料及其制备方法，具体的说是一种铁基 高温自润滑复合材料及其制备方法。 背景技术
研制出具有优异自润滑性能的金属及其合金基高温自润滑材料是解决热动 力机械、高温传动设备等在高温条件下使用摩擦部件的有效途径之一。目前以镍 基、钴基高温合金为基体的高温自润滑材料的研制和应用较多,这些研究大多见 于机理研究和尖端技术领域。对于传统制造业中，在600'C左右可以使用的可作 为工程材料的高温自润滑复合材料的应用和研究较少。报道的在该温度下可使用 的高温自润滑材料无论是金属基自润滑材料还是合金、陶瓷绝大多数是稀有金属 和贵金属作为材料的主成分，例如中国专利公开的CN1034584、 CN1073727、 CN1101681、 CN1083123等，制备这些材料的原材料价格昂贵。铁以及用合金 元素强化的铁合金是廉价的工程材料，具有较低的成本并且铁基材料具有独特的 热处理性能、高性价比等优点。廉价的铁基材料应用于轧钢设备、连铸设备等 可极大的简化机械结构的设计，可减少甚至消除设备的高温润滑维护工作，减轻 工人的劳动强度和降低设备的维护费用。以铁作为材料的基体研制的高温自润滑 材料在解决军用、民用领域的摩擦、磨损与润滑部件将具有实际的工程意义和巨 大的市场潜力。 发明内容
本发明的目的在于提供一种铁基高温自润滑复合材料及其制备方法。 本发明所述的材料在50(TC〜70(TC下具有优异的抗磨特性和良好的自润滑 特性。
根据本发明的目的，我们采用的技术方案如下-
铁基高温自润滑复合材料以铁（Fe)为材料基体，以钼(Mo)和镍（Ni)为基 体强化合金元素，以氟化钙(CaF2)、氟化钡（BaF2)、氧化铅（PbO)、 二硫化钼 (MoS2)和二硫化钨（WS2)复合而成的复合润滑剂为润滑相，采用中频感应加热热压工艺制备而成。
一种铁基高温自润滑复合材料，其特征在于该材料由钼2%〜13%、镍1 %〜9%、氧化铅1%〜7%、 二硫化钼0.5%〜4%、 二硫化钨1.5%〜7%、金属 氟化物0.4%〜6%以及余量的铁组成，按质量百分数计；金属氟化物选自氟化钙、 氟化钡中的一种或两种。
本发明所述材料制备方法为：称取铁粉、钼粉、镍粉、金属氟化物、氧化 铅、二硫化钼以及二硫化钨，置于混料器中混匀并装入石墨模具中，利用中频感 应加热的热压法制成棒料;材料制备参数为热压温度1000〜130(TC,热压压力6〜 lOMPa，保温保压15〜30 min后，随炉自然冷却。
本发明所述的制备方法中，铁粉、钼粉以及镍粉的纯度大于99%，粒度小 于0.076mm。
本发明所述的制备方法中，金属氟化物、氧化铅、二硫化钼以及二硫化钨
的纯度大于99.5 % ，粒度小于0.076mm。
本发明所述的制备方法中，铁粉选自还原铁粉或雾化铁粉。 本发明所述材料的优点是：该材料在50(TC〜70(TC下有优良的抗磨性能并
且可实现自润滑，适应于高温设备滑动部件，实现了结构材料与润滑材料设计的
一体化。因铁粉价格相对较低，与镍基、钴基高温合金相比，材料具有较低的成
本优势。
具体实施方式
实施例1:
按表4配比称取物料，在混料器中混匀并装入石墨模具中，用中频感应加热
的热压工艺，在温度为110(TC、压力为IOMPa，模具内腔为cp45mm的条件下， 烧结30分钟后，随炉自然冷却。材料性能如下表1和表2所示。
表l实施例l所述材料的密度、布氏硬度和抗压强度
密度 布氏硬度 抗压强度MPa
103kg/m3 HB 室温 500°C〜700°C
6.91 180 890 580〜610
表2实施例1所述材料的摩擦系数和磨损率
4<table>table see original document page 5</column></row>
<table>
实施例2:
按表4配比称取物料，在混料器中混匀并装入石墨模具中，用中频感应加
热的热压工艺，在温度为1140 °C、压力为9MPa，模具内腔为cp45mm的条件下， 烧结26分钟后，随炉自然冷却。材料摩擦学性能如下表3所示。 表3实施例2所述材料的摩擦系数和磨损率<table>table see original document page 5</column></row>
<table>
实施例3〜7
表4为实施例1〜7材料质量百分比配比及制备工艺参数。实施例3〜7材料 制备方法除工艺参数不同之外其余同实施例1。实施例3〜7所述材料在500°C〜 700'C下具有优良的抗磨性能并可实现自润滑。
表4实施例1〜7材料质量百分比配比及制备工艺参数
<table>table see original document page 5</column></row>
<table>3 0.6 4.5
余 1200 7.5 22
6774 4 4 3 1.
余 1180 8 25
9 2 6 2
2.5
余 1150 8 28
Claims (5)
1、一种铁基高温自润滑复合材料，其特征在于该材料由钼2％～13％、镍1％～9％、氧化铅1％～7％、二硫化钼0.5％～4％、二硫化钨1.5％～7％、金属氟化物0.4％～6％以及余量的铁组成，按质量百分数计；金属氟化物选自氟化钙、氟化钡中的一种或两种。
2、 如权利要求1所述材料的制备方法，其特征在于称取铁粉、钼粉、镍粉、 金属氟化物、氧化铅、二硫化钼以及二硫化钨，置于混料器中混匀并装入石墨模 具中，利用中频感应加热的热压法制成棒料；材料制备参数为热压温度1000〜 1300。C,热压压力6〜10MPa，保温保压15〜30 min后，随炉自然冷却。
3、 如权利要求2所述的方法，其特征在于铁粉、钼粉以及镍粉的纯度大于 99%，粒度小于0.076mm。
4、 如权利要求2所述的方法，其特征在于金属氟化物、氧化铅、二硫化钼 以及二硫化钨的纯度大于99.5%，粒度小于0.076mm。
5、 如权利要求2所述的方法，其特征在于铁粉选自还原铁粉或雾化铁粉。
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