CN101463294A - Hyperconcentration oil stain rapid cleaning agent and production method thereof - Google Patents
Hyperconcentration oil stain rapid cleaning agent and production method thereof Download PDFInfo
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- CN101463294A CN101463294A CNA2008101431023A CN200810143102A CN101463294A CN 101463294 A CN101463294 A CN 101463294A CN A2008101431023 A CNA2008101431023 A CN A2008101431023A CN 200810143102 A CN200810143102 A CN 200810143102A CN 101463294 A CN101463294 A CN 101463294A
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Abstract
The invention discloses a hyper-concentrated oil stain quick cleansing agent and a production method thereof. The cleansing agent is a product manufactured by a mixed solution and a basic material and assisted by addition agents through mixing, stirring and high-shear homogenization emulsification treatment, wherein the mixed solution is acquired through mixing the raw materials such as purified water, EDTA (disodium ethylene diamine tetraacetate), common salt and the like; the basic material is acquired by homogeneously emulsifying a non-ionic surface active agent, an AE0-9, 6501(coconut oil alcohol amide), OP-10 (nonyl acid polyethylene ether) according to weight percentage; and the addition agents comprise sodium hydroxide, isopropanol, fluid enzyme, kathon, flavor and the like. The product belongs to the hyper-concentrated liquid with less moisture content, small dosage, improves the oil stain removal performance by 40-50 percent compared with the traditional product, has less foam, and is suitable for quick cleansing of various heavy oil stains. The cleansing agent can be sprayed on the surface of the heavy oil stains after the cleansing agent is diluted by water, after the oil stains are naturally dissolved in 3-5 minutes, the object can be clean by wiping the stains. The production process is non-toxic, harmless and non-pollution, and the cleansing agent has the advantages of small investment, low cost, simple and reasonable process and wide application range.
Description
[technical field] patent of the present invention relates to a kind of hyperconcentration greasy dirt fast cleaning agent and the production method thereof of filed of daily-use chemical industry.
[background technology] is present, and domestic and international widely used greasy dirt detergent is that water content is big and be the product of main raw material with 12 alkyl benzene sulphonate (ABS)s mostly.The conference of product water content causes that processing labour intensity is big, and waste water resource increases transportation cost, and usage quantity is also big, and it is poor to remove greasy dirt power.Even the prolongation washing time can not be removed heavy dirty greasy dirt fully, especially to the smoke exhaust ventilator surface in kitchen, mechanical greasy dirt weighs dirty smeary fabric etc. with speckling with, and washing effect is poorer.Traditional in addition greasy dirt detergent is a main raw material with 12 alkyl benzene sulphonate (ABS)s, and biological degradability is poor, causes environmental pollution, and it is also poor to remove heavy dirty greasy dirt effect.Many industries and family wash with water content big liquid ceanser and washing powder usually for reaching quick removal smeary effect, and the one, can not remove greasy dirt fully, two amounts of being to use cause washing cost greatly to be increased, and uses also inconvenient.Therefore, being difficult for consumers in general accepts.And, no matter traditional greasy dirt cleaning products is the big liquid washing agent of water content, or solid detergent, all because of facility investment is big, complex manufacturing makes the producer carry out small-scale production because of reason inconvenience such as fund, technology, costs.
[summary of the invention] the objective of the invention is to: provide a kind of and can reduce the production and transport cost greatly, can adopt the common homemade resource of easily purchasing, use the simple device quality of production to be better than the big liquid greasy dirt detergent of traditional water content and a kind of hyperconcentration greasy dirt fast cleaning agent and the production method thereof that are better than using 12 alkyl benzene sulphonate (ABS)s.
The object of the present invention is achieved like this:
1, greasy dirt fast cleaning agent of the present invention is by pure water, EDTA (disodium ethylene diamine tetraacetate) and salt are by weight the premixed liquid of the mixed dissolving acquisition of 40-60:2-4:2-6 and by nonionogenic tenside AE0-9 (fatty alcohol-polyoxyethylene ether), 6501 (lauric alcohol acid amides) and OP-10 (nonyl phenol polyethenoxy ether) are by weight the basestocks of the ratio acquisition of 5-8:4-7:3-5, after homogenizing emulsifying again by weight with washing auxiliary detergent and additive, sodium hydroxide, Virahol, liquid enzymes, triumphant pine, spices is handled the product that forms by high-shear emulsifying in the lump by the ratio row of 3-5:10-20:1-3:0.03-0.05:0.2-0.3.
2, a kind of production method of hyperconcentration greasy dirt fast cleaning agent is characterized in that may further comprise the steps:
(1) preparation of raw material
(1) preparation of premixed liquid:
Under the normal temperature condition, pure water, EDTA (disodium ethylene diamine tetraacetate) and salt are got material by weight the ratio of 40-60:1-4:2-6, add in the stainless steel stirred vessel, make its mixed dissolution, obtain premixed liquid;
(2) preparation of basestocks
Under the normal temperature condition, nonionogenic tenside AE0-9 (fatty alcohol-polyoxyethylene ether), 6501 (lauric alcohol acid amides) and OP-10 (nonyl phenol polyethenoxy ether) are thrown to the homogenizing emulsifying container by weight the ratio of 5-8:4-7:3-5, homogenizing emulsifying under the condition of mixing speed 70-90 commentaries on classics/min obtains the emulsified block basestocks;
(3) at normal temperatures, washing auxiliary detergent and additive sodium hydroxide, Virahol, liquid enzymes, triumphant pine, spices are stirred under mixing speed 70-90 commentaries on classics/min condition in the ratio of 3-5:10-20:1-3:0.03-0.05:0.2-0.3 form the emulsus compound;
(2) high-shear emulsifying forming processes:
(1) premixed liquid that forms is poured in the stainless-steel vacuum reaction vessel,, under the rotating speed 1500-2000 commentaries on classics/min condition, fully made each material emulsification 3-5 minute at temperature 50-65 ℃;
(2) emulsification shape basestocks and the compound that forms added above-mentioned stainless-steel vacuum container successively
Under same reaction conditions, continue high-shear emulsifying reaction 15-20 minute, make it to become oyster white gala shape form;
(3) material is white or the liquid greasy dirt fast cleaning agent of faint yellow hyperconcentration after the circulating water cooling device on the vacuum reaction container is cooled to room temperature.
The invention has the beneficial effects as follows: 1., therefore can greatly reduce production cost because product of the present invention all adopts the common domestic raw material of easily purchasing.2. the clean effect of product of the present invention is good, be up to the standards through national commission of light industry product quality supervision and inspection station, outward appearance is white or faint yellow liquid state, moisture content and volatile matter＜30%, working substance content 〉=65%, pH value (0.1ag25 ℃)＜3, water-insoluble≤0.01%, GB relative standard's powder decontamination ratio〉2, degreasing is rapid, thorough, consumption is few.This product is sprayed onto the greasy dirt surface can removes greasy dirt after 3-5 minute, save than traditional greasy dirt detergent and produce and use cost 30-50%, application value is better than traditional greasy dirt detergent.3. the facility investment of the method for the invention is little, and technology is reasonable, and is nontoxic in the production use, harmless, pollution-free, is particularly suitable for medium-sized and small enterprises and family and does factory and produce this product.
[embodiment] the present invention is further described below in conjunction with embodiment.
Embodiment 1:(is an example to produce 2kg hyperconcentration greasy dirt fast cleaning agent)
(1) feedstock production:
(1) preparation of premixed liquid: at normal temperatures, with 1200 pure water 80g ethylenediamine tetraacetic acid (EDTA) two steel (EDTA), 120g salt is put into the stainless steel stirred vessel, and it is fully dissolved, and gets the 1400g premixed liquid;
(2) preparation of basestocks: the bamboo agent fatty alcohol-polyoxyethylene ether (AE0-9) of being lived in the 10g surface at normal temperatures, 88g lauric alcohol acid amides (6501) is thrown to the homogenizing emulsifying container, low whipping speed is under 70-90 rev/min the condition, and homogenizing emulsifying obtains 250g emulsification shape basestocks;
(3) at normal temperatures, with washing auxiliary detergent and additive hydroxide steel 62g, Virahol 247g, liquid acid 37g, triumphant loose 0.5g and rosin 3.5g are placed under the mixing speed 70-90 rev/min condition and stir formation 350g emulsus compound;
(2) high-shear emulsifying forming processes:
(1) premixed liquid that forms is poured in the stainless-steel vacuum reaction vessel, under the condition of temperature 50-65 ℃, rotating speed 1500-2000 rev/min, fully made each material emulsification 3-5 minute;
(2) emulsification shape basestocks and the compound that forms added in the above-mentioned stainless-steel vacuum container successively, under same reaction conditions, continue height and cut emulsion reaction 15-20 minute, make it to become oyster white gala shape form;
(3) material cools off to room temperature through the recirculated water on the vacuum reaction container and is 2kg white or the liquid greasy dirt fast cleaning agent of faint yellow hyperconcentration.
Embodiment 2:
(1) feedstock production:
(1) preparation of premixed liquid: under normal temperature condition, with the 1060g pure water, 64g disodium ethylene diamine tetraacetate (EDTA), 106g salt is put into the stainless steel stirred vessel, and it is fully dissolved, and gets the 1230g premixed liquid;
(2) preparation of basestocks: at normal temperatures, with tensio-active agent fatty alcohol-polyoxyethylene ether (AE0-9) 128g, lauric alcohol acid amides (6501) 106g and king's alkylphenol polyoxyethylene (OP-10) 85g, isopropyl alcohol 319g, liquid enzymes 42g, it is to stir under the 70-90 rev/min of condition that triumphant loose 1g and rosin 4g put into stirring velocity, forms 451g emulsus compound.
(2) high-shear emulsifying forming processes:
(1) premixed liquid that forms is poured in the stainless-steel vacuum reaction vessel, under the condition of temperature 50-65 ℃, rotating speed 1500-2000 rev/min, fully made each material emulsification 3-5 minute;
(2) emulsification shape basestocks and the compound that forms added in the above-mentioned stainless-steel vacuum container successively, under same reaction conditions, continue height and cut emulsion reaction 15-20 minute, make it to become oyster white gala shape form;
(3) material cools off to room temperature through the recirculated water on the vacuum reaction container and is 2kg white or the liquid greasy dirt fast cleaning agent of faint yellow hyperconcentration.
Claims (2)
1, a kind of hyperconcentration greasy dirt fast cleaning agent, it is characterized in that: the greasy dirt fast cleaning agent is by pure water, EDTA (disodium ethylene diamine tetraacetate) and salt are by weight the premixed liquid of the mixed dissolving acquisition of 40-60:2-4:2-6 and by nonionogenic tenside AE0-9 (fatty alcohol-polyoxyethylene ether), the basestocks that 6501 (lauric alcohol acid amides) and OP-10 (nonyl phenol polyethenoxy ether) obtain by weight the ratio of 5-8:4-7:3-5 after homogenizing emulsifying again by weight with washing auxiliary detergent and additive sodium hydroxide, Virahol, liquid enzymes, triumphant pine and spices are handled the product that forms by high-shear emulsifying in the lump by the ratio row of 3-5:10-20:1-3:0.03-0.05:0.2-0.3.
2, a kind of production method of hyperconcentration greasy dirt fast cleaning agent is characterized in that may further comprise the steps:
(1) preparation of raw material
(1) preparation of premixed liquid:
Under the normal temperature condition, pure water, EDTA (disodium ethylene diamine tetraacetate) and salt are got material by weight the ratio of 40-60:2-4:2-6, add in the stainless steel stirred vessel, make its mixed dissolution, obtain premixed liquid;
(2) preparation of basestocks:
Under the normal temperature condition, nonionogenic tenside AEO-9 (fatty alcohol-polyoxyethylene ether), 6501 (lauric alcohol acid amides) and OP-10 (nonyl phenol polyethenoxy ether) are thrown to the homogenizing emulsifying container by weight the ratio of 5-8:4-7:3-5, homogenizing emulsifying under the condition of mixing speed 70-90 commentaries on classics/min obtains the emulsified block basestocks;
(3) at normal temperatures, washing auxiliary detergent and additive sodium hydroxide, Virahol, liquid enzymes, Kai Song and spices are stirred under mixing speed 70-90 commentaries on classics/min condition in the ratio of 3-5:10-20:1-3:0.03-0.05:0.2-0.3 form the emulsus compound
(2) high-shear emulsifying forming processes:
(1) premixed liquid that forms is poured in the stainless-steel vacuum reaction vessel,, under the rotating speed 1500-2000 commentaries on classics/min condition, fully made each material emulsification 3-5 minute at temperature 50-65 ℃;
(2) emulsification shape basestocks and the compound that forms added in the above-mentioned stainless-steel vacuum container successively, under same reaction conditions, continue high-shear emulsifying reaction 15-20 minute, make it to become white or faint yellow emulsion state;
(3) material is white or the liquid greasy dirt fast cleaning agent of faint yellow hyperconcentration after the circulating water cooling device on the vacuum reaction container is cooled to the static froth breaking of room temperature.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2008101431023A CN101463294A (en) | 2008-08-28 | 2008-08-28 | Hyperconcentration oil stain rapid cleaning agent and production method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CNA2008101431023A CN101463294A (en) | 2008-08-28 | 2008-08-28 | Hyperconcentration oil stain rapid cleaning agent and production method thereof |
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| CN101463294A true CN101463294A (en) | 2009-06-24 |
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| CNA2008101431023A Pending CN101463294A (en) | 2008-08-28 | 2008-08-28 | Hyperconcentration oil stain rapid cleaning agent and production method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104278282A (en) * | 2013-07-02 | 2015-01-14 | 海安县中丽化工材料有限公司 | Foamless degreasing agent |
| CN104830561A (en) * | 2015-03-16 | 2015-08-12 | 周小燕 | Super-concentrated low-foam high-efficient laundry detergent |
| CN106047522A (en) * | 2016-06-27 | 2016-10-26 | 浙江绿果新材料有限公司 | Hyperconcentration anhydrous laundry detergent as well as preparation method and laundry beads thereof |
| CN111286416A (en) * | 2018-12-10 | 2020-06-16 | 谢道乐 | Colorless and odorless oily dirt detergent and preparation method thereof |
-
2008
- 2008-08-28 CN CNA2008101431023A patent/CN101463294A/en active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104278282A (en) * | 2013-07-02 | 2015-01-14 | 海安县中丽化工材料有限公司 | Foamless degreasing agent |
| CN104830561A (en) * | 2015-03-16 | 2015-08-12 | 周小燕 | Super-concentrated low-foam high-efficient laundry detergent |
| CN106047522A (en) * | 2016-06-27 | 2016-10-26 | 浙江绿果新材料有限公司 | Hyperconcentration anhydrous laundry detergent as well as preparation method and laundry beads thereof |
| CN106047522B (en) * | 2016-06-27 | 2019-06-21 | 浙江绿果新材料有限公司 | A kind of anhydrous liquid detergent of hyperconcetration type and preparation method thereof and solidifying pearl of doing washing |
| CN111286416A (en) * | 2018-12-10 | 2020-06-16 | 谢道乐 | Colorless and odorless oily dirt detergent and preparation method thereof |
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Open date: 20090624 |