CN101444318A - Process for producing high-luminousness olive clear-juice beverage - Google Patents

Process for producing high-luminousness olive clear-juice beverage Download PDF

Info

Publication number
CN101444318A
CN101444318A CNA2008100723950A CN200810072395A CN101444318A CN 101444318 A CN101444318 A CN 101444318A CN A2008100723950 A CNA2008100723950 A CN A2008100723950A CN 200810072395 A CN200810072395 A CN 200810072395A CN 101444318 A CN101444318 A CN 101444318A
Authority
CN
China
Prior art keywords
olive
juice
clear
luminousness
juice beverage
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CNA2008100723950A
Other languages
Chinese (zh)
Other versions
CN101444318B (en
Inventor
吴长江
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Fuzhou Yanfu Olive Co Ltd
Original Assignee
Fuzhou Yanfu Olive Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Fuzhou Yanfu Olive Co Ltd filed Critical Fuzhou Yanfu Olive Co Ltd
Priority to CN2008100723950A priority Critical patent/CN101444318B/en
Publication of CN101444318A publication Critical patent/CN101444318A/en
Application granted granted Critical
Publication of CN101444318B publication Critical patent/CN101444318B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Non-Alcoholic Beverages (AREA)

Abstract

The invention provides a process for producing high-luminousness olive clear-juice beverage. The process comprises the following steps: fresh olives are selected as main materials; frozen olive pulp is produced through the processes of material selection and pretreatment; juice extraction, centrifugation and squeeze, zymohydrolysis, filtration and blending are carried out to produce high-luminousness olive clear juice; and finally, the olive clear-juice beverage is obtained after homogenization. The zymohydrolysis of the centrifugated olive raw juice is carried out by adopting pectase, thereby the olive juice yield is high; and the olive juice obtained by adopting ceramic membrane filtration has high luminousness. Specific production processes comprise material selection, water treatment, pretreatment, juice extraction, centrifugation and two-stage squeeze, the pectase is adopted during the zymohydrolysis, the ceramic membrane filtration is carried out after the vibrating-screen filtration during the filtration, and the blending process is then carried out to obtain the high-luminousness olive clear-juice beverage. The invention has the advantages that the production process is scientific and reasonable, the maneuverability is strong, the control is easy, and the energy consumption is less, the large-scale production of the high-luminousness olive clear juice is applicable, the produced olive clear juice has rich nutrients, good taste and obvious economic benefits.

Description

A kind of process for producing high-luminousness olive clear-juice beverage
Technical field
The invention belongs to the beverage processing field, more specifically relate to a kind of process for producing high-luminousness olive clear-juice beverage.
Background technology
Olive (Canarium album) also claim Chinese olive, Qing Lan, Bai Lan, is Burseraceae (Burseraceae) Canarium plant, is one of the torrid zone, semi-tropical famous-brand and high-quality fruit.The olive nutritive value is very high, and Compendium of Material Medica is put down in writing its energy " the appetizing therapeutic method to keep the adverse qi flowing downward, the antidiarrheal born fluid ends polydipsia, controls sore-throat "; Modern scientific research shows: every 100g olive contains moisture 73g, protein 0.77~1.2g, fatty 6.55g, carbohydrate 5.6~12.0g, calcium 204~400mg, chlorophyll 30mg, carotenoid 7.52~8.05mg, vitamin C 21.12~39.29mg.Olive is at the cultivation history in existing more than 2000 year of China, and Fujian is most important main producing region.
But, because olive is more concentrated picking time, Time To Market is short, and polyphenols content is higher in the fruit, easily brown stain, freshness date is not long, and olive products is mainly based on preserved fruit, and kind is single, economic benefit is lower, and that olive adds state-of-art deeply is lower, and then Higher output is not accompanied by a higher income to have caused the orchard worker, and the sustainable development of whole olive industry is caused tremendous influence.
Summary of the invention
The purpose of this invention is to provide a kind of process for producing high-luminousness olive clear-juice beverage; This production technology is scientific and reasonable, the olive juice productive rate height of enzymolysis; Olive juice light transmittance height, good filtration effect; Use this production technology to produce olive clear-juice beverage, be easy to control, workable, and power consumption is few, is applicable to the large-scale production of high-luminousness olive clear-juice, and the olive clear-juice of producing is nutritious, and features good taste has remarkable economic efficiency.
Process for producing high-luminousness olive clear-juice beverage of the present invention, it is characterized in that: selecting new fresh olive is primary raw material, through selecting materials, preliminary treatment make freeze olive meat, squeeze the juice, centrifugal and squeezing, enzymolysis, filtration, allotment, make high-luminousness olive clear-juice, make olive clear-juice beverage behind the homogeneous.
Remarkable advantage of the present invention is:
(1) the present invention adopts pectinase enzymatic hydrolysis, improved the yield of olive juice, and hydrolysis result is good, simple to operate.Adopt ceramic membrane that olive juice is filtered, the light transmittance height of products obtained therefrom, product appearance is good, and has kept the quality of product preferably.
(2) this production technology is applied to produce high-luminousness olive clear-juice beverage in the deep processing of olive, the production efficiency height is easy to control, and is workable, and power consumption is few, is applicable to the large-scale production of olive clear-juice, has remarkable economic efficiency and social benefit.
(3) the nutritional labeling height of the high-luminousness olive clear-juice of employing technology preparation of the present invention, features good taste, and be convenient to transportation and storage.
The specific embodiment
(1) select materials and water treatment: selecting new fresh olive is primary raw material; The preparation of drinks water stores standby after treatment;
(2) preliminary treatment: new fresh olive after the cylinder classification again through guipure choosing fruit, with the olive of different stage carry out surfing wash fruit again through blanching, cooling, stoning, make after freezing and freeze olive meat;
(3) squeeze the juice: freeze olive meat through thaw, that broken back adopts spiral to squeeze the juice is afterwards centrifugal;
(4) centrifugal and squeezing: adopt supercentrifuge centrifugal to remove pomace and impurity to the olive juice after squeezing the juice through spiral, the rotating speed of centrifuge is 8000rpm, olive slag after centrifugal squeezes with squeezer again, after leave the olive juice of gained in enzymatic vessel together;
(5) enzymolysis: adopt pectase to carry out enzymolysis;
(6) filter: filter with ceramic membrane again after filtering with vibratory sieve earlier;
(7) allotment: after filtering olive juice and various auxiliary material are allocated, made high-luminousness olive clear-juice;
(8) homogeneous: deployed clear juice is carried out homogeneous; Make olive clear-juice beverage.
Olive clear-juice beverage passes through tinning, seals, and the olive clear-juice beverage finished product is made in sterilization; Tinning, seal the mode be evacuated to sealed cans behind the 0.050-0.055MPa that adopts; It is 5min that the heating-up time is adopted in described sterilization, and 95-100 ℃ of constant temperature spray sterilization 15min is cooled to below 40 ℃ through 10min again.
The preparation of drinks water is treated to: water after mechanical filter, activated carbon filtration, micro porous filtration, secondary filter, counter-infiltration in the storage standby, carry with pump.
The enzymatic hydrolysis condition of enzymolysis process is: olive juice 600L/ cylinder, enzyme dosage are 0.03%~0.04% of olive juice volume, enzyme activity unit 50,000 u/g, enzymolysis time 0.8~1.2h, 50 ℃ of hydrolysis temperatures, pH value of solution 3.5.
Be filtered into behind the enzymolysis: adopting membrane aperture again after the olive juice behind the enzymolysis filters with vibratory sieve earlier is the ceramic membrane filter of 0.01~0.05 μ m, filters back product light transmittance and is: 95%~98%.
Be allocated as according to mass percent: olive original juice 45%~55%, rock sugar 5~7%, sodium cellulose glycolate CMC-Na0.08~1.2%, ethyl maltol 0.007~0.009%, all the other are water.
In the allotment feed liquid, can also add other additive, the addition of described other additive as required or specified volume add, such as the addition of other additive mass percent: cycloheptaamylose 0.2% according to olive clear-juice beverage solution, composite phosphate 0.03%, Vc0.01% adds.
Below be several embodiments of the present invention, further specify the present invention, but the present invention is not limited only to this.
Embodiment 1
(1) select materials and water treatment: selecting new fresh olive is primary raw material; The preparation of drinks water stores standby after mechanical filter, activated carbon filtration, micro porous filtration, secondary filter, counter-infiltration, carries with pump.
(2) preliminary treatment: new fresh olive after the cylinder classification again through guipure choosing fruit, with the olive of different stage carry out surfing wash fruit again through blanching, cooling, stoning, make after freezing and freeze olive meat;
(3) squeeze the juice: freeze olive meat through thaw, that broken back adopts spiral to squeeze the juice is afterwards centrifugal;
(4) centrifugal and squeezing: adopt supercentrifuge centrifugal to remove pomace and impurity to the olive juice after squeezing the juice through spiral, the rotating speed of centrifuge is 8000rpm, olive slag after centrifugal squeezes with squeezer again, after leave the olive juice of gained in enzymatic vessel together;
(5) enzymolysis: adopt pectase to carry out enzymolysis; Olive juice 600L/ cylinder, enzyme dosage are 0.03% of olive juice volume, enzyme activity unit 50,000 u/g, enzymolysis time 0.8h, 50 ℃ of hydrolysis temperatures, pH value of solution 3.5.
(6) filter: adopting membrane aperture again after the olive juice behind the enzymolysis filters with vibratory sieve earlier is the ceramic membrane filter of 0.01 μ m, filters back product light transmittance and is: 98%.
(7) allotment: after filtering olive juice and various auxiliary material are allocated, made high-luminousness olive clear-juice; Be allocated as according to mass percent: olive original juice 50%, rock sugar 6%, sodium cellulose glycolate CMC-Na 0.1%, ethyl maltol 0.08%, all the other are water.
(8) homogeneous: deployed clear juice is carried out homogeneous; Make olive clear-juice beverage;
(9) olive clear-juice beverage passes through tinning, seals, and the olive clear-juice beverage finished product is made in sterilization; Tinning, seal the mode be evacuated to sealed cans behind the 0.050MPa that adopts; It is 5min that the heating-up time is adopted in described sterilization, and 95 ℃ of constant temperature spray sterilization 15min are cooled to below 40 ℃ through 10min again, are prepared into the high-luminousness olive clear-juice beverage finished product.
Embodiment 2
(1) select materials and water treatment: selecting new fresh olive is primary raw material; The preparation of drinks water stores standby after mechanical filter, activated carbon filtration, micro porous filtration, secondary filter, counter-infiltration, carries with pump.
(2) preliminary treatment: new fresh olive after the cylinder classification again through guipure choosing fruit, with the olive of different stage carry out surfing wash fruit again through blanching, cooling, stoning, make after freezing and freeze olive meat;
(3) squeeze the juice: freeze olive meat through thaw, that broken back adopts spiral to squeeze the juice is afterwards centrifugal;
(4) centrifugal and squeezing: adopt supercentrifuge centrifugal to remove pomace and impurity to the olive juice after squeezing the juice through spiral, the rotating speed of centrifuge is 8000rpm, olive slag after centrifugal squeezes with squeezer again, after leave the olive juice of gained in enzymatic vessel together;
(5) enzymolysis: adopt pectase to carry out enzymolysis; Olive juice 600L/ cylinder, enzyme dosage are 0.04% of olive juice volume, enzyme activity unit 50,000 u/g, enzymolysis time 1.2h, 50 ℃ of hydrolysis temperatures, pH value of solution 3.5.
(6) filter: adopting membrane aperture again after the olive juice behind the enzymolysis filters with vibratory sieve earlier is the ceramic membrane filter of 0.05 μ m, filters back product light transmittance and is: 95%.
(7) allotment: after filtering olive juice and various auxiliary material are allocated, made high-luminousness olive clear-juice; Be allocated as according to mass percent: olive original juice 55%, rock sugar 7%, sodium cellulose glycolate CMC-Na 1.2%, ethyl maltol 0.009%, all the other are water.
(8) homogeneous: deployed clear juice is carried out homogeneous; Make olive clear-juice beverage;
(9) in olive clear-juice beverage, add cycloheptaamylose 0.2% again, composite phosphate 0.03%, Vc0.01%, described weight is to account for the percentage of juice weight clearly, cycloheptaamylose adds and to account for 0.2% of juice weight clearly, composite phosphate adds and to account for 0.03% of juice weight clearly, and Vc adds and accounts for 0.01% of juice weight clearly.
(10) olive clear-juice beverage passes through tinning, seals, and the olive clear-juice beverage finished product is made in sterilization; Tinning, seal the mode be evacuated to sealed cans behind the 0.055MPa that adopts; It is 5min that the heating-up time is adopted in described sterilization, and 100 ℃ of constant temperature spray sterilization 15min are cooled to below 40 ℃ through 10min again, are prepared into the high-luminousness olive clear-juice beverage finished product.
Embodiment 3
(1) select materials and water treatment: selecting new fresh olive is primary raw material; The preparation of drinks water after mechanical filter, activated carbon filtration, micro porous filtration, secondary filter, counter-infiltration in the storage standby, carry with pump.
(2) preliminary treatment: new fresh olive after the cylinder classification again through guipure choosing fruit, with the olive of different stage carry out surfing wash fruit again through blanching, cooling, stoning, make after freezing and freeze olive meat;
(3) squeeze the juice: freeze olive meat through thaw, that broken back adopts spiral to squeeze the juice is afterwards centrifugal;
(4) centrifugal and squeezing: adopt supercentrifuge centrifugal to remove pomace and impurity to the olive juice after squeezing the juice through spiral, the rotating speed of centrifuge is 8000rpm, olive slag after centrifugal squeezes with squeezer again, after leave the olive juice of gained in enzymatic vessel together;
(5) enzymolysis: adopt pectase to carry out enzymolysis; Olive juice 600L/ cylinder, enzyme dosage are 0.035% of olive juice volume, enzyme activity unit 50,000 u/g, enzymolysis time 1.0h, 50 ℃ of hydrolysis temperatures, pH value of solution 3.5.
(6) filter: adopting membrane aperture again after the olive juice behind the enzymolysis filters with vibratory sieve earlier is the ceramic membrane filter of 0.04 μ m, filters back product light transmittance and is: 96%~97%.
(7) allotment: after filtering olive juice and various auxiliary material are allocated, made high-luminousness olive clear-juice; Be allocated as according to mass percent: olive original juice 45%, rock sugar 5%, sodium cellulose glycolate CMC-Na 0.08%, ethyl maltol 0.007%, all the other are water; According to actual taste and needs, can also in the allotment feed liquid, add other additive, as colouring agent, sweetener, flavouring agent or the like, the addition of other additive as required or specified volume add.
(8) homogeneous: deployed clear juice is carried out homogeneous; Make olive clear-juice beverage;
(9) olive clear-juice beverage passes through tinning, seals, and the olive clear-juice beverage finished product is made in sterilization; Tinning, seal the mode be evacuated to sealed cans behind the 0.052-0.055MPa that adopts; It is 5min that the heating-up time is adopted in described sterilization, and 96-98 ℃ of constant temperature spray sterilization 15min is cooled to below 40 ℃ through 10min again, is prepared into the high-luminousness olive clear-juice beverage finished product.

Claims (10)

1. process for producing high-luminousness olive clear-juice beverage, it is characterized in that: selecting new fresh olive is primary raw material, through selecting materials, preliminary treatment make freeze olive meat, squeeze the juice, centrifugal and squeezing, enzymolysis, filtration, allotment, make high-luminousness olive clear-juice, make olive clear-juice beverage behind the homogeneous.
2. process for producing high-luminousness olive clear-juice beverage according to claim 1 is characterized in that: the concrete steps of described technology are:
(1) select materials and water treatment: selecting new fresh olive is primary raw material; The preparation of drinks water stores standby after treatment;
(2) preliminary treatment: new fresh olive after the cylinder classification again through guipure choosing fruit, with the olive of different stage carry out surfing wash fruit again through blanching, cooling, stoning, make after freezing and freeze olive meat;
(3) squeeze the juice: freeze olive meat through thaw, that broken back adopts spiral to squeeze the juice is afterwards centrifugal;
(4) centrifugal and squeezing: adopt supercentrifuge centrifugal to remove pomace and impurity to the olive juice after squeezing the juice through spiral, the rotating speed of centrifuge is 8000rpm, olive slag after centrifugal squeezes with squeezer again, after leave the olive juice of gained in enzymatic vessel together;
(5) enzymolysis: adopt pectase to carry out enzymolysis;
(6) filter: filter with ceramic membrane again after filtering with vibratory sieve earlier;
(7) allotment: after filtering olive juice and various auxiliary material are allocated, made high-luminousness olive clear-juice;
(8) homogeneous: deployed clear juice is carried out homogeneous; Make olive clear-juice beverage.
3. process for producing high-luminousness olive clear-juice beverage according to claim 2 is characterized in that: described olive clear-juice beverage passes through tinning, seals, and the olive clear-juice beverage finished product is made in sterilization.
4. process for producing high-luminousness olive clear-juice beverage according to claim 3 is characterized in that: described tinning, seal the mode be evacuated to sealed cans behind the 0.050-0.055MPa that adopts; It is 5min that the heating-up time is adopted in described sterilization, and 95-100 ℃ of constant temperature spray sterilization 15min is cooled to below 40 ℃ through 10min again.
5. process for producing high-luminousness olive clear-juice beverage according to claim 2, it is characterized in that: described preparation of drinks water is treated to: water after mechanical filter, activated carbon filtration, micro porous filtration, secondary filter, counter-infiltration in the storage standby, carry with pump.
6. process for producing high-luminousness olive clear-juice beverage according to claim 2, it is characterized in that: the enzymatic hydrolysis condition of described enzymolysis process is: olive juice 600L/ cylinder, enzyme dosage is 0.03%~0.04% of an olive juice volume, enzyme activity unit 50,000 u/g, enzymolysis time 0.8~1.2h, 50 ℃ of hydrolysis temperatures, pH value of solution 3.5.
7. process for producing high-luminousness olive clear-juice beverage according to claim 2, it is characterized in that: be filtered into behind the described enzymolysis: adopting membrane aperture again after the olive juice behind the enzymolysis filters with vibratory sieve earlier is the ceramic membrane filter of 0.01~0.05 μ m, filters back product light transmittance and is: 95%~98%.
8. process for producing high-luminousness olive clear-juice beverage according to claim 2, it is characterized in that: described being allocated as: olive original juice 45%~55% according to mass percent, rock sugar 5~7%, sodium cellulose glycolate CMC-Na0.08~1.2%, ethyl maltol 0.007~0.009%, all the other are water.
9. process for producing high-luminousness olive clear-juice beverage according to claim 8 is characterized in that: in the allotment feed liquid, add other additive, the addition of described other additive as required or specified volume add.
10. process for producing high-luminousness olive clear-juice beverage according to claim 9, it is characterized in that: the addition of described other additive is according to the mass percent of olive clear-juice beverage solution: cycloheptaamylose 0.2%, composite phosphate 0.03%, Vc0.01% adds.
CN2008100723950A 2008-12-18 2008-12-18 Process for producing high-luminousness olive clear-juice beverage Expired - Fee Related CN101444318B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2008100723950A CN101444318B (en) 2008-12-18 2008-12-18 Process for producing high-luminousness olive clear-juice beverage

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2008100723950A CN101444318B (en) 2008-12-18 2008-12-18 Process for producing high-luminousness olive clear-juice beverage

Publications (2)

Publication Number Publication Date
CN101444318A true CN101444318A (en) 2009-06-03
CN101444318B CN101444318B (en) 2012-06-20

Family

ID=40740430

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2008100723950A Expired - Fee Related CN101444318B (en) 2008-12-18 2008-12-18 Process for producing high-luminousness olive clear-juice beverage

Country Status (1)

Country Link
CN (1) CN101444318B (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106690189A (en) * 2016-12-26 2017-05-24 福建农林大学 Olive salting liquid and method for preventing olive precipitates from being generated
CN106723095A (en) * 2015-11-24 2017-05-31 宜兴恒盛农业发展有限公司 Red bayberry takes juice system in a kind of cranberry juice production
CN107156554A (en) * 2017-05-27 2017-09-15 广西北部湾珠乡橄榄食品有限公司 A kind of preparation method of olive fruit juice
CN107183444A (en) * 2017-05-27 2017-09-22 广西北部湾珠乡橄榄食品有限公司 A kind of preparation method of compound olive fruit juice
CN107495029A (en) * 2017-10-12 2017-12-22 浦北县龙腾食品有限公司 A kind of preparation method of olive beverage

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1124598A (en) * 1995-07-19 1996-06-19 昆明天成食品工业有限公司 Clear Yunnan Chinese olive beverage
CN101263921B (en) * 2007-03-12 2011-04-20 福建农林大学 Preparation of olive health care beverage
CN101088385B (en) * 2007-05-25 2010-05-19 郑金营 Recipe and production process of olive powder

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106723095A (en) * 2015-11-24 2017-05-31 宜兴恒盛农业发展有限公司 Red bayberry takes juice system in a kind of cranberry juice production
CN106690189A (en) * 2016-12-26 2017-05-24 福建农林大学 Olive salting liquid and method for preventing olive precipitates from being generated
CN107156554A (en) * 2017-05-27 2017-09-15 广西北部湾珠乡橄榄食品有限公司 A kind of preparation method of olive fruit juice
CN107183444A (en) * 2017-05-27 2017-09-22 广西北部湾珠乡橄榄食品有限公司 A kind of preparation method of compound olive fruit juice
CN107495029A (en) * 2017-10-12 2017-12-22 浦北县龙腾食品有限公司 A kind of preparation method of olive beverage

Also Published As

Publication number Publication date
CN101444318B (en) 2012-06-20

Similar Documents

Publication Publication Date Title
CN102924423B (en) Method for extracting cyanidin from banana peel
CN101948897B (en) Method for extracting shinyleaf yellowhorn oil, shinyleaf yellowhorn polysaccharide and shinyleaf yellowhorn protolysate peptide from shinyleaf yellowhorn
CN101543306B (en) Preparation method of mango condensed thick juice
CN104342337B (en) A kind of production technique of Sunset Abelmoschus Root functional health wine
CN102060830B (en) Method for extracting anthocyanin from fruit dregs of Nitraria sibirica Pall
CN101444318B (en) Process for producing high-luminousness olive clear-juice beverage
CN102511851A (en) Processing method for concentrated juice of red dates
CN106666640A (en) Natural plant nutritional salt capable of replacing sodium chloride and process for preparing natural plant nutritional salt
CN101133894B (en) Method for improving the quantity of orange genus tangerine juice by utilizing complex enzyme
CN102311906A (en) Method for brewing active papaya wine
CN103284082A (en) Method for preparing banana juice from complete banana fruit
CN105454925A (en) Preparation method of concentrated turbid hovenia dulcis juice
CN105039089A (en) Pawpaw peptide liquor and making method thereof
CN106234872A (en) A kind of blue berry composite fruit juice rich in dried apple slices cell lyophilized powder and preparation method thereof
CN101731693B (en) Concentrated honey tree sepum production method
JPH0313865B2 (en)
CN103284030A (en) Method for preparing banana paste from complete banana fruit
CN106472941A (en) A kind of pineapple sarcocarp powder solid beverage technological method for processing
CN111732998A (en) Method for extracting noni seed oil with high oil yield without solvent
CN101791104A (en) Method for preparing sweet agent by utilizing bananas
CN105886221A (en) Manufacturing method of passion fruit composite tea wine
CN104041904A (en) Method for preparing bambusa chungii liquid
CN103980384A (en) Preparation method of water-soluble pectin of shaddock albedo
CN103351940A (en) Manufacturing technology of camellia sinensis seed oil through biological fermentation method
CN101878939B (en) Process for producing concentrated strawberry clear juice

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20120620

Termination date: 20191218

CF01 Termination of patent right due to non-payment of annual fee